#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/69/2216988.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2216988_Fobs loop_ _publ_author_name 'Xiao, Xin' 'Jiang, Ping-Yue' 'Zhang, Yun-Qian' 'Xue, Sai-Feng' 'Zhu, Qian-Jiang' _publ_section_title ; Octane-1,8-diyldipyridinium dibromide dihydrate ; _journal_coeditor_code CI2531 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o183 _journal_volume 64 _journal_year 2008 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.8329 _cell_length_b 13.3000 _cell_length_c 16.5688 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7678 _[local]_cod_data_source_file ci2531Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CI2531 P b c a R = 0.03' _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3467.29 3826.93 63.13 o 4 0 0 3019.27 2888.14 44.73 o 6 0 0 2195.78 2128.97 36.43 o 8 0 0 1131.94 1082.62 29.89 o 10 0 0 1440.49 1430.07 76.52 o 12 0 0 1175.82 990.26 65.56 o 2 1 0 727.05 859.92 11.42 o 4 1 0 13755.93 14125.61 134.40 o 6 1 0 18122.54 17455.07 180.24 o 8 1 0 3208.02 2949.43 45.91 o 10 1 0 690.29 691.28 23.25 o 12 1 0 5.20 25.58 22.16 o 0 2 0 4016.23 4143.31 74.78 o 2 2 0 4800.88 4939.18 60.09 o 4 2 0 1112.27 1120.29 13.32 o 6 2 0 269.08 296.86 6.29 o 8 2 0 424.12 409.84 15.24 o 10 2 0 83.88 95.41 16.12 o 12 2 0 107.96 106.51 19.33 o 2 3 0 32774.43 31730.15 340.94 o 4 3 0 14961.01 15700.50 161.49 o 6 3 0 1329.19 1144.75 15.91 o 8 3 0 149.16 179.00 11.32 o 10 3 0 28.61 25.28 16.06 o 12 3 0 10.95 20.86 19.21 o 0 4 0 61480.92 56445.18 800.23 o 2 4 0 16814.80 16600.12 173.51 o 4 4 0 352.83 308.46 5.44 o 6 4 0 442.18 461.27 10.00 o 8 4 0 122.53 129.12 13.25 o 10 4 0 869.20 857.35 28.55 o 12 4 0 473.63 474.58 24.10 o 2 5 0 991.64 959.23 11.38 o 4 5 0 22829.43 22511.66 245.46 o 6 5 0 9650.55 9501.68 132.32 o 8 5 0 4349.20 4027.88 86.65 o 10 5 0 567.47 601.60 28.76 o 12 5 0 26.03 36.03 20.84 o 0 6 0 8446.46 8342.62 115.43 o 2 6 0 14989.14 14808.41 144.80 o 4 6 0 8225.52 8104.38 95.22 o 6 6 0 2.20 7.09 11.64 o 8 6 0 1067.89 955.70 31.45 o 10 6 0 173.23 186.49 20.61 o 12 6 0 543.18 598.91 72.20 o 2 7 0 3814.37 3920.61 46.54 o 4 7 0 649.75 643.32 11.78 o 6 7 0 743.66 737.37 22.72 o 8 7 0 219.67 212.42 21.37 o 10 7 0 456.03 468.20 38.70 o 0 8 0 2904.77 2962.60 52.14 o 2 8 0 179.01 194.42 7.69 o 4 8 0 100.21 87.70 9.83 o 6 8 0 160.99 154.22 15.13 o 8 8 0 0.85 11.30 19.71 o 10 8 0 24.70 6.28 19.56 o 2 9 0 916.74 834.69 23.59 o 4 9 0 3574.01 3465.98 64.67 o 6 9 0 1348.71 1409.92 38.59 o 8 9 0 968.48 924.82 68.67 o 10 9 0 257.52 271.00 24.75 o 0 10 0 5764.70 5558.64 143.29 o 2 10 0 5922.39 5801.57 158.21 o 4 10 0 1485.31 1527.54 40.74 o 6 10 0 283.99 351.76 18.05 o 8 10 0 692.70 630.94 31.29 o 10 10 0 213.02 249.36 24.28 o 2 11 0 1150.23 1032.84 48.40 o 4 11 0 2779.59 2655.40 56.73 o 6 11 0 417.96 503.38 31.28 o 8 11 0 1350.83 1350.91 52.07 o 0 12 0 446.83 416.97 22.70 o 2 12 0 667.80 688.75 25.72 o 4 12 0 328.54 339.26 18.67 o 6 12 0 32.70 28.65 17.11 o 8 12 0 2.13 8.90 20.72 o 2 13 0 3.40 33.34 17.23 o 4 13 0 167.31 175.20 39.31 o 6 13 0 12.69 18.62 18.37 o 8 13 0 8.29 14.64 22.55 o 0 14 0 1031.55 983.42 56.90 o 2 14 0 176.67 190.34 18.57 o 4 14 0 455.27 451.88 37.39 o 6 14 0 1.06 17.55 19.49 o 2 15 0 303.17 208.89 20.22 o 4 15 0 303.35 337.24 24.24 o 6 15 0 364.67 423.72 29.58 o 0 16 0 450.12 483.02 45.18 o 2 16 0 333.73 328.55 37.77 o 4 16 0 117.41 155.51 22.69 o 2 17 0 7.00 -7.60 24.04 o 1 1 1 395.69 431.46 4.31 o 2 1 1 10876.92 11344.03 97.89 o 3 1 1 5959.90 6270.83 47.77 o 4 1 1 2778.41 2613.72 19.33 o 5 1 1 266.02 224.34 3.14 o 6 1 1 4852.20 5011.53 38.41 o 7 1 1 859.32 839.97 11.73 o 8 1 1 2305.31 2139.32 23.96 o 9 1 1 269.42 266.91 8.50 o 10 1 1 160.35 194.14 11.22 o 11 1 1 42.99 36.77 11.19 o 12 1 1 8.53 11.65 13.67 o 0 2 1 2727.59 3194.17 36.43 o 1 2 1 3793.53 4066.29 35.48 o 2 2 1 69125.03 61279.98 550.98 o 3 2 1 11231.15 11486.04 85.89 o 4 2 1 4892.65 4584.48 33.37 o 5 2 1 1030.79 1064.76 9.11 o 6 2 1 31.40 71.77 3.17 o 7 2 1 226.71 259.74 6.84 o 8 2 1 368.93 358.15 9.62 o 9 2 1 326.98 317.29 11.20 o 10 2 1 881.61 824.32 23.77 o 11 2 1 202.62 233.13 15.80 o 12 2 1 511.51 563.79 30.37 o 1 3 1 29301.70 29292.52 254.11 o 2 3 1 10274.11 10267.06 76.35 o 3 3 1 100.30 111.56 2.00 o 4 3 1 10396.63 10316.99 73.55 o 5 3 1 3235.82 3219.41 24.78 o 6 3 1 10288.23 10000.86 77.34 o 7 3 1 2949.13 2787.84 31.99 o 8 3 1 4203.33 4056.65 48.18 o 9 3 1 239.67 256.48 10.16 o 10 3 1 684.73 655.91 18.38 o 11 3 1 162.54 154.34 16.57 o 12 3 1 23.15 42.58 13.08 o 0 4 1 15542.46 15881.49 156.54 o 1 4 1 7548.67 7726.11 58.16 o 2 4 1 8849.76 8793.30 66.49 o 3 4 1 201.89 178.89 2.77 o 4 4 1 2960.96 2991.59 23.58 o 5 4 1 320.08 312.48 4.22 o 6 4 1 0.56 7.52 3.73 o 7 4 1 37.06 34.62 5.72 o 8 4 1 83.79 64.54 8.24 o 9 4 1 9.77 10.07 9.72 o 10 4 1 756.96 712.14 17.80 o 11 4 1 262.35 279.49 13.92 o 12 4 1 79.13 74.26 13.38 o 1 5 1 269.32 286.72 3.44 o 2 5 1 639.77 732.25 6.63 o 3 5 1 262.54 263.27 3.77 o 4 5 1 1824.65 1995.71 16.84 o 5 5 1 335.71 347.97 5.43 o 6 5 1 50.57 60.23 5.40 o 7 5 1 49.20 55.03 7.42 o 8 5 1 20.98 20.13 8.69 o 9 5 1 0.08 -10.49 10.49 o 10 5 1 11.97 3.77 11.67 o 11 5 1 1.68 32.73 13.73 o 12 5 1 20.62 33.20 15.19 o 0 6 1 7138.98 7244.60 70.80 o 1 6 1 26.65 18.10 1.78 o 2 6 1 3172.63 3144.66 23.97 o 3 6 1 6208.23 6465.10 52.77 o 4 6 1 2254.87 2149.15 18.27 o 5 6 1 249.01 270.56 5.43 o 6 6 1 40.52 44.14 6.15 o 7 6 1 1.71 -8.22 8.22 o 8 6 1 162.79 157.36 11.09 o 9 6 1 9.43 -11.86 11.86 o 10 6 1 115.39 115.71 15.43 o 11 6 1 91.47 84.99 14.80 o 12 6 1 78.80 34.49 45.90 o 1 7 1 50.41 42.97 2.48 o 2 7 1 4796.59 4934.12 41.26 o 3 7 1 1343.75 1348.89 12.71 o 4 7 1 3030.64 2871.60 28.02 o 5 7 1 1373.68 1377.92 18.58 o 6 7 1 5149.76 5228.47 77.75 o 7 7 1 1196.51 1164.53 22.38 o 8 7 1 1710.46 1714.67 49.16 o 9 7 1 139.26 124.23 13.99 o 10 7 1 323.37 330.20 16.38 o 11 7 1 12.45 9.06 14.52 o 0 8 1 13480.90 13467.50 163.10 o 1 8 1 3516.90 3463.10 33.10 o 2 8 1 6406.07 6088.51 53.49 o 3 8 1 1641.50 1674.58 17.80 o 4 8 1 2542.78 2602.20 31.22 o 5 8 1 6.13 4.85 6.67 o 6 8 1 2.61 7.85 9.14 o 7 8 1 84.89 81.93 10.29 o 8 8 1 52.77 20.89 12.21 o 9 8 1 246.01 239.28 16.96 o 10 8 1 681.77 664.49 27.41 o 11 8 1 76.33 73.37 16.06 o 1 9 1 168.26 201.87 7.03 o 2 9 1 1063.08 1011.60 22.71 o 3 9 1 345.78 343.92 11.39 o 4 9 1 948.71 954.63 16.99 o 5 9 1 1543.58 1492.33 23.91 o 6 9 1 2682.52 2693.94 43.47 o 7 9 1 95.55 106.21 12.61 o 8 9 1 297.30 299.06 15.96 o 9 9 1 97.12 78.00 15.28 o 10 9 1 76.32 75.94 15.45 o 0 10 1 514.27 563.65 17.25 o 1 10 1 109.32 108.71 10.41 o 2 10 1 6.56 2.62 6.51 o 3 10 1 2.03 -4.02 6.53 o 4 10 1 12.18 29.02 7.56 o 5 10 1 147.44 120.07 9.19 o 6 10 1 89.98 97.59 10.20 o 7 10 1 95.87 67.09 13.88 o 8 10 1 17.91 10.79 13.48 o 9 10 1 4.55 -14.69 14.69 o 10 10 1 0.13 -3.20 15.01 o 1 11 1 51.91 71.44 8.77 o 2 11 1 261.64 285.69 10.96 o 3 11 1 2.51 2.76 8.19 o 4 11 1 219.19 227.23 11.34 o 5 11 1 231.78 239.66 11.14 o 6 11 1 473.44 485.23 16.12 o 7 11 1 33.57 16.17 12.90 o 8 11 1 151.08 159.69 16.23 o 9 11 1 7.81 -1.85 16.58 o 0 12 1 1468.37 1482.63 34.73 o 1 12 1 838.62 825.29 19.49 o 2 12 1 2248.95 2302.94 38.92 o 3 12 1 47.75 49.82 9.88 o 4 12 1 285.80 306.79 12.93 o 5 12 1 70.55 63.11 11.25 o 6 12 1 0.20 -0.52 11.94 o 7 12 1 0.06 13.00 13.41 o 8 12 1 4.55 1.55 14.87 o 9 12 1 20.72 36.85 16.76 o 1 13 1 1.84 -7.96 9.74 o 2 13 1 243.53 229.33 14.61 o 3 13 1 324.66 314.75 14.15 o 4 13 1 738.29 694.06 19.55 o 5 13 1 118.50 108.97 12.63 o 6 13 1 1004.47 1055.08 24.93 o 7 13 1 216.16 231.10 17.80 o 8 13 1 188.42 233.82 17.83 o 0 14 1 565.28 508.15 41.43 o 1 14 1 141.13 120.62 14.76 o 2 14 1 519.33 507.24 20.92 o 3 14 1 189.72 219.54 17.24 o 4 14 1 57.32 64.71 13.02 o 5 14 1 0.37 -11.01 13.37 o 6 14 1 22.05 5.31 14.35 o 7 14 1 0.85 -7.81 15.19 o 1 15 1 11.78 12.76 11.30 o 2 15 1 0.47 -6.58 11.86 o 3 15 1 21.69 -6.61 12.53 o 4 15 1 36.37 13.41 13.64 o 5 15 1 0.33 -7.66 14.38 o 6 15 1 2.37 -5.15 15.58 o 0 16 1 20.33 26.02 23.10 o 1 16 1 4.32 7.60 12.13 o 2 16 1 149.80 133.06 14.20 o 3 16 1 28.22 20.91 14.14 o 4 16 1 2.41 -7.28 14.30 o 1 17 1 8.95 -0.92 17.30 o 2 17 1 37.72 33.15 14.02 o 0 0 2 22488.61 19051.45 497.00 o 1 0 2 24387.47 23710.85 290.70 o 2 0 2 21688.16 21493.63 270.28 o 3 0 2 29912.56 29414.00 324.69 o 4 0 2 1311.03 1206.37 14.81 o 5 0 2 3279.62 3022.02 34.25 o 6 0 2 35.20 24.12 4.09 o 7 0 2 344.48 303.07 9.98 o 8 0 2 12.15 25.56 7.65 o 9 0 2 1256.80 1250.54 47.58 o 10 0 2 669.93 637.09 28.33 o 11 0 2 807.17 873.05 39.46 o 12 0 2 280.83 307.28 30.36 o 1 1 2 1074.60 1035.87 10.31 o 2 1 2 42.84 53.64 1.58 o 3 1 2 15811.31 16225.65 127.22 o 4 1 2 5730.31 6090.15 46.92 o 5 1 2 12003.00 12414.50 91.11 o 6 1 2 3919.96 3869.31 36.16 o 7 1 2 2346.71 2196.27 27.07 o 8 1 2 1177.24 1111.48 17.12 o 9 1 2 2054.36 1882.07 33.99 o 10 1 2 121.28 105.83 12.09 o 11 1 2 97.64 93.05 13.44 o 12 1 2 13.81 21.82 14.60 o 0 2 2 3636.00 3838.79 43.15 o 1 2 2 1912.71 2012.84 19.18 o 2 2 2 293.94 285.06 3.37 o 3 2 2 5065.16 5229.50 41.70 o 4 2 2 489.90 549.27 5.31 o 5 2 2 2.09 1.99 1.83 o 6 2 2 31.63 19.68 3.03 o 7 2 2 3.59 -0.11 4.77 o 8 2 2 131.08 125.98 6.36 o 9 2 2 218.71 218.08 8.49 o 10 2 2 2.24 7.63 9.71 o 11 2 2 17.83 7.78 10.92 o 12 2 2 63.74 64.64 14.74 o 1 3 2 11978.01 12122.80 99.71 o 2 3 2 3.76 3.72 1.08 o 3 3 2 69.27 78.62 1.92 o 4 3 2 147.06 171.81 2.95 o 5 3 2 692.16 731.80 6.80 o 6 3 2 640.48 605.73 7.38 o 7 3 2 226.62 220.25 6.38 o 8 3 2 315.79 321.34 9.61 o 9 3 2 174.72 158.49 9.94 o 10 3 2 23.80 26.48 10.49 o 11 3 2 4.81 -1.23 11.25 o 12 3 2 18.91 28.46 12.58 o 0 4 2 25720.15 25628.83 239.98 o 1 4 2 21484.69 21157.68 151.65 o 2 4 2 2793.44 2828.76 22.10 o 3 4 2 1292.36 1167.02 10.16 o 4 4 2 571.40 534.16 5.73 o 5 4 2 3591.06 3814.19 29.66 o 6 4 2 28.87 31.67 3.99 o 7 4 2 65.27 63.19 5.97 o 8 4 2 29.84 17.78 7.78 o 9 4 2 1054.17 997.99 20.72 o 10 4 2 284.07 276.60 13.43 o 11 4 2 201.70 236.41 20.59 o 12 4 2 179.75 233.47 18.57 o 1 5 2 130.21 116.55 2.43 o 2 5 2 712.24 664.91 6.20 o 3 5 2 13929.67 13770.94 101.01 o 4 5 2 5437.54 5529.90 42.52 o 5 5 2 7555.84 7517.87 60.72 o 6 5 2 3190.13 3077.01 35.12 o 7 5 2 3659.69 3440.00 43.55 o 8 5 2 1067.45 1001.21 19.81 o 9 5 2 1960.13 1931.84 33.31 o 10 5 2 252.06 261.82 14.37 o 11 5 2 89.94 134.92 18.42 o 12 5 2 0.23 -1.18 14.71 o 0 6 2 2852.11 2799.80 28.44 o 1 6 2 16011.84 15873.93 110.82 o 2 6 2 6162.59 6323.38 46.25 o 3 6 2 2280.53 2231.11 18.59 o 4 6 2 133.99 147.60 3.71 o 5 6 2 2178.64 2174.76 22.59 o 6 6 2 495.07 500.04 10.33 o 7 6 2 258.05 247.10 10.84 o 8 6 2 421.69 425.84 13.89 o 9 6 2 381.58 360.61 15.90 o 10 6 2 129.36 112.52 14.59 o 11 6 2 318.27 378.01 24.80 o 1 7 2 922.59 1017.91 8.84 o 2 7 2 192.74 226.23 4.21 o 3 7 2 696.14 614.89 7.61 o 4 7 2 851.88 819.07 10.86 o 5 7 2 289.63 309.59 7.51 o 6 7 2 8.03 4.49 7.26 o 7 7 2 1323.53 1320.77 24.35 o 8 7 2 338.84 334.51 17.40 o 9 7 2 138.64 164.46 14.26 o 10 7 2 13.42 7.99 16.19 o 11 7 2 2.33 -6.34 14.59 o 0 8 2 655.08 661.27 15.24 o 1 8 2 322.68 350.84 5.87 o 2 8 2 264.09 279.92 5.54 o 3 8 2 18.68 30.67 4.38 o 4 8 2 41.59 35.83 5.71 o 5 8 2 652.29 644.42 18.72 o 6 8 2 98.59 76.66 9.22 o 7 8 2 163.48 112.06 10.54 o 8 8 2 7.05 -3.06 11.93 o 9 8 2 1.96 -13.04 13.04 o 10 8 2 10.16 10.82 15.01 o 11 8 2 1.07 21.96 15.56 o 1 9 2 29.23 24.23 5.57 o 2 9 2 190.07 176.55 7.02 o 3 9 2 1783.52 1721.22 24.42 o 4 9 2 1275.26 1199.66 19.53 o 5 9 2 1464.00 1456.43 24.85 o 6 9 2 670.54 659.19 16.27 o 7 9 2 747.74 769.64 23.47 o 8 9 2 252.67 275.43 15.55 o 9 9 2 297.61 311.93 24.31 o 10 9 2 49.00 48.67 15.85 o 0 10 2 3159.40 3181.96 60.47 o 1 10 2 4290.79 4162.63 59.81 o 2 10 2 998.01 967.36 19.36 o 3 10 2 2792.50 2806.81 41.15 o 4 10 2 708.78 738.88 15.36 o 5 10 2 378.07 413.75 12.16 o 6 10 2 13.21 27.91 9.59 o 7 10 2 197.54 143.78 13.87 o 8 10 2 124.50 77.32 14.25 o 9 10 2 82.83 75.06 18.01 o 10 10 2 50.60 32.35 16.54 o 1 11 2 343.84 366.34 12.26 o 2 11 2 279.06 267.42 10.86 o 3 11 2 790.14 714.63 16.58 o 4 11 2 600.48 586.81 16.79 o 5 11 2 1503.57 1426.49 24.19 o 6 11 2 258.93 277.70 13.85 o 7 11 2 741.22 833.87 21.54 o 8 11 2 176.51 183.64 16.54 o 9 11 2 237.96 271.60 17.66 o 0 12 2 112.68 94.56 11.28 o 1 12 2 681.81 658.83 17.31 o 2 12 2 81.24 87.05 10.16 o 3 12 2 178.76 206.85 13.37 o 4 12 2 100.63 118.69 10.96 o 5 12 2 53.83 70.27 11.38 o 6 12 2 1.24 -11.83 11.83 o 7 12 2 5.41 -13.28 13.28 o 8 12 2 12.55 -14.74 14.74 o 9 12 2 14.46 -5.57 16.40 o 1 13 2 1.46 4.06 9.76 o 2 13 2 9.53 5.57 10.24 o 3 13 2 88.15 100.10 11.72 o 4 13 2 1.79 2.32 11.46 o 5 13 2 43.22 30.13 11.85 o 6 13 2 76.10 73.58 13.48 o 7 13 2 9.71 8.34 14.35 o 8 13 2 2.10 -15.68 15.68 o 0 14 2 555.96 543.34 23.22 o 1 14 2 346.80 366.91 14.59 o 2 14 2 44.76 54.15 11.66 o 3 14 2 178.09 182.81 13.63 o 4 14 2 124.80 125.58 13.82 o 5 14 2 41.71 50.35 13.94 o 6 14 2 2.74 9.79 14.47 o 7 14 2 2.14 -4.44 15.31 o 1 15 2 10.06 1.99 11.19 o 2 15 2 43.25 29.90 12.35 o 3 15 2 184.10 192.32 14.69 o 4 15 2 217.87 220.19 15.82 o 5 15 2 398.19 382.51 18.62 o 6 15 2 35.54 10.27 15.98 o 0 16 2 198.79 223.87 26.68 o 1 16 2 409.79 404.58 16.71 o 2 16 2 29.76 32.30 13.16 o 3 16 2 72.61 69.50 14.46 o 4 16 2 73.70 76.55 15.30 o 1 17 2 1.07 -16.50 17.11 o 2 17 2 18.55 -11.08 16.09 o 1 1 3 3323.15 3537.45 35.46 o 2 1 3 19.15 19.04 1.64 o 3 1 3 12532.09 13069.92 101.28 o 4 1 3 269.89 304.89 4.28 o 5 1 3 3364.87 3370.02 29.79 o 6 1 3 50.76 64.73 3.69 o 7 1 3 3252.34 3102.59 35.94 o 8 1 3 27.05 24.21 6.39 o 9 1 3 702.67 705.14 15.09 o 10 1 3 165.02 192.70 10.02 o 11 1 3 312.32 388.98 23.75 o 12 1 3 22.80 51.15 14.97 o 0 2 3 2343.15 2415.86 33.17 o 1 2 3 27717.59 26682.11 249.12 o 2 2 3 102.72 129.17 2.43 o 3 2 3 28717.39 28274.01 208.38 o 4 2 3 158.68 166.37 2.81 o 5 2 3 3137.75 3154.12 26.43 o 6 2 3 216.67 208.85 4.58 o 7 2 3 384.55 395.10 9.14 o 8 2 3 217.45 211.97 8.39 o 9 2 3 1322.78 1330.34 26.77 o 10 2 3 1.20 0.16 9.00 o 11 2 3 1082.13 1081.12 42.42 o 12 2 3 0.15 2.83 13.46 o 1 3 3 3608.37 3810.57 32.05 o 2 3 3 1151.02 1173.68 10.54 o 3 3 3 16482.05 16657.53 123.36 o 4 3 3 25.71 20.60 1.85 o 5 3 3 12159.80 11559.63 84.30 o 6 3 3 1.30 -1.20 3.51 o 7 3 3 8859.07 8578.01 93.53 o 8 3 3 149.16 165.97 7.73 o 9 3 3 1813.26 1738.35 33.55 o 10 3 3 1.69 18.81 10.92 o 11 3 3 292.79 308.16 14.04 o 12 3 3 5.08 2.21 13.53 o 0 4 3 474.11 489.15 6.34 o 1 4 3 15672.78 15548.92 109.83 o 2 4 3 96.44 99.65 2.30 o 3 4 3 8339.25 8428.62 64.19 o 4 4 3 253.02 237.93 3.54 o 5 4 3 13.17 12.67 2.64 o 6 4 3 135.07 125.89 4.91 o 7 4 3 13.80 16.94 6.11 o 8 4 3 41.54 59.01 8.01 o 9 4 3 432.97 439.45 13.71 o 10 4 3 11.80 -3.90 10.75 o 11 4 3 435.05 410.85 20.90 o 12 4 3 1.81 -10.54 13.19 o 1 5 3 242.22 289.56 3.52 o 2 5 3 201.21 231.95 3.32 o 3 5 3 1474.32 1576.33 12.98 o 4 5 3 853.79 880.53 8.82 o 5 5 3 1109.27 1143.11 11.66 o 6 5 3 78.80 83.36 5.99 o 7 5 3 47.63 49.87 7.22 o 8 5 3 14.52 2.83 8.61 o 9 5 3 2.25 0.60 10.71 o 10 5 3 3.43 8.53 11.91 o 11 5 3 0.09 3.11 13.19 o 12 5 3 0.83 20.47 14.86 o 0 6 3 307.93 361.60 5.73 o 1 6 3 3168.59 3149.94 22.77 o 2 6 3 717.95 731.86 6.64 o 3 6 3 6155.60 6294.18 49.93 o 4 6 3 230.53 217.21 4.34 o 5 6 3 64.41 60.33 4.53 o 6 6 3 80.49 68.41 6.87 o 7 6 3 2.20 3.40 8.41 o 8 6 3 1.90 -1.57 10.85 o 9 6 3 375.49 350.40 15.93 o 10 6 3 4.31 -7.90 13.45 o 11 6 3 156.83 166.81 16.83 o 1 7 3 2570.42 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