#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216826.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216826_Fobs loop_ _publ_author_name 'Chinnakali, K.' 'Sudha, D.' 'Jayagobi, M.' 'Raghunathan, R.' 'Fun, Hoong-Kun' _publ_section_title ; trans-1-Ethyl-4,4,10-trimethyl-2-tosyl-1,2,3,3a,4,11b-hexahydro-11H-pyrrolo[3,4-c]pyrano[5,6-c]quinolin-11-one ; _journal_coeditor_code WN2215 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4650 _journal_page_last o4651 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 109.554 _cell_angle_gamma 90.000 _cell_length_a 24.7027 _cell_length_b 10.2685 _cell_length_c 19.6195 _exptl_crystal_F_000 1984.00 _reflns_d_resolution_high 0.7095 _[local]_cod_data_source_file wn2215Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jg9m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 360.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 60.00 -3.18 3.18 o 2 0 0 25897.00 26041.99 619.62 o 3 0 0 5.61 -1.46 14.45 o 4 0 0 18182.78 17928.54 443.04 o 5 0 0 23.13 2.85 29.76 o 6 0 0 20929.02 19807.63 351.42 o 7 0 0 1078.87 1054.21 39.74 o 8 0 0 7495.73 7041.44 127.74 o 9 0 0 116.51 146.28 25.70 o 10 0 0 10948.84 11769.44 353.42 o 11 0 0 91.23 211.92 26.42 o 12 0 0 296.29 303.06 31.84 o 13 0 0 15.00 28.04 14.17 o 14 0 0 2779.04 2346.47 102.71 o 15 0 0 2.30 25.38 12.88 o 16 0 0 5164.25 4624.30 99.11 o 17 0 0 6.54 121.99 26.35 o 18 0 0 1472.70 1309.65 68.08 o 19 0 0 303.33 340.12 40.42 o 20 0 0 8732.96 8297.99 181.67 o 21 0 0 271.69 427.22 45.44 o 22 0 0 5545.68 5571.14 147.81 o 23 0 0 1156.82 1374.30 74.12 o 24 0 0 1295.91 1464.00 114.67 o 25 0 0 425.43 395.58 102.34 o 26 0 0 2283.00 2440.55 194.87 o 27 0 0 24.76 54.09 60.32 o 28 0 0 2154.65 2468.78 205.74 o 29 0 0 548.51 639.50 136.28 o 30 0 0 132.27 217.81 95.18 o 31 0 0 30.81 -47.33 47.33 o 32 0 0 272.15 421.43 118.38 o 1 1 0 13.72 -3.40 3.40 o 2 1 0 34176.14 30753.83 3057.31 o 3 1 0 107.50 59.11 14.62 o 4 1 0 54943.70 56735.21 1296.63 o 5 1 0 2.69 -5.00 10.34 o 6 1 0 1882.35 2151.91 42.56 o 7 1 0 55.88 74.30 16.46 o 8 1 0 223.25 258.80 16.00 o 9 1 0 0.03 -9.20 9.20 o 10 1 0 3094.53 2908.54 50.33 o 11 1 0 51.15 45.54 12.35 o 12 1 0 6.43 15.71 10.01 o 13 1 0 179.92 150.81 15.66 o 14 1 0 4171.32 4511.95 76.67 o 15 1 0 0.45 27.90 11.52 o 16 1 0 19.93 26.75 12.24 o 17 1 0 0.17 -6.08 10.94 o 18 1 0 5691.55 5630.80 96.27 o 19 1 0 0.11 73.13 17.36 o 20 1 0 1882.77 1826.14 69.52 o 21 1 0 1.34 40.96 17.95 o 22 1 0 926.89 1004.84 59.43 o 23 1 0 13.10 44.68 23.37 o 24 1 0 109.07 82.58 28.31 o 25 1 0 120.97 212.63 38.19 o 26 1 0 1092.92 1288.68 164.64 o 27 1 0 0.82 -2.86 42.10 o 28 1 0 139.41 158.68 60.60 o 29 1 0 4.25 -26.74 39.26 o 30 1 0 16.17 18.53 40.93 o 31 1 0 60.23 76.12 50.73 o 32 1 0 1745.53 2134.31 215.62 o 0 2 0 80.01 24.32 9.65 o 1 2 0 5.55 2.81 5.29 o 2 2 0 8622.12 9702.16 99.72 o 3 2 0 6.65 -8.20 8.20 o 4 2 0 12271.34 12875.88 133.33 o 5 2 0 76.66 75.37 11.07 o 6 2 0 6226.75 6786.70 84.26 o 7 2 0 6.00 26.51 9.62 o 8 2 0 14257.81 14861.30 149.63 o 9 2 0 139.55 141.34 16.41 o 10 2 0 3364.91 3848.36 55.07 o 11 2 0 3.64 24.98 10.15 o 12 2 0 240.54 302.56 18.58 o 13 2 0 6.74 18.00 10.23 o 14 2 0 37.38 79.15 16.22 o 15 2 0 191.29 240.55 19.10 o 16 2 0 3266.85 3346.03 59.49 o 17 2 0 0.01 22.13 12.04 o 18 2 0 2692.39 2684.20 58.61 o 19 2 0 107.27 135.36 21.31 o 20 2 0 7088.00 6944.11 125.43 o 21 2 0 22.32 76.98 19.95 o 22 2 0 368.83 293.07 37.17 o 23 2 0 2.94 9.51 21.20 o 24 2 0 69.70 34.04 32.09 o 25 2 0 10.38 13.02 22.62 o 26 2 0 0.34 -22.29 22.29 o 27 2 0 4.67 20.34 24.51 o 28 2 0 87.33 72.32 52.76 o 29 2 0 0.03 16.88 43.08 o 30 2 0 86.83 56.55 49.52 o 31 2 0 6.72 47.09 48.74 o 32 2 0 318.51 315.13 97.04 o 1 3 0 1.65 7.93 7.47 o 2 3 0 19630.18 20111.49 187.18 o 3 3 0 271.56 268.34 15.58 o 4 3 0 19700.27 20243.95 189.68 o 5 3 0 3.87 -8.87 8.87 o 6 3 0 2492.06 2544.45 52.82 o 7 3 0 59.15 71.46 10.98 o 8 3 0 352.11 355.50 17.59 o 9 3 0 122.05 146.17 14.33 o 10 3 0 0.19 54.87 15.72 o 11 3 0 4.16 0.94 9.76 o 12 3 0 15537.66 17264.63 167.78 o 13 3 0 156.83 182.70 16.01 o 14 3 0 103.71 133.06 15.24 o 15 3 0 2.45 21.08 11.08 o 16 3 0 0.96 4.82 10.62 o 17 3 0 27.35 11.47 13.69 o 18 3 0 3886.95 3591.68 70.94 o 19 3 0 8.07 -8.32 14.05 o 20 3 0 1.19 0.66 17.03 o 21 3 0 10.76 -7.90 20.13 o 22 3 0 5.68 36.72 23.04 o 23 3 0 4.99 6.89 22.14 o 24 3 0 16.33 68.89 25.60 o 25 3 0 47.49 56.09 27.42 o 26 3 0 9.20 34.71 27.62 o 27 3 0 24.16 64.85 29.91 o 28 3 0 0.08 11.96 25.02 o 29 3 0 3.50 19.13 50.64 o 30 3 0 142.49 65.01 62.37 o 31 3 0 103.45 67.50 51.74 o 32 3 0 6.06 4.92 45.78 o 0 4 0 13518.17 13373.57 176.31 o 1 4 0 423.26 470.24 16.69 o 2 4 0 2182.90 1871.92 31.81 o 3 4 0 15.70 32.92 8.02 o 4 4 0 237.08 294.27 13.67 o 5 4 0 57.47 56.29 9.60 o 6 4 0 11015.89 10589.86 111.32 o 7 4 0 16.17 6.56 7.59 o 8 4 0 295.24 451.09 17.97 o 9 4 0 57.01 73.29 11.07 o 10 4 0 336.25 316.50 18.37 o 11 4 0 27.92 31.43 10.78 o 12 4 0 370.12 374.04 23.86 o 13 4 0 181.82 208.69 18.56 o 14 4 0 532.35 595.99 27.91 o 15 4 0 0.20 -4.90 12.47 o 16 4 0 9977.92 9687.14 138.73 o 17 4 0 3.05 2.03 14.65 o 18 4 0 1232.27 1281.60 47.77 o 19 4 0 73.49 109.41 29.01 o 20 4 0 370.96 450.60 41.40 o 21 4 0 27.46 52.19 22.91 o 22 4 0 380.64 359.07 56.68 o 23 4 0 7.19 3.87 28.72 o 24 4 0 217.36 179.68 41.65 o 25 4 0 28.29 59.67 26.23 o 26 4 0 308.25 388.65 48.81 o 27 4 0 75.46 82.84 34.18 o 28 4 0 18.41 81.66 34.06 o 29 4 0 116.42 180.22 87.69 o 30 4 0 158.77 97.17 85.77 o 31 4 0 3.11 56.34 73.04 o 1 5 0 386.28 340.49 14.99 o 2 5 0 6453.02 6861.72 88.04 o 3 5 0 22.36 16.54 9.17 o 4 5 0 18566.80 19335.04 192.18 o 5 5 0 238.06 272.07 14.51 o 6 5 0 2554.56 2740.61 45.24 o 7 5 0 63.26 46.51 10.82 o 8 5 0 224.26 287.81 15.25 o 9 5 0 255.17 269.59 15.97 o 10 5 0 1144.09 1197.39 31.22 o 11 5 0 28.50 -2.37 9.77 o 12 5 0 6558.92 6350.00 87.08 o 13 5 0 92.76 101.07 19.62 o 14 5 0 702.15 679.83 33.70 o 15 5 0 0.31 10.82 14.40 o 16 5 0 618.69 641.89 40.71 o 17 5 0 10.53 27.75 15.55 o 18 5 0 431.47 444.29 32.81 o 19 5 0 14.78 9.06 16.77 o 20 5 0 765.29 844.20 55.10 o 21 5 0 7.62 12.34 23.53 o 22 5 0 6.43 5.34 26.18 o 23 5 0 7.73 35.27 28.24 o 24 5 0 432.30 440.48 66.22 o 25 5 0 190.69 225.51 58.34 o 26 5 0 1177.48 1280.77 88.30 o 27 5 0 122.40 123.99 47.55 o 28 5 0 572.27 764.24 195.14 o 29 5 0 1.96 -16.82 30.47 o 30 5 0 74.27 123.76 131.04 o 0 6 0 4961.41 4975.33 126.96 o 1 6 0 63.28 78.27 11.62 o 2 6 0 1898.93 2098.49 43.67 o 3 6 0 99.23 90.34 13.87 o 4 6 0 183.19 267.18 19.44 o 5 6 0 179.76 159.79 16.81 o 6 6 0 471.60 501.80 30.61 o 7 6 0 13.49 5.44 11.45 o 8 6 0 9.66 7.67 9.68 o 9 6 0 160.52 146.15 23.58 o 10 6 0 178.84 155.18 19.90 o 11 6 0 581.24 603.44 33.41 o 12 6 0 3479.85 3253.31 103.95 o 13 6 0 15.68 34.59 17.63 o 14 6 0 689.67 749.19 41.75 o 15 6 0 164.15 177.62 26.09 o 16 6 0 425.58 458.23 37.15 o 17 6 0 176.79 213.01 31.07 o 18 6 0 1730.48 1733.91 68.53 o 19 6 0 0.04 -8.14 20.09 o 20 6 0 196.58 222.24 34.39 o 21 6 0 6.77 6.57 26.04 o 22 6 0 1267.30 1474.82 84.79 o 23 6 0 0.04 -8.83 24.25 o 24 6 0 6.73 -5.86 30.72 o 25 6 0 55.27 79.46 32.75 o 26 6 0 98.94 101.93 47.40 o 27 6 0 14.84 93.00 47.13 o 28 6 0 630.94 785.74 103.59 o 29 6 0 4.55 114.60 54.55 o 1 7 0 84.76 56.69 12.12 o 2 7 0 12354.11 12488.04 161.60 o 3 7 0 9.62 15.63 14.95 o 4 7 0 2887.18 3299.31 62.80 o 5 7 0 18.03 7.72 11.39 o 6 7 0 2.61 25.94 14.06 o 7 7 0 641.58 631.68 31.10 o 8 7 0 611.64 646.07 32.78 o 9 7 0 25.32 42.01 15.73 o 10 7 0 722.56 736.91 35.62 o 11 7 0 85.32 80.46 20.34 o 12 7 0 382.55 357.46 37.32 o 13 7 0 110.41 83.05 19.30 o 14 7 0 274.47 327.87 30.21 o 15 7 0 48.70 60.85 19.84 o 16 7 0 482.60 484.24 42.53 o 17 7 0 1.18 17.75 18.90 o 18 7 0 3.88 33.86 37.18 o 19 7 0 2.02 14.68 20.27 o 20 7 0 285.72 252.97 36.72 o 21 7 0 248.24 193.53 37.76 o 22 7 0 0.01 -12.40 24.82 o 23 7 0 109.99 98.69 34.48 o 24 7 0 246.85 308.37 49.38 o 25 7 0 27.01 26.92 42.26 o 26 7 0 7.04 11.42 38.27 o 27 7 0 82.94 87.71 70.26 o 28 7 0 141.10 265.58 66.29 o 0 8 0 1777.98 1678.80 65.04 o 1 8 0 16.56 12.78 14.37 o 2 8 0 293.66 230.44 25.57 o 3 8 0 7.09 5.31 22.97 o 4 8 0 686.93 713.48 32.20 o 5 8 0 18.05 16.23 13.11 o 6 8 0 4.73 35.43 14.39 o 7 8 0 5.29 25.14 14.55 o 8 8 0 4.32 17.41 14.79 o 9 8 0 0.32 -9.81 13.17 o 10 8 0 100.52 143.28 20.46 o 11 8 0 0.11 -3.90 13.59 o 12 8 0 205.88 205.46 26.46 o 13 8 0 0.46 0.86 19.13 o 14 8 0 20.11 45.17 21.03 o 15 8 0 27.07 22.00 19.33 o 16 8 0 11.10 -0.80 18.87 o 17 8 0 63.23 58.28 23.52 o 18 8 0 99.47 73.72 25.19 o 19 8 0 118.60 134.28 35.38 o 20 8 0 33.90 106.44 27.41 o 21 8 0 8.95 6.03 35.79 o 22 8 0 314.30 406.02 54.30 o 23 8 0 7.90 132.60 62.57 o 24 8 0 344.82 367.16 70.84 o 25 8 0 28.37 54.50 40.23 o 26 8 0 211.00 263.20 108.90 o 27 8 0 15.15 57.09 45.57 o 1 9 0 1.15 1.29 16.72 o 2 9 0 1368.59 1218.72 60.51 o 3 9 0 105.11 107.92 22.52 o 4 9 0 3141.23 3071.76 77.54 o 5 9 0 0.79 1.63 22.07 o 6 9 0 347.08 416.78 59.55 o 7 9 0 64.29 113.31 23.82 o 8 9 0 68.59 80.09 23.03 o 9 9 0 2.30 23.10 17.84 o 10 9 0 288.86 204.19 30.01 o 11 9 0 78.45 84.18 23.46 o 12 9 0 1717.26 1669.85 64.48 o 13 9 0 25.93 20.73 20.35 o 14 9 0 684.13 678.88 49.04 o 15 9 0 0.19 11.23 19.47 o 16 9 0 318.93 380.48 41.84 o 17 9 0 33.17 22.62 28.47 o 18 9 0 1322.27 1399.49 70.49 o 19 9 0 0.77 31.91 22.46 o 20 9 0 132.71 161.38 40.19 o 21 9 0 1.27 58.23 38.01 o 22 9 0 998.01 1146.67 224.37 o 23 9 0 2.44 -6.11 34.92 o 24 9 0 72.43 72.67 44.03 o 25 9 0 96.98 95.81 82.32 o 0 10 0 351.25 385.90 74.37 o 1 10 0 31.10 7.24 27.08 o 2 10 0 574.69 562.18 47.60 o 3 10 0 60.76 38.91 25.29 o 4 10 0 10.39 -15.86 27.45 o 5 10 0 172.22 136.07 31.95 o 6 10 0 531.63 639.90 76.12 o 7 10 0 8.74 -14.82 24.16 o 8 10 0 79.43 74.55 28.73 o 9 10 0 178.83 169.70 49.44 o 10 10 0 222.13 345.21 44.94 o 11 10 0 12.51 23.04 26.15 o 12 10 0 1193.36 1057.86 79.20 o 13 10 0 1.94 36.76 25.73 o 14 10 0 481.29 461.87 124.45 o 15 10 0 3.77 36.96 22.33 o 16 10 0 8.28 62.13 24.69 o 17 10 0 90.45 88.79 32.89 o 18 10 0 614.23 842.50 76.17 o 19 10 0 4.45 29.81 27.06 o 20 10 0 2.32 0.36 41.75 o 21 10 0 53.09 122.77 47.34 o 22 10 0 344.51 365.90 70.82 o 23 10 0 38.91 51.30 59.32 o 1 11 0 35.74 23.59 58.86 o 2 11 0 153.98 213.65 48.73 o 3 11 0 28.13 40.80 27.28 o 4 11 0 39.82 55.46 27.40 o 5 11 0 101.30 98.43 30.91 o 6 11 0 10.14 46.39 30.41 o 7 11 0 110.77 97.94 32.47 o 8 11 0 126.26 175.62 36.71 o 9 11 0 8.50 50.35 29.17 o 10 11 0 1064.40 1100.30 85.02 o 11 11 0 0.25 46.60 34.45 o 12 11 0 101.35 124.91 35.08 o 13 11 0 190.98 173.84 49.32 o 14 11 0 462.33 487.98 73.34 o 15 11 0 2.84 71.11 80.27 o 16 11 0 100.31 145.48 54.35 o 17 11 0 2.76 83.51 45.22 o 18 11 0 458.11 475.18 135.81 o 19 11 0 16.82 32.02 38.77 o 20 11 0 357.64 365.99 72.46 o 21 11 0 0.11 -6.36 54.35 o 0 12 0 1526.18 1432.64 147.02 o 1 12 0 78.40 116.48 42.21 o 2 12 0 166.78 204.50 48.90 o 3 12 0 31.80 19.01 33.14 o 4 12 0 210.50 256.76 42.76 o 5 12 0 22.16 15.91 27.78 o 6 12 0 2414.68 2819.23 106.53 o 7 12 0 0.37 61.44 31.69 o 8 12 0 1280.02 1455.21 133.23 o 9 12 0 18.92 44.78 61.64 o 10 12 0 18.99 42.29 41.08 o 11 12 0 85.33 35.03 40.88 o 12 12 0 135.14 150.42 83.72 o 13 12 0 0.28 62.72 39.71 o 14 12 0 202.26 171.35 55.30 o 15 12 0 45.99 100.17 46.79 o 16 12 0 430.93 574.52 86.46 o 17 12 0 48.05 128.37 114.54 o 18 12 0 113.25 152.08 54.69 o 1 13 0 0.66 44.22 39.79 o 2 13 0 759.64 803.83 87.72 o 3 13 0 7.45 12.75 35.99 o 4 13 0 2376.14 2314.89 128.07 o 5 13 0 121.17 140.27 46.68 o 6 13 0 1694.92 1888.78 139.19 o 7 13 0 58.22 32.39 51.57 o 8 13 0 215.09 213.76 59.50 o 9 13 0 11.98 22.40 42.10 o 10 13 0 13.69 35.01 41.96 o 11 13 0 0.08 50.23 47.59 o 12 13 0 201.19 163.40 57.79 o 13 13 0 12.30 138.29 48.12 o 14 13 0 27.96 93.42 50.39 o 0 14 0 1512.49 1213.51 156.56 o 1 14 0 6.76 42.65 45.27 o 2 14 0 642.27 800.60 93.54 o 3 14 0 13.69 90.13 48.05 o 4 14 0 813.15 706.12 90.22 o 5 14 0 1.97 48.14 41.18 o 6 14 0 127.26 102.56 47.24 o 7 14 0 28.96 101.09 48.46 o 8 14 0 383.23 437.62 77.71 o -33 1 1 122.01 152.42 58.10 o -32 1 1 325.25 226.56 68.24 o -31 1 1 202.51 135.84 62.60 o -30 1 1 1.33 77.10 51.65 o -29 1 1 31.16 21.86 44.72 o -28 1 1 176.46 70.99 50.06 o -27 1 1 70.66 89.37 37.42 o -26 1 1 3.03 20.75 25.25 o -25 1 1 21.01 24.94 25.31 o -24 1 1 342.54 340.06 35.08 o -23 1 1 508.78 597.60 42.77 o -22 1 1 2749.45 2655.71 69.38 o -21 1 1 137.00 94.18 26.88 o -20 1 1 1762.86 1646.76 59.60 o -19 1 1 2387.69 2127.50 57.07 o -18 1 1 87.87 121.21 19.88 o -17 1 1 705.05 628.01 35.90 o -16 1 1 435.52 416.46 30.46 o -15 1 1 146.95 164.74 21.59 o -14 1 1 867.74 823.28 42.48 o -13 1 1 330.31 191.40 17.97 o -12 1 1 665.91 847.98 28.90 o -11 1 1 4589.58 4616.29 73.98 o -10 1 1 2339.82 2293.08 46.88 o -9 1 1 1854.71 2015.67 42.28 o -8 1 1 3.02 31.61 11.54 o -7 1 1 1401.12 1027.27 30.45 o -6 1 1 0.00 -10.96 10.96 o -5 1 1 1.20 -1.37 8.75 o -4 1 1 7939.39 7609.93 148.39 o -3 1 1 9628.10 9078.14 239.15 o -2 1 1 0.33 -7.75 7.75 o -1 1 1 1669.34 1670.20 42.26 o 0 1 1 40.27 -6.83 6.83 o 1 1 1 6215.89 6054.58 356.64 o 2 1 1 2146.63 1957.00 50.47 o 3 1 1 3185.74 2950.45 34.74 o 4 1 1 7736.21 7344.94 79.72 o 5 1 1 0.40 -8.26 8.26 o 6 1 1 2494.11 2372.87 36.87 o 7 1 1 5120.17 4472.38 54.22 o 8 1 1 834.35 844.99 22.91 o 9 1 1 274.03 213.43 13.64 o 10 1 1 2117.94 2244.89 37.55 o 11 1 1 3240.32 3898.24 51.28 o 12 1 1 1639.39 1659.29 33.09 o 13 1 1 963.08 829.33 29.26 o 14 1 1 23.12 59.06 13.06 o 15 1 1 244.25 249.31 23.42 o 16 1 1 179.13 209.73 23.27 o 17 1 1 3220.27 2717.55 57.29 o 18 1 1 214.55 235.91 24.70 o 19 1 1 106.29 122.28 21.11 o 20 1 1 1517.18 1350.70 60.16 o 21 1 1 144.24 132.55 24.99 o 22 1 1 394.39 375.32 42.38 o 23 1 1 402.70 479.73 48.49 o 24 1 1 215.32 138.06 55.18 o 25 1 1 271.62 178.81 44.25 o 26 1 1 3.91 49.18 42.72 o 27 1 1 1008.20 964.34 105.86 o 28 1 1 37.56 54.92 45.61 o 29 1 1 170.58 128.52 55.66 o 30 1 1 275.98 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