#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:44:07 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181088 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216830.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216830_Fobs loop_ _publ_author_name 'Han, Li-Jun' 'Yang, Shu-Ping' 'Wang, Da-Qi' 'Xia, Hai-Tao' _publ_section_title ; {Bis[2-(3,4-methylenedioxybenzylamino)ethyl]amine}dichloridozinc(II) hemihydrate ; _journal_coeditor_code XU2337 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2929 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.934 _cell_angle_gamma 90.000 _cell_length_a 24.0423 _cell_length_b 13.0193 _cell_length_c 7.2678 _exptl_crystal_F_000 1068.00 _reflns_d_resolution_high 0.8406 _cod_data_source_file xu2337Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070803e in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 227.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3655.59 5333.15 74.79 o 3 0 0 44.78 166.49 44.01 o 4 0 0 34903.25 40838.54 245.16 o 5 0 0 57.07 19.69 17.54 o 6 0 0 19421.54 22919.11 220.68 o 7 0 0 1317.85 1399.88 45.56 o 8 0 0 1545.34 1687.02 57.53 o 9 0 0 729.46 885.03 31.24 o 10 0 0 8906.05 10534.33 108.96 o 11 0 0 85.19 228.94 22.12 o 12 0 0 658.75 705.55 33.82 o 13 0 0 4684.87 5564.98 106.88 o 14 0 0 1086.91 1261.94 77.37 o 15 0 0 85.60 98.01 27.22 o 16 0 0 96.83 122.78 30.02 o 17 0 0 704.75 768.05 53.17 o 18 0 0 158.74 216.52 46.70 o 19 0 0 1068.37 1182.68 145.48 o 20 0 0 1980.14 2155.31 85.32 o 21 0 0 163.44 195.03 39.54 o 22 0 0 415.24 519.95 72.20 o 23 0 0 52.79 67.04 54.88 o 24 0 0 894.80 1241.34 111.80 o 25 0 0 138.45 249.75 70.91 o 26 0 0 890.65 1236.39 116.54 o 27 0 0 181.31 301.19 77.26 o 28 0 0 223.46 287.95 76.62 o 1 1 0 2109.27 1995.70 39.91 o 2 1 0 567.09 666.60 14.41 o 3 1 0 5173.14 4805.15 155.92 o 4 1 0 1526.75 1730.93 48.05 o 5 1 0 308.84 214.66 11.12 o 6 1 0 5749.05 6283.98 105.24 o 7 1 0 132.29 101.93 26.17 o 8 1 0 8021.47 8871.06 72.75 o 9 1 0 1090.09 1079.46 33.47 o 10 1 0 3044.90 3522.35 50.23 o 11 1 0 4281.00 4699.58 113.24 o 12 1 0 91.01 124.63 19.68 o 13 1 0 82.79 153.47 16.73 o 14 1 0 48.36 79.15 15.81 o 15 1 0 2.99 2.41 13.71 o 16 1 0 28.23 32.33 16.53 o 17 1 0 596.89 503.87 29.15 o 18 1 0 9.06 9.85 21.34 o 19 1 0 684.31 767.58 54.85 o 20 1 0 1111.35 1198.28 55.63 o 21 1 0 97.23 165.03 32.84 o 22 1 0 531.89 641.10 46.95 o 23 1 0 2.80 72.89 31.57 o 24 1 0 460.64 481.79 45.72 o 25 1 0 15.48 63.39 41.91 o 26 1 0 44.70 102.43 45.79 o 27 1 0 3.66 23.56 42.41 o 28 1 0 6.58 41.98 42.86 o 0 2 0 8922.10 9154.16 83.36 o 1 2 0 1769.49 2109.85 31.46 o 2 2 0 47189.60 54906.88 1682.80 o 3 2 0 1815.41 2126.45 86.46 o 4 2 0 4561.00 4270.02 64.42 o 5 2 0 1275.50 1255.11 31.71 o 6 2 0 419.36 634.35 20.97 o 7 2 0 3698.10 4352.98 100.04 o 8 2 0 5397.42 5682.53 119.66 o 9 2 0 3024.41 3247.58 51.39 o 10 2 0 8639.80 9576.79 171.19 o 11 2 0 96.14 106.07 42.75 o 12 2 0 3985.13 4195.03 66.85 o 13 2 0 1212.71 1224.67 53.16 o 14 2 0 4371.22 4697.74 74.34 o 15 2 0 90.76 123.97 41.39 o 16 2 0 2828.71 2756.89 61.68 o 17 2 0 7.88 65.96 29.32 o 18 2 0 5434.77 5564.16 194.19 o 19 2 0 55.20 218.13 27.40 o 20 2 0 908.89 936.99 75.42 o 21 2 0 59.67 133.78 28.10 o 22 2 0 2697.03 3117.84 122.00 o 23 2 0 75.82 191.85 36.30 o 24 2 0 801.70 944.29 54.33 o 25 2 0 1.02 37.24 36.81 o 26 2 0 246.40 320.15 42.90 o 27 2 0 4.27 -2.20 37.64 o 28 2 0 330.25 362.58 58.63 o 1 3 0 5826.78 8399.03 144.13 o 2 3 0 6711.41 7892.29 155.08 o 3 3 0 2351.50 3678.82 72.20 o 4 3 0 35.36 42.70 10.21 o 5 3 0 3651.64 4937.85 109.55 o 6 3 0 2507.48 2862.95 39.42 o 7 3 0 3958.99 4951.60 89.27 o 8 3 0 7452.26 9240.29 252.19 o 9 3 0 4250.27 4797.84 112.10 o 10 3 0 1567.56 1688.52 45.68 o 11 3 0 8270.96 9355.33 146.62 o 12 3 0 1.22 27.82 16.62 o 13 3 0 1478.29 1230.41 39.78 o 14 3 0 14.13 23.04 27.66 o 15 3 0 1658.61 1905.95 51.80 o 16 3 0 25.72 18.37 19.06 o 17 3 0 1147.48 1368.27 47.52 o 18 3 0 172.41 182.14 25.06 o 19 3 0 205.10 172.44 26.07 o 20 3 0 1.07 5.79 23.39 o 21 3 0 531.59 626.65 40.78 o 22 3 0 10.09 20.20 26.00 o 23 3 0 301.06 342.62 61.40 o 24 3 0 1.10 14.35 31.26 o 25 3 0 39.65 42.94 32.12 o 26 3 0 11.60 22.23 30.32 o 27 3 0 1.61 8.45 30.99 o 0 4 0 1038.79 1173.65 71.02 o 1 4 0 607.34 823.72 23.54 o 2 4 0 15.45 9.08 10.83 o 3 4 0 10603.26 13383.60 223.50 o 4 4 0 4617.95 5748.63 197.20 o 5 4 0 1.42 -3.16 10.68 o 6 4 0 344.75 330.96 17.46 o 7 4 0 0.88 -8.80 11.14 o 8 4 0 3690.18 4251.62 54.50 o 9 4 0 323.66 399.08 21.39 o 10 4 0 5877.53 6882.34 129.23 o 11 4 0 265.59 236.94 19.51 o 12 4 0 2792.98 2815.68 57.17 o 13 4 0 64.31 59.61 18.68 o 14 4 0 5069.52 5607.06 85.64 o 15 4 0 291.35 316.67 27.80 o 16 4 0 2531.18 2722.27 64.84 o 17 4 0 331.42 422.51 55.93 o 18 4 0 1774.31 2116.74 60.47 o 19 4 0 561.20 624.40 37.79 o 20 4 0 1687.43 1822.46 59.46 o 21 4 0 24.25 62.29 28.87 o 22 4 0 155.59 203.30 32.56 o 23 4 0 42.36 17.96 26.33 o 24 4 0 130.00 175.41 37.33 o 25 4 0 2.58 10.07 30.36 o 26 4 0 71.52 70.16 64.46 o 27 4 0 0.89 48.32 65.10 o 1 5 0 454.82 461.05 21.14 o 2 5 0 2120.09 2572.20 44.99 o 3 5 0 4707.30 5535.88 67.14 o 4 5 0 3285.94 4112.33 62.78 o 5 5 0 2419.47 3097.88 60.31 o 6 5 0 1033.69 1224.11 52.88 o 7 5 0 5248.76 5964.51 178.72 o 8 5 0 665.40 762.18 28.13 o 9 5 0 1538.88 1531.56 37.56 o 10 5 0 1540.90 1768.71 41.08 o 11 5 0 3088.37 3236.50 56.50 o 12 5 0 70.28 69.55 18.49 o 13 5 0 4129.74 4515.06 69.47 o 14 5 0 938.54 1123.69 38.24 o 15 5 0 2436.25 2727.93 63.44 o 16 5 0 104.06 131.33 21.47 o 17 5 0 1929.25 1960.76 82.16 o 18 5 0 22.96 30.74 22.14 o 19 5 0 1999.09 2235.47 65.95 o 20 5 0 0.37 44.63 26.01 o 21 5 0 1677.74 2043.63 105.79 o 22 5 0 168.84 233.78 33.65 o 23 5 0 918.53 1008.62 100.29 o 24 5 0 43.18 78.34 59.83 o 25 5 0 228.50 317.55 83.61 o 26 5 0 66.33 3.23 63.06 o 0 6 0 716.64 847.50 42.53 o 1 6 0 7.34 26.54 14.83 o 2 6 0 2207.68 2449.78 51.12 o 3 6 0 4794.45 5602.22 76.03 o 4 6 0 2453.54 2757.13 73.48 o 5 6 0 1154.12 1041.81 34.64 o 6 6 0 203.37 218.34 21.79 o 7 6 0 2956.13 2951.77 126.02 o 8 6 0 3650.02 4196.05 111.56 o 9 6 0 306.10 265.55 20.83 o 10 6 0 105.54 104.10 18.74 o 11 6 0 869.58 903.31 33.42 o 12 6 0 585.59 607.83 29.97 o 13 6 0 2.77 -8.59 16.60 o 14 6 0 424.00 505.29 28.76 o 15 6 0 36.82 31.60 19.88 o 16 6 0 3.71 -8.09 17.33 o 17 6 0 154.83 97.48 24.27 o 18 6 0 206.56 176.23 28.38 o 19 6 0 935.70 963.54 65.43 o 20 6 0 7.41 28.91 32.28 o 21 6 0 76.60 47.61 43.30 o 22 6 0 20.77 24.69 45.30 o 23 6 0 100.61 36.83 68.01 o 24 6 0 58.40 21.88 42.49 o 25 6 0 25.63 -31.42 59.61 o 26 6 0 0.53 -11.51 60.47 o 1 7 0 14532.58 16638.12 297.32 o 2 7 0 194.70 172.28 21.22 o 3 7 0 8672.55 9644.98 104.16 o 4 7 0 187.90 247.54 24.03 o 5 7 0 12284.78 13862.88 127.29 o 6 7 0 687.34 789.04 34.88 o 7 7 0 4925.27 5251.74 249.04 o 8 7 0 449.21 658.92 29.09 o 9 7 0 1169.77 1309.55 38.60 o 10 7 0 53.16 48.19 17.25 o 11 7 0 340.49 360.90 25.55 o 12 7 0 0.31 -16.63 16.72 o 13 7 0 277.25 424.93 28.22 o 14 7 0 600.97 717.48 33.82 o 15 7 0 767.44 859.44 44.67 o 16 7 0 164.96 177.46 34.08 o 17 7 0 243.56 156.11 46.01 o 18 7 0 222.30 211.70 48.70 o 19 7 0 1857.74 2045.83 177.71 o 20 7 0 0.22 23.54 42.89 o 21 7 0 66.21 91.20 45.95 o 22 7 0 26.10 -12.85 46.32 o 23 7 0 279.89 305.70 61.32 o 24 7 0 7.49 -15.22 45.16 o 25 7 0 376.42 446.89 97.81 o 0 8 0 459.64 598.26 44.06 o 1 8 0 71.32 33.16 19.05 o 2 8 0 469.54 572.32 31.15 o 3 8 0 474.59 531.92 29.97 o 4 8 0 60.01 40.51 19.22 o 5 8 0 21.77 33.42 18.69 o 6 8 0 341.94 355.64 27.88 o 7 8 0 523.08 598.28 39.72 o 8 8 0 43.44 66.54 20.18 o 9 8 0 34.69 9.73 16.21 o 10 8 0 140.57 123.16 24.70 o 11 8 0 1063.95 1331.24 52.47 o 12 8 0 84.38 90.58 25.66 o 13 8 0 74.65 86.77 25.47 o 14 8 0 343.27 387.78 42.11 o 15 8 0 256.92 196.56 47.06 o 16 8 0 63.39 95.81 40.12 o 17 8 0 58.32 24.56 43.45 o 18 8 0 3.35 4.00 38.88 o 19 8 0 5.05 -29.48 37.93 o 20 8 0 74.93 38.84 46.51 o 21 8 0 0.14 9.57 45.30 o 22 8 0 21.06 20.44 45.90 o 23 8 0 54.24 78.96 49.95 o 24 8 0 2.32 37.21 50.76 o 1 9 0 1809.61 2015.34 57.02 o 2 9 0 24.94 34.41 22.37 o 3 9 0 3750.45 3770.02 74.29 o 4 9 0 74.47 62.65 22.28 o 5 9 0 1892.02 2182.81 68.94 o 6 9 0 49.83 107.28 28.90 o 7 9 0 813.31 954.13 50.38 o 8 9 0 630.87 712.43 45.51 o 9 9 0 2565.01 2990.19 122.05 o 10 9 0 17.51 44.22 27.95 o 11 9 0 287.05 448.19 40.73 o 12 9 0 72.42 62.95 31.93 o 13 9 0 975.23 1244.98 62.44 o 14 9 0 76.38 76.88 41.01 o 15 9 0 512.03 607.71 70.43 o 16 9 0 13.79 -13.26 41.65 o 17 9 0 937.63 1074.79 83.01 o 18 9 0 2.11 39.30 42.25 o 19 9 0 317.69 359.56 62.98 o 20 9 0 23.41 19.70 46.86 o 21 9 0 380.79 389.95 78.34 o 22 9 0 3.26 15.89 45.97 o 23 9 0 322.96 273.00 60.11 o 0 10 0 82.78 83.74 32.68 o 1 10 0 196.19 240.40 32.92 o 2 10 0 695.65 755.99 50.00 o 3 10 0 107.63 91.54 30.10 o 4 10 0 212.20 182.49 32.90 o 5 10 0 865.71 785.76 48.71 o 6 10 0 0.91 5.72 23.27 o 7 10 0 14.26 10.02 24.78 o 8 10 0 672.51 671.50 47.73 o 9 10 0 1225.34 1264.80 61.65 o 10 10 0 110.54 135.69 32.81 o 11 10 0 3.81 14.60 28.91 o 12 10 0 756.87 781.46 59.05 o 13 10 0 21.67 -3.24 37.55 o 14 10 0 69.77 51.68 44.89 o 15 10 0 0.04 -3.54 45.20 o 16 10 0 108.00 60.15 49.35 o 17 10 0 1.40 8.83 42.61 o 18 10 0 0.30 -0.24 43.57 o 19 10 0 0.73 3.66 40.59 o 20 10 0 20.15 40.35 46.40 o 21 10 0 46.86 8.76 47.17 o 1 11 0 145.91 116.56 39.53 o 2 11 0 87.48 26.34 33.30 o 3 11 0 5.57 17.83 36.98 o 4 11 0 0.10 -3.62 30.34 o 5 11 0 530.26 562.17 46.27 o 6 11 0 55.60 43.63 30.89 o 7 11 0 206.51 252.10 37.85 o 8 11 0 0.33 10.94 29.82 o 9 11 0 733.20 857.27 56.36 o 10 11 0 108.30 186.02 37.90 o 11 11 0 1524.83 1757.27 76.43 o 12 11 0 348.19 451.22 47.75 o 13 11 0 291.95 439.21 62.13 o 14 11 0 39.31 74.28 63.92 o 15 11 0 1447.98 1768.38 108.56 o 16 11 0 78.57 105.49 51.51 o 17 11 0 779.60 951.49 84.97 o 18 11 0 55.45 39.11 44.90 o 19 11 0 443.86 548.34 108.25 o 20 11 0 82.18 99.32 51.77 o 0 12 0 332.04 399.33 81.78 o 1 12 0 15.78 -9.14 35.02 o 2 12 0 22.63 83.62 38.97 o 3 12 0 66.38 37.45 36.68 o 4 12 0 14.92 6.30 38.92 o 5 12 0 153.80 92.24 43.46 o 6 12 0 340.11 305.66 52.05 o 7 12 0 5.15 2.03 35.94 o 8 12 0 79.23 50.58 40.32 o 9 12 0 437.97 392.80 44.91 o 10 12 0 252.06 261.42 40.66 o 11 12 0 156.26 187.15 39.03 o 12 12 0 474.38 517.16 68.17 o 13 12 0 97.11 126.80 52.75 o 14 12 0 536.53 736.24 106.85 o 15 12 0 131.23 178.17 59.07 o 16 12 0 190.23 222.36 61.11 o 17 12 0 1.63 42.54 52.69 o 18 12 0 139.38 150.72 58.87 o 1 13 0 424.35 593.07 62.99 o 2 13 0 194.93 218.74 54.32 o 3 13 0 355.18 442.11 60.10 o 4 13 0 173.30 222.95 48.73 o 5 13 0 257.81 353.10 57.60 o 6 13 0 409.98 444.40 75.16 o 7 13 0 576.16 681.51 68.32 o 8 13 0 2.03 23.98 40.77 o 9 13 0 110.59 135.79 50.07 o 10 13 0 61.19 88.93 47.44 o 11 13 0 106.55 177.01 82.96 o 12 13 0 18.72 14.74 60.04 o 13 13 0 128.84 235.66 82.21 o 14 13 0 2.80 -35.39 47.17 o 15 13 0 94.26 186.08 62.10 o 0 14 0 548.94 583.98 100.93 o 1 14 0 209.12 189.61 54.99 o 2 14 0 351.55 333.82 60.73 o 3 14 0 38.56 46.50 43.93 o 4 14 0 560.12 655.77 72.37 o 5 14 0 15.61 35.47 39.44 o 6 14 0 403.34 439.13 61.96 o 7 14 0 10.46 59.56 49.19 o 8 14 0 155.75 170.54 50.10 o 9 14 0 5.01 14.51 45.49 o 10 14 0 97.87 73.49 73.71 o 11 14 0 85.12 3.87 65.96 o 12 14 0 47.86 69.08 80.60 o 1 15 0 75.34 94.96 51.20 o 2 15 0 9.46 59.78 44.78 o 3 15 0 89.40 94.11 52.11 o 4 15 0 21.78 7.16 44.33 o 5 15 0 31.61 32.27 52.39 o 6 15 0 13.36 26.49 49.46 o 7 15 0 50.54 23.25 52.33 o -28 1 1 107.15 148.80 48.65 o -27 1 1 460.09 494.22 57.44 o -26 1 1 84.34 180.04 47.36 o -25 1 1 344.75 359.48 51.66 o -24 1 1 166.43 433.68 56.29 o -23 1 1 798.37 959.42 134.88 o -22 1 1 31.64 75.95 32.59 o -21 1 1 68.85 125.29 34.83 o -20 1 1 756.35 950.96 122.40 o -19 1 1 1192.14 1129.85 63.43 o -18 1 1 5.04 70.58 32.17 o -17 1 1 1352.45 1180.59 61.22 o -16 1 1 323.05 267.28 74.30 o -15 1 1 5221.28 4491.05 90.50 o -14 1 1 3198.52 3046.36 73.40 o -13 1 1 2822.86 2553.65 112.98 o -12 1 1 275.43 193.37 37.12 o -11 1 1 7196.45 6107.45 245.65 o -10 1 1 1461.22 1612.01 257.53 o -9 1 1 9450.20 8511.99 216.91 o -8 1 1 136.39 112.66 26.79 o -7 1 1 3457.47 3006.54 56.60 o -6 1 1 1788.90 2046.65 457.24 o -5 1 1 505.75 530.38 94.60 o -4 1 1 697.84 636.40 28.39 o -3 1 1 4280.47 3940.77 115.24 o -2 1 1 71.48 53.48 16.63 o -1 1 1 49098.81 44212.23 1359.50 o 0 1 1 3953.20 3605.70 77.07 o 1 1 1 13318.12 13179.62 177.80 o 2 1 1 283.98 257.93 11.90 o 3 1 1 12916.63 12104.74 234.31 o 4 1 1 1568.37 1663.91 27.83 o 5 1 1 9815.88 8976.30 122.38 o 6 1 1 159.89 135.57 12.12 o 7 1 1 9750.36 8507.94 204.63 o 8 1 1 506.32 607.02 244.40 o 9 1 1 10762.68 9317.02 156.46 o 10 1 1 640.66 476.46 141.57 o 11 1 1 10616.06 9497.63 183.08 o 12 1 1 5946.37 5102.92 65.19 o 13 1 1 1465.84 1733.34 140.70 o 14 1 1 1328.07 1606.33 128.51 o 15 1 1 822.37 885.49 78.95 o 16 1 1 148.70 212.39 52.41 o 17 1 1 771.96 724.22 36.61 o 18 1 1 225.43 270.42 31.75 o 19 1 1 1442.12 1366.11 50.79 o 20 1 1 300.06 269.68 30.68 o 21 1 1 228.06 218.55 30.12 o 22 1 1 303.78 341.37 35.17 o 23 1 1 1451.62 1394.19 57.70 o 24 1 1 143.93 192.34 33.22 o 25 1 1 598.68 641.00 45.06 o 26 1 1 15.21 164.90 40.61 o 27 1 1 523.69 476.55 50.05 o -28 2 1 1.51 30.93 44.66 o -27 2 1 6.89 48.42 42.70 o -26 2 1 10.27 31.53 46.33 o -25 2 1 39.75 44.90 40.80 o -24 2 1 9.84 99.01 34.94 o -23 2 1 310.94 324.25 44.37 o -22 2 1 365.30 300.51 41.05 o -21 2 1 0.82 117.00 49.50 o -20 2 1 267.27 284.07 34.94 o -19 2 1 54.59 104.70 29.80 o -18 2 1 94.98 42.71 22.05 o -17 2 1 0.14 22.13 20.02 o -16 2 1 66.22 91.04 21.06 o -15 2 1 64.14 156.39 43.90 o -14 2 1 1369.08 1149.43 42.52 o -13 2 1 312.01 395.95 25.30 o -12 2 1 1706.24 1438.73 40.86 o -11 2 1 3377.33 3486.73 103.42 o -10 2 1 8474.45 7750.56 123.57 o -9 2 1 1785.24 1791.42 59.49 o -8 2 1 5067.88 4442.58 183.28 o -7 2 1 439.30 723.92 148.59 o -6 2 1 17133.23 14810.50 406.18 o -5 2 1 2940.17 3192.40 304.82 o -4 2 1 21433.96 18410.70 284.44 o -3 2 1 7424.02 6558.38 69.92 o -2 2 1 523.26 459.97 22.99 o -1 2 1 9908.56 9496.65 103.41 o 0 2 1 380.38 350.72 18.39 o 1 2 1 36839.08 34238.50 890.69 o 2 2 1 61.69 49.10 10.95 o 3 2 1 18.48 41.61 7.57 o 4 2 1 5498.73 5473.90 123.09 o 5 2 1 6623.77 7273.50 306.08 o 6 2 1 1990.47 1840.85 89.89 o 7 2 1 5141.90 5381.49 106.22 o 8 2 1 943.00 1122.79 105.07 o 9 2 1 2031.54 2733.50 309.72 o 10 2 1 3333.62 3647.55 165.52 o 11 2 1 54.64 53.18 23.53 o 12 2 1 929.87 964.77 40.10 o 13 2 1 9.01 42.51 35.92 o 14 2 1 1020.96 918.96 38.90 o 15 2 1 30.68 35.29 17.36 o 16 2 1 289.11 211.21 21.76 o 17 2 1 332.06 278.34 24.71 o 18 2 1 119.68 77.85 20.43 o 19 2 1 1180.33 935.39 44.01 o 20 2 1 1122.85 954.16 45.76 o 21 2 1 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3583.55 95.13 o -2 5 2 5.12 1536.69 275.94 o -1 5 2 2372.14 2400.79 54.93 o 0 5 2 1144.14 1437.96 105.52 o 1 5 2 7056.10 6542.52 276.71 o 2 5 2 1455.86 1880.87 154.33 o 3 5 2 2829.40 2226.79 56.09 o 4 5 2 97.43 686.25 202.94 o 5 5 2 5021.00 4420.61 90.20 o 6 5 2 601.45 485.28 27.91 o 7 5 2 4397.37 4105.84 169.96 o 8 5 2 0.76 12.01 12.15 o 9 5 2 6639.85 6710.35 122.24 o 10 5 2 459.45 445.25 24.63 o 11 5 2 4331.43 4300.47 64.89 o 12 5 2 1.98 66.39 23.07 o 13 5 2 274.54 255.18 33.34 o 14 5 2 69.13 336.19 37.44 o 15 5 2 716.11 763.03 50.56 o 16 5 2 139.06 169.90 35.58 o 17 5 2 4.78 4.05 29.88 o 18 5 2 70.50 179.82 43.26 o 19 5 2 325.94 342.98 85.01 o 20 5 2 27.50 131.92 44.26 o 21 5 2 369.12 372.84 59.81 o 22 5 2 0.35 167.53 50.63 o 23 5 2 45.86 47.00 42.61 o 24 5 2 59.88 149.63 45.82 o 25 5 2 28.81 31.60 45.52 o -26 6 2 61.72 54.26 32.81 o -25 6 2 169.74 141.13 35.56 o -24 6 2 28.28 -7.57 30.60 o -23 6 2 194.17 214.12 38.59 o -22 6 2 37.44 35.53 30.29 o -21 6 2 84.13 228.48 41.12 o -20 6 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