#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217042.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217042_Fobs loop_ _publ_author_name 'Pera\H-Fluoren-9-ylidenemethyl)thiophene ; _journal_coeditor_code FJ2086 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o274 _journal_volume 64 _journal_year 2008 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 20.7570 _cell_length_b 44.4340 _cell_length_c 5.6260 _exptl_crystal_F_000 2176.00 _reflns_d_resolution_high 0.7318 _[local]_cod_data_source_file fj2086Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' MI IN FDD2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 465.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/4, y+1/4, z+1/4' 'x+3/4, -y+3/4, z+1/4' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x+1/4, y+3/4, z+3/4' 'x+3/4, -y+5/4, z+3/4' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+3/4, y+1/4, z+3/4' 'x+5/4, -y+3/4, z+3/4' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+3/4, y+3/4, z+1/4' 'x+5/4, -y+5/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -7 18.88 -41.02 81.13 o 3 1 -7 7.28 -6.43 36.23 o 1 3 -7 9.49 -67.19 127.32 o 3 3 -7 51.07 -36.64 245.08 o 5 3 -7 59.07 87.12 139.23 o 7 3 -7 53.97 31.76 163.66 o 1 5 -7 1.73 -7.63 52.51 o 3 5 -7 94.63 155.60 105.06 o 5 5 -7 132.56 109.47 140.40 o 7 5 -7 129.21 142.72 113.47 o 1 7 -7 23.89 -53.82 56.68 o 3 7 -7 162.73 148.20 115.39 o 5 7 -7 129.08 121.98 103.04 o 7 7 -7 17.78 130.38 112.65 o 1 9 -7 323.44 341.18 108.82 o 3 9 -7 156.33 99.87 89.13 o 5 9 -7 67.30 -4.55 53.33 o 7 9 -7 0.10 6.24 48.02 o 9 9 -7 32.48 49.67 161.22 o 1 11 -7 134.73 116.21 118.92 o 3 11 -7 2.16 42.30 94.53 o 5 11 -7 79.74 99.01 93.91 o 7 11 -7 97.29 168.85 112.81 o 9 11 -7 16.01 121.32 176.69 o 1 13 -7 100.23 99.24 151.92 o 3 13 -7 169.45 259.87 120.17 o 5 13 -7 5.97 -62.58 92.99 o 7 13 -7 294.84 418.18 123.72 o 9 13 -7 59.05 291.50 183.20 o 1 15 -7 51.35 74.96 128.10 o 3 15 -7 67.54 44.78 157.96 o 5 15 -7 65.06 153.63 117.69 o 7 15 -7 120.65 60.66 162.02 o 5 17 -7 41.58 3.26 166.10 o 7 17 -7 74.95 79.80 165.29 o 7 19 -7 79.46 -21.98 65.14 o 2 0 -6 1616.13 1767.77 107.06 o 6 0 -6 255.12 284.11 87.24 o 10 0 -6 20.27 36.56 89.47 o 0 2 -6 1191.90 1238.58 102.20 o 2 2 -6 845.94 752.71 75.19 o 4 2 -6 327.12 309.21 69.35 o 6 2 -6 425.99 479.79 72.85 o 8 2 -6 209.20 180.09 62.46 o 10 2 -6 272.70 321.37 65.75 o 12 2 -6 118.50 136.62 77.10 o 2 4 -6 625.68 577.56 64.75 o 4 4 -6 700.08 731.63 67.49 o 6 4 -6 390.67 365.66 70.10 o 8 4 -6 221.99 232.83 68.71 o 10 4 -6 30.12 50.43 77.52 o 12 4 -6 628.97 736.44 88.21 o 0 6 -6 61.15 -13.84 14.66 o 2 6 -6 184.43 150.61 57.15 o 4 6 -6 100.67 98.25 57.10 o 6 6 -6 127.22 169.95 63.43 o 8 6 -6 30.34 -5.29 13.76 o 10 6 -6 238.81 294.95 106.82 o 12 6 -6 195.14 221.79 101.67 o 14 6 -6 12.55 -14.66 23.61 o 2 8 -6 949.92 919.64 86.25 o 4 8 -6 54.03 31.45 84.45 o 6 8 -6 350.90 390.58 61.85 o 8 8 -6 150.65 142.52 99.65 o 10 8 -6 61.36 69.26 105.96 o 12 8 -6 38.77 62.04 110.33 o 14 8 -6 155.23 197.86 153.08 o 0 10 -6 408.72 428.92 103.82 o 2 10 -6 149.10 166.24 70.83 o 4 10 -6 43.44 -15.78 50.37 o 6 10 -6 306.18 237.95 84.53 o 8 10 -6 24.39 42.39 97.47 o 10 10 -6 69.41 81.01 107.45 o 12 10 -6 24.85 57.54 109.25 o 14 10 -6 65.22 35.01 139.23 o 16 10 -6 3.98 53.74 160.40 o 2 12 -6 282.93 271.69 58.16 o 4 12 -6 29.11 -1.14 7.18 o 6 12 -6 18.21 7.39 16.68 o 8 12 -6 89.49 90.37 99.59 o 10 12 -6 29.61 37.30 106.89 o 12 12 -6 330.87 416.25 123.60 o 14 12 -6 32.40 59.44 158.77 o 16 12 -6 159.63 255.67 170.99 o 0 14 -6 58.44 9.44 49.63 o 2 14 -6 494.52 339.65 60.77 o 4 14 -6 165.20 197.32 80.42 o 6 14 -6 157.27 176.54 83.43 o 8 14 -6 16.44 -1.68 11.37 o 10 14 -6 3.59 45.63 102.47 o 12 14 -6 91.75 0.56 84.50 o 14 14 -6 45.18 201.11 157.15 o 16 14 -6 34.71 50.48 77.35 o 2 16 -6 1046.29 1104.63 70.63 o 4 16 -6 161.90 201.39 83.63 o 6 16 -6 45.32 94.69 85.64 o 8 16 -6 13.23 32.86 87.72 o 10 16 -6 24.46 -11.16 48.48 o 12 16 -6 4.68 -41.96 72.61 o 14 16 -6 8.84 -76.54 92.01 o 0 18 -6 149.61 147.24 86.52 o 2 18 -6 180.53 219.12 78.39 o 4 18 -6 78.28 85.46 98.45 o 6 18 -6 227.93 237.22 83.61 o 8 18 -6 33.81 23.67 127.36 o 10 18 -6 374.34 510.11 112.66 o 12 18 -6 16.04 -14.95 39.08 o 14 18 -6 15.94 41.53 859.01 o 2 20 -6 8.27 -23.13 24.01 o 4 20 -6 10.25 3.53 47.07 o 6 20 -6 137.38 134.42 89.38 o 8 20 -6 261.29 369.66 92.67 o 10 20 -6 328.58 385.05 126.08 o 12 20 -6 27.65 -21.95 95.73 o 0 22 -6 57.57 94.14 105.01 o 2 22 -6 305.14 285.07 83.97 o 4 22 -6 85.76 51.68 109.09 o 6 22 -6 115.08 235.01 85.82 o 8 22 -6 190.83 294.47 111.64 o 10 22 -6 179.73 176.31 120.17 o 12 22 -6 25.52 -35.83 81.42 o 2 24 -6 346.64 281.47 91.23 o 4 24 -6 88.44 26.00 82.27 o 6 24 -6 343.40 305.89 94.37 o 8 24 -6 76.87 126.38 122.57 o 10 24 -6 45.02 4.07 187.27 o 12 24 -6 18.88 21.17 167.73 o 0 26 -6 454.85 445.42 142.50 o 2 26 -6 20.77 -29.91 63.25 o 4 26 -6 168.01 238.24 93.35 o 6 26 -6 59.54 46.98 118.47 o 8 26 -6 50.19 245.08 149.82 o 12 26 -6 25.62 -6.51 35.01 o 2 28 -6 38.11 116.88 126.71 o 4 28 -6 59.13 34.20 151.45 o 6 28 -6 70.14 64.32 147.38 o 8 28 -6 263.54 399.81 179.14 o 4 30 -6 174.81 141.68 146.57 o 6 30 -6 244.58 277.66 179.14 o 8 30 -6 140.01 305.34 188.91 o 4 32 -6 55.07 41.53 132.72 o 6 32 -6 172.40 253.23 157.15 o 4 34 -6 33.45 -13.03 43.15 o 6 34 -6 43.53 172.62 169.36 o 1 1 -5 891.50 794.21 50.50 o 3 1 -5 294.96 230.95 43.10 o 5 1 -5 1107.95 1150.67 62.89 o 7 1 -5 16.23 -15.58 18.96 o 9 1 -5 618.08 651.00 40.76 o 11 1 -5 46.96 43.64 39.21 o 13 1 -5 8.46 -5.35 18.94 o 15 1 -5 261.43 249.21 48.13 o 17 1 -5 76.45 80.99 110.53 o 1 3 -5 759.98 826.78 49.25 o 3 3 -5 191.16 163.35 51.28 o 5 3 -5 4057.78 4450.91 84.19 o 7 3 -5 468.82 501.31 33.66 o 9 3 -5 1094.65 1236.77 45.07 o 11 3 -5 606.79 555.24 43.49 o 13 3 -5 50.32 39.53 44.60 o 15 3 -5 104.53 123.47 53.19 o 17 3 -5 438.62 448.02 88.65 o 1 5 -5 916.02 922.13 44.58 o 3 5 -5 446.84 397.18 53.85 o 5 5 -5 2817.40 2829.33 74.11 o 7 5 -5 86.00 64.27 32.95 o 9 5 -5 386.65 400.36 36.94 o 11 5 -5 1219.17 1307.70 47.76 o 13 5 -5 89.02 114.58 40.17 o 15 5 -5 53.17 37.82 36.33 o 17 5 -5 241.64 336.81 89.89 o 1 7 -5 1518.19 1569.07 54.29 o 3 7 -5 1296.29 1421.85 63.18 o 5 7 -5 591.03 570.07 55.49 o 7 7 -5 497.44 433.64 38.50 o 9 7 -5 251.92 207.59 32.82 o 11 7 -5 179.69 163.14 37.01 o 13 7 -5 199.20 159.82 46.91 o 15 7 -5 137.00 154.83 84.27 o 17 7 -5 45.09 11.67 56.29 o 19 7 -5 218.29 304.53 144.94 o 1 9 -5 1922.80 2053.43 70.10 o 3 9 -5 2275.82 2369.12 57.13 o 5 9 -5 1970.40 2106.36 56.29 o 7 9 -5 350.60 273.61 35.92 o 9 9 -5 1318.29 1522.50 61.14 o 11 9 -5 1253.96 1432.84 58.22 o 13 9 -5 128.46 118.81 61.63 o 15 9 -5 34.90 -9.59 73.27 o 17 9 -5 4.08 -13.97 20.04 o 19 9 -5 147.57 158.78 156.34 o 1 11 -5 169.39 89.02 40.23 o 3 11 -5 192.47 106.33 38.82 o 5 11 -5 773.32 681.55 43.67 o 7 11 -5 52.25 5.62 28.49 o 9 11 -5 1202.38 1293.49 59.08 o 11 11 -5 190.82 164.16 72.00 o 13 11 -5 89.96 79.35 68.78 o 15 11 -5 10.67 -6.53 13.42 o 17 11 -5 152.50 155.52 136.79 o 19 11 -5 13.68 22.80 49.67 o 1 13 -5 302.12 209.78 52.31 o 3 13 -5 532.14 513.65 79.05 o 5 13 -5 1329.98 1299.79 47.81 o 7 13 -5 303.32 289.18 38.03 o 9 13 -5 808.41 846.17 52.36 o 11 13 -5 348.51 307.18 73.48 o 13 13 -5 309.71 431.01 78.44 o 15 13 -5 174.20 229.58 101.52 o 17 13 -5 56.33 2.44 12.21 o 19 13 -5 6.58 67.58 146.56 o 1 15 -5 519.75 466.27 56.21 o 3 15 -5 1049.88 1104.70 57.96 o 5 15 -5 20.00 -8.53 16.78 o 7 15 -5 199.06 201.26 51.27 o 9 15 -5 429.56 449.74 68.76 o 11 15 -5 19.08 30.09 78.67 o 13 15 -5 122.94 43.58 74.43 o 15 15 -5 188.98 182.50 92.41 o 17 15 -5 154.87 149.01 147.38 o 19 15 -5 65.95 48.85 193.79 o 1 17 -5 88.83 70.78 70.77 o 3 17 -5 988.05 906.98 49.96 o 5 17 -5 383.21 348.99 43.58 o 7 17 -5 72.73 -10.16 18.90 o 9 17 -5 536.12 447.37 68.40 o 11 17 -5 938.65 1042.07 93.35 o 13 17 -5 40.85 47.62 84.77 o 15 17 -5 192.28 290.76 107.76 o 17 17 -5 14.97 -39.90 138.42 o 19 17 -5 137.59 211.70 175.88 o 1 19 -5 32.87 25.45 36.32 o 3 19 -5 217.83 175.90 43.89 o 5 19 -5 437.89 458.88 50.45 o 7 19 -5 38.55 12.06 69.59 o 9 19 -5 373.86 295.73 66.26 o 11 19 -5 73.60 142.24 99.19 o 13 19 -5 215.84 347.07 91.49 o 15 19 -5 3.14 -18.30 25.24 o 17 19 -5 12.17 34.20 154.70 o 19 19 -5 41.17 21.98 74.09 o 1 21 -5 162.33 128.00 51.07 o 3 21 -5 268.44 219.17 50.39 o 5 21 -5 87.58 105.55 46.16 o 7 21 -5 430.59 444.25 69.83 o 9 21 -5 307.77 287.30 70.82 o 11 21 -5 3.88 -23.93 45.01 o 13 21 -5 220.07 263.64 86.26 o 15 21 -5 97.03 267.97 130.28 o 17 21 -5 8.44 32.57 145.75 o 1 23 -5 13.71 -3.10 53.06 o 3 23 -5 85.32 140.34 50.47 o 5 23 -5 143.76 84.61 52.83 o 7 23 -5 90.67 38.65 97.39 o 9 23 -5 376.24 277.15 72.69 o 11 23 -5 154.32 270.36 90.03 o 13 23 -5 20.87 -15.02 79.03 o 15 23 -5 24.28 35.83 175.06 o 17 23 -5 91.65 114.81 152.26 o 1 25 -5 774.40 776.47 64.24 o 3 25 -5 734.13 729.87 61.71 o 5 25 -5 93.26 143.24 98.67 o 7 25 -5 97.22 75.16 76.52 o 9 25 -5 6.29 -1.74 53.87 o 11 25 -5 225.22 261.26 74.08 o 13 25 -5 0.68 -37.00 45.53 o 15 25 -5 135.00 234.50 154.71 o 1 27 -5 31.22 -0.78 40.76 o 3 27 -5 146.40 115.37 56.44 o 5 27 -5 292.32 315.66 87.27 o 7 27 -5 638.28 669.73 91.91 o 9 27 -5 334.67 353.91 75.46 o 11 27 -5 57.27 114.04 76.26 o 13 27 -5 76.03 76.88 106.38 o 15 27 -5 84.63 -4.07 1213.21 o 1 29 -5 228.46 200.33 62.03 o 3 29 -5 39.63 51.42 45.34 o 5 29 -5 211.66 222.37 77.71 o 7 29 -5 144.06 153.11 87.69 o 9 29 -5 165.45 196.17 74.79 o 11 29 -5 138.35 168.47 82.84 o 13 29 -5 44.91 70.02 147.38 o 1 31 -5 289.87 337.05 66.05 o 3 31 -5 17.61 41.54 81.73 o 5 31 -5 23.17 21.92 105.20 o 7 31 -5 142.66 169.57 90.11 o 9 31 -5 100.75 125.57 75.17 o 11 31 -5 74.87 117.34 110.02 o 13 31 -5 24.63 77.35 151.45 o 1 33 -5 365.25 364.09 67.80 o 3 33 -5 19.63 120.55 86.95 o 5 33 -5 152.78 131.12 93.23 o 7 33 -5 80.69 56.95 60.88 o 9 33 -5 5.61 4.63 22.90 o 11 33 -5 157.46 177.41 110.33 o 1 35 -5 21.26 75.36 95.94 o 3 35 -5 580.08 636.08 96.65 o 5 35 -5 25.16 102.31 108.68 o 7 35 -5 390.88 528.48 153.90 o 9 35 -5 239.09 164.48 159.60 o 1 37 -5 162.26 114.21 82.91 o 3 37 -5 91.98 135.20 88.93 o 5 37 -5 92.92 212.52 143.31 o 7 37 -5 86.08 11.40 27.68 o 9 37 -5 49.27 118.06 157.15 o 1 39 -5 99.47 91.19 146.56 o 3 39 -5 27.05 -62.70 86.31 o 5 39 -5 117.10 175.88 144.94 o 7 39 -5 276.24 258.12 156.34 o 1 41 -5 15.39 83.87 144.93 o 3 41 -5 43.70 142.49 149.82 o 5 41 -5 33.17 51.30 324.06 o 7 41 -5 10.72 -41.53 565.89 o 3 43 -5 193.05 382.70 160.41 o 5 43 -5 18.08 -19.54 19.54 o 3 45 -5 73.73 132.72 168.55 o 0 0 -4 5354.80 5194.94 106.60 o 4 0 -4 786.26 806.27 55.79 o 8 0 -4 1464.71 1510.07 80.25 o 12 0 -4 266.47 357.80 104.64 o 16 0 -4 447.28 409.04 90.68 o 20 0 -4 1020.00 1223.97 127.55 o 24 0 -4 47.98 191.34 172.62 o 2 2 -4 4317.40 4581.76 59.77 o 4 2 -4 3651.34 3685.96 46.74 o 6 2 -4 3124.09 3281.91 33.15 o 8 2 -4 1606.05 1709.37 36.97 o 10 2 -4 720.51 690.98 38.24 o 12 2 -4 1332.49 1318.62 58.55 o 14 2 -4 63.81 2.51 28.42 o 16 2 -4 138.07 116.68 54.69 o 18 2 -4 4.10 -25.85 25.85 o 20 2 -4 35.74 53.12 68.32 o 22 2 -4 66.67 110.00 99.88 o 24 2 -4 85.07 271.79 119.74 o 0 4 -4 599.79 572.38 50.55 o 2 4 -4 482.97 436.21 31.46 o 4 4 -4 286.92 223.21 28.76 o 6 4 -4 274.36 225.26 14.42 o 8 4 -4 180.89 176.98 25.11 o 10 4 -4 1465.60 1497.62 44.38 o 12 4 -4 900.14 806.15 50.03 o 14 4 -4 160.25 148.34 49.90 o 16 4 -4 14.38 -0.23 18.77 o 18 4 -4 193.25 245.24 64.25 o 20 4 -4 325.09 379.88 74.69 o 22 4 -4 235.81 360.12 112.81 o 2 6 -4 3869.44 4174.01 60.50 o 4 6 -4 2176.23 2132.16 38.34 o 6 6 -4 3208.50 3156.20 40.21 o 8 6 -4 4771.88 5214.08 56.35 o 10 6 -4 2292.26 2620.95 66.38 o 12 6 -4 800.34 779.21 47.35 o 14 6 -4 481.57 450.96 50.88 o 16 6 -4 65.94 76.93 58.08 o 18 6 -4 90.29 38.30 52.77 o 20 6 -4 56.49 7.52 85.01 o 22 6 -4 54.97 -10.59 56.18 o 0 8 -4 1573.38 1379.73 74.05 o 2 8 -4 1106.34 1155.84 40.74 o 4 8 -4 2006.93 2051.78 38.04 o 6 8 -4 209.83 217.96 21.79 o 8 8 -4 260.03 191.69 17.63 o 10 8 -4 133.39 120.45 32.02 o 12 8 -4 447.06 425.21 36.89 o 14 8 -4 190.09 182.15 45.49 o 16 8 -4 821.43 822.53 85.63 o 18 8 -4 231.69 179.47 88.70 o 20 8 -4 71.17 35.20 50.68 o 22 8 -4 94.51 109.11 166.10 o 2 10 -4 2293.00 2207.44 42.46 o 4 10 -4 1274.87 1323.23 34.59 o 6 10 -4 1088.78 1098.11 41.40 o 8 10 -4 2704.12 2764.02 42.12 o 10 10 -4 415.52 440.81 36.38 o 12 10 -4 2224.25 2255.02 50.15 o 14 10 -4 140.42 123.28 52.14 o 16 10 -4 487.72 456.05 61.32 o 18 10 -4 80.48 82.50 64.94 o 20 10 -4 186.14 214.23 74.51 o 22 10 -4 52.24 186.46 148.19 o 0 12 -4 2400.47 2608.95 91.67 o 2 12 -4 1853.79 1949.58 49.12 o 4 12 -4 675.44 656.11 29.85 o 6 12 -4 559.45 481.28 27.29 o 8 12 -4 221.04 194.01 24.54 o 10 12 -4 471.71 513.19 36.34 o 12 12 -4 1100.52 1052.51 46.61 o 14 12 -4 318.59 312.90 41.14 o 16 12 -4 513.67 428.69 61.33 o 18 12 -4 52.46 16.04 32.62 o 20 12 -4 35.80 35.45 98.56 o 22 12 -4 74.10 184.02 175.06 o 2 14 -4 1520.95 1386.67 44.71 o 4 14 -4 1255.64 1338.65 45.71 o 6 14 -4 4721.61 4837.14 50.23 o 8 14 -4 6328.37 6735.62 81.31 o 10 14 -4 153.34 115.28 29.61 o 12 14 -4 1302.95 1337.24 89.89 o 14 14 -4 309.87 274.60 40.85 o 16 14 -4 4.19 31.35 66.01 o 18 14 -4 293.32 336.02 73.49 o 20 14 -4 1.72 5.70 11.40 o 22 14 -4 7.13 21.98 153.07 o 0 16 -4 10812.61 11306.94 160.35 o 2 16 -4 1062.48 1007.14 45.60 o 4 16 -4 1870.23 1825.46 46.64 o 6 16 -4 877.87 907.26 37.84 o 8 16 -4 582.44 507.94 50.37 o 10 16 -4 6.72 0.68 10.94 o 12 16 -4 1488.92 1518.48 37.18 o 14 16 -4 252.99 212.95 55.15 o 16 16 -4 149.54 161.64 59.98 o 18 16 -4 42.64 66.11 99.50 o 20 16 -4 317.66 586.28 179.14 o 2 18 -4 142.63 142.26 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3 8366.97 8956.62 95.13 o 7 3 3 7341.73 7646.75 88.52 o 9 3 3 2182.58 2050.96 40.35 o 11 3 3 1548.62 1601.73 29.57 o 13 3 3 1993.37 2008.27 40.93 o 15 3 3 1905.20 1877.85 41.75 o 17 3 3 333.89 331.15 27.80 o 19 3 3 4.64 -39.85 39.85 o 21 3 3 153.78 132.87 75.27 o 23 3 3 25.65 62.96 81.88 o 1 5 3 10390.58 10706.96 55.52 o 3 5 3 4698.59 4686.96 34.19 o 5 5 3 1626.15 1763.90 27.70 o 7 5 3 1043.78 1030.64 32.95 o 9 5 3 755.68 691.52 30.14 o 11 5 3 3137.28 3100.63 48.53 o 13 5 3 1162.65 1167.63 37.18 o 15 5 3 3359.91 3373.67 71.29 o 17 5 3 461.51 393.15 38.48 o 19 5 3 117.28 5.02 41.21 o 21 5 3 125.18 22.49 77.65 o 23 5 3 32.89 -39.31 72.45 o 1 7 3 11065.25 11244.08 83.98 o 3 7 3 7058.06 7575.46 55.54 o 5 7 3 2061.69 2050.19 28.57 o 7 7 3 594.53 527.23 25.89 o 9 7 3 421.55 405.75 28.93 o 11 7 3 157.21 136.52 28.95 o 13 7 3 4249.89 4231.97 61.06 o 15 7 3 208.40 145.15 36.43 o 17 7 3 60.62 68.59 69.41 o 19 7 3 817.35 909.34 85.32 o 21 7 3 228.26 242.15 74.81 o 23 7 3 47.11 90.69 81.52 o 1 9 3 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1315.31 1480.96 42.57 o 11 9 5 1250.43 1435.98 62.41 o 13 9 5 130.58 85.26 51.35 o 15 9 5 32.82 33.29 76.41 o 17 9 5 3.41 -2.75 24.21 o 19 9 5 147.91 211.63 100.71 o 1 11 5 170.16 125.05 35.15 o 3 11 5 200.71 191.38 23.81 o 5 11 5 764.63 705.27 21.59 o 7 11 5 49.94 30.44 13.05 o 9 11 5 1209.33 1283.80 48.15 o 11 11 5 199.06 146.78 45.00 o 13 11 5 86.85 115.53 53.29 o 15 11 5 9.57 20.73 69.32 o 17 11 5 152.38 80.27 75.56 o 19 11 5 13.83 49.04 105.60 o 1 13 5 308.53 267.44 37.61 o 3 13 5 519.46 472.11 19.72 o 5 13 5 1323.20 1373.64 32.42 o 7 13 5 315.48 297.63 28.47 o 9 13 5 820.28 919.21 43.40 o 11 13 5 357.63 352.94 60.07 o 13 13 5 303.55 316.54 69.62 o 15 13 5 177.43 143.58 71.97 o 17 13 5 58.70 163.16 71.73 o 19 13 5 6.36 67.58 135.98 o 1 15 5 544.83 457.32 44.16 o 3 15 5 1064.21 1046.19 47.89 o 5 15 5 22.20 1.64 15.06 o 7 15 5 201.06 180.92 37.89 o 9 15 5 427.18 474.51 61.40 o 11 15 5 19.35 32.08 57.67 o 13 15 5 120.18 76.72 63.93 o 15 15 5 192.43 225.29 71.32 o 17 15 5 157.78 100.97 107.76 o 1 17 5 90.62 95.14 42.71 o 3 17 5 984.82 978.33 49.90 o 5 17 5 399.44 523.78 90.20 o 7 17 5 76.31 23.20 30.19 o 9 17 5 527.05 494.59 67.44 o 11 17 5 938.93 1034.47 70.22 o 13 17 5 40.84 61.59 70.35 o 15 17 5 186.74 107.47 94.14 o 17 17 5 15.32 36.78 138.52 o 1 19 5 33.36 22.58 20.57 o 3 19 5 208.83 191.19 47.62 o 5 19 5 431.11 450.74 90.39 o 7 19 5 44.60 -23.61 70.17 o 9 19 5 376.08 256.82 92.15 o 11 19 5 77.43 94.49 91.53 o 13 19 5 223.17 231.88 103.93 o 15 19 5 3.49 -13.92 49.46 o 17 19 5 12.13 2.00 121.48 o 1 21 5 161.59 82.12 48.09 o 3 21 5 270.33 238.29 52.77 o 5 21 5 85.73 131.78 59.18 o 7 21 5 443.26 552.75 102.20 o 9 21 5 320.03 211.63 120.11 o 11 21 5 4.72 -7.33 50.67 o 13 21 5 219.99 255.01 114.37 o 15 21 5 97.55 182.52 114.16 o 17 21 5 8.56 -14.69 40.33 o 1 23 5 11.20 57.37 68.15 o 3 23 5 80.81 100.15 96.08 o 5 23 5 146.88 92.91 74.90 o 7 23 5 92.65 94.45 114.81 o 9 23 5 371.95 423.36 101.62 o 11 23 5 152.47 211.54 102.57 o 13 23 5 18.59 84.27 100.76 o 15 23 5 25.95 49.89 161.69 o 17 23 5 94.84 176.69 176.69 o 1 25 5 757.57 698.60 84.63 o 3 25 5 738.09 719.09 114.83 o 5 25 5 84.89 97.62 92.33 o 7 25 5 93.68 -50.48 79.80 o 9 25 5 6.79 -62.70 100.15 o 11 25 5 227.27 153.93 102.56 o 13 25 5 0.73 3.94 135.99 o 15 25 5 132.78 142.09 115.15 o 17 25 5 40.69 116.43 168.55 o 1 27 5 31.30 -48.19 52.42 o 3 27 5 142.69 141.68 101.78 o 5 27 5 288.29 354.82 78.12 o 7 27 5 634.15 573.30 131.92 o 9 27 5 339.22 262.20 154.71 o 11 27 5 54.80 110.74 98.53 o 13 27 5 70.96 69.21 113.42 o 15 27 5 85.82 107.48 166.92 o 17 27 5 11.57 8.96 30.94 o 1 29 5 229.74 232.62 80.45 o 3 29 5 39.04 10.58 96.89 o 5 29 5 219.41 213.10 79.28 o 7 29 5 138.97 306.16 154.71 o 9 29 5 166.93 109.11 132.72 o 11 29 5 140.65 125.39 163.66 o 13 29 5 42.42 113.99 170.17 o 15 29 5 198.01 276.85 169.37 o 1 31 5 280.87 354.21 81.71 o 3 31 5 15.81 11.40 39.08 o 7 31 5 140.43 125.39 142.49 o 9 31 5 102.53 182.39 161.22 o 11 31 5 73.72 95.27 138.42 o 1 33 5 359.03 395.78 83.66 o 3 33 5 21.55 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349.86 536.61 166.93 o 8 24 6 75.83 173.43 138.42 o 10 24 6 44.64 48.04 425.03 o 12 24 6 20.01 105.85 153.89 o 0 26 6 450.32 578.16 147.39 o 2 26 6 19.87 -42.69 106.53 o 4 26 6 174.24 265.19 98.60 o 8 26 6 49.71 66.77 140.86 o 10 26 6 96.57 41.53 145.75 o 12 26 6 26.59 58.62 253.22 o 2 28 6 40.22 8.38 72.42 o 4 28 6 56.98 85.49 137.61 o 8 28 6 268.38 283.37 156.34 o 10 28 6 157.76 115.62 167.74 o 0 30 6 32.25 101.78 143.30 o 2 30 6 13.65 -26.87 251.60 o 4 30 6 173.72 232.88 151.45 o 8 30 6 139.33 169.36 175.88 o 2 32 6 101.29 61.07 142.49 o 4 32 6 56.98 57.81 166.92 o 8 32 6 1.91 88.75 166.10 o 2 34 6 7.51 28.50 143.30 o 4 34 6 31.82 75.72 156.33 o 1 1 7 19.39 46.41 174.24 o 1 3 7 9.70 25.24 172.62 o 1 5 7 1.99 52.92 260.55 o 1 7 7 21.60 78.98 175.87 o 3 7 7 160.05 222.29 184.02 o 1 9 7 325.33 452.94 114.98 o 3 9 7 151.21 262.19 180.76 o 1 11 7 135.76 223.46 112.69 o 3 11 7 2.36 -7.33 30.13 o 1 13 7 101.30 62.97 109.76 o 1 15 7 48.96 17.38 64.73 o 1 17 7 321.40 335.28 122.76 o 1 19 7 24.15 -23.32 56.78 o 1 21 7 34.23 89.03 119.47 o 1 23 7 24.73 81.83 111.69 o