#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/70/2217017.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217017_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Svoboda, Ingrid' 'Foro, Sabine' 'Paulus, Helmut' 'Fuess, Hartmut' _publ_section_title ; 2,2-Dichloro-N-(3,5-dimethylphenyl)acetamide ; _journal_coeditor_code DN2290 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o209 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.990 _cell_angle_gamma 90.000 _cell_length_a 11.4120 _cell_length_b 10.5700 _cell_length_c 9.1630 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8402 _[local]_cod_data_source_file dn2290Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' G10' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 104.32 106.21 0.76 o 2 0 0 2945.54 2770.24 30.93 o 3 0 0 13025.06 12571.57 46.64 o 4 0 0 8217.27 8266.23 72.83 o 5 0 0 166.75 97.53 6.00 o 6 0 0 808.28 820.35 5.00 o 7 0 0 15.94 9.23 0.71 o 8 0 0 356.14 336.34 4.82 o 9 0 0 262.34 271.27 3.71 o 10 0 0 18.32 13.21 1.04 o 11 0 0 3.12 0.21 2.79 o 12 0 0 8.80 4.39 0.99 o 1 1 0 2440.23 2409.45 9.80 o 2 1 0 2851.94 2879.57 11.16 o 3 1 0 242.89 240.61 1.39 o 4 1 0 206.03 196.36 3.10 o 5 1 0 2252.88 2459.24 5.65 o 6 1 0 92.84 73.08 2.73 o 7 1 0 40.45 34.15 3.32 o 8 1 0 0.66 0.64 0.42 o 9 1 0 6.15 7.18 1.04 o 10 1 0 224.69 233.86 2.75 o 11 1 0 0.12 0.82 0.55 o 12 1 0 0.01 0.30 0.57 o 0 2 0 3020.75 3110.68 11.85 o 1 2 0 1431.85 1497.45 9.02 o 2 2 0 129.51 122.85 2.22 o 3 2 0 479.78 490.89 2.36 o 4 2 0 1097.43 1196.46 3.56 o 5 2 0 118.06 141.83 2.01 o 6 2 0 278.21 276.69 4.19 o 7 2 0 0.48 0.82 0.39 o 8 2 0 10.44 6.56 1.50 o 9 2 0 59.84 52.80 3.72 o 10 2 0 0.62 -0.46 0.46 o 11 2 0 1.53 1.46 0.55 o 12 2 0 0.09 -0.09 0.60 o 1 3 0 6558.45 6963.60 40.39 o 2 3 0 910.88 987.49 9.02 o 3 3 0 728.12 802.03 4.66 o 4 3 0 253.54 265.68 3.01 o 5 3 0 383.87 474.05 2.60 o 6 3 0 37.17 31.44 2.34 o 7 3 0 366.95 405.31 2.85 o 8 3 0 108.44 121.64 3.89 o 9 3 0 30.00 36.74 2.59 o 10 3 0 2.96 1.40 0.75 o 11 3 0 0.07 -0.01 0.54 o 12 3 0 1.49 1.27 0.87 o 0 4 0 10855.91 12451.69 61.18 o 1 4 0 417.20 401.80 3.72 o 2 4 0 6263.38 6599.03 32.49 o 3 4 0 2374.34 2445.96 5.35 o 4 4 0 2722.82 2896.77 7.28 o 5 4 0 551.92 512.42 5.55 o 6 4 0 901.08 988.52 7.02 o 7 4 0 220.28 210.79 10.78 o 8 4 0 30.68 15.64 2.99 o 9 4 0 3.57 1.48 0.77 o 10 4 0 0.00 -0.01 0.50 o 11 4 0 2.43 1.82 0.60 o 12 4 0 1.44 0.82 0.88 o 1 5 0 81.34 70.31 1.38 o 2 5 0 139.42 128.40 2.34 o 3 5 0 206.14 253.96 2.40 o 4 5 0 70.73 59.80 3.01 o 5 5 0 116.80 148.79 1.65 o 6 5 0 178.97 207.09 2.06 o 7 5 0 311.21 340.79 7.60 o 8 5 0 135.98 141.43 1.95 o 9 5 0 6.34 2.53 0.56 o 10 5 0 94.72 92.04 6.25 o 11 5 0 0.21 0.90 0.77 o 0 6 0 254.51 263.53 11.38 o 1 6 0 0.28 0.30 0.35 o 2 6 0 21.11 29.36 1.01 o 3 6 0 19.92 17.01 0.59 o 4 6 0 361.17 386.11 4.13 o 5 6 0 22.21 17.39 0.64 o 6 6 0 16.73 12.44 0.58 o 7 6 0 1.25 0.42 0.59 o 8 6 0 15.78 14.14 1.06 o 9 6 0 2.23 1.97 0.54 o 10 6 0 74.45 81.26 5.06 o 11 6 0 4.16 2.72 0.75 o 1 7 0 142.09 143.25 1.71 o 2 7 0 152.50 173.03 5.34 o 3 7 0 264.95 319.40 8.30 o 4 7 0 9.16 4.52 1.45 o 5 7 0 13.30 12.62 1.57 o 6 7 0 7.17 2.10 0.50 o 7 7 0 1.26 -0.08 0.42 o 8 7 0 10.81 5.64 0.65 o 9 7 0 1.00 1.03 0.58 o 10 7 0 34.33 22.74 4.02 o 0 8 0 202.35 225.48 4.22 o 1 8 0 432.34 506.71 13.29 o 2 8 0 734.78 853.72 11.34 o 3 8 0 103.07 117.00 2.42 o 4 8 0 28.63 25.76 1.28 o 5 8 0 18.21 16.06 0.97 o 6 8 0 24.27 27.87 3.69 o 7 8 0 2.19 1.31 1.49 o 8 8 0 21.59 22.34 1.29 o 9 8 0 0.02 0.90 0.79 o 1 9 0 44.23 35.74 2.66 o 2 9 0 32.37 28.87 1.46 o 3 9 0 255.33 296.95 3.80 o 4 9 0 3.81 4.25 1.38 o 5 9 0 11.92 10.72 1.03 o 6 9 0 0.54 0.64 1.17 o 7 9 0 3.63 1.74 0.84 o 8 9 0 28.05 26.32 2.01 o 0 10 0 12.13 11.11 1.21 o 1 10 0 5.22 5.68 0.74 o 2 10 0 119.51 128.86 4.13 o 3 10 0 0.03 0.29 0.82 o 4 10 0 7.46 7.92 0.89 o 5 10 0 0.47 -0.13 1.05 o 6 10 0 12.54 12.82 1.10 o 7 10 0 5.47 0.97 0.90 o 1 11 0 11.76 10.95 0.96 o 2 11 0 2.34 -0.16 0.65 o 3 11 0 22.67 16.00 1.13 o 4 11 0 5.66 3.42 0.85 o 5 11 0 1.81 1.66 0.85 o 6 11 0 0.06 1.34 0.92 o 0 12 0 1.67 2.25 1.22 o 1 12 0 22.43 25.46 1.40 o 2 12 0 4.22 -0.34 0.80 o 3 12 0 8.81 10.30 1.32 o -13 1 1 4.28 5.13 1.78 o -12 1 1 43.04 35.25 8.00 o -11 1 1 33.88 33.46 11.13 o -10 1 1 15.56 12.28 5.05 o -9 1 1 94.01 91.02 3.35 o -8 1 1 76.01 65.64 9.54 o -7 1 1 90.46 102.90 7.19 o -6 1 1 536.14 548.94 3.99 o -5 1 1 1556.41 1654.56 11.31 o -4 1 1 91.36 77.46 4.76 o -3 1 1 1169.59 1058.88 13.44 o -2 1 1 1.04 -10.90 56.02 o -1 1 1 1351.87 1315.81 5.85 o 0 1 1 2280.85 2134.49 20.36 o 1 1 1 482.33 459.00 3.66 o 2 1 1 305.18 287.51 7.47 o 3 1 1 290.38 283.31 14.81 o 4 1 1 466.50 494.81 10.55 o 5 1 1 11.13 10.10 1.08 o 6 1 1 283.13 278.44 3.33 o 7 1 1 57.61 48.97 4.93 o 8 1 1 310.76 324.97 10.74 o 9 1 1 40.21 35.24 5.15 o 10 1 1 32.63 29.75 9.33 o 11 1 1 33.89 30.59 7.14 o 12 1 1 10.65 13.78 6.71 o -12 2 1 112.29 124.21 18.69 o -11 2 1 4.55 7.18 2.64 o -10 2 1 462.03 507.37 5.46 o -9 2 1 357.97 403.10 11.17 o -8 2 1 885.80 975.20 6.78 o -7 2 1 1160.40 1150.92 6.41 o -6 2 1 1134.17 1034.78 5.68 o -5 2 1 1812.82 1810.35 7.04 o -4 2 1 2039.66 1924.42 13.35 o -3 2 1 2576.56 2338.56 6.66 o -2 2 1 5130.71 5215.60 97.35 o -1 2 1 2042.92 2141.62 34.25 o 0 2 1 5363.85 5239.29 47.37 o 1 2 1 67.89 55.10 3.21 o 2 2 1 15.74 13.01 5.01 o 3 2 1 453.59 458.15 3.35 o 4 2 1 0.38 0.54 0.61 o 5 2 1 39.55 39.69 7.94 o 6 2 1 34.00 43.12 4.17 o 7 2 1 51.02 34.69 5.92 o 8 2 1 94.85 73.39 5.97 o 9 2 1 171.55 184.26 13.08 o 10 2 1 18.19 19.52 8.22 o 11 2 1 0.25 0.35 1.38 o 12 2 1 0.21 -0.76 0.76 o -12 3 1 10.82 8.02 1.01 o -11 3 1 0.76 1.04 0.77 o -10 3 1 45.72 30.54 9.24 o -9 3 1 13.57 15.48 7.59 o -8 3 1 2.13 1.23 0.64 o -7 3 1 0.62 0.18 0.60 o -6 3 1 990.09 1034.58 5.86 o -5 3 1 165.43 207.46 9.20 o -4 3 1 0.43 1.26 1.13 o -3 3 1 1729.99 1717.94 6.41 o -2 3 1 8106.67 8620.40 79.76 o -1 3 1 8313.07 9354.01 22.28 o 0 3 1 2732.36 2777.96 12.30 o 1 3 1 1989.88 1952.32 14.11 o 2 3 1 8.09 4.17 0.58 o 3 3 1 23.11 30.18 1.26 o 4 3 1 50.85 59.16 1.53 o 5 3 1 190.88 224.78 4.31 o 6 3 1 0.08 0.49 0.65 o 7 3 1 107.99 103.21 3.59 o 8 3 1 468.40 540.31 5.54 o 9 3 1 64.81 70.46 6.49 o 10 3 1 37.15 33.75 5.70 o 11 3 1 29.74 28.16 5.66 o -12 4 1 8.78 5.61 1.18 o -11 4 1 7.56 6.75 2.04 o -10 4 1 25.54 18.86 4.34 o -9 4 1 26.75 15.45 5.49 o -8 4 1 37.82 38.86 2.64 o -7 4 1 268.96 279.08 7.42 o -6 4 1 78.33 78.92 4.97 o -5 4 1 133.29 150.15 4.33 o -4 4 1 645.20 762.23 4.86 o -3 4 1 84.06 84.48 3.94 o -2 4 1 2225.86 2349.13 43.49 o -1 4 1 48.90 61.63 1.31 o 0 4 1 42.42 44.44 1.12 o 1 4 1 2.12 0.46 1.14 o 2 4 1 409.06 415.75 14.17 o 3 4 1 808.81 853.36 4.95 o 4 4 1 363.70 365.24 3.52 o 5 4 1 21.60 20.13 6.31 o 6 4 1 153.25 151.71 6.20 o 7 4 1 339.93 354.16 6.25 o 8 4 1 372.78 421.53 5.16 o 9 4 1 94.08 90.47 10.44 o 10 4 1 83.22 86.43 2.72 o 11 4 1 34.93 34.89 9.15 o -12 5 1 53.11 76.04 5.28 o -11 5 1 31.11 35.39 9.60 o -10 5 1 18.77 18.18 8.19 o -9 5 1 131.85 146.21 3.00 o -8 5 1 39.04 28.46 14.08 o -7 5 1 495.15 575.82 19.46 o -6 5 1 206.01 211.73 5.94 o -5 5 1 26.50 17.04 9.37 o -4 5 1 42.95 45.36 5.73 o -3 5 1 246.28 255.81 2.87 o -2 5 1 925.13 921.68 13.91 o -1 5 1 47.25 44.19 11.70 o 0 5 1 104.32 129.11 12.48 o 1 5 1 997.79 1115.73 23.89 o 2 5 1 1168.56 1334.05 5.96 o 3 5 1 9.27 19.48 2.64 o 4 5 1 228.66 258.46 19.14 o 5 5 1 127.97 119.03 3.02 o 6 5 1 338.59 354.73 5.62 o 7 5 1 83.13 79.17 6.30 o 8 5 1 8.89 8.56 2.95 o 9 5 1 2.69 2.94 0.92 o 10 5 1 110.31 135.49 7.67 o 11 5 1 11.72 11.18 1.27 o -11 6 1 36.30 28.76 7.88 o -10 6 1 113.89 130.40 3.18 o -9 6 1 58.62 54.94 9.32 o -8 6 1 177.56 189.13 7.36 o -7 6 1 205.04 215.13 3.40 o -6 6 1 611.91 698.68 12.01 o -5 6 1 1257.79 1399.35 15.95 o -4 6 1 173.60 178.55 5.70 o -3 6 1 2.71 3.73 0.78 o -2 6 1 2958.07 3271.50 19.10 o -1 6 1 180.19 156.56 2.21 o 0 6 1 268.24 309.11 12.53 o 1 6 1 0.39 0.45 0.53 o 2 6 1 324.13 299.44 10.99 o 3 6 1 82.87 76.19 14.76 o 4 6 1 70.21 91.24 7.99 o 5 6 1 148.72 145.82 11.53 o 6 6 1 23.42 16.49 1.40 o 7 6 1 103.62 97.35 19.74 o 8 6 1 0.82 -0.86 0.86 o 9 6 1 1.02 1.86 0.92 o 10 6 1 3.76 2.20 1.10 o -10 7 1 6.22 9.37 1.07 o -9 7 1 4.26 2.49 0.84 o -8 7 1 1.21 2.12 0.81 o -7 7 1 0.01 1.14 0.73 o -6 7 1 10.95 8.78 1.27 o -5 7 1 105.92 110.20 4.50 o -4 7 1 373.23 384.51 4.21 o -3 7 1 32.35 31.67 2.03 o -2 7 1 868.09 1007.23 20.80 o -1 7 1 40.99 39.78 3.87 o 0 7 1 443.08 480.89 6.71 o 1 7 1 3.96 2.15 0.57 o 2 7 1 15.21 24.43 1.33 o 3 7 1 1.08 2.43 0.61 o 4 7 1 0.17 -0.66 0.95 o 5 7 1 21.79 30.91 1.57 o 6 7 1 204.23 240.20 12.89 o 7 7 1 117.96 148.11 3.95 o 8 7 1 0.78 0.02 0.90 o 9 7 1 39.71 45.10 2.24 o 10 7 1 154.37 203.10 5.55 o -10 8 1 22.68 15.94 1.84 o -9 8 1 15.49 11.29 1.58 o -8 8 1 0.21 0.96 1.04 o -7 8 1 78.88 80.25 3.38 o -6 8 1 19.47 13.44 1.45 o -5 8 1 44.41 50.95 2.55 o -4 8 1 3.40 1.25 0.91 o -3 8 1 2.75 3.43 0.97 o -2 8 1 23.03 17.74 1.38 o -1 8 1 5.93 5.78 1.02 o 0 8 1 326.26 384.80 5.74 o 1 8 1 336.07 357.70 5.64 o 2 8 1 37.09 45.23 2.25 o 3 8 1 55.08 55.58 2.54 o 4 8 1 422.30 459.73 7.21 o 5 8 1 112.00 112.11 3.88 o 6 8 1 65.11 61.44 2.98 o 7 8 1 22.34 17.10 1.67 o 8 8 1 198.74 225.50 5.90 o 9 8 1 1.62 0.05 1.20 o -9 9 1 45.49 50.70 4.12 o -8 9 1 20.03 26.53 1.97 o -7 9 1 19.42 26.02 1.95 o -6 9 1 93.09 94.96 3.62 o -5 9 1 47.69 55.30 2.73 o -4 9 1 143.61 157.24 4.25 o -3 9 1 42.30 39.01 3.84 o -2 9 1 178.10 164.67 4.18 o -1 9 1 65.11 69.53 2.81 o 0 9 1 268.79 268.53 5.23 o 1 9 1 2.07 1.26 0.97 o 2 9 1 118.18 127.99 3.75 o 3 9 1 11.27 5.92 1.16 o 4 9 1 143.49 155.24 4.33 o 5 9 1 11.29 9.49 1.82 o 6 9 1 5.96 3.64 1.37 o 7 9 1 65.81 60.97 5.31 o 8 9 1 14.78 12.89 1.68 o -8 10 1 30.20 23.12 2.10 o -7 10 1 27.74 23.26 1.99 o -6 10 1 15.73 13.22 1.60 o -5 10 1 56.07 51.96 4.94 o -4 10 1 56.33 59.79 2.95 o -3 10 1 0.04 -0.83 0.83 o -2 10 1 72.18 76.38 3.11 o -1 10 1 59.58 60.42 2.77 o 0 10 1 0.38 1.90 1.08 o 1 10 1 35.89 21.92 1.64 o 2 10 1 21.69 11.39 1.39 o 3 10 1 16.86 18.51 1.61 o 4 10 1 19.02 9.07 1.40 o 5 10 1 1.81 3.33 1.40 o 6 10 1 6.90 6.62 1.41 o 7 10 1 0.35 1.06 1.22 o -6 11 1 0.29 0.48 1.18 o -5 11 1 25.33 22.69 1.93 o -4 11 1 6.52 7.08 1.28 o -3 11 1 0.00 0.12 1.02 o -2 11 1 23.08 16.73 1.61 o -1 11 1 0.07 0.94 1.06 o 0 11 1 4.75 5.85 1.18 o 1 11 1 3.33 3.16 1.20 o 2 11 1 2.47 1.27 1.23 o 3 11 1 1.32 -0.70 0.97 o 4 11 1 14.40 10.00 1.42 o 5 11 1 0.69 0.43 1.07 o -4 12 1 31.17 24.01 2.05 o -3 12 1 0.77 2.65 1.19 o -2 12 1 5.38 3.46 1.39 o -1 12 1 4.05 4.11 1.24 o 0 12 1 19.00 22.75 1.91 o 1 12 1 3.58 4.47 1.25 o 2 12 1 6.76 9.96 1.55 o 3 12 1 27.37 28.87 2.14 o -13 0 2 1.37 1.40 1.25 o -12 0 2 58.41 65.46 5.96 o -11 0 2 0.81 1.91 1.20 o -10 0 2 46.78 28.39 2.07 o -9 0 2 10.18 19.01 1.48 o -8 0 2 27.25 32.24 2.54 o -7 0 2 269.01 254.20 4.42 o -6 0 2 1703.37 1995.60 11.15 o -5 0 2 2872.41 2897.61 12.93 o -4 0 2 695.28 671.83 5.56 o -3 0 2 30.78 25.18 2.03 o -2 0 2 9108.21 7679.32 19.20 o -1 0 2 758.35 653.39 4.76 o 0 0 2 820.99 818.75 5.32 o 1 0 2 51.48 19.16 1.35 o 2 0 2 1278.29 1394.63 8.12 o 3 0 2 189.52 133.34 2.99 o 4 0 2 5.86 3.49 0.96 o 5 0 2 601.27 564.07 6.68 o 6 0 2 228.03 252.80 4.91 o 7 0 2 17.66 16.81 1.47 o 8 0 2 227.42 232.80 5.51 o 9 0 2 49.38 51.27 3.88 o 10 0 2 117.07 109.68 4.38 o 11 0 2 57.78 73.45 5.19 o -13 1 2 0.66 1.13 1.51 o -12 1 2 0.85 -0.20 0.77 o -11 1 2 40.99 36.71 2.85 o -10 1 2 6.88 6.48 2.83 o -9 1 2 1.88 0.54 0.64 o -8 1 2 15.06 14.87 1.48 o -7 1 2 1.40 9.46 5.37 o -6 1 2 281.42 271.61 14.31 o -5 1 2 253.40 279.40 9.51 o -4 1 2 2354.21 2434.99 12.38 o -3 1 2 2329.76 2496.59 7.24 o -2 1 2 1108.29 1084.08 5.88 o -1 1 2 8510.63 8176.92 13.47 o 0 1 2 6084.76 5931.78 79.58 o 1 1 2 5499.01 5321.99 11.15 o 2 1 2 1733.22 1683.01 11.54 o 3 1 2 93.22 58.59 3.76 o 4 1 2 1997.38 1874.50 8.03 o 5 1 2 1693.22 1732.11 8.39 o 6 1 2 335.19 347.13 12.97 o 7 1 2 49.59 47.04 2.75 o 8 1 2 1223.63 1413.74 9.36 o 9 1 2 76.84 83.73 8.97 o 10 1 2 0.01 -0.08 0.79 o 11 1 2 0.45 0.39 0.84 o -13 2 2 0.27 1.29 0.89 o -12 2 2 5.78 6.37 2.64 o -11 2 2 4.07 4.84 1.39 o -10 2 2 10.77 7.27 1.67 o -9 2 2 1.38 0.56 0.68 o -8 2 2 0.82 0.82 0.63 o -7 2 2 179.79 185.66 3.42 o -6 2 2 426.73 440.57 17.27 o -5 2 2 692.21 664.82 4.44 o -4 2 2 175.58 162.49 14.34 o -3 2 2 26.29 22.82 3.24 o -2 2 2 2073.55 1988.98 11.40 o -1 2 2 12.35 9.61 0.64 o 0 2 2 121.41 97.99 6.19 o 1 2 2 939.17 993.34 26.42 o 2 2 2 3.21 3.11 0.62 o 3 2 2 201.09 197.67 7.46 o 4 2 2 159.07 161.02 2.55 o 5 2 2 17.51 13.91 4.05 o 6 2 2 4.30 3.14 1.00 o 7 2 2 65.38 73.98 2.19 o 8 2 2 120.32 136.11 7.58 o 9 2 2 89.96 95.14 4.08 o 10 2 2 15.27 12.32 1.86 o 11 2 2 1.98 -0.59 0.87 o -12 3 2 0.37 0.19 0.79 o -11 3 2 11.01 8.88 2.20 o -10 3 2 0.01 0.12 0.71 o -9 3 2 69.04 72.23 4.32 o -8 3 2 0.01 0.11 0.58 o -7 3 2 520.88 570.75 4.80 o -6 3 2 467.44 494.33 7.48 o -5 3 2 237.35 226.77 8.36 o -4 3 2 194.51 197.64 3.01 o -3 3 2 1043.26 1089.50 5.35 o -2 3 2 668.06 643.60 3.77 o -1 3 2 1075.61 1074.32 7.05 o 0 3 2 426.08 405.89 5.66 o 1 3 2 2120.05 2096.12 7.97 o 2 3 2 2733.26 2748.73 8.82 o 3 3 2 2141.70 2379.75 8.82 o 4 3 2 345.82 308.72 3.55 o 5 3 2 255.48 245.81 9.52 o 6 3 2 722.80 813.70 6.86 o 7 3 2 7.81 6.21 2.02 o 8 3 2 21.75 18.69 1.24 o 9 3 2 0.31 -0.79 0.79 o 10 3 2 0.02 1.21 0.90 o 11 3 2 5.03 3.71 1.06 o -12 4 2 37.28 26.35 10.05 o -11 4 2 1.20 -0.90 0.90 o -10 4 2 3.13 0.68 1.48 o -9 4 2 31.99 34.32 3.97 o -8 4 2 22.20 28.49 2.04 o -7 4 2 0.02 0.33 0.62 o -6 4 2 277.47 345.10 19.81 o -5 4 2 0.04 1.17 0.66 o -4 4 2 22.58 15.24 3.11 o -3 4 2 387.62 420.15 10.53 o -2 4 2 315.13 305.72 2.85 o -1 4 2 57.13 41.13 2.49 o 0 4 2 495.96 414.73 3.12 o 1 4 2 407.42 397.29 8.34 o 2 4 2 12.93 24.67 4.73 o 3 4 2 20.45 11.72 3.36 o 4 4 2 881.61 1033.81 6.45 o 5 4 2 27.43 28.80 8.27 o 6 4 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