#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/69/2216953.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216953_Fobs loop_ _publ_author_name 'Y\?ild\?ir\?im, Sema \"Ozt\"urk' 'McKee, Vickie' 'Khardli, Fatim-Zahra' 'Mimouni, Mostafa' 'Hadda, Taibi Ben' _publ_section_title ; Rubidium(I) monensinate dihydrate ; _journal_coeditor_code BT2658 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m154 _journal_page_last m155 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 12.5298 _cell_length_b 16.3610 _cell_length_c 19.3422 _exptl_crystal_F_000 1688.00 _reflns_d_resolution_high 0.7482 _[local]_cod_data_source_file bt2658Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Sema5 - MON-Rb in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4580.83 5099.32 367.10 o 4 0 0 949.15 953.74 35.56 o 6 0 0 934.20 867.71 34.16 o 8 0 0 4312.31 3761.21 133.13 o 10 0 0 1068.58 1076.34 59.76 o 12 0 0 264.96 212.51 42.14 o 14 0 0 1332.16 1387.73 78.39 o 16 0 0 427.47 434.94 48.50 o 1 1 0 28142.74 30960.46 1168.66 o 2 1 0 11216.22 11534.04 390.12 o 3 1 0 4195.65 4494.65 172.35 o 4 1 0 3045.65 3168.63 85.65 o 5 1 0 53.29 73.77 6.65 o 6 1 0 1146.53 1250.57 32.82 o 7 1 0 5151.67 4872.77 120.21 o 8 1 0 145.55 142.73 9.72 o 9 1 0 968.36 950.11 32.59 o 10 1 0 122.81 135.74 15.02 o 11 1 0 234.77 271.15 22.67 o 12 1 0 4189.90 3964.06 124.62 o 13 1 0 224.34 262.57 27.57 o 14 1 0 41.60 85.83 35.01 o 15 1 0 101.07 99.29 27.12 o 16 1 0 149.97 233.62 46.86 o 1 2 0 27195.27 28861.28 762.11 o 2 2 0 1854.21 2103.52 56.16 o 3 2 0 238.15 298.99 22.32 o 4 2 0 3327.43 3562.30 144.21 o 5 2 0 9927.63 9680.23 258.90 o 6 2 0 127.64 123.49 9.59 o 7 2 0 151.85 142.69 10.99 o 8 2 0 0.41 -10.12 10.68 o 9 2 0 6782.93 6598.70 178.65 o 10 2 0 2920.68 2824.56 80.20 o 11 2 0 2248.40 2113.82 70.93 o 12 2 0 122.49 115.87 24.24 o 13 2 0 767.75 845.16 38.01 o 14 2 0 333.79 326.62 28.47 o 15 2 0 78.49 141.74 27.07 o 16 2 0 30.87 49.49 28.53 o 1 3 0 166.01 194.66 8.02 o 2 3 0 6195.49 6418.82 169.80 o 3 3 0 7131.41 7372.39 201.51 o 4 3 0 9565.37 9875.39 263.54 o 5 3 0 5513.63 5905.82 158.59 o 6 3 0 1631.72 1664.70 47.41 o 7 3 0 2844.99 2914.62 80.54 o 8 3 0 2581.39 2538.26 71.51 o 9 3 0 552.16 529.27 22.04 o 10 3 0 160.85 145.50 16.14 o 11 3 0 254.65 226.17 18.61 o 12 3 0 1556.93 1515.05 55.84 o 13 3 0 1380.53 1333.53 52.64 o 14 3 0 6.41 82.13 32.16 o 15 3 0 719.12 666.62 42.88 o 16 3 0 3.57 -0.21 31.80 o 0 4 0 43040.41 43929.88 1510.11 o 1 4 0 1007.65 1081.09 30.38 o 2 4 0 8972.99 9073.62 239.62 o 3 4 0 2685.06 2763.77 68.48 o 4 4 0 293.33 343.79 13.51 o 5 4 0 14944.93 16518.69 440.15 o 6 4 0 6620.81 6779.42 182.23 o 7 4 0 1271.24 1393.84 41.44 o 8 4 0 7954.68 7904.65 212.69 o 9 4 0 2105.28 1987.91 58.32 o 10 4 0 254.31 263.64 18.22 o 11 4 0 67.79 44.26 16.42 o 12 4 0 907.03 872.76 44.80 o 13 4 0 23.63 35.15 22.70 o 14 4 0 1979.51 1867.29 78.09 o 15 4 0 1.26 40.30 30.87 o 16 4 0 138.43 171.77 35.16 o 1 5 0 4796.64 4795.85 127.38 o 2 5 0 86.75 79.64 6.19 o 3 5 0 16.81 -0.99 5.59 o 4 5 0 8750.08 8464.52 223.89 o 5 5 0 10025.77 10648.38 284.75 o 6 5 0 175.86 156.80 10.91 o 7 5 0 1806.52 1723.88 49.97 o 8 5 0 51.19 71.49 12.74 o 9 5 0 766.20 697.06 33.66 o 10 5 0 7240.41 7244.84 195.96 o 11 5 0 105.92 91.51 17.47 o 12 5 0 1152.03 1113.93 45.72 o 13 5 0 622.83 663.10 50.09 o 14 5 0 109.41 104.40 29.19 o 15 5 0 498.64 494.79 39.73 o 16 5 0 44.55 12.44 33.69 o 0 6 0 25.38 13.67 10.62 o 1 6 0 336.70 408.31 16.19 o 2 6 0 7.25 9.44 6.83 o 3 6 0 1817.88 1761.36 54.66 o 4 6 0 22.97 47.44 9.02 o 5 6 0 384.54 360.63 14.61 o 6 6 0 50.32 56.18 9.88 o 7 6 0 138.52 146.71 12.60 o 8 6 0 171.53 180.75 14.73 o 9 6 0 4344.29 4292.53 118.14 o 10 6 0 276.19 324.10 19.50 o 11 6 0 822.86 862.11 37.42 o 12 6 0 36.17 9.67 20.16 o 13 6 0 900.66 850.94 45.55 o 14 6 0 157.30 134.03 34.35 o 15 6 0 269.55 217.96 34.78 o 16 6 0 12.76 -5.25 34.53 o 1 7 0 7933.76 7899.92 209.60 o 2 7 0 6529.67 7097.28 210.61 o 3 7 0 10.88 -4.16 7.07 o 5 7 0 5913.04 6113.10 162.92 o 6 7 0 221.39 199.82 11.85 o 7 7 0 210.52 182.94 13.61 o 8 7 0 1128.60 1097.57 36.19 o 9 7 0 2879.30 2660.80 76.01 o 10 7 0 21.82 17.87 17.85 o 11 7 0 162.09 106.74 21.74 o 12 7 0 718.58 725.87 34.49 o 13 7 0 503.42 484.94 50.90 o 14 7 0 321.36 302.93 34.47 o 15 7 0 468.34 537.52 42.26 o 0 8 0 8087.06 8284.08 286.43 o 2 8 0 10666.65 11003.67 291.35 o 3 8 0 490.18 518.67 19.06 o 4 8 0 240.01 280.44 13.09 o 5 8 0 664.21 639.39 22.70 o 6 8 0 4274.79 4013.69 108.83 o 7 8 0 107.85 146.36 17.54 o 8 8 0 3923.44 3895.26 119.66 o 9 8 0 239.36 213.15 19.83 o 10 8 0 80.28 72.99 19.09 o 11 8 0 142.39 94.69 20.79 o 12 8 0 825.35 785.14 36.70 o 13 8 0 187.19 170.02 30.12 o 14 8 0 1998.37 2122.71 87.41 o 15 8 0 80.95 124.63 34.55 o 1 9 0 97.17 106.92 9.82 o 2 9 0 49.86 22.38 9.03 o 3 9 0 334.79 342.08 18.70 o 4 9 0 2092.56 2154.73 60.14 o 5 9 0 349.29 330.77 15.66 o 6 9 0 1124.90 994.68 32.33 o 7 9 0 9647.50 9731.32 289.68 o 8 9 0 55.26 28.84 16.70 o 9 9 0 3107.99 3183.17 99.98 o 10 9 0 645.95 588.30 29.58 o 11 9 0 37.69 48.66 20.87 o 12 9 0 492.29 449.06 29.17 o 13 9 0 813.96 739.57 48.97 o 14 9 0 211.90 241.04 34.54 o 15 9 0 111.31 163.56 35.96 o 0 10 0 497.62 434.77 24.81 o 1 10 0 1218.54 1266.77 37.85 o 2 10 0 1898.85 2049.60 57.69 o 3 10 0 2603.42 2620.15 72.50 o 4 10 0 63.09 64.99 11.41 o 5 10 0 5835.85 5891.53 178.60 o 6 10 0 1279.62 1160.93 42.31 o 7 10 0 899.29 811.87 34.72 o 8 10 0 830.99 759.09 33.86 o 9 10 0 230.76 230.27 33.07 o 10 10 0 20.61 10.89 19.63 o 11 10 0 1140.23 1051.24 44.55 o 12 10 0 278.93 198.75 25.74 o 13 10 0 256.61 274.09 28.47 o 14 10 0 2.20 1.79 31.59 o 1 11 0 894.26 888.15 29.44 o 2 11 0 875.37 878.15 29.76 o 3 11 0 214.41 199.13 14.08 o 4 11 0 874.34 826.69 29.05 o 5 11 0 4376.11 4323.26 117.17 o 6 11 0 1636.45 1567.98 53.93 o 7 11 0 2661.56 2545.00 81.71 o 8 11 0 332.56 312.29 36.96 o 9 11 0 291.16 354.54 32.98 o 10 11 0 39.62 34.07 20.60 o 11 11 0 99.39 61.33 22.94 o 12 11 0 680.09 694.21 38.44 o 13 11 0 251.76 211.20 28.23 o 14 11 0 394.76 373.35 39.29 o 0 12 0 6859.11 6754.83 236.16 o 1 12 0 262.63 267.61 15.92 o 2 12 0 1863.80 1796.73 52.76 o 3 12 0 11.18 -6.41 12.50 o 4 12 0 285.07 253.09 16.36 o 5 12 0 606.01 564.35 23.00 o 6 12 0 2342.96 2231.93 72.74 o 7 12 0 23.16 10.88 17.36 o 8 12 0 878.97 851.21 37.02 o 9 12 0 64.31 40.26 20.15 o 10 12 0 652.04 670.94 33.47 o 11 12 0 38.24 9.88 22.75 o 12 12 0 165.10 169.69 26.58 o 13 12 0 20.96 -26.07 26.20 o 14 12 0 531.35 589.12 69.04 o 1 13 0 1751.35 1760.12 52.16 o 2 13 0 1897.72 1956.80 57.30 o 3 13 0 194.03 213.40 16.49 o 4 13 0 1595.03 1607.14 49.13 o 5 13 0 354.44 315.66 18.71 o 6 13 0 32.23 34.42 18.96 o 7 13 0 2287.44 2224.45 73.96 o 8 13 0 167.63 197.14 21.85 o 9 13 0 651.78 609.63 31.90 o 10 13 0 944.21 938.78 41.41 o 11 13 0 13.56 -45.64 22.82 o 12 13 0 151.13 160.82 27.25 o 13 13 0 183.81 166.99 29.64 o 0 14 0 1373.84 1269.12 64.73 o 1 14 0 293.37 335.32 19.17 o 2 14 0 35.90 5.96 14.82 o 3 14 0 4689.88 4798.91 131.35 o 4 14 0 2985.18 2906.87 82.20 o 5 14 0 807.40 832.85 36.07 o 6 14 0 199.48 208.68 21.23 o 7 14 0 647.25 603.84 30.41 o 8 14 0 32.49 44.00 20.72 o 9 14 0 251.66 199.92 24.38 o 10 14 0 23.84 25.04 23.23 o 11 14 0 486.43 521.95 33.21 o 12 14 0 158.62 192.37 29.83 o 1 15 0 816.74 771.70 33.00 o 2 15 0 912.23 914.90 34.41 o 3 15 0 23.60 43.50 16.43 o 4 15 0 24.41 10.45 16.20 o 5 15 0 351.22 349.65 27.96 o 6 15 0 220.82 216.58 22.76 o 7 15 0 1416.35 1439.55 71.25 o 8 15 0 8.63 2.45 29.31 o 9 15 0 1021.76 1001.53 44.00 o 10 15 0 558.23 503.37 32.58 o 11 15 0 7.24 17.95 26.02 o 12 15 0 364.16 397.84 33.75 o 0 16 0 2714.66 2783.08 125.44 o 1 16 0 128.11 116.50 19.75 o 2 16 0 3047.42 3141.11 98.76 o 3 16 0 552.60 565.09 28.80 o 4 16 0 194.70 185.72 20.25 o 5 16 0 127.79 99.65 21.26 o 6 16 0 913.84 959.08 43.49 o 7 16 0 144.64 169.12 23.65 o 8 16 0 427.75 372.59 28.24 o 9 16 0 2.89 -25.21 23.15 o 10 16 0 11.80 -44.34 24.75 o 11 16 0 73.55 34.34 27.15 o 1 17 0 1849.43 1800.57 62.73 o 2 17 0 851.27 934.39 40.61 o 3 17 0 2.26 16.31 19.93 o 4 17 0 198.18 211.51 26.63 o 5 17 0 120.09 105.06 22.44 o 6 17 0 102.89 84.00 23.03 o 7 17 0 1101.97 1092.90 46.61 o 8 17 0 4.13 28.18 23.98 o 9 17 0 157.42 195.39 27.55 o 10 17 0 370.12 375.78 32.34 o 0 18 0 146.47 102.86 55.59 o 1 18 0 265.02 240.48 24.90 o 2 18 0 4.10 11.61 21.35 o 3 18 0 1117.30 1249.03 49.88 o 4 18 0 128.82 152.85 28.96 o 5 18 0 290.64 266.53 29.59 o 6 18 0 44.09 44.48 25.51 o 7 18 0 130.90 116.35 25.56 o 8 18 0 179.50 172.76 27.52 o 9 18 0 339.48 358.63 31.51 o 1 19 0 21.60 -0.20 23.48 o 2 19 0 1662.88 1716.59 62.87 o 3 19 0 206.85 184.76 44.29 o 4 19 0 200.47 241.71 33.91 o 5 19 0 192.40 241.69 30.48 o 6 19 0 8.54 32.16 27.62 o 7 19 0 738.17 818.89 45.37 o 8 19 0 12.47 -4.79 28.78 o 0 20 0 87.11 129.96 38.04 o 1 20 0 15.81 59.13 37.21 o 2 20 0 650.38 739.62 37.97 o 3 20 0 182.51 196.05 30.72 o 4 20 0 75.12 138.33 36.62 o 5 20 0 1.56 -2.65 28.50 o 6 20 0 427.26 463.90 37.12 o 1 21 0 188.83 195.62 29.19 o 2 21 0 6.82 9.17 26.55 o 3 21 0 317.62 338.64 35.63 o 4 21 0 162.10 217.34 33.17 o 1 0 1 22514.13 23249.37 615.52 o 2 0 1 838.43 816.77 26.08 o 3 0 1 12044.15 12159.86 358.57 o 4 0 1 1895.54 1996.14 52.89 o 5 0 1 7293.66 7393.68 180.75 o 6 0 1 1215.15 1185.10 31.56 o 7 0 1 748.74 696.21 21.20 o 8 0 1 611.61 593.53 19.18 o 9 0 1 277.28 246.86 12.84 o 10 0 1 1591.97 1468.56 52.24 o 11 0 1 4680.80 4355.95 135.00 o 12 0 1 105.34 51.87 20.44 o 13 0 1 305.19 297.97 25.98 o 14 0 1 65.13 118.13 30.35 o 16 0 1 14.80 39.05 28.14 o -16 1 1 137.36 175.50 29.91 o -15 1 1 516.09 491.91 33.07 o -14 1 1 384.02 347.33 28.47 o -13 1 1 203.64 252.13 25.31 o -12 1 1 58.37 61.54 24.27 o -11 1 1 697.35 571.89 41.48 o -10 1 1 501.31 528.30 22.76 o -9 1 1 271.42 258.18 12.99 o -8 1 1 70.23 48.60 8.73 o -7 1 1 656.85 673.80 20.73 o -6 1 1 8216.05 8201.03 200.57 o -5 1 1 3314.57 3043.29 75.50 o -4 1 1 12678.24 12765.60 311.22 o -3 1 1 5276.77 5454.67 146.33 o -2 1 1 16798.03 17380.08 462.95 o -1 1 1 31608.04 31675.07 853.62 o 0 1 1 26562.38 22499.43 803.99 o 1 1 1 30394.27 32567.52 958.88 o 2 1 1 14497.37 16496.70 883.78 o 3 1 1 4254.20 4658.84 189.48 o 4 1 1 13325.57 13441.97 396.04 o 5 1 1 3073.48 2925.67 84.59 o 6 1 1 7871.19 7797.27 209.26 o 7 1 1 488.37 511.82 19.05 o 8 1 1 10.02 10.11 10.55 o 9 1 1 468.23 424.50 18.97 o 10 1 1 166.23 143.98 15.40 o 11 1 1 592.10 552.40 28.34 o 12 1 1 32.24 23.19 26.47 o 13 1 1 226.94 216.97 27.41 o 14 1 1 310.33 314.37 28.05 o 15 1 1 601.30 553.91 34.55 o 16 1 1 151.87 167.49 29.70 o -16 2 1 266.13 314.99 31.82 o -15 2 1 141.66 216.05 34.61 o -14 2 1 54.14 54.17 23.99 o -13 2 1 857.18 871.46 38.77 o -12 2 1 1315.40 1293.31 49.99 o -11 2 1 264.26 248.23 21.87 o -10 2 1 1628.04 1599.75 49.31 o -9 2 1 990.31 929.23 32.13 o -8 2 1 3875.63 3741.04 102.79 o -7 2 1 1901.48 1809.43 51.80 o -6 2 1 11214.36 11498.33 307.39 o -5 2 1 235.10 219.46 11.01 o -4 2 1 1999.31 2145.87 53.59 o -3 2 1 2835.29 2681.60 82.22 o -2 2 1 8952.16 8888.05 236.89 o -1 2 1 9127.60 9786.91 262.88 o 0 2 1 6981.88 7790.24 210.00 o 1 2 1 11082.07 12712.53 335.68 o 2 2 1 8205.90 8661.06 230.96 o 3 2 1 2972.47 3190.97 160.47 o 4 2 1 2153.53 2415.30 95.61 o 5 2 1 85.41 82.48 7.74 o 6 2 1 11382.28 11837.08 316.27 o 7 2 1 1716.93 1620.91 46.96 o 8 2 1 3799.37 3700.86 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18.34 o 9 4 1 4810.64 4614.01 126.40 o 10 4 1 1943.35 1936.86 58.12 o 11 4 1 3185.04 3086.44 87.69 o 12 4 1 437.10 413.12 32.29 o 13 4 1 511.45 484.62 30.16 o 14 4 1 167.57 142.50 42.39 o 15 4 1 227.85 215.07 33.75 o 16 4 1 39.13 89.73 68.39 o -16 5 1 138.08 192.00 36.32 o -15 5 1 632.56 656.05 43.50 o -14 5 1 146.50 131.72 30.41 o -13 5 1 136.87 150.76 28.42 o -12 5 1 748.04 740.66 34.89 o -11 5 1 576.06 533.05 24.55 o -10 5 1 3.99 -10.33 14.80 o -9 5 1 854.64 849.61 31.26 o -8 5 1 743.92 718.28 26.47 o -7 5 1 5361.00 5474.21 148.13 o -6 5 1 77.74 83.13 9.78 o -5 5 1 1824.01 1762.24 45.23 o -4 5 1 16840.13 17414.00 392.64 o -3 5 1 5576.92 5791.25 156.78 o -2 5 1 2316.43 2411.64 59.81 o -1 5 1 99.26 96.02 5.68 o 0 5 1 1499.18 1649.81 41.39 o 1 5 1 515.84 559.75 17.59 o 2 5 1 1362.33 1528.09 42.55 o 3 5 1 4470.32 4841.18 144.32 o 4 5 1 16900.53 17764.72 523.97 o 5 5 1 1785.19 1838.18 57.53 o 6 5 1 299.38 356.05 15.03 o 7 5 1 5341.19 5557.42 150.12 o 8 5 1 488.69 489.15 20.22 o 9 5 1 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71.48 87.16 77.20 o 1 8 23 29.68 3.29 46.64 o 2 8 23 157.60 199.59 43.99 o 3 8 23 449.03 506.60 42.10 o 4 8 23 206.70 212.19 37.79 o -3 9 23 49.82 20.23 43.81 o -2 9 23 95.56 24.84 43.22 o -1 9 23 344.76 371.71 48.47 o 0 9 23 18.13 22.38 42.74 o 1 9 23 205.81 150.93 44.17 o 2 9 23 144.35 124.12 43.91 o 3 9 23 27.69 -4.12 41.39 o 0 0 24 1273.03 1178.16 170.59 o 1 0 24 141.03 203.07 35.07 o 2 0 24 454.08 600.17 68.79 o 3 0 24 3.62 84.68 84.64 o 4 0 24 90.47 185.68 72.87 o 5 0 24 10.17 37.60 35.64 o 6 0 24 343.85 332.79 39.54 o -6 1 24 14.20 52.18 58.29 o -5 1 24 313.87 278.66 37.60 o -4 1 24 400.72 380.37 38.79 o -3 1 24 277.88 420.08 108.45 o -2 1 24 465.39 496.92 43.87 o -1 1 24 421.04 436.73 45.83 o 0 1 24 0.50 65.41 33.57 o 1 1 24 412.30 446.76 39.53 o 2 1 24 393.21 440.51 39.49 o 3 1 24 299.36 380.35 63.72 o 4 1 24 452.57 432.60 50.81 o 5 1 24 311.19 307.13 38.25 o 6 1 24 2.17 71.84 36.05 o -5 2 24 477.80 447.81 46.59 o -4 2 24 26.74 84.71 64.25 o -3 2 24 695.96 759.47 58.44 o -2 2 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58.92 o -1 2 25 444.08 506.56 41.92 o 0 2 25 420.34 422.71 40.82 o 1 2 25 423.03 456.27 49.09 o 2 2 25 488.69 509.63 61.96 o 3 2 25 43.26 48.63 37.51 o -3 3 25 21.28 79.08 41.16 o -2 3 25 151.69 162.58 37.22 o -1 3 25 234.12 295.89 48.86 o 0 3 25 142.88 178.05 38.06 o 1 3 25 245.17 294.79 62.96 o 2 3 25 123.36 164.51 83.80 o 3 3 25 45.09 18.44 57.21 o -2 4 25 68.17 109.76 36.79 o -1 4 25 137.96 224.84 44.60 o 0 4 25 0.61 -1.62 36.57 o 1 4 25 85.20 195.54 38.52 o 2 4 25 123.99 80.92 37.82 o -1 5 25 984.18 1119.26 81.70 o 0 5 25 97.19 81.28 38.34 o 1 5 25 888.60 894.09 60.21 o