#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/70/2217015.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217015_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Svoboda, Ingrid' 'Foro, Sabine' 'Paulus, Helmut' 'Fuess, Hartmut' _publ_section_title ; 2,2-Dichloro-N-(2,3-dimethylphenyl)acetamide ; _journal_coeditor_code DN2288 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o234 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _exptl_crystal_F_000 960.00 _[local]_cod_data_source_file dn2288Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' g31' _shelx_refln_list_code 4 _shelx_f_calc_maximum 276.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1390.48 1361.19 8.84 o 4 0 0 14831.19 14418.95 91.03 o 6 0 0 11875.03 11773.54 97.47 o 8 0 0 29502.32 29484.58 571.26 o 10 0 0 1359.47 1510.32 19.37 o 12 0 0 316.34 356.91 14.04 o 14 0 0 54.85 47.42 3.29 o 16 0 0 948.82 930.56 19.06 o 18 0 0 802.88 751.21 19.04 o 20 0 0 30.39 31.64 4.15 o 22 0 0 228.44 229.87 7.83 o 24 0 0 400.38 412.54 19.61 o 1 1 0 1270.50 1312.73 19.11 o 3 1 0 2064.04 1935.69 30.39 o 5 1 0 10873.98 11070.34 89.38 o 7 1 0 10.82 10.26 3.39 o 9 1 0 20554.17 21348.31 331.87 o 11 1 0 850.09 711.14 12.33 o 13 1 0 1111.14 1059.42 17.42 o 15 1 0 176.44 185.41 15.33 o 17 1 0 1341.55 1335.63 101.08 o 19 1 0 170.64 135.81 10.90 o 21 1 0 3.11 13.16 5.12 o 23 1 0 123.53 104.46 5.14 o 25 1 0 89.36 89.23 9.01 o 0 2 0 860.59 1172.71 20.32 o 2 2 0 29.39 36.95 2.40 o 4 2 0 715.39 759.67 27.19 o 6 2 0 1654.77 1775.05 26.97 o 8 2 0 212.90 258.46 9.08 o 10 2 0 846.53 782.22 16.54 o 12 2 0 798.80 792.62 14.65 o 14 2 0 87.56 88.33 4.65 o 16 2 0 58.33 54.12 9.64 o 18 2 0 146.02 121.11 9.79 o 20 2 0 956.39 950.14 48.36 o 22 2 0 6.28 -3.69 11.27 o 1 3 0 45.88 67.44 5.84 o 3 3 0 549.09 679.32 24.79 o 5 3 0 595.10 598.49 13.03 o 7 3 0 1689.57 1753.29 91.33 o 9 3 0 3023.51 2986.99 34.85 o 11 3 0 115.85 139.27 11.01 o 13 3 0 177.55 190.58 6.49 o 15 3 0 50.97 58.25 4.27 o 17 3 0 424.32 420.91 14.05 o 19 3 0 9.84 16.28 5.79 o 21 3 0 2.76 9.37 5.69 o 0 4 0 147.74 137.34 7.24 o 2 4 0 230.86 231.67 9.16 o 4 4 0 36.65 44.58 2.81 o 6 4 0 524.06 515.46 13.82 o 8 4 0 789.31 800.97 17.37 o 10 4 0 1029.79 936.08 21.57 o 12 4 0 798.57 886.14 21.62 o 14 4 0 181.58 166.97 7.13 o 16 4 0 6.21 5.15 5.45 o 1 5 0 511.54 488.91 19.65 o 3 5 0 101.72 85.13 4.18 o 5 5 0 22.22 32.36 3.77 o 7 5 0 190.00 189.97 7.42 o 9 5 0 22.92 10.91 5.77 o 11 5 0 123.44 135.35 6.03 o -25 1 1 1.47 12.40 6.49 o -23 1 1 8.26 7.30 16.73 o -21 1 1 184.33 168.72 10.27 o -19 1 1 18.65 16.10 5.37 o -17 1 1 2.93 -4.16 5.98 o -15 1 1 0.14 4.51 4.88 o -13 1 1 1290.66 1393.15 23.13 o -11 1 1 269.05 371.43 10.16 o -9 1 1 2006.55 2120.22 27.35 o -7 1 1 1568.49 1424.30 14.89 o -5 1 1 20788.81 22465.84 330.90 o -3 1 1 2602.77 2608.52 20.71 o -1 1 1 10508.95 10777.46 118.53 o 1 1 1 36491.56 36175.69 109.06 o 3 1 1 12499.81 13467.25 78.52 o 5 1 1 2658.23 2782.42 27.10 o 7 1 1 4099.47 3820.52 25.02 o 9 1 1 1289.65 1484.53 40.94 o 11 1 1 1260.67 1329.16 34.10 o 13 1 1 6.52 8.11 4.65 o 15 1 1 26.08 24.30 3.08 o 17 1 1 3204.47 2949.41 90.13 o 19 1 1 82.65 63.93 7.57 o 21 1 1 7.78 6.17 9.94 o 23 1 1 74.52 85.96 14.89 o 25 1 1 80.16 88.48 8.75 o -22 2 1 39.92 33.62 3.50 o -20 2 1 573.30 589.95 35.43 o -18 2 1 246.50 256.18 7.67 o -16 2 1 546.71 549.44 32.43 o -14 2 1 499.35 495.52 12.17 o -12 2 1 285.29 306.21 9.56 o -10 2 1 894.00 881.50 17.43 o -8 2 1 3411.26 3621.19 29.35 o -6 2 1 21.00 16.05 2.58 o -4 2 1 115.45 143.70 3.84 o -2 2 1 60.16 82.65 3.25 o 0 2 1 4196.66 4133.58 24.55 o 2 2 1 6.35 2.11 2.40 o 4 2 1 7851.26 8228.15 38.59 o 6 2 1 2900.75 2749.41 23.42 o 8 2 1 10684.06 11169.90 205.01 o 10 2 1 401.93 518.58 11.21 o 12 2 1 4360.71 4352.42 58.18 o 14 2 1 2408.53 2544.64 36.58 o 16 2 1 436.01 456.05 13.13 o 18 2 1 45.89 65.75 4.22 o 20 2 1 41.58 59.05 10.56 o 22 2 1 53.77 55.67 5.91 o -21 3 1 1.49 -5.35 5.69 o -19 3 1 373.25 349.28 24.68 o -17 3 1 132.20 158.11 6.46 o -15 3 1 421.86 395.62 21.87 o -13 3 1 14.24 13.72 5.19 o -11 3 1 338.16 357.98 11.00 o -9 3 1 18.16 31.62 5.43 o -7 3 1 660.43 679.76 31.51 o -5 3 1 1261.33 1333.58 22.28 o -3 3 1 562.24 586.80 38.20 o -1 3 1 1009.30 1110.55 16.63 o 1 3 1 205.56 243.61 7.26 o 3 3 1 1135.13 1186.29 23.42 o 5 3 1 2352.09 2269.81 23.56 o 7 3 1 1099.45 1131.13 18.15 o 9 3 1 30.98 17.19 4.73 o 11 3 1 963.44 911.41 31.51 o 13 3 1 272.79 254.61 23.01 o 15 3 1 336.73 320.14 8.53 o 17 3 1 12.99 22.89 5.10 o 19 3 1 209.91 202.46 6.89 o 21 3 1 19.02 18.82 5.69 o -16 4 1 0.74 2.57 5.45 o -14 4 1 0.08 -0.88 21.87 o -12 4 1 328.93 332.57 10.82 o -10 4 1 42.25 72.43 8.98 o -8 4 1 176.63 232.56 8.05 o -6 4 1 540.50 604.09 63.28 o -4 4 1 334.49 336.10 10.68 o -2 4 1 121.93 97.50 9.97 o 0 4 1 1252.83 1191.99 22.39 o 2 4 1 337.10 310.04 10.37 o 4 4 1 217.17 248.29 6.69 o 6 4 1 7.65 2.94 4.15 o 8 4 1 533.00 517.54 13.03 o 10 4 1 1084.65 1057.84 19.90 o 12 4 1 354.96 397.50 36.13 o 14 4 1 9.32 4.80 5.08 o 16 4 1 37.59 50.36 3.62 o -11 5 1 31.02 41.33 4.02 o -9 5 1 44.54 57.71 5.73 o -7 5 1 29.10 20.31 5.17 o -5 5 1 0.08 -3.80 3.80 o -3 5 1 4.30 7.46 7.50 o -1 5 1 7.52 6.10 5.20 o 1 5 1 6.20 8.81 4.91 o 3 5 1 6.25 14.46 4.12 o 5 5 1 80.37 115.73 10.01 o 7 5 1 5.31 -4.18 4.36 o 9 5 1 138.64 124.85 15.96 o 11 5 1 94.30 75.44 4.02 o -24 0 2 137.83 161.88 10.97 o -22 0 2 2.25 11.16 6.39 o -20 0 2 633.65 647.50 16.67 o -18 0 2 36.10 42.59 12.56 o -16 0 2 1681.56 1561.11 52.80 o -14 0 2 87.65 101.13 12.04 o -12 0 2 7728.67 7732.12 44.23 o -10 0 2 18691.64 19056.70 228.57 o -8 0 2 2997.67 2886.82 105.14 o -6 0 2 15439.23 14864.73 383.55 o -4 0 2 21305.18 20459.18 103.14 o -2 0 2 1390.19 1476.15 9.61 o 0 0 2 5944.15 5887.36 69.33 o 2 0 2 5765.65 5764.82 20.57 o 4 0 2 6765.78 6466.37 50.70 o 6 0 2 564.18 566.68 11.82 o 8 0 2 1131.95 1158.28 49.99 o 10 0 2 18.26 5.03 4.17 o 12 0 2 3080.38 3270.84 84.30 o 14 0 2 4639.88 4493.59 68.64 o 16 0 2 352.44 370.57 11.89 o 18 0 2 4405.20 4504.70 45.73 o 20 0 2 732.79 734.85 18.16 o 22 0 2 805.49 846.00 51.01 o 24 0 2 65.60 58.21 5.35 o -25 1 2 148.05 169.99 9.35 o -23 1 2 383.85 365.48 10.33 o -21 1 2 166.38 158.24 8.42 o -19 1 2 7.87 16.21 5.37 o -17 1 2 312.40 300.86 13.00 o -15 1 2 3592.90 3552.91 97.09 o -13 1 2 87.22 90.35 6.61 o -11 1 2 789.89 819.72 13.19 o -9 1 2 22.73 29.51 3.99 o -7 1 2 5401.28 5528.56 83.41 o -5 1 2 3787.60 3871.07 49.33 o -3 1 2 18535.20 18818.79 60.35 o -1 1 2 4103.42 4238.54 93.18 o 1 1 2 308.96 470.28 10.68 o 3 1 2 3016.30 2896.33 36.94 o 5 1 2 92.43 104.95 3.08 o 7 1 2 3611.67 3305.43 23.60 o 9 1 2 15131.98 15457.96 241.57 o 11 1 2 2.50 -1.11 3.92 o 13 1 2 11.51 10.05 4.43 o 15 1 2 17.22 28.64 6.43 o 17 1 2 2406.36 2422.48 47.15 o 19 1 2 136.87 117.04 9.75 o 21 1 2 41.59 32.62 4.43 o 23 1 2 68.95 64.07 9.38 o 25 1 2 21.44 2.73 10.90 o -22 2 2 1.96 -0.36 6.02 o -20 2 2 0.80 -10.04 4.72 o -18 2 2 116.60 115.03 7.06 o -16 2 2 391.95 445.32 13.11 o -14 2 2 239.50 221.93 6.65 o -12 2 2 81.88 62.43 3.06 o -10 2 2 1.50 -3.17 3.58 o -8 2 2 1135.74 1087.40 17.93 o -6 2 2 39.67 47.28 2.43 o -4 2 2 589.09 697.89 12.85 o -2 2 2 8.17 -0.30 2.66 o 0 2 2 2679.74 2801.16 19.89 o 2 2 2 5570.12 5408.58 40.46 o 4 2 2 538.79 585.13 39.79 o 6 2 2 513.26 477.80 9.33 o 8 2 2 4132.34 4004.98 80.92 o 10 2 2 832.99 844.75 27.60 o 12 2 2 149.84 156.73 5.09 o 14 2 2 233.91 176.15 5.58 o 16 2 2 1080.59 1136.43 22.39 o 18 2 2 495.24 434.60 14.13 o 20 2 2 18.45 12.34 6.34 o 22 2 2 97.60 94.17 6.35 o -21 3 2 16.61 4.02 5.69 o -19 3 2 87.71 62.31 5.16 o -17 3 2 262.75 289.39 11.12 o -15 3 2 48.87 37.10 3.40 o -13 3 2 0.00 0.01 7.35 o -11 3 2 78.23 56.96 5.76 o -9 3 2 686.04 708.92 14.06 o -7 3 2 369.37 328.89 9.93 o -5 3 2 509.76 516.43 15.85 o -3 3 2 2060.61 1918.82 32.92 o -1 3 2 11.37 5.59 2.31 o 1 3 2 1822.90 1822.23 33.29 o 3 3 2 210.65 184.66 4.70 o 5 3 2 783.64 760.71 13.82 o 7 3 2 1187.69 1170.30 16.82 o 9 3 2 1496.11 1408.38 19.58 o 11 3 2 408.46 380.81 38.38 o 13 3 2 33.73 22.66 6.72 o 15 3 2 105.47 122.29 4.27 o 17 3 2 1.72 0.00 4.75 o 19 3 2 33.51 40.52 3.47 o 21 3 2 2.65 -5.39 13.37 o -16 4 2 116.29 113.26 5.45 o -14 4 2 24.00 20.85 6.65 o -12 4 2 20.20 28.15 14.85 o -10 4 2 176.85 179.61 6.14 o -8 4 2 1.10 0.99 7.17 o -6 4 2 505.18 523.87 13.84 o -4 4 2 280.53 275.17 7.06 o -2 4 2 1388.11 1343.08 21.15 o 0 4 2 129.77 83.03 4.54 o 2 4 2 851.13 838.52 21.72 o 4 4 2 479.71 429.52 11.99 o 6 4 2 1.49 -6.89 8.83 o 8 4 2 328.96 268.02 7.26 o 10 4 2 191.82 172.80 8.27 o 12 4 2 0.76 8.11 4.88 o 14 4 2 91.42 106.05 5.87 o 16 4 2 159.70 149.48 9.12 o -11 5 2 54.49 59.93 4.05 o -9 5 2 74.20 55.88 3.84 o -7 5 2 33.03 29.42 4.37 o -5 5 2 45.02 37.20 7.54 o -3 5 2 1.29 -1.47 4.99 o -1 5 2 980.68 913.21 29.44 o 1 5 2 80.19 69.90 3.73 o 3 5 2 187.72 163.56 14.63 o 5 5 2 147.61 144.12 6.69 o 7 5 2 473.85 500.76 14.89 o 9 5 2 48.03 36.26 5.32 o 11 5 2 5.21 -5.76 5.76 o -25 1 3 9.96 23.27 7.75 o -23 1 3 37.27 29.65 3.47 o -21 1 3 44.54 15.23 6.13 o -19 1 3 1050.23 978.05 22.28 o -17 1 3 143.28 162.86 7.39 o -15 1 3 641.87 633.13 54.93 o -13 1 3 27.24 25.14 6.06 o -11 1 3 1902.45 1763.73 20.75 o -9 1 3 6483.49 6878.23 158.61 o -7 1 3 6274.21 6292.03 33.15 o -5 1 3 95.77 165.36 5.43 o -3 1 3 20745.36 21597.46 149.17 o -1 1 3 33305.01 33302.64 95.11 o 1 1 3 3902.94 3938.81 44.95 o 3 1 3 4499.88 4056.26 33.74 o 5 1 3 861.92 867.00 13.14 o 7 1 3 2025.55 1899.55 18.76 o 9 1 3 2779.45 2781.31 30.71 o 11 1 3 715.28 811.58 16.29 o 13 1 3 1333.06 1293.39 31.11 o 15 1 3 808.05 781.62 31.03 o 17 1 3 508.49 473.92 13.17 o 19 1 3 77.93 93.98 8.75 o 21 1 3 467.52 513.09 27.30 o 23 1 3 87.81 88.93 5.25 o -22 2 3 100.42 127.88 5.98 o -20 2 3 351.36 347.94 17.55 o -18 2 3 539.62 485.71 14.83 o -16 2 3 0.18 -4.47 5.03 o -14 2 3 372.63 386.95 19.95 o -12 2 3 93.42 102.95 8.72 o -10 2 3 1132.48 1185.76 17.88 o -8 2 3 17.02 14.55 2.77 o -6 2 3 2392.73 2423.95 22.38 o -4 2 3 1071.34 960.30 14.50 o -2 2 3 356.74 431.14 8.29 o 0 2 3 807.26 732.61 10.64 o 2 2 3 16744.81 16826.01 132.60 o 4 2 3 5933.79 6025.30 33.19 o 6 2 3 796.21 932.17 18.88 o 8 2 3 2737.43 2762.29 28.09 o 10 2 3 687.08 661.60 20.43 o 12 2 3 872.55 944.17 17.25 o 14 2 3 29.36 19.50 5.43 o 16 2 3 0.01 -1.82 5.32 o 18 2 3 237.69 200.33 11.60 o 20 2 3 59.08 56.15 7.28 o 22 2 3 71.59 57.80 4.24 o -21 3 3 21.45 8.65 9.31 o -19 3 3 17.11 17.16 6.94 o -17 3 3 147.63 158.76 7.94 o -15 3 3 236.01 246.19 14.07 o -13 3 3 122.79 114.82 4.95 o -11 3 3 2990.11 3109.44 133.69 o -9 3 3 554.08 593.47 25.08 o -7 3 3 163.21 169.68 5.30 o -5 3 3 194.04 167.56 8.64 o -3 3 3 307.16 359.81 10.42 o -1 3 3 4.52 7.42 2.32 o 1 3 3 2342.06 2368.70 29.86 o 3 3 3 1566.43 1483.64 17.11 o 5 3 3 379.23 321.96 8.96 o 7 3 3 47.39 43.74 3.19 o 9 3 3 741.49 762.33 14.86 o 11 3 3 1167.57 1206.82 34.21 o 13 3 3 262.48 272.42 11.23 o 15 3 3 93.40 125.97 4.95 o 17 3 3 1.41 2.25 4.75 o 19 3 3 31.31 45.72 3.50 o 21 3 3 43.00 51.93 4.17 o -16 4 3 3.02 -3.58 11.67 o -14 4 3 14.57 20.29 18.43 o -12 4 3 273.53 332.03 8.89 o -10 4 3 208.59 180.61 6.14 o -8 4 3 834.98 890.35 25.56 o -6 4 3 204.37 195.88 10.34 o -4 4 3 191.64 181.77 12.93 o -2 4 3 34.52 35.92 5.50 o 0 4 3 599.52 577.86 17.47 o 2 4 3 79.64 107.26 3.92 o 4 4 3 1.21 1.11 8.53 o 6 4 3 34.12 41.68 3.80 o 8 4 3 18.33 18.28 4.06 o 10 4 3 14.62 7.66 4.62 o 12 4 3 129.85 140.21 10.08 o 14 4 3 273.05 322.09 8.53 o 16 4 3 112.65 135.28 5.50 o -9 5 3 0.10 4.38 4.56 o -7 5 3 3.35 -3.96 3.73 o -5 5 3 81.80 114.31 8.79 o -3 5 3 90.79 99.28 8.42 o -1 5 3 16.02 13.74 3.69 o 1 5 3 28.39 48.01 3.50 o 3 5 3 1.94 19.98 5.28 o 5 5 3 16.98 13.48 6.43 o 7 5 3 330.72 307.33 9.32 o 9 5 3 402.47 426.66 11.61 o -24 0 4 8.32 -2.53 5.40 o -22 0 4 5.16 -5.50 6.65 o -20 0 4 1325.66 1217.00 98.16 o -18 0 4 1406.60 1412.59 48.32 o -16 0 4 2035.69 2024.41 30.78 o -14 0 4 1417.05 1230.55 19.88 o -12 0 4 337.54 307.79 40.37 o -10 0 4 2378.60 2704.61 56.17 o -8 0 4 14949.03 14827.16 153.29 o -6 0 4 20783.44 19891.35 64.63 o -4 0 4 4710.25 4790.47 35.05 o -2 0 4 19763.47 19158.44 55.52 o 0 0 4 76593.87 76290.87 810.39 o 2 0 4 51.38 59.30 4.95 o 4 0 4 8133.04 7776.49 32.07 o 6 0 4 14411.05 15114.07 185.26 o 8 0 4 8661.07 8208.97 40.02 o 10 0 4 3932.02 3837.87 78.59 o 12 0 4 456.12 343.72 10.71 o 14 0 4 6144.06 6175.84 81.49 o 16 0 4 9720.09 9807.29 79.38 o 18 0 4 180.08 163.98 28.26 o 20 0 4 6.35 14.12 5.71 o 22 0 4 0.68 5.73 6.47 o 24 0 4 92.21 101.72 5.45 o -23 1 4 0.07 0.01 12.34 o -21 1 4 21.21 14.24 6.18 o -19 1 4 163.84 159.81 5.58 o -17 1 4 606.76 609.74 18.62 o -15 1 4 41.02 31.02 4.06 o -13 1 4 433.63 433.43 11.34 o -11 1 4 405.02 434.65 10.79 o -9 1 4 390.50 544.81 10.56 o -7 1 4 516.64 465.80 14.15 o -5 1 4 16.83 -2.94 3.10 o -3 1 4 16815.07 16121.54 92.39 o -1 1 4 48591.34 47691.26 379.45 o 1 1 4 23432.10 23882.32 69.26 o 3 1 4 4894.85 4438.55 34.96 o 5 1 4 12297.40 12029.73 46.16 o 7 1 4 16617.51 16988.98 114.23 o 9 1 4 5874.91 6563.48 112.54 o 11 1 4 110.26 101.02 3.60 o 13 1 4 280.27 281.66 14.04 o 15 1 4 418.93 422.63 28.15 o 17 1 4 11.80 14.21 5.40 o 19 1 4 736.08 696.79 25.34 o 21 1 4 48.20 52.41 4.80 o 23 1 4 9.59 11.45 7.20 o -22 2 4 39.66 39.10 6.57 o -20 2 4 283.05 263.63 8.73 o -18 2 4 53.92 42.13 5.61 o -16 2 4 2.89 -7.17 3.83 o -14 2 4 106.31 118.41 4.54 o -12 2 4 1059.79 970.84 17.60 o -10 2 4 0.82 0.01 3.68 o -8 2 4 6.79 17.51 2.48 o -6 2 4 1328.16 1256.07 17.79 o -4 2 4 2037.43 2100.22 20.00 o -2 2 4 3274.08 3861.91 24.94 o 0 2 4 5708.99 6270.62 215.70 o 2 2 4 978.70 991.73 13.05 o 4 2 4 1868.64 1870.06 18.81 o 6 2 4 2565.59 2784.84 48.71 o 8 2 4 13.07 3.02 4.69 o 10 2 4 1484.35 1547.48 22.49 o 12 2 4 37.70 30.04 3.16 o 14 2 4 29.16 29.20 3.41 o 16 2 4 9.12 12.76 5.14 o 18 2 4 199.93 191.84 6.91 o 20 2 4 8.01 0.00 9.16 o 22 2 4 8.14 8.94 9.16 o -21 3 4 181.70 199.94 7.67 o -19 3 4 167.04 171.06 7.02 o -17 3 4 76.00 32.51 4.55 o -15 3 4 73.44 87.76 4.33 o -13 3 4 909.05 965.26 35.35 o -11 3 4 3954.07 4047.89 120.81 o -9 3 4 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