#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217026.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217026_Fobs loop_ _publ_author_name 'Li, Xiu-Bing' 'Shang, Run-Ling' 'Sun, Bai-Wang' _publ_section_title ; Diaquabis(picolinato N-oxide-\k^2^O,O')zinc(II) ; _journal_coeditor_code ER2040 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m131 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.370 _cell_angle_gamma 90.000 _cell_length_a 6.6837 _cell_length_b 15.7376 _cell_length_c 6.9935 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file er2040Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.39 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 27.27 5.27 1.38 o 2 0 0 3895.51 3811.51 32.70 o 3 0 0 8051.92 8399.78 49.53 o 4 0 0 1234.64 1169.12 44.99 o 5 0 0 895.20 816.61 24.17 o 6 0 0 563.59 557.14 16.74 o 7 0 0 31.24 42.28 10.08 o 1 1 0 1360.14 1647.26 11.92 o 2 1 0 897.91 1212.75 8.79 o 3 1 0 37.29 41.72 2.92 o 4 1 0 0.05 0.82 1.33 o 5 1 0 387.97 408.86 10.14 o 6 1 0 0.11 0.00 1.90 o 7 1 0 0.00 0.58 2.97 o 0 2 0 5784.32 5979.08 35.71 o 1 2 0 4638.84 4599.07 20.95 o 2 2 0 5166.63 4945.00 27.05 o 3 2 0 5220.27 5278.52 31.63 o 4 2 0 1706.12 1610.67 16.51 o 5 2 0 4.78 4.99 2.31 o 6 2 0 2522.70 2465.83 30.94 o 7 2 0 195.91 241.79 11.02 o 1 3 0 26.61 21.39 2.03 o 2 3 0 19.81 39.36 1.51 o 3 3 0 1175.53 1444.16 11.77 o 4 3 0 1.65 0.00 1.17 o 5 3 0 283.98 292.21 7.73 o 6 3 0 24.80 35.38 7.36 o 7 3 0 0.59 0.23 3.16 o 0 4 0 8475.57 8985.91 60.84 o 1 4 0 12.14 28.66 1.52 o 2 4 0 435.32 206.34 3.50 o 3 4 0 3698.01 3501.54 24.54 o 4 4 0 552.06 423.01 9.00 o 5 4 0 621.71 582.43 13.21 o 6 4 0 1772.91 1726.92 35.36 o 7 4 0 96.43 96.39 7.87 o 1 5 0 543.11 597.78 6.14 o 2 5 0 437.23 537.81 6.26 o 3 5 0 14.77 21.98 1.55 o 4 5 0 58.88 71.61 3.87 o 5 5 0 5.16 2.90 2.27 o 6 5 0 50.46 44.01 8.44 o 0 6 0 4681.35 4600.72 29.68 o 1 6 0 82.18 231.93 3.42 o 2 6 0 18.80 12.91 1.39 o 3 6 0 2832.32 2755.06 18.31 o 4 6 0 447.28 392.37 8.27 o 5 6 0 73.81 68.43 10.43 o 6 6 0 791.70 784.82 17.46 o 1 7 0 872.76 1155.14 12.35 o 2 7 0 0.29 0.00 1.00 o 3 7 0 140.12 177.99 5.89 o 4 7 0 231.95 260.61 7.72 o 5 7 0 19.91 16.73 4.59 o 6 7 0 18.37 13.06 7.04 o 0 8 0 5502.35 5794.85 61.48 o 1 8 0 360.46 241.51 4.06 o 2 8 0 438.56 359.37 6.02 o 3 8 0 587.57 525.58 7.72 o 4 8 0 422.74 379.37 8.60 o 5 8 0 26.49 35.98 5.56 o 6 8 0 166.75 183.61 9.40 o 1 9 0 16.55 20.60 1.50 o 2 9 0 368.31 368.70 6.40 o 3 9 0 92.56 103.76 4.65 o 4 9 0 258.33 244.16 7.21 o 5 9 0 263.45 244.94 11.86 o 6 9 0 10.91 12.05 3.73 o 0 10 0 1337.80 1076.16 13.57 o 1 10 0 597.46 455.95 9.61 o 2 10 0 1224.34 1180.75 14.92 o 3 10 0 1455.00 1442.30 16.89 o 4 10 0 4.26 5.57 2.43 o 5 10 0 25.72 36.51 4.80 o 6 10 0 337.65 345.08 22.49 o 1 11 0 169.61 207.21 5.05 o 2 11 0 0.49 0.00 1.25 o 3 11 0 1087.56 1054.97 14.60 o 4 11 0 95.77 93.06 5.22 o 5 11 0 25.08 15.89 3.46 o 0 12 0 1425.33 1241.66 20.68 o 1 12 0 972.45 879.39 10.87 o 2 12 0 9.86 9.86 1.88 o 3 12 0 1050.85 1060.83 15.03 o 4 12 0 461.59 474.53 12.73 o 5 12 0 448.31 475.52 16.98 o 1 13 0 133.46 149.18 5.42 o 2 13 0 692.70 728.91 12.18 o 3 13 0 170.85 183.48 7.78 o 4 13 0 39.85 39.38 4.95 o 5 13 0 129.60 98.19 9.24 o 0 14 0 212.85 220.35 14.59 o 1 14 0 716.49 630.21 17.12 o 2 14 0 307.97 307.89 9.63 o 3 14 0 880.73 867.60 17.02 o 4 14 0 433.06 433.34 12.84 o 1 15 0 53.56 52.55 6.35 o 2 15 0 8.00 0.89 2.30 o 3 15 0 10.89 14.47 4.49 o 4 15 0 56.24 65.97 7.99 o 0 16 0 665.07 750.02 28.78 o 1 16 0 475.34 527.03 16.99 o 2 16 0 532.51 533.31 17.25 o 3 16 0 499.81 498.13 17.57 o 1 17 0 64.38 37.95 6.23 o 2 17 0 1.17 4.27 3.76 o 3 17 0 3.24 2.16 5.90 o 0 18 0 265.31 279.60 19.29 o 1 18 0 546.19 579.56 19.30 o -7 1 1 178.58 201.81 9.52 o -6 1 1 100.87 113.93 5.69 o -5 1 1 1616.74 1676.04 18.06 o -4 1 1 919.93 860.41 13.12 o -3 1 1 2470.73 2513.76 15.43 o -2 1 1 4138.92 4151.50 20.24 o -1 1 1 5151.66 5213.26 29.42 o 0 1 1 4776.31 4929.05 28.22 o 1 1 1 1516.27 1499.85 14.88 o 2 1 1 1256.65 1198.32 9.24 o 3 1 1 763.54 623.28 7.01 o 4 1 1 1147.62 1124.93 17.11 o 5 1 1 106.47 81.27 5.89 o 6 1 1 476.75 458.01 16.73 o -7 2 1 45.93 49.10 5.75 o -6 2 1 261.19 271.45 9.52 o -5 2 1 511.66 576.18 10.15 o -4 2 1 2.19 1.98 0.97 o -3 2 1 626.43 808.40 6.14 o -2 2 1 609.93 714.88 5.35 o -1 2 1 1127.86 1239.57 10.42 o 0 2 1 2028.88 2526.33 14.45 o 1 2 1 104.72 116.30 2.94 o 2 2 1 55.04 70.90 2.23 o 3 2 1 328.11 385.84 5.92 o 4 2 1 1.66 6.41 2.25 o 5 2 1 3.37 0.85 1.99 o 6 2 1 268.32 237.82 9.94 o -7 3 1 228.06 259.32 10.47 o -6 3 1 1118.65 1072.55 19.04 o -5 3 1 158.31 151.36 5.41 o -4 3 1 405.09 345.41 5.77 o -3 3 1 3333.93 3491.29 21.34 o -2 3 1 679.50 516.56 4.87 o -1 3 1 748.03 588.30 5.41 o 0 3 1 1557.21 1355.20 13.53 o 1 3 1 2553.45 2329.99 15.28 o 2 3 1 4912.92 5156.29 30.63 o 3 3 1 654.19 548.40 8.64 o 4 3 1 773.12 716.67 13.76 o 5 3 1 1694.54 1642.82 23.80 o 6 3 1 234.81 246.51 10.17 o -7 4 1 7.26 7.55 3.29 o -6 4 1 33.49 38.80 4.83 o -5 4 1 208.49 239.68 8.15 o -4 4 1 141.67 156.25 4.00 o -3 4 1 1394.68 1735.57 10.79 o -2 4 1 48.72 55.55 1.70 o -1 4 1 705.71 849.96 7.92 o 0 4 1 682.18 845.39 6.64 o 1 4 1 1184.02 1429.28 10.96 o 2 4 1 71.30 105.21 3.55 o 3 4 1 167.48 181.07 5.15 o 4 4 1 132.18 118.30 6.14 o 5 4 1 176.21 167.53 9.57 o 6 4 1 22.22 19.63 4.30 o -7 5 1 398.58 380.71 12.93 o -6 5 1 505.39 480.88 12.99 o -5 5 1 950.46 935.57 16.49 o -4 5 1 832.13 801.17 11.12 o -3 5 1 27.37 7.54 0.94 o -2 5 1 1815.97 1859.40 16.84 o -1 5 1 672.16 541.77 5.52 o 0 5 1 973.47 766.86 6.71 o 1 5 1 3908.32 3849.51 21.12 o 2 5 1 809.04 585.80 7.08 o 3 5 1 2800.48 2905.04 23.51 o 4 5 1 1480.29 1450.70 20.61 o 5 5 1 596.91 589.16 14.31 o 6 5 1 442.25 455.28 13.94 o -7 6 1 17.55 17.01 4.05 o -6 6 1 116.55 108.82 7.08 o -5 6 1 40.48 41.18 4.40 o -4 6 1 171.63 195.41 7.19 o -3 6 1 127.86 134.95 3.49 o -2 6 1 406.46 533.94 6.45 o -1 6 1 7.42 5.75 0.95 o 0 6 1 3262.28 4078.03 24.16 o 1 6 1 655.86 712.64 7.62 o 2 6 1 92.40 80.91 2.89 o 3 6 1 749.83 762.52 11.23 o 4 6 1 5.55 2.51 1.68 o 5 6 1 36.15 29.39 4.23 o 6 6 1 27.14 29.91 6.00 o -7 7 1 189.83 197.27 13.82 o -6 7 1 239.72 253.17 17.47 o -5 7 1 1459.80 1306.08 20.15 o -4 7 1 716.56 666.60 10.73 o -3 7 1 1520.07 1531.98 15.36 o -2 7 1 1939.13 1854.36 13.87 o -1 7 1 2068.31 2063.03 12.77 o 0 7 1 2762.69 2735.89 16.87 o 1 7 1 1243.56 1045.79 9.94 o 2 7 1 1566.63 1466.61 18.02 o 3 7 1 647.36 591.75 13.62 o 4 7 1 809.56 784.91 12.82 o 5 7 1 177.96 204.54 9.45 o 6 7 1 129.29 154.23 9.18 o -6 8 1 0.43 0.00 2.46 o -5 8 1 4.97 8.80 2.75 o -4 8 1 269.42 335.16 7.78 o -3 8 1 4.20 8.05 1.44 o -2 8 1 0.66 1.07 0.97 o -1 8 1 430.13 577.21 5.91 o 0 8 1 507.06 575.80 6.95 o 1 8 1 723.61 809.71 9.01 o 2 8 1 1.32 6.70 1.44 o 3 8 1 127.33 107.37 4.86 o 4 8 1 17.84 34.56 4.37 o 5 8 1 75.03 73.01 6.24 o 6 8 1 10.71 1.64 3.73 o -6 9 1 336.40 372.75 22.16 o -5 9 1 759.86 735.54 15.40 o -4 9 1 445.45 403.56 8.78 o -3 9 1 2704.32 2623.19 21.71 o -2 9 1 2267.84 2258.86 16.95 o -1 9 1 2461.95 2480.61 16.01 o 0 9 1 1056.41 1035.16 9.09 o 1 9 1 1752.91 1726.43 14.44 o 2 9 1 1322.22 1233.39 12.64 o 3 9 1 9.96 13.00 2.38 o 4 9 1 681.67 644.16 12.19 o 5 9 1 132.75 150.02 8.45 o -6 10 1 36.36 30.70 6.14 o -5 10 1 143.76 106.72 6.77 o -4 10 1 594.50 599.00 13.28 o -3 10 1 281.96 294.07 9.05 o -2 10 1 360.93 379.66 7.15 o -1 10 1 340.19 375.56 6.29 o 0 10 1 83.20 83.47 2.81 o 1 10 1 117.93 143.96 4.18 o 2 10 1 763.99 882.71 10.89 o 3 10 1 60.75 66.60 4.32 o 4 10 1 200.98 194.38 7.08 o 5 10 1 1.88 0.00 2.57 o -6 11 1 92.70 93.98 9.55 o -5 11 1 422.55 434.37 12.49 o -4 11 1 718.35 694.81 14.78 o -3 11 1 264.16 236.59 6.74 o -2 11 1 2872.53 2622.50 23.28 o -1 11 1 289.89 255.18 6.50 o 0 11 1 544.70 548.49 7.97 o 1 11 1 2223.90 2167.79 17.78 o 2 11 1 163.67 160.41 4.94 o 3 11 1 655.46 663.40 11.95 o 4 11 1 184.04 200.95 7.59 o 5 11 1 279.56 286.91 20.50 o -5 12 1 5.05 1.41 2.75 o -4 12 1 0.57 1.29 2.28 o -3 12 1 2.07 1.24 1.66 o -2 12 1 417.80 463.75 11.44 o -1 12 1 133.30 150.67 7.43 o 0 12 1 320.97 354.50 9.53 o 1 12 1 5.83 6.05 3.07 o 2 12 1 1090.17 1129.10 17.44 o 3 12 1 25.53 24.01 3.23 o 4 12 1 5.45 6.42 2.58 o 5 12 1 5.92 3.29 3.30 o -5 13 1 432.90 439.82 13.29 o -4 13 1 140.83 145.85 7.92 o -3 13 1 31.40 29.45 4.07 o -2 13 1 231.89 213.38 6.73 o -1 13 1 727.27 691.55 11.56 o 0 13 1 306.21 290.21 8.97 o 1 13 1 478.81 473.63 9.71 o 2 13 1 399.10 396.26 12.50 o 3 13 1 504.98 497.39 13.04 o 4 13 1 923.42 906.08 18.75 o -5 14 1 0.08 0.00 2.56 o -4 14 1 213.34 210.19 9.13 o -3 14 1 20.69 17.52 3.60 o -2 14 1 63.40 53.88 4.24 o -1 14 1 2.89 4.57 2.80 o 0 14 1 43.59 44.55 4.57 o 1 14 1 54.20 51.13 4.78 o 2 14 1 51.26 50.65 4.22 o 3 14 1 15.96 19.29 3.83 o 4 14 1 24.73 24.32 7.14 o -4 15 1 168.75 196.84 9.46 o -3 15 1 82.19 96.38 6.70 o -2 15 1 855.37 838.18 14.17 o -1 15 1 31.21 36.08 4.43 o 0 15 1 50.24 72.56 8.30 o 1 15 1 1335.38 1276.45 27.86 o 2 15 1 332.81 352.29 13.67 o 3 15 1 142.87 169.52 13.32 o -4 16 1 39.08 33.99 5.27 o -3 16 1 5.61 3.29 3.44 o -2 16 1 0.52 0.00 2.90 o -1 16 1 4.72 8.01 4.14 o 0 16 1 227.90 191.88 11.07 o 1 16 1 100.51 121.74 17.20 o 2 16 1 1.28 2.26 5.07 o 3 16 1 82.87 100.30 9.58 o -3 17 1 267.34 298.98 20.74 o -2 17 1 469.51 478.42 44.77 o -1 17 1 322.19 325.62 14.07 o 0 17 1 214.67 195.86 11.35 o 1 17 1 361.89 383.30 15.25 o 2 17 1 190.15 223.06 19.07 o -2 18 1 1.15 2.69 4.03 o -1 18 1 110.92 101.73 9.62 o 0 18 1 1.88 2.14 6.14 o 1 18 1 71.43 69.71 8.31 o -7 0 2 693.27 734.12 19.61 o -6 0 2 1027.72 956.56 20.39 o -5 0 2 281.07 243.50 22.52 o -4 0 2 2815.26 2626.15 29.21 o -3 0 2 966.10 724.04 12.12 o -2 0 2 318.18 670.31 14.25 o -1 0 2 28693.61 30900.54 313.32 o 0 0 2 7404.43 10095.45 68.90 o 1 0 2 167.06 386.19 8.20 o 2 0 2 854.35 710.07 12.39 o 3 0 2 527.24 492.83 11.01 o 4 0 2 6.72 2.26 3.80 o 5 0 2 130.17 151.23 14.19 o 6 0 2 267.64 289.15 20.24 o -7 1 2 2.82 4.28 3.26 o -6 1 2 334.84 350.41 9.28 o -5 1 2 492.39 519.17 10.25 o -4 1 2 16.09 25.74 2.31 o -3 1 2 66.99 66.53 2.73 o -2 1 2 234.66 376.44 7.43 o -1 1 2 65.40 78.75 2.70 o 0 1 2 4899.93 5736.47 34.88 o 1 1 2 53.64 71.76 2.62 o 2 1 2 286.72 350.15 8.95 o 3 1 2 6.49 6.14 1.78 o 4 1 2 2.10 6.62 3.89 o 5 1 2 16.43 24.46 5.04 o 6 1 2 45.03 28.35 6.07 o -7 2 2 919.38 857.82 24.32 o -6 2 2 3.97 5.03 2.37 o -5 2 2 560.31 522.82 9.34 o -4 2 2 1734.34 1574.67 13.67 o -3 2 2 3344.25 3234.22 16.94 o -2 2 2 650.76 1184.73 9.93 o -1 2 2 1579.66 1472.11 10.83 o 0 2 2 3078.17 2949.98 22.25 o 1 2 2 33.39 7.17 1.71 o 2 2 2 1775.99 1820.64 15.37 o 3 2 2 655.22 636.74 11.34 o 4 2 2 100.03 97.85 7.55 o 5 2 2 1754.75 1783.77 34.52 o 6 2 2 95.07 123.78 10.67 o -7 3 2 11.53 10.30 4.48 o -6 3 2 64.34 66.60 5.40 o -5 3 2 2.77 0.71 1.42 o -4 3 2 17.56 10.10 1.15 o -3 3 2 456.96 590.03 6.30 o -2 3 2 395.37 535.96 6.28 o -1 3 2 1573.50 1948.04 13.20 o 0 3 2 78.85 125.07 3.41 o 1 3 2 140.74 135.61 5.13 o 2 3 2 518.62 604.76 10.15 o 3 3 2 478.47 573.90 11.01 o 4 3 2 9.91 23.08 4.24 o 5 3 2 239.00 219.26 11.30 o 6 3 2 4.42 6.65 4.34 o -7 4 2 944.83 919.73 19.07 o -6 4 2 273.77 254.34 9.06 o -5 4 2 4.54 3.22 1.92 o -4 4 2 2038.05 2024.61 15.30 o -3 4 2 695.16 487.23 5.91 o -2 4 2 112.89 36.68 2.80 o -1 4 2 8385.30 8658.80 52.04 o 0 4 2 2570.49 2438.46 16.57 o 1 4 2 998.32 925.01 11.70 o 2 4 2 3615.15 3824.38 27.03 o 3 4 2 1944.14 1952.56 24.84 o 4 4 2 250.78 261.67 9.11 o 5 4 2 1174.95 1204.64 26.56 o -7 5 2 33.32 43.11 5.34 o -6 5 2 30.32 20.61 3.68 o -5 5 2 25.51 25.12 3.32 o -4 5 2 61.33 46.48 3.09 o -3 5 2 286.87 357.65 4.52 o -2 5 2 278.46 363.65 5.22 o -1 5 2 24.81 44.77 2.88 o 0 5 2 242.69 266.82 4.96 o 1 5 2 191.37 200.59 4.22 o 2 5 2 19.48 18.26 2.26 o 3 5 2 106.92 119.10 4.90 o 4 5 2 0.38 1.26 2.03 o 5 5 2 157.05 137.92 9.93 o -7 6 2 755.42 710.96 17.03 o -6 6 2 249.30 255.23 13.67 o -5 6 2 478.07 484.56 9.51 o -4 6 2 2143.11 2129.14 22.05 o -3 6 2 1306.35 1115.80 8.44 o -2 6 2 550.50 390.31 5.20 o -1 6 2 8737.64 8953.69 56.11 o 0 6 2 2012.84 1897.49 14.74 o 1 6 2 1319.40 1284.86 11.52 o 2 6 2 5421.14 5769.63 37.11 o 3 6 2 1460.16 1461.85 17.17 o 4 6 2 193.48 205.20 8.37 o 5 6 2 946.87 955.27 19.66 o -7 7 2 68.04 59.88 8.11 o -6 7 2 11.30 10.05 4.21 o -5 7 2 64.31 62.62 4.07 o -4 7 2 18.34 12.38 3.06 o -3 7 2 262.42 325.18 5.66 o -2 7 2 3.42 6.33 1.53 o -1 7 2 126.32 150.22 8.47 o 0 7 2 995.92 1154.90 16.69 o 1 7 2 2.48 3.95 1.16 o 2 7 2 15.13 9.17 1.61 o 3 7 2 0.00 0.00 1.53 o 4 7 2 56.66 58.64 5.46 o 5 7 2 15.75 16.39 3.95 o -7 8 2 622.83 615.99 20.74 o -6 8 2 748.36 750.94 45.91 o -5 8 2 1021.54 971.37 17.04 o -4 8 2 1900.41 1848.09 22.92 o -3 8 2 2747.79 2747.29 22.84 o -2 8 2 1295.98 1213.17 12.52 o -1 8 2 6141.06 6431.84 45.78 o 0 8 2 1266.98 1120.68 11.51 o 1 8 2 488.91 440.27 10.20 o 2 8 2 1185.46 1113.74 12.75 o 3 8 2 1594.63 1558.68 18.58 o 4 8 2 136.96 144.19 7.85 o 5 8 2 606.76 621.27 30.99 o -6 9 2 234.73 194.84 11.75 o -5 9 2 141.19 135.28 7.16 o -4 9 2 91.26 83.34 5.65 o -3 9 2 654.63 729.00 11.17 o -2 9 2 0.98 0.00 1.17 o -1 9 2 157.87 181.89 7.68 o 0 9 2 52.33 37.86 2.86 o 1 9 2 7.16 11.02 1.68 o 2 9 2 0.00 1.10 1.24 o 3 9 2 180.50 200.93 6.77 o 4 9 2 235.11 217.13 11.01 o 5 9 2 1.59 1.32 2.90 o -6 10 2 283.37 270.58 13.27 o -5 10 2 280.53 295.24 10.01 o -4 10 2 2453.93 2304.42 43.59 o -3 10 2 2305.93 2316.23 22.09 o -2 10 2 169.77 149.26 5.26 o -1 10 2 1450.96 1433.04 16.08 o 0 10 2 1469.88 1451.33 15.94 o 1 10 2 627.50 611.05 11.92 o 2 10 2 1156.42 1134.49 13.14 o 3 10 2 63.55 57.80 4.39 o 4 10 2 276.09 268.02 8.65 o 5 10 2 768.20 757.29 18.41 o -6 11 2 110.95 92.48 9.47 o -5 11 2 3.94 1.94 2.49 o -4 11 2 164.89 151.19 7.50 o -3 11 2 145.77 147.89 5.87 o -2 11 2 172.54 185.35 8.67 o -1 11 2 65.54 53.96 3.72 o 0 11 2 192.11 227.66 6.41 o 1 11 2 3.05 2.63 1.67 o 2 11 2 774.97 774.60 12.79 o 3 11 2 686.03 681.29 15.36 o 4 11 2 6.78 10.59 3.59 o -6 12 2 230.78 286.68 14.31 o -5 12 2 89.80 104.20 7.66 o -4 12 2 556.63 557.31 13.76 o -3 12 2 16.69 19.19 2.49 o -2 12 2 1331.09 1345.93 17.03 o -1 12 2 775.64 794.15 12.59 o 0 12 2 593.72 608.56 13.13 o 1 12 2 92.50 92.24 6.00 o 2 12 2 900.11 880.28 14.14 o 3 12 2 768.87 735.12 16.41 o 4 12 2 186.46 229.91 10.22 o -5 13 2 49.39 44.28 5.45 o -4 13 2 85.44 82.38 6.43 o -3 13 2 560.50 553.51 14.23 o -2 13 2 131.89 143.86 7.57 o -1 13 2 32.66 25.87 3.07 o 0 13 2 55.01 63.56 5.26 o 1 13 2 129.59 151.32 6.29 o 2 13 2 148.40 141.73 7.67 o 3 13 2 24.13 24.11 4.24 o 4 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