#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/69/2216941.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216941_Fobs loop_ _publ_author_name 'Hussain, Altaf' 'Siddiqui, Hamid Latif' 'Zia-ur-Rehman, Muhammad' 'Elsegood, Mark R. J.' 'M. Khan, Khalid' _publ_section_title ; 4-Hydroxy-4,6a,6b,9,9,12a,14b-heptamethylperhydropicen-3-one hemihydrate isolated from Adiantum incisum ; _journal_coeditor_code BT2638 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o264 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.725 _cell_angle_gamma 90.000 _cell_length_a 6.4432 _cell_length_b 57.4770 _cell_length_c 7.2226 _exptl_crystal_F_000 972.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file bt2638Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' GW30 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25.52 22.94 7.56 o 3 0 0 911.83 821.33 29.96 o 4 0 0 3645.38 3570.97 177.25 o 2 1 0 519.99 462.02 18.52 o 3 1 0 192.52 176.77 7.49 o 4 1 0 929.08 939.19 101.81 o 5 1 0 1212.60 1093.36 73.29 o 6 1 0 44.09 43.44 33.88 o 2 2 0 853.50 830.71 47.68 o 3 2 0 146.65 111.99 5.79 o 4 2 0 1174.10 1193.31 46.18 o 2 3 0 1377.10 1202.00 64.38 o 3 3 0 97.71 99.29 5.46 o 4 3 0 1378.54 1479.43 50.63 o 5 3 0 480.96 571.95 55.22 o 6 3 0 31.67 -30.64 41.20 o 2 4 0 181.11 177.33 9.14 o 3 4 0 241.48 224.17 6.99 o 4 4 0 415.69 391.71 26.76 o 5 4 0 797.15 898.98 70.44 o 6 4 0 182.80 220.14 55.30 o 2 5 0 1664.43 1559.96 34.82 o 3 5 0 168.95 170.38 7.70 o 4 5 0 582.90 538.92 24.44 o 5 5 0 448.54 502.06 32.51 o 6 5 0 62.91 86.39 49.34 o 2 6 0 1349.55 1284.89 41.42 o 3 6 0 378.22 353.69 7.66 o 4 6 0 431.69 528.53 23.66 o 6 6 0 21.91 76.49 55.03 o 2 7 0 492.79 389.87 10.53 o 3 7 0 270.06 245.70 7.59 o 4 7 0 943.80 938.75 34.91 o 5 7 0 671.85 901.07 43.42 o 6 7 0 60.60 60.55 29.05 o 2 8 0 349.64 315.23 5.82 o 3 8 0 32.67 23.37 6.51 o 4 8 0 614.51 591.92 23.85 o 5 8 0 1869.19 1903.10 76.25 o 2 9 0 393.37 327.21 6.25 o 3 9 0 134.72 138.77 8.22 o 4 9 0 606.32 561.76 27.04 o 5 9 0 512.15 459.25 31.75 o 6 9 0 65.82 196.93 54.92 o 1 10 0 2072.97 1982.70 24.28 o 2 10 0 872.08 841.99 15.52 o 3 10 0 166.76 171.49 8.72 o 4 10 0 53.40 10.86 23.84 o 6 10 0 277.25 303.55 28.64 o 1 11 0 2848.80 2769.76 34.52 o 2 11 0 24.32 8.90 4.33 o 3 11 0 107.74 104.32 7.00 o 4 11 0 351.00 387.70 24.50 o 5 11 0 634.53 666.85 26.28 o 6 11 0 275.05 277.96 44.21 o 1 12 0 501.16 565.91 8.86 o 2 12 0 362.53 372.46 6.32 o 3 12 0 12.61 18.96 6.97 o 4 12 0 560.06 592.10 25.87 o 5 12 0 287.53 244.88 21.32 o 1 13 0 2613.78 2355.31 28.43 o 2 13 0 1071.39 1046.11 11.88 o 3 13 0 48.38 62.76 11.49 o 4 13 0 484.48 536.55 22.05 o 5 13 0 21.08 46.33 32.66 o 6 13 0 218.99 285.40 31.84 o 0 14 0 156.95 142.16 5.15 o 1 14 0 188.97 137.52 4.75 o 2 14 0 28.62 34.14 5.53 o 3 14 0 78.28 83.06 6.40 o 4 14 0 68.08 57.47 19.36 o 5 14 0 97.42 124.34 64.06 o 6 14 0 211.92 217.30 39.19 o 1 15 0 1219.50 1210.38 16.27 o 2 15 0 527.88 504.82 7.61 o 3 15 0 7.80 4.81 6.57 o 4 15 0 51.37 20.88 12.76 o 5 15 0 275.84 375.29 25.96 o 6 15 0 33.28 44.50 38.52 o 0 16 0 3714.59 3834.79 64.18 o 1 16 0 2043.13 1983.90 27.59 o 2 16 0 145.45 133.47 4.59 o 3 16 0 14.98 8.01 10.32 o 4 16 0 104.00 61.88 13.89 o 5 16 0 558.61 586.94 53.66 o 6 16 0 19.36 16.29 27.43 o 1 17 0 7612.12 7220.81 86.04 o 2 17 0 292.71 278.74 5.70 o 3 17 0 389.60 388.92 10.62 o 4 17 0 14.77 1.17 13.41 o 5 17 0 718.66 721.82 42.22 o 6 17 0 27.70 82.72 31.40 o 0 18 0 103.83 94.31 6.18 o 1 18 0 1665.88 1637.52 25.06 o 2 18 0 86.60 72.47 5.12 o 3 18 0 164.38 176.83 9.57 o 4 18 0 8.55 -0.88 17.10 o 6 18 0 17.49 29.63 30.71 o 1 19 0 1026.02 1004.64 13.73 o 2 19 0 1470.94 1362.14 15.85 o 3 19 0 407.01 390.55 11.11 o 4 19 0 88.62 94.93 19.10 o 5 19 0 388.05 468.09 22.27 o 6 19 0 55.96 82.06 41.81 o 0 20 0 3598.44 3765.22 64.10 o 1 20 0 2388.11 2377.68 25.64 o 2 20 0 161.22 170.57 7.12 o 3 20 0 274.16 289.59 9.57 o 4 20 0 277.96 231.04 19.73 o 5 20 0 517.64 452.94 29.24 o 6 20 0 4.12 15.90 31.28 o 1 21 0 1116.02 1109.23 14.04 o 2 21 0 184.34 157.63 6.32 o 3 21 0 83.26 113.97 12.59 o 4 21 0 231.78 190.45 18.17 o 5 21 0 37.42 46.41 49.09 o 6 21 0 17.35 24.03 33.98 o 0 22 0 5.27 2.13 7.17 o 1 22 0 2227.47 2337.37 23.80 o 2 22 0 500.64 446.49 9.77 o 3 22 0 150.15 145.65 10.40 o 4 22 0 160.39 168.34 21.19 o 5 22 0 178.44 386.19 52.18 o 6 22 0 1.29 13.91 69.75 o 1 23 0 810.40 845.80 12.02 o 2 23 0 132.83 130.56 6.30 o 3 23 0 39.73 56.97 11.97 o 4 23 0 186.20 198.96 15.02 o 5 23 0 578.66 688.36 46.22 o 6 23 0 28.10 15.78 35.01 o 0 24 0 24486.13 27377.32 1046.25 o 1 24 0 2649.54 2827.76 29.39 o 2 24 0 50.08 44.32 10.31 o 3 24 0 247.63 261.41 13.30 o 4 24 0 27.95 4.75 28.32 o 5 24 0 411.25 532.69 54.47 o 6 24 0 69.12 76.18 40.73 o 1 25 0 6149.61 6490.55 75.90 o 2 25 0 374.66 323.57 9.82 o 3 25 0 73.07 29.00 15.52 o 4 25 0 281.65 323.75 20.78 o 5 25 0 778.62 682.64 47.41 o 6 25 0 50.67 47.59 46.88 o 0 26 0 129.92 183.97 11.16 o 1 26 0 1844.59 1940.79 29.68 o 2 26 0 364.82 359.60 10.63 o 3 26 0 396.37 412.38 15.25 o 4 26 0 475.91 515.92 36.30 o 5 26 0 24.33 33.04 32.73 o 6 26 0 28.97 73.29 29.27 o 1 27 0 971.42 899.69 12.06 o 2 27 0 692.01 677.09 14.01 o 3 27 0 81.63 80.90 32.72 o 4 27 0 1252.77 1257.66 87.50 o 5 27 0 79.50 76.23 38.39 o 6 27 0 33.86 30.71 33.23 o 1 28 0 326.92 326.26 7.49 o 2 28 0 18.28 13.82 7.84 o 3 28 0 14.27 14.20 20.77 o 4 28 0 1276.57 1267.43 58.35 o 5 28 0 43.45 21.15 29.20 o 6 28 0 12.96 15.96 64.23 o 1 29 0 202.51 193.58 6.26 o 2 29 0 43.21 55.05 13.91 o 3 29 0 33.53 51.17 26.56 o 4 29 0 331.16 336.45 34.45 o 5 29 0 96.35 50.56 38.50 o 6 29 0 37.71 14.32 53.88 o 0 30 0 139.11 147.70 9.89 o 1 30 0 28.55 32.23 6.67 o 2 30 0 15.74 4.41 8.94 o 3 30 0 250.97 287.66 17.92 o 4 30 0 155.78 171.44 35.67 o 5 30 0 5.47 -2.53 28.26 o 6 30 0 17.03 -17.23 70.55 o 1 31 0 272.45 305.36 8.39 o 2 31 0 31.34 33.57 10.77 o 3 31 0 89.18 141.33 20.72 o 4 31 0 205.40 183.73 32.39 o 5 31 0 34.07 32.25 52.15 o 6 31 0 37.82 112.58 68.28 o 0 32 0 117.06 99.31 9.45 o 1 32 0 2015.97 2138.53 26.28 o 2 32 0 98.94 87.79 12.51 o 3 32 0 267.49 266.16 16.00 o 4 32 0 101.57 89.72 64.91 o 5 32 0 66.92 106.69 45.80 o 6 32 0 25.30 -12.27 35.36 o 1 33 0 201.92 223.63 9.22 o 2 33 0 17.96 7.41 12.73 o 3 33 0 12.92 24.57 19.75 o 4 33 0 476.50 351.35 27.56 o 5 33 0 47.58 77.52 30.95 o 6 33 0 6.57 26.63 44.41 o 0 34 0 147.24 137.44 10.03 o 1 34 0 31.42 63.10 8.12 o 2 34 0 668.81 667.71 19.64 o 3 34 0 23.25 50.16 16.57 o 4 34 0 50.54 2.24 41.64 o 5 34 0 23.64 48.26 28.49 o 6 34 0 107.48 75.16 53.31 o 1 35 0 48.41 48.00 10.21 o 2 35 0 87.57 86.85 14.33 o 3 35 0 32.62 89.46 71.80 o 4 35 0 150.20 159.79 33.04 o 5 35 0 274.35 261.73 65.35 o 0 36 0 1473.52 1595.87 33.60 o 1 36 0 976.10 1026.88 16.84 o 2 36 0 126.48 130.53 13.29 o 3 36 0 78.47 115.29 17.47 o 4 36 0 6.37 5.34 37.42 o 5 36 0 207.24 237.75 64.91 o 1 37 0 237.80 252.61 10.42 o 2 37 0 814.55 843.25 20.32 o 3 37 0 107.55 111.01 18.39 o 4 37 0 43.61 -4.96 46.32 o 5 37 0 36.98 96.55 45.19 o 0 38 0 220.89 213.62 22.70 o 1 38 0 39.20 33.33 12.16 o 2 38 0 85.70 102.54 28.18 o 3 38 0 65.08 20.80 20.52 o 4 38 0 71.27 25.30 35.71 o 5 38 0 2.26 -13.15 31.87 o 1 39 0 637.11 626.80 17.42 o 2 39 0 474.71 484.85 21.05 o 3 39 0 56.07 13.43 21.90 o 4 39 0 237.32 240.71 47.25 o 5 39 0 150.38 199.86 52.43 o 0 40 0 1506.64 1565.99 51.88 o 1 40 0 358.60 351.06 15.14 o 2 40 0 26.27 22.53 12.36 o 3 40 0 12.76 -10.49 16.07 o 5 40 0 1.42 40.02 35.41 o 1 41 0 23.38 25.47 11.32 o 2 41 0 252.15 284.17 22.15 o 3 41 0 113.15 91.00 22.36 o 4 41 0 385.44 408.97 61.33 o 5 41 0 15.65 26.64 63.54 o 0 42 0 126.05 107.52 23.67 o 1 42 0 9.57 3.77 10.41 o 2 42 0 60.17 55.34 16.08 o 3 42 0 166.20 115.93 25.37 o 4 42 0 120.63 95.12 40.54 o 5 42 0 28.76 49.63 41.44 o 1 43 0 10.06 28.19 14.13 o 2 43 0 551.45 543.78 20.47 o 3 43 0 188.62 211.34 31.92 o 4 43 0 65.41 70.27 23.79 o 0 44 0 473.96 500.59 30.60 o 1 44 0 448.68 505.32 19.16 o 2 44 0 2.54 17.07 15.04 o 3 44 0 82.02 -27.13 45.26 o 4 44 0 11.42 38.05 43.20 o 1 45 0 285.43 321.83 22.21 o 2 45 0 373.07 346.94 22.26 o 3 45 0 432.76 440.39 37.74 o 4 45 0 137.23 185.07 74.14 o 5 45 0 85.83 82.61 79.48 o 0 46 0 150.04 166.85 28.46 o 1 46 0 226.02 242.06 15.03 o 2 46 0 45.60 7.75 17.19 o 3 46 0 804.59 766.10 45.01 o 4 46 0 35.91 47.35 29.37 o 5 46 0 4.41 -11.07 33.37 o 1 47 0 85.54 106.64 22.91 o 2 47 0 211.34 201.71 24.22 o 3 47 0 33.11 23.52 20.62 o 4 47 0 26.78 30.94 51.63 o 5 47 0 22.65 55.50 69.84 o 0 48 0 356.26 393.08 22.28 o 1 48 0 341.97 351.70 22.13 o 2 48 0 96.35 64.66 18.69 o 3 48 0 34.51 -14.21 37.62 o 4 48 0 2.22 36.52 28.55 o 1 49 0 99.20 49.53 39.51 o 2 49 0 108.03 52.71 23.16 o 3 49 0 150.18 71.03 38.19 o 4 49 0 27.45 79.23 39.91 o 0 50 0 79.76 158.16 49.58 o 1 50 0 9.14 52.84 22.34 o 2 50 0 651.11 639.92 32.49 o 3 50 0 8.18 44.45 20.94 o 4 50 0 3.81 37.65 36.40 o 1 51 0 75.48 61.88 22.43 o 2 51 0 21.29 27.34 25.60 o 3 51 0 136.29 112.69 22.60 o 4 51 0 3.94 4.14 51.11 o 0 52 0 252.18 223.11 20.61 o 1 52 0 17.50 48.76 22.91 o 2 52 0 10.25 5.35 18.55 o 3 52 0 55.81 31.46 27.95 o 4 52 0 7.31 -3.15 46.60 o 1 53 0 116.94 60.66 58.94 o 2 53 0 258.51 265.02 25.64 o 3 53 0 38.80 35.19 30.84 o 4 53 0 22.01 -18.49 68.01 o 0 54 0 13.54 7.74 27.92 o 1 54 0 105.10 98.00 25.64 o 2 54 0 17.09 53.10 24.16 o 3 54 0 76.32 75.56 53.17 o 4 54 0 0.21 44.45 41.71 o 1 55 0 94.91 106.72 24.95 o 2 55 0 76.08 118.98 23.77 o 3 55 0 9.19 6.76 25.03 o 4 55 0 42.79 21.21 32.94 o 0 56 0 282.00 318.85 33.40 o 1 56 0 199.07 188.69 33.63 o 2 56 0 11.97 -3.31 41.31 o 3 56 0 29.46 -10.79 23.51 o 1 57 0 81.30 27.33 38.97 o 2 57 0 12.34 44.76 30.54 o 3 57 0 9.26 -12.83 25.88 o 0 58 0 3.66 -26.95 52.74 o 1 58 0 5.01 0.69 24.33 o 2 58 0 6.64 1.97 49.68 o 3 58 0 44.51 17.18 32.83 o 1 59 0 59.23 22.16 33.20 o 2 59 0 39.75 212.48 64.23 o 3 59 0 31.25 -13.69 24.58 o 0 60 0 63.94 34.48 29.92 o 1 60 0 22.24 0.71 37.86 o 2 60 0 47.06 50.92 45.61 o 3 60 0 12.94 -47.61 31.74 o 1 61 0 4.23 0.25 30.03 o 2 61 0 107.98 122.31 49.87 o 3 61 0 22.69 -31.33 28.06 o 0 62 0 18.13 81.74 72.85 o 1 62 0 22.72 -10.87 41.29 o 2 62 0 102.89 122.71 92.78 o 1 63 0 93.81 49.24 126.39 o 2 63 0 103.90 92.67 35.50 o 0 64 0 165.51 260.66 73.51 o 1 64 0 179.47 127.33 120.71 o 2 64 0 13.07 24.95 32.49 o 1 65 0 45.57 137.82 99.55 o 2 65 0 28.15 73.48 48.16 o 0 66 0 36.35 46.31 54.97 o 1 66 0 19.78 53.30 35.41 o 1 67 0 10.93 7.67 35.32 o 0 68 0 263.23 305.27 43.79 o -7 0 1 184.98 234.85 66.91 o -6 0 1 75.30 124.60 48.73 o -5 0 1 4.86 41.65 21.67 o -4 0 1 24.34 44.45 13.64 o -3 0 1 521.47 518.81 17.54 o -2 0 1 508.17 362.94 32.92 o 1 0 1 118.36 97.26 4.91 o 2 0 1 659.57 614.51 23.92 o 3 0 1 543.40 498.84 20.15 o 4 0 1 318.51 582.74 174.42 o 6 0 1 13.25 66.69 43.15 o -7 1 1 189.84 275.18 68.06 o -6 1 1 273.42 189.59 45.37 o -5 1 1 260.04 235.10 62.46 o -4 1 1 491.77 420.60 12.87 o -3 1 1 269.22 327.24 14.96 o -2 1 1 135.91 153.54 7.02 o 1 1 1 664.79 700.15 10.66 o 2 1 1 3071.11 2776.43 66.82 o 3 1 1 311.43 299.38 10.74 o 4 1 1 2127.06 1921.08 59.82 o 5 1 1 50.07 22.51 34.28 o 6 1 1 77.12 170.94 54.36 o -7 2 1 95.13 184.09 61.96 o -6 2 1 47.53 26.72 49.91 o -5 2 1 766.79 762.82 31.02 o -4 2 1 90.03 106.01 12.01 o -3 2 1 594.59 665.79 28.24 o -2 2 1 187.68 111.65 5.72 o 1 2 1 499.62 517.18 9.09 o 2 2 1 2782.19 2672.89 41.53 o 3 2 1 119.61 240.50 59.53 o 4 2 1 431.91 487.15 85.88 o 5 2 1 40.45 -34.17 35.97 o -7 3 1 106.79 186.44 49.94 o -6 3 1 216.73 298.20 56.48 o -5 3 1 66.74 59.53 25.97 o -4 3 1 21.59 18.61 7.41 o -3 3 1 1175.39 1302.29 33.77 o -2 3 1 391.94 359.34 12.89 o 1 3 1 3596.32 3446.92 55.89 o 2 3 1 155.41 213.85 8.59 o 3 3 1 5014.59 4864.66 112.19 o 4 3 1 396.28 402.43 26.83 o 5 3 1 263.78 222.03 30.67 o 6 3 1 20.42 36.11 149.24 o -7 4 1 95.85 190.34 73.04 o -6 4 1 662.59 590.67 40.50 o -5 4 1 199.00 311.45 20.69 o -4 4 1 167.59 149.10 13.76 o -3 4 1 574.74 616.23 18.70 o -2 4 1 568.61 573.75 12.34 o 1 4 1 4.85 16.37 4.23 o 2 4 1 765.36 770.73 16.20 o 3 4 1 964.65 956.68 47.65 o 4 4 1 334.50 334.52 15.19 o 5 4 1 75.89 130.05 26.31 o 6 4 1 3.07 35.18 40.18 o -7 5 1 1.00 -27.79 67.57 o -6 5 1 6.13 98.52 119.14 o -5 5 1 619.57 678.44 31.73 o -4 5 1 111.27 99.24 10.13 o -3 5 1 1520.60 1503.60 26.93 o -2 5 1 1456.19 1323.95 44.96 o 1 5 1 1427.88 1222.66 28.33 o 2 5 1 912.28 907.97 16.44 o 3 5 1 2401.79 2247.72 61.57 o 4 5 1 181.76 187.88 16.42 o 5 5 1 148.91 96.23 42.60 o -7 6 1 2.77 39.56 68.94 o -6 6 1 13.91 18.55 27.19 o -5 6 1 104.41 109.21 30.44 o -4 6 1 80.12 83.66 9.19 o -3 6 1 147.59 211.53 24.57 o -2 6 1 1605.41 1417.57 35.48 o 1 6 1 4280.81 4056.28 53.63 o 2 6 1 3078.25 3182.23 46.77 o 3 6 1 341.51 359.99 14.52 o 4 6 1 161.18 173.51 24.53 o 5 6 1 382.18 334.96 24.32 o 6 6 1 21.16 21.85 33.73 o -7 7 1 31.24 55.25 38.06 o -6 7 1 2.32 -11.35 30.37 o -5 7 1 241.95 342.72 33.46 o -4 7 1 26.02 27.10 10.28 o -3 7 1 2923.97 3238.84 61.52 o -2 7 1 10744.78 10668.70 198.13 o 1 7 1 292.46 256.52 6.55 o 2 7 1 4305.52 4599.68 90.80 o 3 7 1 379.23 342.71 13.87 o 4 7 1 338.36 293.89 27.72 o 5 7 1 79.04 135.44 24.77 o 6 7 1 18.95 -39.45 47.12 o -7 8 1 75.37 95.93 67.38 o -6 8 1 117.10 102.07 20.96 o -5 8 1 614.83 630.17 33.79 o -4 8 1 0.62 -10.70 10.02 o -3 8 1 1239.19 1223.09 27.82 o -2 8 1 10730.78 10575.02 179.98 o 1 8 1 64.14 38.28 3.95 o 2 8 1 4823.50 4981.73 108.17 o 3 8 1 617.63 542.63 18.53 o 4 8 1 1177.36 1074.28 42.50 o 5 8 1 67.66 168.88 34.30 o 6 8 1 20.63 -13.94 53.69 o -7 9 1 17.73 51.09 63.79 o -6 9 1 114.99 65.20 36.66 o -5 9 1 571.06 568.60 27.76 o -4 9 1 48.09 77.99 13.62 o -3 9 1 77.34 130.43 20.74 o -2 9 1 667.98 595.66 29.99 o 1 9 1 2421.80 2275.04 31.37 o 2 9 1 1765.46 1853.05 49.67 o 3 9 1 314.00 298.45 15.20 o 4 9 1 141.55 200.89 27.51 o 5 9 1 257.28 270.40 24.78 o 6 9 1 4.13 -27.46 28.87 o -7 10 1 0.92 -45.15 58.48 o -6 10 1 27.34 36.58 23.54 o -5 10 1 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5415.85 171.73 o -2 8 2 2032.92 2040.77 30.76 o -1 8 2 66.47 46.70 4.57 o 0 8 2 101.79 83.59 6.00 o 1 8 2 9481.88 10243.14 148.20 o 2 8 2 1684.05 1818.19 40.74 o 3 8 2 47.65 44.61 24.18 o 4 8 2 53.74 -3.91 23.70 o 5 8 2 29.17 28.91 61.38 o -7 9 2 43.62 -63.16 56.81 o -6 9 2 71.60 81.01 32.66 o -5 9 2 95.96 106.21 18.61 o -4 9 2 108.22 125.93 17.01 o -3 9 2 1882.22 1911.11 51.24 o -2 9 2 2876.81 2909.85 36.29 o -1 9 2 524.05 544.14 11.28 o 0 9 2 1446.24 1430.02 21.44 o 1 9 2 1780.78 1885.93 52.23 o 2 9 2 3113.00 3139.21 57.36 o 3 9 2 172.69 164.13 35.24 o 4 9 2 206.50 182.69 40.00 o 5 9 2 22.75 175.96 41.67 o -6 10 2 151.85 173.77 46.02 o -5 10 2 4.79 -1.21 15.02 o -4 10 2 501.87 494.81 17.51 o -3 10 2 368.84 355.43 16.52 o -2 10 2 504.11 500.15 13.13 o -1 10 2 3226.71 3276.04 46.13 o 0 10 2 420.53 460.47 12.49 o 1 10 2 4351.44 4637.19 69.48 o 2 10 2 33.30 51.38 12.12 o 3 10 2 71.38 120.83 21.04 o 4 10 2 348.33 339.59 25.05 o 5 10 2 275.03 222.88 40.11 o -7 11 2 16.80 13.28 66.17 o -6 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69.24 o -6 22 2 56.23 69.25 46.62 o -5 22 2 273.69 295.77 19.62 o -4 22 2 122.88 78.14 33.81 o -3 22 2 355.06 359.10 15.13 o -2 22 2 260.49 257.46 7.08 o -1 22 2 566.53 512.52 9.41 o 0 22 2 871.39 865.28 14.34 o 1 22 2 44.14 40.77 7.54 o 2 22 2 105.63 95.87 9.56 o 3 22 2 39.77 42.18 23.38 o 4 22 2 101.44 137.74 32.70 o 5 22 2 7.22 24.81 28.99 o -7 23 2 49.63 115.75 75.51 o -6 23 2 18.06 52.95 24.98 o -5 23 2 97.39 153.96 32.65 o -4 23 2 59.96 76.97 14.14 o -3 23 2 119.16 129.13 10.74 o -2 23 2 139.13 122.57 6.35 o -1 23 2 368.96 367.37 8.67 o 0 23 2 36.78 32.14 5.37 o 1 23 2 166.08 172.87 8.71 o 2 23 2 112.85 139.19 8.96 o 3 23 2 196.03 229.05 13.16 o 4 23 2 43.06 30.79 40.79 o 5 23 2 100.88 73.12 32.78 o -7 24 2 19.54 53.85 69.59 o -6 24 2 52.46 37.04 26.38 o -5 24 2 3.13 6.09 15.79 o -4 24 2 48.61 33.67 13.92 o -3 24 2 564.55 559.45 16.31 o -2 24 2 331.29 381.73 8.97 o -1 24 2 142.76 135.96 5.94 o 0 24 2 282.70 273.44 7.91 o 1 24 2 87.42 97.55 9.68 o 2 24 2 301.13 308.77 11.71 o 3 24 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56.89 7.67 o 2 27 2 126.25 150.05 14.89 o 3 27 2 156.22 174.07 18.54 o 4 27 2 70.92 35.91 23.47 o 5 27 2 47.98 21.80 24.44 o -6 28 2 73.73 86.40 53.41 o -5 28 2 35.49 53.22 21.83 o -4 28 2 117.08 102.14 17.90 o -3 28 2 1383.15 1403.50 22.37 o -2 28 2 105.04 120.75 9.43 o -1 28 2 1.21 2.65 5.57 o 0 28 2 210.42 208.04 8.20 o 1 28 2 62.99 80.74 9.23 o 2 28 2 1004.50 1025.48 24.91 o 3 28 2 248.21 273.49 24.20 o 4 28 2 44.76 9.80 23.25 o 5 28 2 9.80 21.87 45.89 o -6 29 2 52.71 35.59 59.16 o -5 29 2 21.46 24.99 22.75 o -4 29 2 17.41 19.93 14.75 o -3 29 2 168.35 188.04 18.19 o -2 29 2 249.02 227.72 9.46 o -1 29 2 7.50 0.96 6.09 o 0 29 2 196.70 186.15 8.35 o 1 29 2 32.87 20.66 13.15 o 2 29 2 93.62 122.26 16.10 o 3 29 2 514.81 440.39 18.88 o 4 29 2 31.15 68.39 28.83 o 5 29 2 24.08 20.11 27.47 o -5 30 2 49.29 73.25 24.79 o -4 30 2 282.80 383.16 25.42 o -3 30 2 107.47 99.00 14.55 o -2 30 2 244.33 247.10 9.67 o -1 30 2 483.33 442.63 10.99 o 0 30 2 235.11 260.72 14.31 o 1 30 2 30.21 33.09 9.95 o 2 30 2 98.76 100.03 17.59 o 3 30 2 251.27 244.54 19.96 o 4 30 2 209.48 238.58 30.51 o 5 30 2 39.78 52.36 40.48 o -6 31 2 220.22 239.80 60.48 o -5 31 2 128.03 170.07 44.76 o -4 31 2 1315.35 1350.18 48.89 o -3 31 2 162.39 191.28 16.11 o -2 31 2 15.00 9.55 9.87 o -1 31 2 142.17 127.54 7.83 o 0 31 2 1282.00 1295.68 23.37 o 1 31 2 179.40 184.52 11.99 o 2 31 2 611.09 528.66 19.90 o 3 31 2 49.47 33.21 16.94 o 4 31 2 146.76 135.20 37.59 o 5 31 2 52.51 -19.96 46.16 o -6 32 2 58.73 68.31 28.00 o -5 32 2 72.68 73.13 43.67 o -4 32 2 700.43 698.17 32.11 o -3 32 2 2232.87 2138.33 49.24 o -2 32 2 1291.04 1353.13 22.06 o -1 32 2 132.49 138.11 7.78 o 0 32 2 119.73 135.27 11.78 o 1 32 2 903.99 903.69 20.43 o 2 32 2 1494.55 1434.54 37.56 o 3 32 2 407.68 355.96 24.48 o 4 32 2 68.81 53.27 34.22 o 5 32 2 36.62 48.44 33.08 o -4 33 2 96.85 126.72 42.82 o -3 33 2 335.81 355.60 21.38 o -2 33 2 1893.71 1994.97 31.54 o -1 33 2 2.20 -12.36 8.24 o 0 33 2 71.62 92.15 12.73 o 1 33 2 285.51 285.01 21.88 o 2 33 2 2009.45 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57.88 o 4 36 2 108.90 77.86 45.01 o -6 37 2 24.67 -10.13 72.92 o -5 37 2 325.54 333.16 62.04 o -4 37 2 424.87 413.19 38.98 o -3 37 2 711.26 676.55 27.28 o -2 37 2 131.61 157.38 9.44 o -1 37 2 886.75 953.20 22.96 o 0 37 2 990.13 989.11 19.32 o 1 37 2 413.46 435.63 26.11 o 2 37 2 811.26 818.18 25.24 o 3 37 2 175.25 154.90 41.72 o 4 37 2 61.22 164.34 37.96 o -6 38 2 41.77 78.99 51.06 o -5 38 2 399.35 468.73 68.28 o -4 38 2 76.74 163.25 39.78 o -3 38 2 2.20 13.82 15.63 o -2 38 2 353.47 382.81 13.76 o -1 38 2 262.04 260.08 16.95 o 0 38 2 405.51 425.09 15.50 o 1 38 2 1265.13 1215.86 27.44 o 2 38 2 283.39 285.63 16.02 o 3 38 2 66.49 82.87 62.50 o 4 38 2 267.36 325.83 38.89 o -6 39 2 88.31 150.91 59.55 o -5 39 2 385.86 399.68 46.05 o -4 39 2 256.08 302.66 37.37 o -3 39 2 246.55 218.89 16.51 o -2 39 2 169.32 136.46 13.80 o -1 39 2 1213.45 1230.39 27.22 o 0 39 2 1365.43 1335.05 29.06 o 1 39 2 1746.64 1697.74 35.80 o 2 39 2 81.88 116.02 16.67 o 3 39 2 267.16 326.36 35.30 o 4 39 2 213.48 202.57 38.47 o -6 40 2 34.99 69.19 67.53 o -5 40 2 68.48 -10.77 77.11 o -4 40 2 321.18 368.46 31.78 o -3 40 2 252.73 189.73 20.60 o -2 40 2 686.58 674.64 20.98 o -1 40 2 142.57 165.06 14.18 o 0 40 2 186.73 214.53 19.06 o 1 40 2 510.11 488.33 19.79 o 2 40 2 214.51 210.97 18.08 o 3 40 2 13.92 45.42 24.70 o 4 40 2 52.68 58.32 34.41 o -6 41 2 96.02 128.59 68.09 o -4 41 2 703.14 749.28 37.42 o -3 41 2 101.46 85.03 22.44 o -2 41 2 791.53 774.00 25.92 o -1 41 2 181.57 197.63 13.81 o 0 41 2 1694.60 1605.08 33.33 o 1 41 2 189.43 183.89 15.24 o 2 41 2 132.51 185.00 19.03 o 3 41 2 62.51 26.75 25.37 o 4 41 2 8.90 86.21 45.11 o -5 42 2 852.84 917.79 72.17 o -4 42 2 186.49 227.95 38.60 o -3 42 2 141.11 182.27 26.67 o -2 42 2 74.12 68.54 17.38 o -1 42 2 321.45 255.92 15.80 o 0 42 2 984.86 930.21 26.79 o 1 42 2 370.38 348.83 16.63 o 2 42 2 80.43 84.20 15.38 o 3 42 2 24.30 17.58 19.40 o 4 42 2 193.77 263.81 44.34 o -5 43 2 0.46 12.06 28.19 o -4 43 2 110.55 76.30 63.89 o -3 43 2 1123.74 1137.51 38.33 o -2 43 2 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127.76 o 0 10 3 42.09 16.87 6.91 o 1 10 3 314.69 347.74 27.14 o 2 10 3 18.76 25.38 14.77 o 3 10 3 937.02 749.01 49.99 o 4 10 3 54.88 75.73 46.19 o -7 11 3 16.05 6.13 30.34 o -6 11 3 33.59 4.45 24.35 o -5 11 3 174.05 204.26 29.13 o -4 11 3 10.61 16.02 8.17 o -3 11 3 209.28 257.27 10.06 o -2 11 3 1351.56 1377.11 27.46 o -1 11 3 917.50 1168.18 120.79 o 0 11 3 88.54 174.00 19.30 o 1 11 3 269.85 302.69 19.07 o 2 11 3 26.57 6.45 11.73 o 3 11 3 142.17 105.95 35.43 o 4 11 3 14.16 55.16 27.66 o -7 12 3 3.03 15.47 45.41 o -6 12 3 35.34 11.95 31.57 o -5 12 3 405.27 346.90 25.25 o -4 12 3 40.96 28.86 14.84 o -3 12 3 75.22 65.22 11.17 o -2 12 3 863.84 781.17 67.90 o -1 12 3 3327.23 3437.26 130.16 o 0 12 3 1359.71 1427.62 28.40 o 1 12 3 706.68 780.20 25.02 o 2 12 3 19.01 24.50 12.30 o 5 12 3 153.60 247.50 55.36 o -7 13 3 42.09 68.97 28.14 o -6 13 3 70.30 70.50 23.25 o -5 13 3 257.09 282.41 18.87 o -4 13 3 196.91 163.06 17.31 o -3 13 3 12.55 6.07 7.36 o -2 13 3 876.25 854.00 20.69 o -1 13 3 10412.78 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