#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/69/2216901.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216901_Fobs loop_ _publ_author_name 'Marshall, Colin' 'Harrison, William T. A.' _publ_section_title ; (4S,5S)-2,2-Dimethyl-4,5-bis(3-methyl-2-thioxo-2,3-dihydro-1H-imidazol-1-ylmethyl)-1,3-dioxolane ; _journal_coeditor_code BI2249 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o58 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 103.193 _cell_angle_gamma 90.000 _cell_length_a 10.4619 _cell_length_b 8.6043 _cell_length_c 20.2491 _exptl_crystal_F_000 752.00 _reflns_d_resolution_high 0.7704 _[local]_cod_data_source_file bi2249Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CM338 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 129.70 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -10 0 406.65 236.46 62.69 o 3 -10 0 3.74 -3.84 8.65 o 1 -9 0 689.23 672.91 41.82 o 2 -9 0 11.13 11.36 11.36 o 3 -9 0 872.13 873.93 87.89 o 4 -9 0 31.52 33.46 8.59 o 0 -8 0 1825.71 1650.13 82.84 o 1 -8 0 107.86 84.28 8.92 o 2 -8 0 286.11 318.37 32.94 o 3 -8 0 74.77 70.68 8.19 o 4 -8 0 227.34 231.91 23.36 o 5 -8 0 13.78 11.72 8.56 o 6 -8 0 319.39 297.01 30.63 o 1 -7 0 30.39 31.73 4.46 o 2 -7 0 107.14 109.60 7.78 o 3 -7 0 647.16 664.53 30.68 o 4 -7 0 173.93 184.30 12.22 o 5 -7 0 316.46 332.83 18.10 o 6 -7 0 126.42 119.78 14.22 o 7 -7 0 415.94 412.24 37.47 o 0 -6 0 1335.48 1446.19 71.64 o 1 -6 0 68.30 61.26 5.21 o 2 -6 0 18.46 17.54 3.75 o 3 -6 0 6.65 16.67 3.82 o 4 -6 0 511.86 554.69 20.96 o 5 -6 0 65.29 73.78 12.01 o 6 -6 0 417.25 417.64 22.65 o 7 -6 0 107.21 82.18 12.76 o 8 -6 0 325.57 346.11 37.96 o 1 -5 0 302.81 344.12 12.51 o 2 -5 0 170.41 190.03 8.30 o 3 -5 0 108.27 127.73 5.76 o 4 -5 0 382.59 442.32 20.19 o 5 -5 0 239.20 278.00 13.06 o 6 -5 0 77.84 78.23 12.20 o 7 -5 0 159.77 166.79 14.99 o 8 -5 0 90.06 92.55 12.57 o 0 -4 0 47.80 54.15 6.07 o 1 -4 0 7.78 6.70 2.80 o 2 -4 0 471.92 584.23 20.27 o 3 -4 0 66.70 79.72 4.50 o 4 -4 0 1449.80 1640.33 51.40 o 5 -4 0 41.81 46.23 6.08 o 6 -4 0 1609.15 1810.29 64.67 o 7 -4 0 431.45 474.20 20.64 o 8 -4 0 54.06 58.77 6.26 o 9 -4 0 1.21 3.76 2.74 o 10 -4 0 565.26 759.04 88.08 o 1 -3 0 563.33 666.64 23.87 o 2 -3 0 30.32 34.34 2.47 o 3 -3 0 942.98 1000.06 32.85 o 4 -3 0 153.39 158.64 6.15 o 5 -3 0 320.79 349.19 22.37 o 6 -3 0 306.85 357.20 16.30 o 7 -3 0 875.60 938.82 65.11 o 0 -2 0 541.45 582.74 30.19 o 1 -2 0 68.82 74.20 3.55 o 3 -2 0 216.42 210.97 7.56 o 4 -2 0 7378.40 7287.90 298.25 o 5 -2 0 149.97 154.24 5.42 o 6 -2 0 231.57 89.70 10.16 o 9 -2 0 348.99 407.99 34.75 o 1 -1 0 1676.97 1860.46 67.58 o 2 -1 0 315.42 276.86 8.60 o 4 -1 0 179.93 169.23 13.60 o 5 -1 0 1368.07 1339.36 54.81 o 6 -1 0 7.03 7.11 2.85 o 7 -1 0 1177.35 222.54 561.24 o 8 -1 0 38.61 22.03 5.34 o 9 -1 0 51.73 48.79 2.58 o 10 -1 0 110.44 117.91 6.24 o 3 0 0 219.29 175.70 5.82 o 4 0 0 6297.37 5875.79 185.82 o 5 0 0 106.01 101.16 3.35 o 6 0 0 279.45 314.09 22.62 o 7 0 0 45.67 40.86 4.22 o 8 0 0 68.51 58.54 3.21 o 9 0 0 227.23 121.84 99.58 o 10 0 0 17.49 21.80 2.61 o 11 0 0 1.76 0.44 1.35 o 12 0 0 0.21 5.30 6.94 o 1 1 0 1677.33 1386.64 519.82 o 2 1 0 316.66 266.30 15.70 o 4 1 0 179.90 174.85 4.25 o 5 1 0 1344.88 1306.93 63.37 o 6 1 0 8.14 6.10 1.06 o 7 1 0 1204.38 1198.42 55.66 o 8 1 0 39.07 38.68 3.52 o 9 1 0 53.97 45.91 6.43 o 10 1 0 115.52 111.45 6.61 o 11 1 0 265.89 285.42 38.58 o 12 1 0 108.14 120.82 24.29 o 13 1 0 10.50 9.14 9.80 o 0 2 0 477.24 533.99 30.22 o 1 2 0 69.23 74.01 5.13 o 3 2 0 211.04 201.59 6.86 o 4 2 0 7441.32 7422.81 465.81 o 5 2 0 152.47 145.35 8.33 o 6 2 0 227.95 249.34 10.87 o 7 2 0 586.69 634.70 43.11 o 8 2 0 287.51 286.05 9.77 o 9 2 0 349.35 361.68 28.20 o 10 2 0 199.32 211.57 21.70 o 11 2 0 296.06 260.34 22.18 o 12 2 0 127.60 130.62 19.31 o 13 2 0 66.48 71.25 12.95 o 1 3 0 533.38 603.63 21.88 o 2 3 0 31.09 34.24 2.32 o 3 3 0 952.51 990.15 31.59 o 4 3 0 156.38 168.69 20.79 o 5 3 0 308.41 357.21 30.22 o 6 3 0 303.91 305.61 19.59 o 7 3 0 857.40 895.25 49.62 o 8 3 0 312.29 321.31 28.03 o 9 3 0 320.18 310.44 16.04 o 10 3 0 154.93 179.50 12.83 o 11 3 0 280.41 310.20 27.89 o 12 3 0 35.88 30.00 7.88 o 0 4 0 52.86 47.70 4.39 o 1 4 0 7.83 8.77 1.94 o 2 4 0 480.30 548.76 20.36 o 3 4 0 65.73 72.04 4.25 o 4 4 0 1423.53 1579.82 79.90 o 5 4 0 40.73 42.75 5.00 o 6 4 0 1599.30 1597.66 107.06 o 7 4 0 428.57 433.94 42.70 o 8 4 0 54.31 50.63 3.24 o 9 4 0 1.26 3.37 2.06 o 10 4 0 560.65 581.17 25.22 o 11 4 0 148.19 181.38 18.03 o 12 4 0 9.61 12.33 6.15 o 1 5 0 303.82 326.32 12.32 o 2 5 0 172.72 180.01 7.69 o 3 5 0 108.31 112.64 10.10 o 4 5 0 383.30 411.81 13.79 o 5 5 0 249.42 240.80 10.21 o 6 5 0 73.70 72.59 8.17 o 7 5 0 159.67 148.02 11.39 o 8 5 0 86.85 80.46 6.94 o 9 5 0 152.70 159.80 17.96 o 10 5 0 150.51 185.24 20.56 o 11 5 0 32.55 11.34 8.73 o 0 6 0 1331.79 1476.79 65.02 o 1 6 0 67.29 74.59 5.34 o 2 6 0 19.65 16.43 3.06 o 3 6 0 5.61 7.95 2.90 o 4 6 0 522.53 542.44 19.78 o 5 6 0 63.32 58.67 4.74 o 6 6 0 407.49 386.87 34.32 o 7 6 0 114.71 121.31 8.66 o 8 6 0 338.38 312.05 24.83 o 9 6 0 20.56 19.18 4.06 o 10 6 0 27.93 26.16 11.64 o 11 6 0 44.63 39.11 10.10 o 1 7 0 26.77 28.36 8.22 o 2 7 0 109.32 114.23 8.06 o 3 7 0 635.78 659.38 25.23 o 4 7 0 176.71 180.79 9.69 o 5 7 0 325.68 333.41 15.78 o 6 7 0 126.32 113.20 9.09 o 7 7 0 417.56 394.07 27.30 o 8 7 0 41.53 38.18 5.86 o 9 7 0 102.19 112.84 14.88 o 10 7 0 73.12 68.92 13.34 o 0 8 0 1868.72 2041.12 114.79 o 1 8 0 107.94 112.59 8.57 o 2 8 0 281.68 315.42 16.85 o 3 8 0 73.03 69.00 6.90 o 4 8 0 226.25 230.90 14.36 o 5 8 0 13.72 19.08 6.01 o 6 8 0 316.40 324.61 25.69 o 7 8 0 46.93 49.80 7.87 o 8 8 0 125.65 143.11 19.79 o 9 8 0 43.79 49.16 15.95 o 1 9 0 695.91 695.99 50.48 o 2 9 0 11.06 9.83 7.47 o 3 9 0 869.93 956.99 47.70 o 4 9 0 32.25 27.20 6.73 o 5 9 0 80.85 68.83 8.36 o 6 9 0 21.11 14.93 5.92 o 7 9 0 596.19 640.55 62.03 o 0 10 0 1007.09 1081.99 106.91 o 1 10 0 11.58 8.48 6.62 o 2 10 0 414.20 379.62 38.73 o 3 10 0 3.77 11.14 12.16 o 4 10 0 1031.18 958.71 132.92 o 5 10 0 4.34 -3.93 6.68 o 1 11 0 87.78 92.56 11.78 o 2 11 0 20.08 22.92 9.95 o -3 -10 1 11.99 0.00 14.00 o -2 -10 1 2.30 0.33 8.98 o 1 -10 1 250.86 145.66 35.43 o 2 -10 1 0.24 -1.62 8.12 o -4 -9 1 379.08 363.16 39.03 o -3 -9 1 9.93 13.39 8.29 o -2 -9 1 376.97 346.91 30.03 o -1 -9 1 32.50 30.60 6.42 o 0 -9 1 846.47 749.62 84.96 o 1 -9 1 83.42 76.51 9.57 o 2 -9 1 258.23 218.79 21.88 o 3 -9 1 38.36 36.81 9.03 o 4 -9 1 93.54 75.54 14.08 o -6 -8 1 29.67 25.36 7.82 o -5 -8 1 304.72 322.62 35.05 o -4 -8 1 8.77 9.77 5.27 o -3 -8 1 289.04 303.95 18.79 o -2 -8 1 204.48 200.52 14.59 o -1 -8 1 266.05 296.14 17.42 o 0 -8 1 32.89 32.89 6.13 o 1 -8 1 460.15 473.03 27.65 o 2 -8 1 16.94 10.24 6.30 o 3 -8 1 153.64 169.00 12.76 o 4 -8 1 112.32 93.35 12.21 o 5 -8 1 337.33 333.54 31.26 o -7 -7 1 247.20 249.83 28.77 o -6 -7 1 342.27 405.24 37.11 o -5 -7 1 164.47 185.95 24.94 o -4 -7 1 1452.89 1621.92 76.67 o -3 -7 1 240.76 247.56 12.58 o -2 -7 1 1885.62 2010.54 83.61 o -1 -7 1 126.70 128.30 9.42 o 0 -7 1 1667.13 1792.32 77.05 o 1 -7 1 47.29 43.07 5.63 o 2 -7 1 1713.50 1951.79 87.78 o 3 -7 1 142.55 154.52 10.46 o 4 -7 1 486.75 527.91 25.37 o 5 -7 1 13.94 11.36 10.32 o 6 -7 1 92.35 98.13 11.72 o 7 -7 1 7.65 15.15 4.72 o -8 -6 1 140.67 156.78 15.62 o -7 -6 1 155.51 182.44 11.12 o -6 -6 1 187.54 187.58 19.24 o -5 -6 1 1482.56 1690.33 75.34 o -4 -6 1 2.89 5.17 4.91 o -3 -6 1 162.97 178.90 9.32 o -2 -6 1 18.06 12.91 5.71 o -1 -6 1 5549.64 6256.14 186.34 o 0 -6 1 57.76 68.36 5.08 o 1 -6 1 313.85 365.35 14.81 o 2 -6 1 24.69 20.99 3.74 o 3 -6 1 4074.01 4559.64 176.83 o 4 -6 1 21.02 25.59 3.82 o 5 -6 1 20.46 27.37 4.23 o 6 -6 1 9.59 8.97 4.52 o 7 -6 1 29.06 42.69 7.40 o 8 -6 1 56.96 48.58 7.58 o -9 -5 1 41.07 57.80 6.23 o -8 -5 1 1078.59 1381.58 116.54 o -7 -5 1 21.41 24.99 4.22 o -6 -5 1 562.96 588.14 25.16 o -5 -5 1 16.31 18.66 3.77 o -4 -5 1 1904.04 2128.94 75.04 o -3 -5 1 82.28 83.29 5.33 o -2 -5 1 690.53 755.47 24.51 o -1 -5 1 1.91 0.89 2.80 o 0 -5 1 328.92 316.92 11.43 o 1 -5 1 83.11 80.38 5.56 o 2 -5 1 8044.00 9323.45 310.48 o 3 -5 1 96.53 104.58 5.77 o 4 -5 1 574.69 663.12 23.05 o 5 -5 1 140.77 149.39 7.03 o 6 -5 1 5538.91 6434.61 267.12 o 7 -5 1 146.80 158.24 8.01 o 8 -5 1 580.41 620.97 49.93 o 9 -5 1 21.13 28.19 4.31 o -11 -4 1 190.09 188.32 23.69 o -10 -4 1 135.14 189.77 13.78 o -9 -4 1 399.39 357.23 27.80 o -8 -4 1 163.92 193.62 13.78 o -7 -4 1 292.01 343.89 22.62 o -6 -4 1 10.47 15.07 4.16 o -5 -4 1 4473.39 4966.43 165.22 o -4 -4 1 69.17 90.19 7.47 o -3 -4 1 250.09 277.74 16.69 o -2 -4 1 11.99 12.39 2.13 o -1 -4 1 9115.45 10444.64 315.20 o 0 -4 1 3.16 5.71 1.66 o 1 -4 1 1315.24 1599.76 51.76 o 2 -4 1 24.79 24.27 2.96 o 3 -4 1 3979.73 4355.31 163.38 o 4 -4 1 20.45 21.83 2.43 o 5 -4 1 814.70 893.80 31.65 o 6 -4 1 182.98 206.14 8.89 o 7 -4 1 686.42 759.98 28.72 o 8 -4 1 142.30 95.13 9.09 o 9 -4 1 565.03 745.70 40.92 o -11 -3 1 42.09 45.29 3.62 o -10 -3 1 68.01 85.55 5.85 o -8 -3 1 2244.22 2565.89 110.09 o -7 -3 1 279.05 308.07 13.94 o -6 -3 1 111.87 125.55 8.51 o -5 -3 1 126.55 140.93 5.76 o -4 -3 1 702.39 731.26 22.52 o -3 -3 1 94.44 106.08 4.60 o -2 -3 1 183.37 194.86 7.22 o -1 -3 1 11.42 11.34 1.91 o 0 -3 1 5539.25 6160.90 190.30 o 1 -3 1 25.20 24.98 2.25 o 2 -3 1 12.80 6.80 1.77 o 3 -3 1 14.55 13.69 1.66 o 4 -3 1 730.44 917.78 29.13 o 5 -3 1 95.17 113.91 5.49 o 6 -3 1 5244.65 2881.18 335.47 o 7 -3 1 19.74 13.78 2.74 o 8 -3 1 304.49 367.30 17.46 o -11 -2 1 395.83 522.87 27.94 o -10 -2 1 154.52 181.34 10.69 o -9 -2 1 288.91 312.41 23.91 o -7 -2 1 937.21 1055.47 44.77 o -6 -2 1 101.90 110.17 6.75 o -5 -2 1 856.01 832.76 37.85 o -4 -2 1 308.55 294.80 8.91 o -3 -2 1 2318.93 2237.84 68.43 o -2 -2 1 97.87 107.02 5.52 o -1 -2 1 2780.57 2707.35 94.01 o 0 -2 1 3.22 3.43 2.54 o 1 -2 1 425.34 470.04 17.93 o 2 -2 1 760.14 739.33 31.37 o 3 -2 1 821.68 875.71 28.47 o 4 -2 1 42.84 42.70 2.39 o 5 -2 1 694.42 733.73 31.04 o 6 -2 1 250.46 282.05 13.83 o 7 -2 1 6.82 7.63 1.73 o 8 -2 1 94.25 107.65 5.30 o -11 -1 1 60.73 75.04 7.33 o -10 -1 1 507.11 543.32 27.90 o -9 -1 1 38.91 33.64 3.03 o -8 -1 1 1440.17 1505.86 39.39 o -7 -1 1 59.93 52.22 3.86 o -6 -1 1 1066.64 1071.29 31.95 o -5 -1 1 515.13 488.59 14.51 o -4 -1 1 455.66 429.64 13.87 o -3 -1 1 84.87 73.75 4.09 o -1 -1 1 96.00 94.52 3.29 o 1 -1 1 219.04 220.66 6.95 o 2 -1 1 5938.36 6441.44 347.32 o 3 -1 1 150.93 155.60 7.14 o 4 -1 1 129.02 122.38 4.81 o 5 -1 1 0.78 1.17 1.51 o 6 -1 1 984.49 900.46 25.90 o 7 -1 1 84.34 88.48 3.93 o 8 -1 1 340.36 364.94 13.72 o 9 -1 1 43.04 44.97 3.69 o -13 0 1 106.82 99.39 13.75 o -12 0 1 78.90 94.56 14.15 o -11 0 1 103.34 79.13 23.45 o -10 0 1 233.71 281.37 32.44 o -9 0 1 114.83 96.32 5.66 o -8 0 1 57.99 57.52 3.05 o -7 0 1 166.02 142.93 4.85 o -6 0 1 4.12 4.01 1.14 o -5 0 1 518.18 526.41 30.03 o -4 0 1 389.12 344.77 8.83 o -3 0 1 3632.83 3288.85 86.61 o -2 0 1 24.93 16.78 0.98 o 2 0 1 785.67 332.82 194.52 o 3 0 1 2.14 12.06 9.58 o 4 0 1 0.62 1.25 3.72 o 5 0 1 6.07 3.19 2.46 o 6 0 1 478.37 327.35 150.90 o 7 0 1 706.05 749.35 31.89 o 8 0 1 2.73 -2.30 2.92 o 9 0 1 23.09 29.97 3.06 o 10 0 1 276.52 327.00 11.31 o 11 0 1 69.73 65.60 12.05 o 12 0 1 26.67 30.66 10.21 o -13 1 1 1.00 -1.98 10.16 o -12 1 1 62.71 81.47 18.54 o -11 1 1 60.60 64.69 11.33 o -10 1 1 499.74 515.50 28.04 o -9 1 1 40.69 42.45 5.34 o -8 1 1 1439.37 1391.68 77.04 o -7 1 1 60.09 60.05 5.42 o -6 1 1 1095.96 1103.97 37.17 o -5 1 1 517.94 502.69 12.25 o -4 1 1 465.77 472.72 25.78 o -3 1 1 85.22 74.48 2.88 o -1 1 1 95.79 59.73 4.61 o 1 1 1 218.42 213.32 13.64 o 2 1 1 5951.75 5957.28 703.72 o 3 1 1 152.76 153.81 9.60 o 4 1 1 128.91 124.32 6.32 o 5 1 1 0.44 0.50 0.96 o 6 1 1 991.59 908.18 39.05 o 7 1 1 83.44 94.32 12.25 o 8 1 1 340.40 362.95 27.19 o 9 1 1 49.09 52.88 3.01 o 10 1 1 460.50 177.21 216.38 o 11 1 1 18.77 17.84 3.55 o 12 1 1 179.27 171.30 23.14 o 13 1 1 178.45 145.14 23.44 o -13 2 1 2.15 3.59 6.68 o -12 2 1 116.44 114.96 11.20 o -11 2 1 394.66 539.87 28.68 o -10 2 1 150.63 155.19 12.07 o -9 2 1 283.49 302.16 13.72 o -8 2 1 156.27 167.01 6.51 o -7 2 1 934.01 965.30 35.77 o -6 2 1 100.62 103.70 4.00 o -5 2 1 872.02 746.16 25.34 o -4 2 1 303.55 286.54 8.88 o -3 2 1 2348.44 2209.37 70.22 o -2 2 1 99.68 111.18 4.08 o -1 2 1 2752.19 2725.07 94.67 o 0 2 1 3.41 2.69 0.96 o 1 2 1 425.97 471.43 18.23 o 2 2 1 757.49 820.63 24.81 o 3 2 1 800.06 807.62 50.39 o 4 2 1 41.93 40.81 3.35 o 5 2 1 687.79 698.43 45.24 o 6 2 1 259.12 254.41 6.29 o 7 2 1 9.70 8.55 1.21 o 8 2 1 94.67 88.31 8.94 o 9 2 1 1316.20 1351.91 87.38 o 10 2 1 389.21 367.44 29.27 o 11 2 1 87.48 92.58 8.87 o 12 2 1 87.56 106.58 14.96 o -12 3 1 437.92 464.26 87.06 o -11 3 1 39.02 44.49 8.23 o -10 3 1 63.94 63.15 7.35 o -9 3 1 157.79 142.49 7.64 o -8 3 1 2241.50 2311.65 118.02 o -7 3 1 275.00 268.33 11.04 o -6 3 1 117.32 114.14 4.87 o -5 3 1 130.79 126.62 4.48 o -4 3 1 722.77 727.65 48.72 o -3 3 1 95.18 103.24 4.87 o -2 3 1 195.82 220.99 8.35 o -1 3 1 11.66 15.32 1.74 o 0 3 1 5569.44 5595.21 446.23 o 1 3 1 24.87 23.05 2.39 o 2 3 1 17.27 11.76 1.69 o 3 3 1 14.61 14.84 1.76 o 4 3 1 748.00 887.23 96.70 o 5 3 1 95.23 90.74 8.88 o 6 3 1 5224.41 5819.93 598.91 o 7 3 1 20.93 17.61 4.62 o 8 3 1 307.46 294.37 11.05 o 9 3 1 349.47 347.22 19.26 o 10 3 1 684.57 714.92 70.38 o 11 3 1 41.24 52.83 5.91 o 12 3 1 22.55 22.56 4.69 o -12 4 1 25.40 17.21 5.72 o -11 4 1 193.28 215.14 43.57 o -10 4 1 139.50 139.43 8.12 o -9 4 1 405.66 414.52 16.92 o -8 4 1 160.23 158.50 10.12 o -7 4 1 310.54 315.04 34.33 o -6 4 1 10.65 11.67 1.88 o -5 4 1 4418.82 5355.48 220.79 o -4 4 1 68.09 78.39 14.89 o -3 4 1 241.06 293.18 10.03 o -2 4 1 12.29 13.60 4.30 o -1 4 1 9151.09 10527.83 376.05 o 0 4 1 3.18 2.82 1.54 o 1 4 1 1306.11 1538.64 52.86 o 2 4 1 24.88 23.74 2.62 o 3 4 1 3946.66 4212.16 129.18 o 4 4 1 20.56 22.97 2.75 o 5 4 1 825.53 846.10 40.99 o 6 4 1 184.45 174.23 15.47 o 7 4 1 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