#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2216843.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216843_Fobs loop_ _publ_author_name 'Mague, Joel T.' 'Punji, Benudhar' 'Ganesamoorthy, Chelladurai' 'Balakrishna, Maravanji S.' _publ_section_title ; O-2-Naphthyl diphenylselenophosphinate ; _journal_coeditor_code XU2359 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4645 _journal_volume 63 _journal_year 2007 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.672 _cell_angle_gamma 90.000 _cell_length_a 9.9490 _cell_length_b 19.0444 _cell_length_c 9.9552 _exptl_crystal_F_000 824.00 _reflns_d_resolution_high 0.7389 _[local]_cod_data_source_file xu2359Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' msb386_0m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 215.30 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 75.03 77.75 2.85 o 4 0 0 1630.18 1495.32 29.62 o 6 0 0 3674.23 3421.66 59.97 o 8 0 0 3619.63 3477.13 63.37 o 10 0 0 726.94 771.26 32.94 o 12 0 0 10.13 31.05 14.83 o 1 1 0 4588.23 4592.25 55.34 o 2 1 0 518.16 472.93 9.35 o 3 1 0 6662.78 6607.46 70.71 o 4 1 0 354.64 345.02 5.13 o 5 1 0 3086.27 2959.44 33.97 o 6 1 0 177.59 145.19 6.28 o 7 1 0 1800.57 1638.88 23.41 o 8 1 0 1097.60 945.48 16.05 o 9 1 0 1005.82 931.93 16.92 o 10 1 0 844.39 796.81 16.46 o 11 1 0 47.23 50.38 8.45 o 12 1 0 318.89 321.35 14.49 o 0 2 0 9977.04 8827.41 293.56 o 1 2 0 355.08 315.96 4.67 o 2 2 0 5007.42 5105.35 57.46 o 3 2 0 724.47 781.34 10.41 o 4 2 0 37.39 41.83 2.13 o 5 2 0 9.42 2.59 2.45 o 6 2 0 9.22 26.00 3.69 o 7 2 0 214.22 198.10 10.17 o 8 2 0 136.60 140.31 7.68 o 9 2 0 683.36 673.80 14.35 o 10 2 0 50.80 63.60 8.22 o 11 2 0 393.22 414.22 15.31 o 12 2 0 83.41 114.28 11.56 o 1 3 0 13139.50 12816.18 144.04 o 2 3 0 99.48 111.81 3.57 o 3 3 0 11027.27 11054.22 97.66 o 4 3 0 125.64 150.72 4.02 o 5 3 0 1916.36 1709.45 23.89 o 6 3 0 1102.66 1032.21 15.64 o 7 3 0 7771.48 7452.06 83.70 o 8 3 0 857.97 795.07 14.57 o 9 3 0 1026.00 985.80 17.53 o 10 3 0 24.18 45.46 9.03 o 11 3 0 135.37 149.40 11.85 o 12 3 0 181.43 214.54 13.88 o 0 4 0 4894.51 4679.20 57.10 o 1 4 0 834.57 760.10 9.61 o 2 4 0 20331.22 19294.17 184.04 o 3 4 0 675.48 658.24 8.10 o 4 4 0 4572.23 4204.30 38.62 o 5 4 0 260.60 302.75 5.23 o 6 4 0 4596.26 4359.65 47.36 o 7 4 0 993.61 1013.42 14.68 o 8 4 0 1170.97 1026.47 17.10 o 9 4 0 1877.01 1820.41 26.19 o 10 4 0 1092.38 1140.54 23.17 o 11 4 0 142.42 183.23 12.61 o 12 4 0 108.52 174.75 13.38 o 1 5 0 158.93 156.99 3.90 o 2 5 0 1922.73 1846.03 20.37 o 3 5 0 124.77 92.05 3.11 o 4 5 0 216.84 278.67 5.01 o 5 5 0 2300.87 2204.19 25.98 o 6 5 0 4.99 4.96 3.86 o 7 5 0 111.27 99.82 5.76 o 8 5 0 71.32 83.43 7.05 o 9 5 0 147.27 134.19 9.88 o 10 5 0 689.24 697.63 18.09 o 11 5 0 252.98 284.00 15.34 o 12 5 0 133.63 159.05 17.33 o 0 6 0 15143.67 14223.71 170.58 o 1 6 0 62.84 80.84 3.55 o 2 6 0 2283.23 2090.08 21.90 o 3 6 0 311.79 304.13 6.78 o 4 6 0 1988.49 1958.57 23.44 o 5 6 0 601.56 526.09 8.00 o 6 6 0 1058.94 971.80 14.60 o 7 6 0 3.30 1.29 4.85 o 8 6 0 1399.68 1236.90 21.15 o 9 6 0 13.33 18.53 8.72 o 10 6 0 76.18 88.95 11.03 o 11 6 0 263.37 272.30 15.43 o 12 6 0 82.06 136.14 14.21 o 1 7 0 8496.00 7892.43 73.33 o 2 7 0 2743.41 2671.11 26.64 o 3 7 0 6685.34 6126.60 57.75 o 4 7 0 970.81 974.85 11.75 o 5 7 0 5443.70 4916.73 49.80 o 6 7 0 1407.38 1263.06 16.44 o 7 7 0 4814.01 4544.01 60.33 o 8 7 0 170.55 135.40 8.52 o 9 7 0 1246.11 1217.28 26.07 o 10 7 0 184.34 214.33 14.05 o 11 7 0 346.15 357.40 17.89 o 12 7 0 17.75 23.72 12.46 o 0 8 0 5045.56 5160.18 64.13 o 1 8 0 1.08 3.96 2.25 o 2 8 0 1817.84 1598.07 17.19 o 3 8 0 1032.70 998.60 12.65 o 4 8 0 14268.98 14155.25 130.74 o 5 8 0 73.44 97.63 5.25 o 6 8 0 301.36 263.16 8.39 o 7 8 0 35.50 22.46 6.97 o 8 8 0 102.17 113.39 9.03 o 9 8 0 3.88 -0.35 8.88 o 10 8 0 494.51 518.58 22.39 o 11 8 0 361.79 359.73 17.36 o 12 8 0 162.57 178.34 27.50 o 1 9 0 519.85 468.28 6.41 o 2 9 0 182.99 156.03 4.89 o 3 9 0 293.81 305.98 6.41 o 4 9 0 79.56 51.79 4.60 o 5 9 0 28.45 23.34 5.08 o 6 9 0 1922.65 1729.57 24.70 o 7 9 0 1012.69 994.30 22.45 o 8 9 0 601.85 601.48 24.48 o 9 9 0 366.17 320.97 12.08 o 10 9 0 14.12 10.97 10.60 o 11 9 0 12.16 17.18 11.97 o 0 10 0 1122.63 953.11 15.61 o 1 10 0 406.91 353.39 5.80 o 2 10 0 13768.04 13814.64 127.71 o 3 10 0 916.58 876.09 12.88 o 4 10 0 5366.13 5053.68 54.15 o 5 10 0 1019.03 982.36 15.75 o 6 10 0 1302.27 1228.43 19.65 o 7 10 0 851.91 788.48 20.38 o 8 10 0 389.84 389.75 13.27 o 9 10 0 251.81 243.81 12.23 o 10 10 0 820.89 884.93 37.45 o 11 10 0 1.92 12.97 12.49 o 1 11 0 5550.78 5552.42 47.87 o 2 11 0 5.63 3.31 3.58 o 3 11 0 6838.70 6467.19 64.89 o 4 11 0 74.00 69.38 6.23 o 5 11 0 3949.45 3753.25 44.77 o 6 11 0 399.45 353.40 10.89 o 7 11 0 834.09 817.65 16.28 o 8 11 0 316.61 313.79 13.03 o 9 11 0 127.38 116.67 11.26 o 10 11 0 6.82 12.30 11.45 o 11 11 0 1652.06 1745.33 81.44 o 0 12 0 1288.16 1324.94 20.86 o 1 12 0 94.66 105.84 6.11 o 2 12 0 172.27 191.93 6.69 o 3 12 0 60.01 61.27 5.80 o 4 12 0 837.62 755.21 14.95 o 5 12 0 948.72 878.77 15.71 o 6 12 0 532.46 491.78 12.21 o 7 12 0 251.56 236.10 9.98 o 8 12 0 18.57 14.45 10.66 o 9 12 0 33.08 32.04 9.86 o 10 12 0 245.71 228.54 18.95 o 11 12 0 5.36 -1.44 12.70 o 1 13 0 227.45 201.27 6.76 o 2 13 0 309.25 290.84 8.69 o 3 13 0 3019.48 2837.69 35.44 o 4 13 0 11.04 11.05 6.46 o 5 13 0 1550.03 1425.63 21.63 o 6 13 0 65.92 67.10 7.85 o 7 13 0 549.93 558.75 14.51 o 8 13 0 67.73 57.67 10.11 o 9 13 0 365.73 366.13 15.32 o 10 13 0 29.72 13.83 10.18 o 11 13 0 177.25 211.75 37.79 o 0 14 0 1970.73 1888.60 33.95 o 1 14 0 11.10 3.27 5.30 o 2 14 0 1617.15 1490.60 23.89 o 3 14 0 105.63 117.05 7.95 o 4 14 0 10548.52 10224.95 113.26 o 5 14 0 12.63 19.53 7.41 o 6 14 0 997.13 1000.99 21.00 o 7 14 0 94.17 81.51 9.11 o 8 14 0 365.40 346.30 15.26 o 9 14 0 23.85 12.06 10.65 o 10 14 0 329.45 345.60 18.34 o 1 15 0 1324.16 1318.99 23.22 o 2 15 0 1201.09 1164.58 18.86 o 3 15 0 4431.70 4365.17 52.27 o 4 15 0 1925.59 1913.74 27.26 o 5 15 0 151.63 157.31 9.72 o 6 15 0 36.62 26.57 8.35 o 7 15 0 171.68 162.98 10.69 o 8 15 0 10.55 0.12 10.50 o 9 15 0 112.22 126.88 12.90 o 10 15 0 6.26 -1.09 11.17 o 0 16 0 3.20 5.38 16.92 o 1 16 0 119.05 109.18 9.67 o 2 16 0 158.28 142.02 9.48 o 3 16 0 37.72 39.01 8.50 o 4 16 0 62.55 63.70 9.23 o 5 16 0 26.56 18.89 8.46 o 6 16 0 36.05 28.77 9.46 o 7 16 0 265.52 260.07 12.58 o 8 16 0 1.15 -4.41 11.11 o 9 16 0 70.59 53.05 12.52 o 10 16 0 20.67 33.16 18.39 o 1 17 0 290.19 285.24 11.76 o 2 17 0 90.04 100.33 10.00 o 3 17 0 4344.89 4290.59 64.16 o 4 17 0 35.92 36.22 9.52 o 5 17 0 2347.27 2310.39 34.67 o 6 17 0 5.29 21.38 9.88 o 7 17 0 146.45 149.12 11.72 o 8 17 0 54.05 60.69 13.28 o 9 17 0 97.04 105.03 13.88 o 0 18 0 2087.60 2224.63 69.29 o 1 18 0 167.97 162.90 16.94 o 2 18 0 3311.49 3342.80 48.51 o 3 18 0 869.97 840.34 21.66 o 4 18 0 487.22 508.40 26.12 o 5 18 0 724.25 725.46 18.22 o 6 18 0 1132.45 1163.90 28.83 o 7 18 0 180.96 182.71 13.41 o 8 18 0 372.96 405.20 19.95 o 9 18 0 181.35 232.94 31.63 o 1 19 0 1128.32 1214.38 44.61 o 2 19 0 22.63 60.59 15.85 o 3 19 0 284.78 293.84 17.87 o 4 19 0 15.53 8.15 10.90 o 5 19 0 353.24 337.51 18.66 o 6 19 0 349.19 310.87 17.36 o 7 19 0 229.52 248.02 14.97 o 8 19 0 23.94 11.86 14.17 o 0 20 0 583.10 540.71 45.56 o 1 20 0 12.73 -4.56 15.47 o 2 20 0 1236.80 1301.94 36.55 o 3 20 0 0.79 -17.34 17.34 o 4 20 0 188.02 190.84 13.95 o 5 20 0 38.13 29.05 11.91 o 6 20 0 112.85 90.10 14.29 o 7 20 0 1.39 20.89 13.08 o 8 20 0 23.93 0.46 32.60 o 1 21 0 2638.06 2893.62 141.43 o 2 21 0 295.50 356.83 28.19 o 3 21 0 777.75 859.95 32.58 o 4 21 0 47.31 37.87 17.18 o 5 21 0 324.58 364.06 21.49 o 6 21 0 303.24 264.24 17.66 o 7 21 0 561.52 603.53 21.67 o 0 22 0 1572.85 1786.74 114.42 o 1 22 0 165.28 177.17 25.53 o 2 22 0 36.20 15.89 21.95 o 3 22 0 19.72 6.23 17.44 o 4 22 0 145.50 147.85 24.36 o 5 22 0 2.99 -16.28 16.28 o 6 22 0 347.99 371.64 21.46 o 1 23 0 17.52 6.52 22.37 o 2 23 0 63.03 42.05 41.27 o 3 23 0 14.26 1.89 24.69 o 4 23 0 37.08 20.10 18.84 o 5 23 0 54.71 54.23 23.23 o 0 24 0 189.88 232.74 55.66 o 1 24 0 19.09 1.41 23.98 o 2 24 0 468.25 615.47 47.69 o 3 24 0 154.44 161.81 26.95 o 4 24 0 275.95 259.90 43.49 o 1 25 0 921.25 1133.33 47.45 o 2 25 0 32.86 5.18 36.76 o -11 0 1 637.54 624.24 20.80 o -9 0 1 1562.20 1430.09 29.25 o -7 0 1 6339.87 6191.71 104.41 o -5 0 1 10250.61 11058.11 179.07 o -3 0 1 2009.53 2260.24 45.96 o -1 0 1 15648.98 18703.76 606.79 o 1 0 1 5600.12 5816.16 83.25 o 3 0 1 5153.30 4954.23 110.75 o 5 0 1 4136.89 3839.09 52.50 o 7 0 1 7072.00 6735.02 123.40 o 9 0 1 1333.22 1256.81 30.54 o 11 0 1 893.86 998.28 33.66 o -13 1 1 77.58 134.61 43.49 o -12 1 1 60.54 96.41 11.58 o -11 1 1 1312.87 1272.30 26.10 o -10 1 1 230.18 240.66 10.59 o -9 1 1 1930.97 1810.41 25.57 o -8 1 1 887.85 828.09 14.44 o -7 1 1 209.01 171.46 6.71 o -6 1 1 195.04 166.13 5.80 o -5 1 1 8312.15 8798.02 95.43 o -4 1 1 1224.05 1233.33 23.04 o -3 1 1 8275.15 8621.29 87.22 o -2 1 1 13529.61 15264.57 172.51 o -1 1 1 2934.51 3410.02 49.58 o 0 1 1 101.27 119.13 2.89 o 1 1 1 16357.85 16526.55 165.46 o 2 1 1 3576.38 3613.35 39.94 o 3 1 1 2425.50 2307.18 33.10 o 4 1 1 2648.66 2559.59 26.45 o 5 1 1 2346.78 2281.10 25.69 o 6 1 1 1267.79 1122.32 14.43 o 7 1 1 181.55 143.49 7.90 o 8 1 1 2503.40 2476.36 32.43 o 9 1 1 3.42 -4.80 6.66 o 10 1 1 764.06 771.34 16.72 o 11 1 1 2.69 18.38 11.06 o 12 1 1 13.38 22.03 10.76 o -13 2 1 724.14 679.79 63.16 o -12 2 1 747.47 781.12 27.49 o -11 2 1 81.98 101.94 10.38 o -10 2 1 1134.22 1126.37 20.73 o -9 2 1 903.73 842.11 15.59 o -8 2 1 2050.38 1951.76 26.16 o -7 2 1 512.21 467.94 9.75 o -6 2 1 558.88 464.39 7.66 o -5 2 1 224.32 202.28 5.82 o -4 2 1 5892.29 6112.94 60.38 o -3 2 1 3937.68 4318.42 45.89 o -2 2 1 46352.83 50149.37 561.81 o -1 2 1 2529.88 2629.86 30.50 o 0 2 1 1610.96 1643.41 23.91 o 1 2 1 3.88 4.54 1.43 o 2 2 1 1060.04 1058.52 12.17 o 3 2 1 104.13 105.05 3.40 o 4 2 1 1127.88 989.28 11.39 o 5 2 1 275.47 268.11 5.23 o 6 2 1 274.04 229.45 6.95 o 7 2 1 3048.12 2920.26 31.85 o 8 2 1 301.10 283.19 12.87 o 9 2 1 60.64 52.78 7.68 o 10 2 1 337.68 342.23 12.31 o 11 2 1 44.76 23.07 9.62 o 12 2 1 465.16 579.10 21.26 o -13 3 1 86.34 82.84 41.94 o -12 3 1 36.16 43.76 10.63 o -11 3 1 120.08 126.17 11.03 o -10 3 1 227.79 252.14 11.44 o -9 3 1 309.29 303.00 10.19 o -8 3 1 3211.35 3209.01 39.72 o -7 3 1 1142.80 1087.20 16.26 o -6 3 1 1299.56 1262.88 17.28 o -5 3 1 155.47 234.20 5.27 o -4 3 1 151.16 114.97 4.13 o -3 3 1 2107.61 2268.66 24.35 o -2 3 1 17626.72 18284.41 194.18 o -1 3 1 845.44 853.75 13.80 o 0 3 1 10105.71 9954.79 95.18 o 1 3 1 11790.97 11727.98 107.44 o 2 3 1 3213.20 3142.55 32.97 o 3 3 1 1.96 -2.09 2.09 o 4 3 1 2441.12 2360.71 25.01 o 5 3 1 153.29 151.67 5.43 o 6 3 1 5133.23 4827.05 49.47 o 7 3 1 281.66 275.64 7.68 o 8 3 1 5112.06 4945.43 54.88 o 9 3 1 13.39 24.01 7.31 o 10 3 1 542.12 585.30 14.77 o 11 3 1 30.79 20.01 10.25 o 12 3 1 341.28 446.95 17.81 o -13 4 1 96.31 101.21 34.69 o -12 4 1 66.60 73.35 11.33 o -11 4 1 118.87 116.56 11.04 o -10 4 1 1052.36 1002.39 20.86 o -9 4 1 1773.64 1730.38 26.72 o -8 4 1 5.69 7.52 5.43 o -7 4 1 530.21 522.78 10.59 o -6 4 1 133.91 132.69 5.05 o -5 4 1 3361.54 3365.69 33.14 o -4 4 1 1046.28 1075.56 11.72 o -3 4 1 2745.65 2636.02 26.96 o -2 4 1 1597.43 1501.12 21.16 o -1 4 1 2815.48 2721.94 33.00 o 0 4 1 11880.01 11884.91 108.89 o 1 4 1 4185.55 4046.76 36.51 o 2 4 1 861.11 872.93 11.39 o 3 4 1 3827.99 3581.30 37.86 o 4 4 1 1958.89 2285.06 23.24 o 5 4 1 9552.77 9335.71 87.58 o 6 4 1 475.33 434.16 8.21 o 7 4 1 2454.32 2300.42 26.13 o 8 4 1 41.57 35.90 5.96 o 9 4 1 4024.39 3950.19 49.04 o 10 4 1 122.23 125.21 11.06 o 11 4 1 241.19 247.64 16.47 o 12 4 1 154.75 203.41 14.43 o -12 5 1 476.04 498.52 18.97 o -11 5 1 889.10 932.74 27.24 o -10 5 1 564.44 509.02 17.12 o -9 5 1 1800.94 1640.51 27.84 o -8 5 1 2130.75 2036.18 30.54 o -7 5 1 1421.37 1354.79 19.33 o -6 5 1 1090.84 1073.24 18.87 o -5 5 1 2165.84 2070.95 23.09 o -4 5 1 1230.51 1133.39 13.25 o -3 5 1 8692.96 8486.89 112.50 o -2 5 1 354.57 330.27 6.92 o -1 5 1 4879.01 4822.12 52.40 o 0 5 1 447.55 444.94 4.95 o 1 5 1 1581.46 1542.29 13.97 o 2 5 1 1402.45 1324.34 14.01 o 3 5 1 29.89 41.74 2.94 o 4 5 1 1991.85 1955.57 21.21 o 5 5 1 3524.64 3369.72 33.66 o 6 5 1 44.66 41.58 4.33 o 7 5 1 1.12 -4.40 4.40 o 8 5 1 107.47 99.13 6.82 o 9 5 1 13.23 23.60 6.92 o 10 5 1 197.36 199.26 12.52 o 11 5 1 27.83 27.07 10.55 o 12 5 1 137.52 163.07 14.96 o -12 6 1 211.37 255.43 15.85 o -11 6 1 2.46 -3.18 11.03 o -10 6 1 356.37 361.40 15.07 o -9 6 1 1444.32 1439.38 27.40 o -8 6 1 1622.54 1442.09 26.40 o -7 6 1 290.29 256.71 10.56 o -6 6 1 3227.67 3104.65 34.59 o -5 6 1 706.99 659.09 9.31 o -4 6 1 575.85 533.95 8.58 o -3 6 1 707.30 637.64 9.38 o -2 6 1 1549.00 1550.93 20.03 o -1 6 1 4229.52 3982.12 39.60 o 0 6 1 1818.49 1624.30 14.78 o 1 6 1 756.76 651.06 7.14 o 2 6 1 5242.20 5223.96 47.36 o 3 6 1 555.25 687.68 9.30 o 4 6 1 3.43 4.34 3.04 o 5 6 1 6230.42 5996.00 63.09 o 6 6 1 14.48 11.74 4.29 o 7 6 1 5005.82 4682.55 51.11 o 8 6 1 69.13 80.70 7.46 o 9 6 1 787.18 755.57 16.90 o 10 6 1 0.10 7.58 10.03 o 11 6 1 78.46 77.11 13.00 o 12 6 1 9.90 31.34 16.15 o -12 7 1 300.39 372.69 17.86 o -11 7 1 133.62 129.25 12.52 o -10 7 1 812.99 769.29 20.47 o -9 7 1 144.85 133.69 10.71 o -8 7 1 230.19 255.63 11.91 o -7 7 1 618.31 555.58 11.76 o -6 7 1 1455.38 1421.47 22.65 o -5 7 1 74.03 70.61 4.31 o -4 7 1 1930.71 1633.46 18.06 o -3 7 1 2453.41 2401.16 26.30 o -2 7 1 7978.81 7577.15 81.98 o -1 7 1 38.61 51.08 2.88 o 0 7 1 6317.63 5987.08 50.14 o 1 7 1 2001.28 1957.68 17.86 o 2 7 1 11874.67 11518.17 98.35 o 3 7 1 89.15 97.92 3.98 o 4 7 1 3015.77 2715.24 28.87 o 5 7 1 1090.01 999.16 13.99 o 6 7 1 4978.15 4817.83 52.15 o 7 7 1 34.80 23.60 5.44 o 8 7 1 2145.77 2021.49 36.04 o 9 7 1 323.85 354.28 18.20 o 10 7 1 806.60 770.61 21.47 o 11 7 1 13.01 26.33 11.92 o 12 7 1 829.15 811.29 58.50 o -12 8 1 510.93 586.96 24.33 o -11 8 1 117.45 123.68 12.77 o -10 8 1 990.10 986.60 23.52 o -9 8 1 205.00 204.78 12.46 o -8 8 1 330.10 322.34 13.12 o -7 8 1 116.47 120.73 7.56 o -6 8 1 169.89 145.03 7.33 o -5 8 1 3108.53 2846.12 33.84 o -4 8 1 3915.78 3870.03 39.37 o -3 8 1 1562.15 1409.03 18.24 o -2 8 1 4464.85 4302.51 45.42 o -1 8 1 790.23 803.04 9.39 o 0 8 1 824.90 751.16 8.10 o 1 8 1 2362.88 2214.86 21.70 o 2 8 1 1303.53 1389.51 14.19 o 3 8 1 7796.61 7622.09 68.92 o 4 8 1 1007.80 922.59 12.36 o 5 8 1 918.80 859.55 12.86 o 6 8 1 173.97 186.64 7.50 o 7 8 1 55.73 41.28 6.46 o 8 8 1 9.11 7.39 7.56 o 9 8 1 961.60 921.86 19.74 o 10 8 1 21.39 17.69 10.90 o 11 8 1 1019.05 1105.44 46.19 o -12 9 1 61.99 90.05 16.24 o -11 9 1 110.66 112.44 13.23 o -10 9 1 67.45 80.94 11.51 o -9 9 1 1461.52 1398.50 34.00 o -8 9 1 41.61 42.95 7.28 o -7 9 1 5612.79 5200.06 63.97 o -6 9 1 1.55 2.53 5.80 o -5 9 1 4040.91 3729.20 40.78 o -4 9 1 454.87 456.41 9.39 o -3 9 1 174.07 153.30 4.77 o -2 9 1 1170.66 1068.60 15.42 o -1 9 1 102.44 76.39 4.48 o 0 9 1 3298.90 3356.49 29.54 o 1 9 1 2402.90 2203.56 21.08 o 2 9 1 31.51 37.15 3.10 o 3 9 1 144.61 131.70 4.51 o 4 9 1 27.25 31.81 4.82 o 5 9 1 50.73 63.11 5.67 o 6 9 1 855.57 784.36 14.89 o 7 9 1 359.21 316.71 11.52 o 8 9 1 130.61 151.83 10.28 o 9 9 1 48.92 85.49 9.87 o 10 9 1 23.84 35.99 11.74 o 11 9 1 139.22 177.80 15.35 o -11 10 1 33.23 30.07 12.16 o -10 10 1 62.68 63.14 11.76 o -9 10 1 361.70 351.34 15.42 o -8 10 1 1066.63 995.48 20.45 o -7 10 1 1651.32 1609.94 24.89 o -6 10 1 2823.38 2761.26 37.01 o -5 10 1 2683.35 2426.65 30.34 o -4 10 1 35.76 66.39 5.67 o -3 10 1 2820.16 2643.63 31.94 o -2 10 1 378.71 426.95 7.87 o -1 10 1 1802.97 1606.30 16.37 o 0 10 1 109.93 194.52 4.58 o 1 10 1 3945.57 3897.31 35.45 o 2 10 1 1733.46 1658.94 17.05 o 3 10 1 5863.22 5523.42 55.75 o 4 10 1 210.56 201.06 8.76 o 5 10 1 2405.86 2261.04 28.88 o 6 10 1 13.87 18.80 6.55 o 7 10 1 94.13 90.37 7.80 o 8 10 1 278.12 277.15 13.40 o 9 10 1 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