#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/68/2216857.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216857_Fobs loop_ _publ_author_name 'Butcher, Ray J.' 'Jasinski, Jerry P.' 'Kushawaha, Sruendra K.' 'Bharty, Manoj K.' 'Singh, Nand K.' _publ_section_title ; N'-[Bis(benzylsulfanyl)methylene]-2-furohydrazide ; _journal_coeditor_code ZL2079 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4590 _journal_page_last o4591 _journal_volume 63 _journal_year 2007 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 109.983 _cell_angle_beta 94.781 _cell_angle_gamma 90.201 _cell_length_a 9.2058 _cell_length_b 9.2663 _cell_length_c 11.3877 _exptl_crystal_F_000 400.00 _reflns_d_resolution_high 0.6996 _[local]_cod_data_source_file zl2079Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sk2m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 93.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1143.87 1170.17 17.64 o 2 0 0 1019.16 1080.04 12.85 o 3 0 0 5449.17 5619.45 66.74 o 4 0 0 1204.08 1365.48 31.78 o 5 0 0 284.06 246.88 3.32 o 6 0 0 1493.10 1509.25 18.10 o 7 0 0 13.03 14.59 0.57 o 8 0 0 179.80 165.89 3.35 o 9 0 0 327.27 305.35 9.44 o 10 0 0 56.52 55.90 1.72 o 11 0 0 3.45 4.68 1.21 o 12 0 0 183.15 200.99 6.94 o 13 0 0 29.13 38.55 2.71 o -13 1 0 22.30 29.52 2.43 o -12 1 0 55.87 56.21 3.24 o -11 1 0 252.95 245.14 4.92 o -10 1 0 37.26 34.18 1.83 o -9 1 0 278.71 275.27 5.10 o -8 1 0 493.16 464.69 7.69 o -7 1 0 42.11 44.41 1.80 o -6 1 0 39.75 27.88 0.92 o -5 1 0 1271.08 1306.57 15.65 o -4 1 0 45.87 58.12 0.98 o -3 1 0 24.76 28.03 0.53 o -2 1 0 5754.26 5525.06 214.08 o -1 1 0 244.78 273.73 4.12 o 0 1 0 428.71 399.79 13.66 o 1 1 0 119.69 121.35 1.42 o 2 1 0 147.58 174.97 2.25 o 3 1 0 241.98 282.81 3.58 o 4 1 0 2694.10 2924.67 34.74 o 5 1 0 112.91 124.20 1.88 o 6 1 0 346.20 332.28 4.43 o 7 1 0 171.12 167.34 2.58 o 8 1 0 1.72 0.95 0.28 o 9 1 0 320.30 308.36 7.61 o 10 1 0 293.58 286.03 8.28 o 11 1 0 78.60 65.73 3.33 o 12 1 0 97.76 102.14 4.53 o 13 1 0 16.39 19.82 1.98 o -12 2 0 29.97 31.26 1.42 o -11 2 0 16.52 17.05 1.06 o -10 2 0 150.04 149.43 4.12 o -9 2 0 26.97 23.95 1.12 o -8 2 0 136.15 130.93 2.87 o -7 2 0 242.45 233.02 11.40 o -6 2 0 8.06 12.52 0.63 o -5 2 0 162.13 179.94 2.50 o -4 2 0 29.61 22.37 1.05 o -3 2 0 19.59 14.57 0.53 o -2 2 0 6.44 6.03 0.47 o -1 2 0 346.89 351.40 4.32 o 0 2 0 932.58 1057.19 12.59 o 1 2 0 2353.38 2536.45 38.89 o 2 2 0 2303.64 2569.30 33.11 o 3 2 0 420.46 491.02 6.08 o 4 2 0 201.54 222.07 2.99 o 5 2 0 895.71 1002.71 12.18 o 6 2 0 56.36 53.97 1.09 o 7 2 0 13.40 9.22 0.47 o 8 2 0 103.86 101.42 2.47 o 9 2 0 473.65 446.02 7.79 o 10 2 0 92.90 91.14 2.53 o 11 2 0 10.95 8.42 1.29 o 12 2 0 3.03 3.80 1.18 o -12 3 0 95.43 91.58 2.73 o -11 3 0 19.39 17.60 1.10 o -10 3 0 0.11 -0.20 0.43 o -9 3 0 82.06 75.41 2.14 o -8 3 0 50.91 47.93 1.57 o -7 3 0 32.40 27.08 1.41 o -6 3 0 83.14 82.20 2.00 o -5 3 0 483.59 456.40 14.44 o -4 3 0 183.10 164.44 3.54 o -3 3 0 324.94 363.43 5.73 o -2 3 0 1242.13 1289.27 15.38 o -1 3 0 117.95 147.46 2.77 o 0 3 0 146.26 140.99 1.91 o 1 3 0 979.51 1018.83 12.17 o 2 3 0 1545.03 1777.82 21.10 o 3 3 0 1018.53 1085.04 13.05 o 4 3 0 871.54 920.61 11.17 o 5 3 0 7.60 15.73 0.48 o 6 3 0 17.51 20.75 0.61 o 7 3 0 1377.29 1212.50 25.96 o 8 3 0 210.14 197.27 4.05 o 9 3 0 79.49 69.34 2.11 o 10 3 0 153.97 146.41 3.51 o 11 3 0 46.30 43.85 2.70 o 12 3 0 18.52 19.50 1.88 o -12 4 0 1.95 2.51 0.71 o -11 4 0 85.41 88.53 2.63 o -10 4 0 173.24 168.09 3.83 o -9 4 0 156.31 147.98 3.40 o -8 4 0 247.55 232.89 4.54 o -7 4 0 304.40 281.66 5.11 o -6 4 0 39.51 24.86 1.01 o -5 4 0 443.40 418.72 7.98 o -4 4 0 0.14 3.31 0.40 o -3 4 0 204.19 193.38 2.64 o -2 4 0 324.24 315.26 3.54 o -1 4 0 851.82 768.90 9.32 o 0 4 0 23.03 33.99 0.69 o 1 4 0 598.85 593.41 7.28 o 2 4 0 2167.62 2224.56 34.12 o 3 4 0 665.91 713.27 8.76 o 4 4 0 750.82 821.25 10.09 o 5 4 0 394.71 345.21 5.95 o 6 4 0 1388.29 1315.30 64.48 o 7 4 0 205.84 210.35 4.22 o 8 4 0 553.76 550.71 9.35 o 9 4 0 138.64 126.57 3.14 o 10 4 0 167.57 158.57 3.78 o 11 4 0 363.60 362.54 7.05 o 12 4 0 166.68 184.11 6.54 o -12 5 0 21.79 23.67 1.37 o -11 5 0 5.92 5.51 0.79 o -10 5 0 138.99 143.62 3.52 o -9 5 0 445.56 423.75 7.59 o -8 5 0 64.26 56.66 1.81 o -7 5 0 224.67 216.91 4.92 o -6 5 0 845.76 776.82 12.19 o -5 5 0 353.95 335.48 10.91 o -4 5 0 643.37 603.85 9.47 o -3 5 0 622.31 623.25 7.75 o -2 5 0 58.52 69.49 1.81 o -1 5 0 554.25 575.88 7.15 o 0 5 0 3.82 8.16 0.43 o 1 5 0 514.41 561.22 6.99 o 2 5 0 370.97 363.22 4.70 o 3 5 0 354.70 359.52 4.68 o 4 5 0 173.65 180.12 3.53 o 5 5 0 582.81 542.71 16.96 o 6 5 0 2.23 2.64 0.51 o 7 5 0 0.80 0.37 0.42 o 8 5 0 129.18 125.13 3.10 o 9 5 0 3.75 5.52 0.71 o 10 5 0 31.72 31.15 1.79 o 11 5 0 68.65 62.16 2.88 o -11 6 0 6.47 7.69 0.91 o -10 6 0 30.61 30.71 1.51 o -9 6 0 1.59 1.43 0.68 o -8 6 0 5.37 3.83 0.63 o -7 6 0 111.54 95.86 2.48 o -6 6 0 9.12 5.74 0.66 o -5 6 0 28.21 17.93 0.91 o -4 6 0 79.82 67.64 1.76 o -3 6 0 6.87 9.22 0.60 o -2 6 0 79.63 76.80 1.38 o -1 6 0 724.48 800.38 9.87 o 0 6 0 109.07 107.64 1.76 o 1 6 0 3.77 1.80 0.25 o 2 6 0 92.72 89.43 1.53 o 3 6 0 60.84 54.78 1.59 o 4 6 0 5.02 4.87 0.58 o 5 6 0 330.04 313.78 5.72 o 6 6 0 33.80 31.43 1.70 o 7 6 0 124.75 125.70 3.10 o 8 6 0 2.05 2.17 0.61 o 9 6 0 8.44 10.62 0.94 o 10 6 0 49.46 48.66 1.98 o 11 6 0 9.88 11.79 0.99 o -11 7 0 18.05 20.98 1.31 o -10 7 0 12.21 13.57 1.29 o -9 7 0 0.30 -0.19 0.41 o -8 7 0 13.31 9.20 0.87 o -7 7 0 67.63 54.14 1.84 o -6 7 0 122.77 106.48 2.64 o -5 7 0 54.12 58.05 1.78 o -4 7 0 196.91 191.33 3.77 o -3 7 0 331.31 298.94 8.98 o -2 7 0 15.18 11.97 0.53 o -1 7 0 18.38 17.52 0.63 o 0 7 0 24.42 15.76 0.60 o 1 7 0 199.35 194.43 2.89 o 2 7 0 22.45 20.14 1.10 o 3 7 0 607.82 589.77 9.68 o 4 7 0 238.13 209.06 4.20 o 5 7 0 0.30 4.85 1.01 o 6 7 0 15.63 14.57 1.68 o 7 7 0 75.59 67.85 2.19 o 8 7 0 2.99 2.05 0.59 o 9 7 0 34.26 33.51 1.63 o 10 7 0 99.87 108.17 3.19 o -10 8 0 0.08 0.18 1.28 o -9 8 0 54.98 50.04 1.99 o -8 8 0 204.01 198.02 4.41 o -7 8 0 0.01 0.02 0.71 o -6 8 0 67.01 61.75 1.99 o -5 8 0 143.69 128.12 3.01 o -4 8 0 0.32 2.14 1.27 o -3 8 0 17.35 20.91 1.01 o -2 8 0 354.89 320.77 7.84 o -1 8 0 6.52 6.74 0.83 o 0 8 0 329.02 331.26 4.62 o 1 8 0 1230.03 1193.96 18.39 o 2 8 0 222.84 207.00 4.17 o 3 8 0 286.60 287.37 5.45 o 4 8 0 592.52 598.33 10.10 o 5 8 0 88.75 84.50 2.44 o 6 8 0 381.02 390.32 7.29 o 7 8 0 339.52 331.99 6.53 o 8 8 0 2.83 1.61 0.64 o 9 8 0 104.18 105.35 3.17 o -9 9 0 13.30 16.88 3.66 o -8 9 0 3.48 3.59 0.69 o -7 9 0 308.07 310.38 6.11 o -6 9 0 1.06 1.18 0.47 o -5 9 0 440.97 410.49 7.36 o -4 9 0 568.36 565.56 13.95 o -3 9 0 179.20 159.84 4.69 o -2 9 0 257.66 250.76 4.73 o -1 9 0 175.31 167.06 3.42 o 0 9 0 8.47 8.34 0.73 o 1 9 0 105.34 105.80 2.66 o 2 9 0 208.40 204.79 4.28 o 3 9 0 7.10 6.09 0.73 o 4 9 0 391.55 391.13 7.25 o 5 9 0 146.58 141.47 3.52 o 6 9 0 4.10 4.28 0.77 o 7 9 0 117.13 116.09 3.27 o 8 9 0 204.35 211.72 4.95 o -8 10 0 4.35 7.29 0.77 o -7 10 0 5.45 8.46 1.42 o -6 10 0 84.27 75.24 4.86 o -5 10 0 120.29 110.89 2.95 o -4 10 0 1.04 1.97 0.52 o -3 10 0 13.37 12.74 1.34 o -2 10 0 25.07 19.35 1.22 o -1 10 0 109.31 103.15 4.00 o 0 10 0 13.55 15.20 1.47 o 1 10 0 67.48 70.95 2.17 o 2 10 0 1.74 2.02 0.63 o 3 10 0 37.02 38.75 1.66 o 4 10 0 47.97 48.58 1.91 o 5 10 0 95.32 93.34 2.85 o 6 10 0 0.90 1.87 0.98 o 7 10 0 77.93 76.13 2.64 o -6 11 0 35.27 39.20 1.69 o -5 11 0 15.88 19.36 1.16 o -4 11 0 11.82 16.04 0.96 o -3 11 0 1.97 1.88 0.82 o -2 11 0 7.11 6.68 1.23 o -1 11 0 45.29 53.02 2.89 o 0 11 0 10.35 9.67 1.33 o 1 11 0 15.95 20.77 1.82 o 2 11 0 51.10 56.69 2.08 o 3 11 0 48.65 49.58 1.96 o 4 11 0 3.13 5.64 1.24 o 5 11 0 0.02 0.66 0.55 o -3 12 0 43.39 50.47 3.00 o -2 12 0 5.94 6.65 1.18 o -1 12 0 45.30 44.09 2.74 o 0 12 0 59.80 57.90 3.19 o 1 12 0 9.79 11.65 1.53 o 2 12 0 55.13 52.42 3.00 o 3 12 0 119.30 125.95 4.96 o -3 -12 1 20.61 26.67 1.48 o -2 -12 1 2.96 3.40 1.05 o -1 -12 1 11.07 14.85 1.66 o 0 -12 1 54.85 60.10 3.23 o 1 -12 1 1.44 0.60 0.87 o 2 -12 1 5.39 6.40 1.15 o 3 -12 1 1.51 4.56 0.90 o 4 -12 1 14.12 13.10 1.41 o -6 -11 1 151.38 162.34 4.21 o -5 -11 1 13.36 15.69 1.22 o -4 -11 1 64.27 62.00 2.26 o -3 -11 1 79.74 82.68 2.60 o -2 -11 1 171.00 180.77 4.19 o -1 -11 1 0.46 -0.02 0.75 o 0 -11 1 2.95 2.58 0.96 o 1 -11 1 22.55 20.29 1.79 o 2 -11 1 6.51 5.05 0.83 o 3 -11 1 57.50 58.81 3.22 o 4 -11 1 37.00 38.14 1.67 o 5 -11 1 76.24 84.19 2.57 o 6 -11 1 72.20 73.04 2.40 o -7 -10 1 93.31 96.20 5.00 o -6 -10 1 348.15 342.05 6.87 o -5 -10 1 151.81 154.23 3.86 o -4 -10 1 1.72 1.95 0.61 o -3 -10 1 69.02 68.52 2.22 o -2 -10 1 154.24 146.91 3.49 o -1 -10 1 58.02 55.20 1.87 o 0 -10 1 308.32 301.56 8.39 o 1 -10 1 165.52 159.58 5.30 o 2 -10 1 4.46 5.13 1.06 o 3 -10 1 31.04 26.33 1.25 o 4 -10 1 46.39 46.38 1.72 o 5 -10 1 35.34 35.42 1.52 o 6 -10 1 15.91 15.45 1.09 o 7 -10 1 148.04 152.84 3.78 o 8 -10 1 0.92 1.35 0.51 o -9 -9 1 0.26 1.36 0.57 o -8 -9 1 165.93 167.13 4.21 o -7 -9 1 125.26 119.07 3.31 o -6 -9 1 1.84 1.41 1.03 o -5 -9 1 165.84 154.35 3.69 o -4 -9 1 41.21 38.99 1.61 o -3 -9 1 31.83 31.61 1.40 o -2 -9 1 30.37 33.02 1.39 o -1 -9 1 25.93 24.36 1.16 o 0 -9 1 2.95 2.68 0.62 o 1 -9 1 106.34 111.40 2.52 o 2 -9 1 32.37 28.51 1.15 o 3 -9 1 41.09 37.78 1.40 o 4 -9 1 62.99 65.92 2.00 o 5 -9 1 152.59 140.26 3.28 o 6 -9 1 4.49 4.46 0.67 o 7 -9 1 53.12 52.36 2.27 o 8 -9 1 3.30 3.60 0.71 o 9 -9 1 13.03 14.68 1.10 o -10 -8 1 21.24 25.14 2.71 o -9 -8 1 3.24 2.46 1.46 o -8 -8 1 3.48 4.76 0.81 o -7 -8 1 132.20 126.64 4.67 o -6 -8 1 58.08 53.05 1.93 o -5 -8 1 66.12 64.60 2.07 o -4 -8 1 174.63 168.23 3.69 o -3 -8 1 15.14 13.22 0.91 o -2 -8 1 388.14 368.72 6.53 o -1 -8 1 110.89 94.88 6.08 o 0 -8 1 11.64 10.88 0.54 o 1 -8 1 86.42 79.37 1.56 o 2 -8 1 180.99 170.40 3.38 o 3 -8 1 7.41 6.90 0.64 o 4 -8 1 129.60 111.66 2.65 o 5 -8 1 0.47 1.81 0.60 o 6 -8 1 127.97 109.51 2.77 o 7 -8 1 24.29 18.65 1.30 o 8 -8 1 76.34 71.63 2.75 o 9 -8 1 1.40 1.73 0.60 o 10 -8 1 6.54 6.54 0.83 o -10 -7 1 19.18 19.59 1.31 o -9 -7 1 0.08 0.00 0.50 o -8 -7 1 40.05 34.70 1.83 o -7 -7 1 33.05 26.09 1.45 o -6 -7 1 96.91 94.86 2.67 o -5 -7 1 348.97 342.47 6.25 o -4 -7 1 564.72 518.14 8.72 o -3 -7 1 31.13 25.66 1.13 o -2 -7 1 290.91 277.96 5.04 o -1 -7 1 8.63 8.12 0.41 o 0 -7 1 0.31 0.02 0.20 o 1 -7 1 7.01 5.93 0.39 o 2 -7 1 4.84 3.57 0.42 o 3 -7 1 7.82 6.15 0.55 o 4 -7 1 2.26 3.72 0.53 o 5 -7 1 55.72 43.69 1.55 o 6 -7 1 10.12 10.52 0.78 o 7 -7 1 0.14 0.25 0.42 o 8 -7 1 31.25 27.32 1.35 o 9 -7 1 4.38 4.56 1.14 o 10 -7 1 15.99 12.84 1.50 o 11 -7 1 49.89 52.60 2.10 o -11 -6 1 46.22 45.75 1.97 o -10 -6 1 62.15 66.78 3.14 o -9 -6 1 534.51 530.87 9.47 o -8 -6 1 653.64 642.35 10.91 o -7 -6 1 3.89 5.82 0.75 o -6 -6 1 248.38 240.40 4.74 o -5 -6 1 123.40 108.46 2.60 o -4 -6 1 162.06 165.01 3.39 o -3 -6 1 505.51 484.61 7.99 o -2 -6 1 483.97 511.13 6.49 o -1 -6 1 953.25 1010.59 12.30 o 0 -6 1 1830.36 1861.25 22.16 o 1 -6 1 367.17 375.96 4.91 o 2 -6 1 473.24 483.69 6.17 o 3 -6 1 323.94 295.80 5.06 o 4 -6 1 34.88 33.93 2.54 o 5 -6 1 126.96 120.66 2.66 o 6 -6 1 384.50 346.63 6.10 o 7 -6 1 33.35 35.61 1.40 o 8 -6 1 12.31 12.03 0.94 o 9 -6 1 218.24 202.05 4.40 o 10 -6 1 2.86 4.11 0.70 o 11 -6 1 1.03 0.73 1.65 o -11 -5 1 82.64 78.64 2.61 o -10 -5 1 88.31 81.56 2.55 o -9 -5 1 837.47 875.16 14.33 o -8 -5 1 163.93 152.31 3.52 o -7 -5 1 69.71 72.22 2.10 o -6 -5 1 897.97 909.03 14.33 o -5 -5 1 1062.01 956.88 49.00 o -4 -5 1 8.53 8.78 0.64 o -3 -5 1 554.72 536.63 8.61 o -2 -5 1 256.30 262.39 3.49 o -1 -5 1 46.68 33.33 0.73 o 0 -5 1 145.77 120.04 2.19 o 1 -5 1 150.65 141.45 2.07 o 2 -5 1 531.90 606.81 8.03 o 3 -5 1 307.47 270.07 3.61 o 4 -5 1 27.78 15.97 0.74 o 5 -5 1 291.49 304.49 5.30 o 6 -5 1 421.69 371.59 6.37 o 7 -5 1 8.75 7.64 0.69 o 8 -5 1 5.11 4.66 0.63 o 9 -5 1 351.89 340.80 6.34 o 10 -5 1 113.89 108.79 2.95 o 11 -5 1 1.85 2.54 0.64 o 12 -5 1 0.40 1.31 0.68 o -12 -4 1 0.01 2.68 0.93 o -11 -4 1 22.79 20.84 1.28 o -10 -4 1 5.48 5.32 0.75 o -9 -4 1 42.94 37.51 1.54 o -8 -4 1 5.35 2.25 0.59 o -7 -4 1 158.96 137.98 3.08 o -6 -4 1 261.43 266.02 16.66 o -5 -4 1 542.77 584.64 9.40 o -4 -4 1 49.04 51.09 1.41 o -3 -4 1 810.54 871.75 23.37 o -2 -4 1 511.35 581.88 7.20 o -1 -4 1 189.83 203.97 2.72 o 0 -4 1 909.33 946.74 12.48 o 1 -4 1 1884.63 1969.31 23.25 o 2 -4 1 998.24 1120.73 13.41 o 3 -4 1 876.45 901.87 10.96 o 4 -4 1 308.29 293.76 4.92 o 5 -4 1 70.09 71.68 1.74 o 6 -4 1 58.68 53.90 1.55 o 7 -4 1 432.47 436.86 7.36 o 8 -4 1 0.73 1.10 0.42 o 9 -4 1 389.39 378.15 8.40 o 10 -4 1 695.84 693.32 11.50 o 11 -4 1 2.72 2.81 0.63 o 12 -4 1 0.51 0.76 0.52 o -12 -3 1 0.92 2.40 1.05 o -11 -3 1 26.67 26.88 2.14 o -10 -3 1 8.25 5.23 0.71 o -9 -3 1 43.61 41.00 1.56 o -8 -3 1 56.35 50.42 1.66 o -7 -3 1 88.82 88.71 2.22 o -6 -3 1 98.48 83.40 1.45 o -5 -3 1 27.30 29.20 0.71 o -4 -3 1 118.78 126.93 2.64 o -3 -3 1 2135.08 2418.57 39.44 o -2 -3 1 50.01 64.08 1.39 o -1 -3 1 686.78 730.37 12.88 o 0 -3 1 235.70 225.63 2.90 o 1 -3 1 1578.11 1654.51 19.61 o 2 -3 1 439.56 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o 2 -3 14 0.04 0.40 0.49 o 3 -3 14 22.38 20.99 1.44 o 4 -3 14 88.20 85.32 2.65 o 5 -3 14 80.59 82.84 2.63 o -7 -2 14 46.73 51.38 2.19 o -6 -2 14 80.92 83.48 2.54 o -5 -2 14 2.95 5.10 0.75 o -4 -2 14 32.70 33.04 1.55 o -3 -2 14 145.90 129.11 4.39 o -2 -2 14 406.04 412.96 7.63 o -1 -2 14 88.68 88.90 2.67 o 0 -2 14 396.81 388.48 7.30 o 1 -2 14 144.42 143.28 6.27 o 2 -2 14 9.44 9.96 0.95 o 3 -2 14 26.36 27.43 1.47 o 4 -2 14 9.64 10.25 0.99 o 5 -2 14 0.16 1.02 0.52 o -6 -1 14 271.07 285.44 5.82 o -5 -1 14 78.14 71.38 2.36 o -4 -1 14 2.45 1.41 0.53 o -3 -1 14 21.38 19.79 1.64 o -2 -1 14 17.97 18.45 1.61 o -1 -1 14 0.25 0.53 0.49 o 0 -1 14 55.95 56.73 2.10 o 1 -1 14 1.94 1.30 0.57 o 2 -1 14 5.66 5.29 0.79 o 3 -1 14 33.67 31.40 2.07 o 4 -1 14 8.96 9.69 0.92 o -6 0 14 0.14 1.60 0.80 o -5 0 14 29.86 34.01 2.28 o -4 0 14 34.29 37.20 1.74 o -3 0 14 48.12 46.87 1.93 o -2 0 14 13.49 13.41 1.09 o -1 0 14 76.45 77.75 2.55 o 0 0 14 53.64 50.47 2.00 o 1 0 14 37.19 35.57 1.68 o 2 0 14 0.22 0.50 0.49 o 3 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15 49.49 51.50 2.01 o 3 -6 15 0.25 1.52 0.84 o -5 -5 15 123.21 122.62 5.07 o -4 -5 15 3.32 2.79 1.09 o -3 -5 15 12.09 11.86 0.97 o -2 -5 15 5.10 4.35 0.72 o -1 -5 15 43.49 41.81 1.77 o 0 -5 15 60.68 55.40 2.09 o 1 -5 15 7.21 7.67 0.90 o 2 -5 15 104.88 103.14 3.01 o 3 -5 15 0.09 0.80 0.92 o 4 -5 15 17.48 19.90 1.73 o -6 -4 15 49.73 52.00 3.05 o -5 -4 15 8.92 12.30 0.83 o -4 -4 15 238.29 246.40 8.38 o -3 -4 15 92.47 89.34 2.70 o -2 -4 15 8.49 6.83 0.85 o -1 -4 15 529.60 517.23 9.25 o 0 -4 15 5.63 7.63 0.89 o 1 -4 15 46.06 39.81 1.79 o 2 -4 15 150.55 150.12 5.08 o 3 -4 15 18.34 20.87 1.33 o 4 -4 15 9.23 6.11 1.13 o -5 -3 15 29.28 28.59 1.43 o -4 -3 15 534.58 542.87 9.58 o -3 -3 15 107.74 99.60 2.92 o -2 -3 15 7.56 7.73 0.90 o -1 -3 15 166.60 170.96 4.12 o 0 -3 15 243.71 243.71 5.28 o 1 -3 15 2.47 2.14 0.66 o 2 -3 15 59.71 62.32 2.28 o 3 -3 15 146.06 139.74 3.89 o -5 -2 15 2.18 2.04 0.55 o -4 -2 15 1.16 1.34 0.55 o -3 -2 15 0.84 0.98 0.54 o -2 -2 15 1.10 1.14 0.77 o -1 -2 15 4.23 5.52 0.85 o 0 -2 15 123.62 124.30 3.41 o 1 -2 15 0.06 0.82 0.59 o 2 -2 15 33.80 35.73 2.27 o 3 -2 15 3.37 2.66 0.64 o -4 -1 15 5.31 6.92 0.81 o -3 -1 15 82.93 82.90 2.68 o -2 -1 15 29.02 31.40 1.62 o -1 -1 15 0.83 0.03 0.54 o 0 -1 15 1.80 4.12 0.79 o 1 -1 15 48.79 50.42 2.05 o 2 -1 15 0.87 0.91 0.54 o -3 0 15 32.99 34.47 1.71 o -2 0 15 268.33 265.17 5.91 o -1 0 15 5.52 4.01 0.79 o 0 0 15 41.44 43.45 1.93 o 1 0 15 43.29 39.47 1.81 o -2 -6 16 264.77 279.28 5.79 o -1 -6 16 67.55 66.03 2.31 o 0 -6 16 120.73 123.72 3.39 o -3 -5 16 126.24 124.23 4.17 o -2 -5 16 133.01 140.73 3.65 o -1 -5 16 146.48 151.00 3.84 o 0 -5 16 28.58 27.83 1.50 o 1 -5 16 97.25 109.52 3.27 o -3 -4 16 8.35 10.40 1.12 o -2 -4 16 120.53 115.13 3.24 o -1 -4 16 117.19 108.39 3.16 o 0 -4 16 6.42 9.91 1.14 o 1 -4 16 173.01 175.26 4.33 o -2 -3 16 0.23 0.77 0.52 o -1 -3 16 12.29 14.36 1.14 o 0 -3 16 13.61 14.96 1.15 o