#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:44:29 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181089 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/69/2216954.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2216954_Fobs
loop_
_publ_author_name
'Lutz, Martin'
'Spek, Anthony L.'
'van der Geer, Erwin P. L.'
'van Koten, Gerard'
'Klein Gebbink, Robertus J. M.'
_publ_section_title
;
 Indole-3-thiouronium iodide
;
_journal_coeditor_code           BT2659
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              o195
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 102.648
_cell_angle_gamma                90.000
_cell_length_a                   10.5098
_cell_length_b                   10.6264
_cell_length_c                   10.6951
_exptl_crystal_F_000             616.00
_reflns_d_resolution_high        0.7697
_cod_data_source_file            bt2659Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' s3842a'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            259.12
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 1622.93 1513.93 25.43 o
2 0 0 32189.08 30354.50 559.72 o
3 0 0 8877.42 8959.88 164.72 o
4 0 0 15425.14 15316.90 268.21 o
5 0 0 1979.72 1657.39 37.38 o
6 0 0 9690.01 9429.39 173.36 o
7 0 0 4367.10 4338.94 87.58 o
8 0 0 776.60 794.40 24.76 o
9 0 0 8679.47 8904.20 192.57 o
10 0 0 844.43 837.33 27.25 o
11 0 0 3810.04 3888.31 120.14 o
12 0 0 315.27 307.29 37.14 o
1 1 0 145.24 153.07 2.26 o
2 1 0 17.16 32.12 0.93 o
3 1 0 5644.23 5464.42 63.36 o
4 1 0 73.08 74.39 2.45 o
5 1 0 15.42 30.40 2.29 o
6 1 0 2111.06 2230.64 32.68 o
7 1 0 148.63 150.23 5.33 o
8 1 0 2211.72 2216.30 40.41 o
9 1 0 1475.04 1459.89 28.96 o
10 1 0 223.17 231.79 9.90 o
11 1 0 62.16 49.75 8.72 o
12 1 0 1144.07 1207.01 40.51 o
13 1 0 5.33 -13.25 22.37 o
0 2 0 9263.40 10656.90 268.65 o
1 2 0 9120.53 9384.68 106.66 o
2 2 0 28096.24 27376.84 298.20 o
3 2 0 1349.31 1318.28 20.01 o
4 2 0 9938.42 9614.73 105.62 o
5 2 0 4033.78 4092.98 52.13 o
6 2 0 5843.64 5936.50 82.20 o
7 2 0 6811.28 6899.45 94.11 o
8 2 0 3895.90 3861.24 60.32 o
9 2 0 3768.76 3900.11 66.23 o
10 2 0 365.98 358.14 14.44 o
11 2 0 4519.28 4636.86 117.28 o
12 2 0 1.28 4.78 24.56 o
13 2 0 3022.88 3120.15 136.46 o
1 3 0 17131.84 17991.28 203.60 o
2 3 0 5087.78 5044.09 61.31 o
3 3 0 16599.28 16706.63 200.48 o
4 3 0 4660.24 4658.04 61.25 o
5 3 0 7227.98 7208.61 81.65 o
6 3 0 4366.36 4459.20 59.36 o
7 3 0 2562.72 2554.55 39.57 o
8 3 0 1784.24 1805.83 29.81 o
9 3 0 10.20 9.03 6.77 o
10 3 0 2377.16 2349.99 54.89 o
11 3 0 1.87 8.80 11.81 o
12 3 0 1746.90 1776.65 54.37 o
13 3 0 94.48 106.57 26.49 o
0 4 0 4875.99 5246.01 102.64 o
1 4 0 436.84 428.56 7.78 o
2 4 0 7985.98 8094.64 93.84 o
3 4 0 6.77 11.18 1.97 o
4 4 0 2790.26 2849.12 41.78 o
5 4 0 667.68 636.46 11.35 o
6 4 0 301.14 280.35 6.46 o
7 4 0 2066.40 2134.71 36.73 o
8 4 0 23.75 19.86 4.65 o
9 4 0 765.93 725.99 17.99 o
10 4 0 14.67 10.88 8.00 o
11 4 0 206.20 214.22 13.14 o
12 4 0 100.64 93.24 16.15 o
1 5 0 27576.68 28869.87 311.96 o
2 5 0 317.08 335.21 6.81 o
3 5 0 6162.95 6174.25 70.60 o
4 5 0 6388.06 6577.21 96.68 o
5 5 0 16829.87 16842.05 194.78 o
6 5 0 2513.15 2457.00 35.60 o
7 5 0 4204.87 4134.34 65.17 o
8 5 0 6107.35 6077.74 92.51 o
9 5 0 808.66 773.69 19.02 o
10 5 0 4781.30 4881.09 92.67 o
11 5 0 406.46 397.67 17.51 o
12 5 0 2260.60 2281.95 80.77 o
0 6 0 8.07 28.97 4.09 o
1 6 0 376.52 340.94 7.32 o
2 6 0 3977.07 4171.82 52.43 o
3 6 0 22.25 28.12 3.35 o
4 6 0 38.81 51.96 3.62 o
5 6 0 51.11 62.63 3.70 o
6 6 0 1516.68 1482.55 23.42 o
7 6 0 179.64 195.45 8.74 o
8 6 0 352.21 357.31 11.51 o
9 6 0 1.23 5.06 8.23 o
10 6 0 138.34 134.89 11.01 o
11 6 0 92.76 83.19 10.93 o
12 6 0 237.40 217.02 26.35 o
1 7 0 12634.26 13057.32 164.05 o
2 7 0 2715.88 2838.86 37.92 o
3 7 0 18124.00 18829.92 213.11 o
4 7 0 387.89 393.65 8.30 o
5 7 0 1753.18 1739.20 28.18 o
6 7 0 4234.74 4310.76 58.81 o
7 7 0 2436.20 2380.93 41.11 o
8 7 0 1970.08 2021.09 39.87 o
9 7 0 956.27 918.47 22.35 o
10 7 0 1361.77 1370.62 30.72 o
11 7 0 36.54 53.27 14.51 o
0 8 0 4859.60 4842.69 96.11 o
1 8 0 3.11 2.32 3.96 o
2 8 0 2391.96 2402.20 34.73 o
3 8 0 528.87 506.91 10.06 o
4 8 0 839.75 801.33 14.31 o
5 8 0 2283.63 2233.44 35.08 o
6 8 0 1634.32 1600.50 25.63 o
7 8 0 709.52 692.84 17.90 o
8 8 0 213.68 222.34 11.44 o
9 8 0 2935.29 3079.84 61.87 o
10 8 0 351.93 336.56 22.85 o
1 9 0 2303.47 2323.52 38.21 o
2 9 0 24.14 24.64 3.86 o
3 9 0 635.22 594.88 10.99 o
4 9 0 586.79 544.89 12.62 o
5 9 0 1525.39 1525.48 27.40 o
6 9 0 271.78 271.05 9.21 o
7 9 0 384.18 366.65 15.52 o
8 9 0 1263.55 1252.21 33.96 o
9 9 0 161.11 138.30 13.11 o
10 9 0 1176.50 1197.14 53.41 o
0 10 0 8851.70 8768.79 188.81 o
1 10 0 10.07 21.41 4.84 o
2 10 0 4400.18 4424.45 72.16 o
3 10 0 1328.36 1323.64 24.62 o
4 10 0 4771.31 4742.80 76.09 o
5 10 0 1298.03 1257.92 25.63 o
6 10 0 1508.30 1491.86 33.36 o
7 10 0 1687.76 1733.58 48.33 o
8 10 0 487.38 450.54 18.95 o
9 10 0 1452.87 1308.78 44.06 o
1 11 0 293.74 294.68 10.26 o
2 11 0 100.48 87.34 7.80 o
3 11 0 123.60 122.27 9.69 o
4 11 0 4.83 11.59 8.52 o
5 11 0 15.05 16.44 8.26 o
6 11 0 0.00 -0.87 12.28 o
7 11 0 0.13 6.56 13.78 o
8 11 0 4.75 1.83 36.74 o
0 12 0 635.11 663.98 35.30 o
1 12 0 256.44 248.97 11.17 o
2 12 0 4834.57 4886.69 85.96 o
3 12 0 14.72 26.54 11.62 o
4 12 0 2698.33 2641.31 57.42 o
5 12 0 693.86 607.84 20.37 o
6 12 0 683.12 742.29 30.60 o
1 13 0 1148.73 1154.06 25.14 o
2 13 0 27.08 27.80 10.76 o
3 13 0 31.03 21.66 15.77 o
4 13 0 804.39 749.57 34.93 o
-12 1 1 10.83 17.83 11.85 o
-11 1 1 4613.14 4530.55 114.49 o
-10 1 1 1714.73 1725.25 42.48 o
-9 1 1 8093.18 8132.21 139.71 o
-8 1 1 3279.59 3352.94 57.41 o
-7 1 1 8105.24 8340.30 111.11 o
-6 1 1 13184.61 13573.33 161.91 o
-5 1 1 3736.38 3624.16 56.11 o
-4 1 1 38587.31 36930.17 469.72 o
-3 1 1 2365.86 2340.49 33.81 o
-2 1 1 6327.91 6416.94 80.89 o
-1 1 1 98.27 110.99 2.03 o
0 1 1 14804.71 14868.01 160.09 o
1 1 1 46.71 47.02 1.17 o
2 1 1 24469.29 24685.24 265.06 o
3 1 1 12527.49 12698.38 129.10 o
4 1 1 7670.94 7743.54 102.53 o
5 1 1 16688.45 17627.24 213.71 o
6 1 1 4750.07 4769.69 67.16 o
7 1 1 9903.23 9889.20 137.39 o
8 1 1 1412.73 1456.72 28.69 o
9 1 1 6546.60 6702.39 106.14 o
10 1 1 236.74 246.74 9.64 o
11 1 1 5432.65 5639.06 102.69 o
12 1 1 43.48 24.03 12.97 o
13 1 1 1938.93 1965.63 94.19 o
-13 2 1 89.72 66.83 22.43 o
-12 2 1 1375.00 1358.49 43.96 o
-11 2 1 101.17 79.21 11.73 o
-10 2 1 2432.46 2501.71 57.54 o
-9 2 1 216.81 208.64 7.83 o
-8 2 1 257.01 239.87 6.64 o
-7 2 1 4483.79 4456.12 63.97 o
-6 2 1 3676.89 3561.00 48.80 o
-5 2 1 245.16 200.57 3.83 o
-4 2 1 15.49 23.09 1.96 o
-3 2 1 16046.38 15567.49 267.53 o
-2 2 1 735.69 769.62 14.32 o
-1 2 1 18967.78 19423.08 393.33 o
0 2 1 1721.09 1817.89 26.23 o
1 2 1 2521.31 2688.63 33.51 o
2 2 1 1545.79 1656.10 22.78 o
3 2 1 6958.11 7157.91 98.45 o
4 2 1 3089.43 3099.27 38.51 o
5 2 1 6719.18 7252.93 86.47 o
6 2 1 2357.52 2387.66 39.44 o
7 2 1 46.67 53.53 5.00 o
8 2 1 6601.35 6871.38 99.95 o
9 2 1 1094.59 1087.59 23.17 o
10 2 1 1153.27 1139.82 24.47 o
11 2 1 0.31 1.92 9.37 o
12 2 1 831.08 813.25 31.52 o
-13 3 1 720.22 673.45 44.80 o
-12 3 1 70.28 69.47 14.50 o
-11 3 1 3834.00 3785.97 98.74 o
-10 3 1 39.10 44.45 7.09 o
-9 3 1 890.70 869.46 22.05 o
-8 3 1 3856.97 3695.75 59.06 o
-7 3 1 1974.03 1877.28 33.46 o
-6 3 1 4388.20 4329.25 57.88 o
-5 3 1 6095.65 6239.51 75.56 o
-4 3 1 1390.40 1290.44 19.89 o
-3 3 1 714.84 787.93 13.24 o
-2 3 1 23771.42 22767.73 255.04 o
-1 3 1 21.62 30.69 1.52 o
0 3 1 2780.33 2855.65 35.62 o
1 3 1 3857.73 3977.78 49.66 o
2 3 1 9385.41 9360.51 143.27 o
3 3 1 7732.47 7914.38 107.85 o
4 3 1 13030.90 13563.60 149.36 o
5 3 1 2811.85 2962.37 37.26 o
6 3 1 952.78 973.54 15.27 o
7 3 1 4692.21 4819.60 68.88 o
8 3 1 219.83 231.09 7.46 o
9 3 1 5231.30 5169.09 93.79 o
10 3 1 679.16 649.68 21.16 o
11 3 1 758.95 720.76 23.53 o
12 3 1 454.44 467.56 23.96 o
-12 4 1 1996.97 2042.96 61.08 o
-11 4 1 992.80 997.01 35.38 o
-10 4 1 2781.89 2772.28 56.84 o
-9 4 1 3521.40 3575.87 69.79 o
-8 4 1 9157.11 9370.70 145.76 o
-7 4 1 1814.47 1845.60 29.90 o
-6 4 1 2803.89 2753.30 39.14 o
-5 4 1 18472.25 18710.16 202.68 o
-4 4 1 4096.19 4058.42 54.66 o
-3 4 1 10003.00 10025.99 126.73 o
-2 4 1 122.17 129.17 3.22 o
-1 4 1 9239.78 9615.31 128.61 o
0 4 1 3179.09 3293.99 49.18 o
1 4 1 30963.29 31594.54 339.23 o
2 4 1 1268.66 1178.48 17.22 o
3 4 1 7978.45 7727.96 102.65 o
4 4 1 3427.17 3306.83 42.56 o
5 4 1 2544.34 2492.47 35.22 o
6 4 1 8727.37 8619.74 101.08 o
7 4 1 3876.80 3829.07 60.60 o
8 4 1 5285.40 5388.67 82.25 o
9 4 1 94.42 110.63 8.62 o
10 4 1 8549.16 8527.57 167.03 o
11 4 1 31.83 31.36 16.30 o
12 4 1 2516.86 2517.52 88.85 o
-12 5 1 0.89 -16.24 16.24 o
-11 5 1 12.70 5.69 10.49 o
-10 5 1 660.59 636.64 18.80 o
-9 5 1 144.26 141.55 7.99 o
-8 5 1 86.23 80.16 9.25 o
-7 5 1 10.52 33.28 3.84 o
-6 5 1 42.73 50.71 3.33 o
-5 5 1 0.06 15.33 7.32 o
-4 5 1 2500.62 2665.39 37.73 o
-3 5 1 376.66 373.16 7.24 o
-2 5 1 127.10 122.28 3.79 o
-1 5 1 181.27 214.62 5.24 o
0 5 1 1266.17 1318.78 21.41 o
1 5 1 8.62 7.22 2.22 o
2 5 1 435.40 419.63 7.47 o
3 5 1 49.04 63.94 2.49 o
4 5 1 1260.05 1286.79 20.05 o
5 5 1 804.64 797.48 13.64 o
6 5 1 389.86 347.74 7.24 o
7 5 1 51.93 30.55 4.79 o
8 5 1 364.47 332.93 10.09 o
9 5 1 391.03 379.32 12.59 o
10 5 1 69.30 55.53 10.08 o
11 5 1 369.18 327.61 16.70 o
12 5 1 24.55 34.54 25.79 o
-12 6 1 3773.85 3809.57 106.19 o
-11 6 1 323.21 327.83 14.99 o
-10 6 1 5039.47 4961.95 94.90 o
-9 6 1 1258.11 1265.28 27.62 o
-8 6 1 5308.04 5352.68 89.78 o
-7 6 1 3644.20 3545.65 57.03 o
-6 6 1 3871.59 3798.18 52.27 o
-5 6 1 7692.62 7565.35 90.32 o
-4 6 1 1111.27 1050.83 19.68 o
-3 6 1 11724.42 11812.09 139.35 o
-2 6 1 6.56 28.03 5.18 o
-1 6 1 14224.59 14293.47 177.56 o
0 6 1 41.46 72.45 4.08 o
1 6 1 9290.57 9190.38 105.83 o
2 6 1 3076.76 3210.08 42.01 o
3 6 1 8360.32 8419.93 103.60 o
4 6 1 5745.61 5681.55 73.05 o
5 6 1 3489.84 3507.09 47.77 o
6 6 1 7375.55 7539.30 95.25 o
7 6 1 1179.95 1188.53 23.28 o
8 6 1 6362.96 6290.54 96.91 o
9 6 1 261.66 247.84 11.15 o
10 6 1 3500.30 3441.68 77.59 o
11 6 1 76.19 63.62 13.92 o
-11 7 1 410.18 394.53 17.07 o
-10 7 1 38.17 34.32 9.37 o
-9 7 1 442.58 444.94 14.23 o
-8 7 1 717.20 736.92 18.66 o
-7 7 1 196.58 203.48 7.80 o
-6 7 1 2330.55 2347.26 34.82 o
-5 7 1 1.46 5.37 3.36 o
-4 7 1 1844.04 1863.65 29.72 o
-3 7 1 0.18 10.17 4.06 o
-2 7 1 4537.38 4468.60 68.09 o
-1 7 1 261.46 275.19 6.82 o
0 7 1 786.78 827.60 20.15 o
1 7 1 125.99 129.73 3.98 o
2 7 1 777.33 782.77 13.56 o
3 7 1 381.54 363.70 7.81 o
4 7 1 2097.83 2134.14 31.32 o
5 7 1 2034.69 2027.08 30.18 o
6 7 1 1067.26 1026.22 21.41 o
7 7 1 1182.96 1155.37 23.27 o
8 7 1 5.96 -7.73 7.73 o
9 7 1 513.19 497.40 16.70 o
10 7 1 185.87 192.36 13.88 o
11 7 1 110.23 69.71 24.50 o
-11 8 1 40.74 4.36 15.70 o
-10 8 1 1726.65 1768.88 39.39 o
-9 8 1 574.87 581.84 17.30 o
-8 8 1 646.07 652.98 17.65 o
-7 8 1 4750.64 4883.60 76.27 o
-6 8 1 3151.03 3165.24 50.82 o
-5 8 1 1552.17 1509.86 24.21 o
-4 8 1 346.91 329.58 7.86 o
-3 8 1 5061.49 5087.57 71.10 o
-2 8 1 21.11 28.49 3.76 o
-1 8 1 5146.84 5068.62 76.23 o
0 8 1 12.21 16.02 5.48 o
1 8 1 2504.03 2594.43 38.84 o
2 8 1 1722.27 1704.22 26.00 o
3 8 1 5052.80 5075.78 66.98 o
4 8 1 2630.13 2635.40 39.63 o
5 8 1 2068.02 2009.52 33.86 o
6 8 1 1819.93 1794.82 33.87 o
7 8 1 18.57 16.22 7.76 o
8 8 1 3503.52 3698.71 79.49 o
9 8 1 245.15 226.48 14.35 o
10 8 1 1426.74 1441.93 39.27 o
-10 9 1 692.08 689.68 24.72 o
-9 9 1 2280.73 2357.52 50.21 o
-8 9 1 395.86 362.15 14.56 o
-7 9 1 1382.46 1378.19 27.05 o
-6 9 1 2678.04 2693.09 42.42 o
-5 9 1 208.00 208.55 6.94 o
-4 9 1 6143.98 6156.14 90.61 o
-3 9 1 892.98 853.24 16.29 o
-2 9 1 1522.32 1515.10 27.55 o
-1 9 1 714.31 696.27 15.90 o
0 9 1 6679.51 6502.02 93.94 o
1 9 1 1299.51 1306.38 25.62 o
2 9 1 6039.58 5907.99 79.65 o
3 9 1 768.73 766.08 15.70 o
4 9 1 1790.45 1819.85 31.12 o
5 9 1 3052.07 3006.57 51.20 o
6 9 1 2677.16 2667.38 51.24 o
7 9 1 2110.67 2185.06 46.13 o
8 9 1 531.25 553.34 20.73 o
9 9 1 1217.65 1183.26 33.98 o
-9 10 1 56.01 42.70 18.72 o
-8 10 1 380.39 335.53 18.80 o
-7 10 1 148.20 155.95 10.72 o
-6 10 1 102.66 109.61 9.44 o
-5 10 1 1141.83 1108.16 23.51 o
-4 10 1 67.07 72.08 6.57 o
-3 10 1 362.10 361.21 9.46 o
-2 10 1 84.39 71.97 5.32 o
-1 10 1 3.88 15.09 5.37 o
0 10 1 416.79 404.43 11.39 o
1 10 1 1922.27 1904.21 35.44 o
2 10 1 64.52 61.22 6.50 o
3 10 1 23.68 25.46 6.78 o
4 10 1 1264.10 1249.01 25.46 o
5 10 1 43.57 37.58 6.73 o
6 10 1 787.26 804.65 21.45 o
7 10 1 1033.43 1070.49 30.89 o
8 10 1 3.87 11.14 13.58 o
-8 11 1 1503.43 1418.75 72.46 o
-7 11 1 1388.41 1423.48 36.72 o
-6 11 1 2125.92 2168.86 49.78 o
-5 11 1 1314.26 1278.14 29.20 o
-4 11 1 2209.16 2203.98 40.87 o
-3 11 1 166.68 147.56 9.08 o
-2 11 1 7102.42 6941.42 107.10 o
-1 11 1 90.41 84.00 6.51 o
0 11 1 3583.25 3536.13 55.62 o
1 11 1 225.63 211.45 9.26 o
2 11 1 1069.61 1057.42 24.53 o
3 11 1 1379.21 1354.24 33.22 o
4 11 1 2442.45 2392.73 46.88 o
5 11 1 872.34 836.03 21.10 o
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-6 12 1 1.38 -16.70 16.70 o
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-3 12 1 313.46 310.22 14.36 o
-2 12 1 0.25 6.23 7.41 o
-1 12 1 114.37 104.64 8.20 o
0 12 1 233.50 228.67 10.25 o
1 12 1 843.87 790.20 19.12 o
2 12 1 49.77 51.60 7.53 o
3 12 1 166.36 145.65 11.46 o
4 12 1 121.86 123.67 11.72 o
5 12 1 346.08 296.51 15.28 o
6 12 1 223.22 219.76 37.48 o
-4 13 1 493.69 476.66 27.76 o
-3 13 1 54.67 28.08 13.24 o
-2 13 1 1968.79 1948.02 40.50 o
-1 13 1 44.52 38.18 10.86 o
0 13 1 1664.20 1640.51 32.58 o
1 13 1 509.55 493.77 16.72 o
2 13 1 1177.88 1122.12 35.22 o
3 13 1 373.92 338.85 47.39 o
4 13 1 789.27 722.64 33.74 o
-12 0 2 185.40 188.85 28.22 o
-11 0 2 2668.80 2792.34 90.46 o
-10 0 2 3735.19 3736.24 115.37 o
-9 0 2 2495.29 2459.49 79.91 o
-8 0 2 9268.78 9040.47 399.58 o
-7 0 2 4845.50 4733.39 117.19 o
-6 0 2 5599.53 5112.41 101.15 o
-5 0 2 689.68 666.10 15.45 o
-4 0 2 28429.58 26442.04 709.57 o
-3 0 2 19.75 24.24 1.98 o
-2 0 2 37690.18 33479.91 596.07 o
-1 0 2 2754.35 2796.27 46.07 o
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1 0 2 29534.91 28541.32 893.46 o
2 0 2 44099.54 42946.75 916.53 o
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5 0 2 18462.22 19756.69 335.53 o
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