#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/70/2217068.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217068_Fobs loop_ _publ_author_name 'Yin, Gangqiang' _publ_section_title ; Bis[\m-methylenebis(diphenylphosphine)]bis[(5-nitro-1,10-phenanthroline)silver(I)] bis(hexafluoridoantimonate) ; _journal_coeditor_code GK2121 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m264 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.936 _cell_angle_gamma 90.000 _cell_length_a 12.8034 _cell_length_b 23.3993 _cell_length_c 13.5580 _exptl_crystal_F_000 1880.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file gk2121Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 14 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 394.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 135376.08 140753.08 6905.56 o 4 0 0 28463.73 28575.53 330.24 o 6 0 0 17977.80 17710.38 179.96 o 8 0 0 2736.18 2690.06 76.75 o 10 0 0 1502.61 1650.64 83.26 o 12 0 0 3612.48 3640.77 182.52 o 2 1 0 18639.96 18594.19 110.98 o 3 1 0 747.43 895.81 29.22 o 4 1 0 7632.18 7600.13 86.07 o 5 1 0 51696.43 53453.31 249.53 o 6 1 0 3220.87 2912.63 46.87 o 7 1 0 1980.68 1855.41 41.85 o 8 1 0 5589.08 5363.34 79.45 o 9 1 0 71.40 76.12 21.46 o 10 1 0 611.44 578.09 36.91 o 11 1 0 978.74 876.19 51.63 o 12 1 0 210.39 200.18 43.26 o 13 1 0 3739.62 3828.86 122.67 o 2 2 0 53671.24 55846.01 265.88 o 3 2 0 1283.41 1528.20 32.13 o 4 2 0 335.92 361.00 16.56 o 5 2 0 2703.66 2747.36 41.13 o 6 2 0 6849.52 6320.17 66.63 o 7 2 0 6.00 36.50 12.88 o 8 2 0 441.88 489.07 29.64 o 9 2 0 372.84 449.60 29.53 o 10 2 0 2630.35 2575.76 63.54 o 11 2 0 3462.75 3265.37 82.41 o 12 2 0 27.89 65.42 36.64 o 13 2 0 422.04 458.89 53.35 o 1 3 0 33256.66 33904.04 255.28 o 2 3 0 67.33 115.74 10.49 o 3 3 0 40833.33 40944.31 207.71 o 4 3 0 13740.12 13665.81 135.09 o 5 3 0 582.80 662.62 21.94 o 6 3 0 30035.00 30729.66 218.25 o 7 3 0 37.00 60.02 12.20 o 8 3 0 12380.59 13025.95 109.64 o 9 3 0 712.35 820.90 42.19 o 10 3 0 13588.29 13620.96 164.28 o 11 3 0 4193.55 4121.58 96.79 o 12 3 0 4988.58 4673.77 135.92 o 13 3 0 43.18 62.64 23.69 o 0 4 0 5535.67 5750.82 75.96 o 1 4 0 42211.54 42431.65 261.86 o 2 4 0 8206.50 8382.44 82.89 o 3 4 0 6160.22 5531.91 68.63 o 4 4 0 17079.69 17411.17 149.55 o 5 4 0 24049.63 22950.45 136.15 o 6 4 0 2710.77 2723.05 40.48 o 7 4 0 39833.73 40559.76 218.30 o 8 4 0 48.47 88.82 16.61 o 9 4 0 25572.62 26046.44 211.33 o 10 4 0 788.64 705.23 51.84 o 11 4 0 9687.82 9637.29 212.14 o 12 4 0 111.22 65.93 28.74 o 13 4 0 2009.60 1799.04 93.17 o 1 5 0 21804.11 22276.90 231.92 o 2 5 0 4065.85 3871.45 44.74 o 3 5 0 448.22 537.62 12.85 o 4 5 0 324.83 324.90 32.03 o 5 5 0 208.74 164.42 20.23 o 6 5 0 14857.75 14812.46 109.43 o 7 5 0 503.78 530.42 21.80 o 8 5 0 4819.20 4821.58 92.34 o 9 5 0 1928.00 2026.69 84.89 o 10 5 0 5328.77 5175.97 105.41 o 11 5 0 1754.26 1786.86 71.26 o 12 5 0 3153.33 3110.40 100.42 o 13 5 0 921.08 868.32 99.84 o 0 6 0 11617.89 12017.35 187.11 o 1 6 0 13.35 33.35 9.89 o 2 6 0 3911.12 3839.62 60.49 o 3 6 0 7179.03 7102.34 70.87 o 4 6 0 844.21 789.37 24.17 o 5 6 0 4691.60 4757.96 59.31 o 6 6 0 737.03 752.47 49.67 o 7 6 0 2093.18 2131.43 62.71 o 8 6 0 2438.06 2453.63 62.88 o 9 6 0 5684.60 5969.80 135.87 o 10 6 0 2417.15 2394.96 76.99 o 11 6 0 65.45 108.90 24.90 o 12 6 0 922.79 1044.05 87.37 o 13 6 0 222.46 201.47 48.48 o 1 7 0 47679.71 48507.40 202.01 o 2 7 0 42.88 26.20 23.97 o 3 7 0 25451.85 25748.40 310.88 o 4 7 0 2757.38 2511.02 76.75 o 5 7 0 14279.80 14621.41 139.31 o 6 7 0 7392.17 7575.10 119.91 o 7 7 0 960.01 792.72 39.58 o 8 7 0 5288.24 5364.19 93.17 o 9 7 0 143.11 116.50 27.53 o 10 7 0 2293.18 2089.89 68.71 o 11 7 0 116.66 193.31 43.10 o 12 7 0 48.89 119.25 32.52 o 13 7 0 3774.58 3672.33 118.71 o 0 8 0 34952.15 34918.10 279.25 o 1 8 0 44.59 27.42 6.73 o 2 8 0 27503.24 27808.74 210.15 o 3 8 0 917.57 979.48 42.27 o 4 8 0 27377.87 27075.45 146.71 o 5 8 0 192.68 213.01 36.70 o 6 8 0 12075.76 12109.35 165.71 o 7 8 0 1288.41 1325.69 43.62 o 8 8 0 1265.51 1181.91 49.86 o 9 8 0 2139.41 2021.33 79.10 o 10 8 0 1229.97 1240.52 55.55 o 11 8 0 946.87 759.54 64.50 o 12 8 0 2430.17 2403.36 119.20 o 1 9 0 15874.37 16487.56 151.26 o 2 9 0 2072.83 2132.76 65.55 o 3 9 0 818.52 742.68 61.80 o 4 9 0 4372.00 4559.90 95.94 o 5 9 0 9399.79 9537.17 74.31 o 6 9 0 1661.99 1523.46 37.98 o 7 9 0 1.88 22.91 18.22 o 8 9 0 589.68 527.08 39.59 o 9 9 0 55.52 40.40 19.23 o 10 9 0 1898.30 1832.09 76.84 o 11 9 0 88.50 25.12 43.63 o 12 9 0 12.55 89.96 35.29 o 0 10 0 5807.56 5447.81 91.67 o 1 10 0 28.48 34.23 14.65 o 2 10 0 26958.96 27917.43 208.76 o 3 10 0 2714.01 2755.42 84.33 o 4 10 0 4217.30 4015.12 129.21 o 5 10 0 5343.44 5249.76 125.71 o 6 10 0 263.21 204.20 43.03 o 7 10 0 85.75 104.53 17.84 o 8 10 0 688.61 681.64 50.95 o 9 10 0 12816.22 13649.27 211.48 o 10 10 0 1444.19 1379.93 84.88 o 11 10 0 1835.01 1815.13 80.29 o 12 10 0 2433.31 2274.74 90.53 o 1 11 0 15614.79 15470.17 141.40 o 2 11 0 2353.71 2101.56 90.97 o 3 11 0 20559.69 20901.50 372.34 o 4 11 0 62549.60 65651.98 679.58 o 5 11 0 5062.84 5266.99 88.52 o 6 11 0 14544.01 15072.20 172.23 o 7 11 0 58.88 64.41 15.56 o 8 11 0 16139.31 16570.60 245.59 o 9 11 0 880.66 597.51 87.32 o 10 11 0 14180.89 14765.80 255.33 o 11 11 0 1415.00 1341.05 71.65 o 12 11 0 1082.16 933.88 73.83 o 0 12 0 505.97 732.35 34.24 o 1 12 0 3366.25 3197.28 110.58 o 2 12 0 571.86 720.11 23.56 o 3 12 0 13289.42 12819.03 188.29 o 4 12 0 86.72 44.57 22.81 o 5 12 0 18227.95 18175.58 219.21 o 6 12 0 186.81 141.42 31.89 o 7 12 0 985.16 974.87 75.19 o 8 12 0 2545.46 2608.09 99.93 o 9 12 0 16315.93 17191.75 276.18 o 10 12 0 1439.26 1412.78 99.03 o 11 12 0 2645.50 2585.60 120.68 o 12 12 0 156.59 149.27 34.69 o 1 13 0 2122.90 2161.43 40.47 o 2 13 0 5450.39 5617.63 130.70 o 3 13 0 717.78 739.67 63.23 o 4 13 0 997.30 1006.62 62.57 o 5 13 0 128.86 63.94 18.19 o 6 13 0 4706.20 4624.95 113.07 o 7 13 0 3594.28 3657.23 176.99 o 8 13 0 219.84 200.61 32.12 o 9 13 0 112.55 58.62 49.45 o 10 13 0 508.94 581.51 51.73 o 11 13 0 345.65 322.68 60.89 o 0 14 0 6753.66 6695.19 143.02 o 1 14 0 4715.73 4452.09 92.03 o 2 14 0 5147.12 4988.72 105.27 o 3 14 0 4261.21 3702.63 491.99 o 4 14 0 5791.32 5790.96 145.31 o 5 14 0 15496.62 15866.10 181.13 o 6 14 0 4779.31 4804.40 162.72 o 7 14 0 22444.80 23002.90 373.69 o 8 14 0 3660.21 3444.72 114.72 o 9 14 0 1346.33 1318.89 83.73 o 10 14 0 114.58 86.78 30.59 o 11 14 0 3264.67 3383.99 121.79 o 1 15 0 29273.13 30031.36 355.41 o 2 15 0 3453.92 3480.60 102.23 o 3 15 0 32886.73 34568.77 512.88 o 4 15 0 773.90 692.12 78.16 o 5 15 0 8568.52 8450.19 190.11 o 6 15 0 19721.71 20119.78 256.42 o 7 15 0 1817.33 1756.28 112.51 o 8 15 0 3978.55 4048.20 108.70 o 9 15 0 713.35 644.62 59.89 o 10 15 0 2289.17 2239.55 107.67 o 11 15 0 338.25 312.74 46.67 o 0 16 0 12269.84 13268.30 329.09 o 1 16 0 99.72 136.46 77.81 o 2 16 0 8466.96 8432.66 141.80 o 3 16 0 1744.66 1555.07 96.15 o 4 16 0 4825.10 4491.49 129.58 o 5 16 0 483.03 538.76 97.32 o 6 16 0 500.27 459.55 58.25 o 7 16 0 245.00 198.19 39.75 o 8 16 0 44.60 35.53 51.24 o 9 16 0 59.42 94.93 27.88 o 10 16 0 2150.25 2068.38 109.56 o 11 16 0 3181.76 3207.85 117.98 o 1 17 0 6088.76 6245.49 153.26 o 2 17 0 0.44 1.58 19.87 o 3 17 0 737.44 753.82 73.70 o 4 17 0 2509.03 2423.07 139.86 o 5 17 0 3415.44 3277.14 138.85 o 6 17 0 442.64 372.43 53.65 o 7 17 0 203.22 173.30 33.45 o 8 17 0 861.01 745.75 156.32 o 9 17 0 58.66 45.32 27.41 o 10 17 0 321.61 292.33 61.52 o 0 18 0 29691.62 31097.45 318.59 o 1 18 0 151.74 173.99 37.91 o 2 18 0 14036.46 14625.08 145.61 o 3 18 0 1994.62 2048.40 96.45 o 4 18 0 11708.95 11284.82 210.64 o 5 18 0 3587.10 3588.80 230.60 o 6 18 0 3073.47 2932.39 246.45 o 7 18 0 3033.72 2994.94 158.90 o 8 18 0 783.67 633.52 76.88 o 9 18 0 1423.09 1338.68 114.27 o 10 18 0 439.60 413.99 101.99 o 1 19 0 14926.76 15326.71 229.29 o 2 19 0 13.16 76.74 30.20 o 3 19 0 2882.94 2898.99 103.97 o 4 19 0 14379.34 14793.72 266.87 o 5 19 0 5568.19 5268.39 179.84 o 6 19 0 10412.36 10741.74 296.76 o 7 19 0 532.55 505.86 99.20 o 8 19 0 5235.45 5121.84 150.18 o 9 19 0 27.66 54.59 32.79 o 0 20 0 2280.46 2403.15 85.77 o 1 20 0 461.85 550.42 62.56 o 2 20 0 329.93 248.51 37.80 o 3 20 0 29.90 4.65 32.91 o 4 20 0 2245.81 2123.27 138.96 o 5 20 0 526.86 469.02 83.93 o 6 20 0 1528.11 1348.79 291.95 o 7 20 0 1.30 199.83 170.64 o 8 20 0 901.50 844.92 92.06 o 9 20 0 1323.04 1390.66 107.17 o 1 21 0 1103.81 1017.27 69.75 o 2 21 0 3262.20 3568.25 194.63 o 3 21 0 535.33 429.92 75.74 o 4 21 0 8.07 115.65 40.90 o 5 21 0 3819.15 3721.51 218.61 o 6 21 0 4098.64 4476.44 210.98 o 7 21 0 139.84 117.66 36.68 o 8 21 0 3929.87 3885.74 137.83 o 0 22 0 9325.89 9759.33 289.13 o 1 22 0 6629.59 6757.13 142.39 o 2 22 0 843.55 826.88 81.33 o 3 22 0 2771.18 2747.36 145.27 o 4 22 0 171.59 128.88 29.68 o 5 22 0 5144.56 4915.94 159.04 o 6 22 0 2133.61 2075.28 121.76 o 7 22 0 12480.33 12708.84 550.19 o 8 22 0 1212.64 1041.46 103.42 o 1 23 0 4216.94 4328.01 138.58 o 2 23 0 1603.31 1709.85 142.92 o 3 23 0 100.76 153.66 50.77 o 4 23 0 3.04 50.21 34.35 o 5 23 0 1426.97 1456.52 145.74 o 6 23 0 3066.65 3130.86 157.94 o 7 23 0 0.09 16.54 29.05 o 0 24 0 1545.85 1368.07 125.52 o 1 24 0 1360.32 1210.96 64.09 o 2 24 0 700.91 648.63 65.69 o 3 24 0 394.40 288.45 68.48 o 4 24 0 262.15 124.33 36.79 o 5 24 0 73.38 66.60 30.89 o 6 24 0 660.28 492.59 63.92 o 1 25 0 4454.41 4350.39 193.30 o 2 25 0 18.30 78.32 41.36 o 3 25 0 8147.41 8739.97 209.66 o 4 25 0 577.94 518.24 69.70 o 5 25 0 900.29 759.81 79.03 o 0 26 0 6163.29 6079.19 281.14 o 1 26 0 1169.02 1172.15 108.98 o 2 26 0 8248.93 8716.60 359.65 o 3 26 0 196.55 83.23 42.03 o 4 26 0 3193.16 3081.20 212.97 o 1 27 0 871.11 773.87 181.00 o 2 27 0 210.65 175.83 61.59 o 3 27 0 1901.33 1730.53 198.86 o -13 0 1 1035.05 1196.92 176.06 o -11 0 1 17838.10 18303.94 275.12 o -9 0 1 19350.18 19756.56 257.63 o -7 0 1 48300.68 48372.95 705.05 o -5 0 1 28079.15 27782.60 335.07 o -3 0 1 38693.20 39701.15 181.37 o 1 0 1 9486.55 9364.54 97.98 o 5 0 1 185.90 184.18 27.76 o 7 0 1 25791.19 26503.72 324.41 o 9 0 1 4776.46 4451.47 147.59 o 11 0 1 1263.09 1325.03 97.99 o -13 1 1 35.16 52.36 24.56 o -12 1 1 5809.43 5780.91 133.60 o -11 1 1 154.36 139.13 24.35 o -10 1 1 5651.63 5766.92 104.76 o -9 1 1 1522.74 1423.06 55.89 o -8 1 1 7360.12 7427.96 111.22 o -7 1 1 4995.55 4901.63 64.51 o -6 1 1 27533.70 26574.95 146.29 o -5 1 1 13720.10 13581.40 114.44 o -4 1 1 14376.80 14262.35 98.44 o -3 1 1 63199.50 63835.81 221.61 o -2 1 1 3949.38 3933.39 43.28 o 1 1 1 2329.57 2490.79 30.29 o 2 1 1 2596.30 2753.30 53.81 o 3 1 1 25502.09 26644.71 264.37 o 4 1 1 10088.22 10723.13 104.29 o 5 1 1 8390.57 8000.55 89.65 o 6 1 1 8773.50 9300.53 96.51 o 7 1 1 4002.34 3858.82 71.76 o 8 1 1 274.37 255.56 26.27 o 9 1 1 7535.02 7922.87 124.27 o 10 1 1 264.89 243.07 38.82 o 11 1 1 6593.79 6559.43 142.56 o 12 1 1 2491.09 2267.00 104.80 o -13 2 1 305.37 227.97 47.45 o -12 2 1 2059.27 1909.90 86.25 o -11 2 1 119.94 108.90 25.68 o -10 2 1 6075.52 6009.24 110.65 o -9 2 1 14814.57 15032.25 121.62 o -8 2 1 14143.78 14637.91 141.88 o -7 2 1 10.18 35.09 13.30 o -6 2 1 1912.12 1796.23 32.58 o -5 2 1 1763.94 1723.77 28.83 o -4 2 1 20535.68 20277.06 130.27 o -3 2 1 6924.24 7209.86 56.84 o -2 2 1 3257.59 3237.01 34.13 o 1 2 1 54.91 93.75 9.23 o 2 2 1 1276.27 1375.15 33.71 o 4 2 1 1510.32 1267.43 36.97 o 5 2 1 33141.08 33995.99 221.35 o 6 2 1 7430.10 7218.52 81.93 o 7 2 1 452.11 462.23 33.93 o 8 2 1 9368.77 9395.52 97.30 o 9 2 1 175.90 192.75 24.39 o 10 2 1 5981.30 5911.75 92.76 o 11 2 1 405.03 470.16 46.66 o 12 2 1 2494.23 2367.45 110.95 o -13 3 1 5172.35 5212.95 144.40 o -12 3 1 301.60 302.38 44.81 o -11 3 1 3749.53 3787.40 92.57 o -10 3 1 2799.99 2635.26 60.94 o -9 3 1 4181.10 4270.24 70.07 o -8 3 1 7038.01 7074.71 94.69 o -7 3 1 63.38 79.66 11.77 o -6 3 1 399.35 357.97 21.45 o -5 3 1 80.82 114.07 11.57 o -4 3 1 2002.57 1915.10 28.52 o -3 3 1 12263.25 11987.08 79.86 o -2 3 1 10953.79 11338.97 67.54 o -1 3 1 31507.62 31864.24 104.78 o 0 3 1 11053.84 11117.15 58.70 o 1 3 1 7498.88 7287.91 47.46 o 2 3 1 10642.39 10553.65 83.36 o 3 3 1 16482.00 16638.13 158.94 o 4 3 1 41103.69 41262.48 271.50 o 5 3 1 4547.62 4407.42 58.72 o 6 3 1 5611.07 5255.73 65.03 o 7 3 1 208.38 220.65 30.39 o 8 3 1 556.76 529.52 29.49 o 9 3 1 8506.29 8510.88 130.17 o 10 3 1 1298.81 1155.25 77.74 o 11 3 1 741.09 669.78 51.73 o 12 3 1 792.27 776.81 58.66 o -13 4 1 322.34 275.62 62.84 o -12 4 1 5415.91 5717.00 162.74 o -11 4 1 826.35 848.09 48.91 o -10 4 1 8047.03 8303.91 129.97 o -9 4 1 237.29 222.38 23.48 o -8 4 1 274.17 280.24 35.82 o -7 4 1 69.82 133.58 15.88 o -6 4 1 3436.56 3745.84 48.25 o -5 4 1 804.48 845.13 22.61 o -4 4 1 2628.03 2410.92 34.41 o -3 4 1 146.33 109.60 11.36 o -2 4 1 126020.61 127720.77 406.52 o -1 4 1 96.97 112.91 7.96 o 0 4 1 97149.88 100425.26 261.20 o 1 4 1 37309.47 37991.51 170.96 o 2 4 1 6651.38 6437.76 81.53 o 3 4 1 10300.36 10186.07 363.32 o 4 4 1 37190.91 36849.20 357.60 o 5 4 1 923.17 1013.88 45.07 o 6 4 1 1880.36 1871.91 49.09 o 7 4 1 3876.25 3916.00 79.64 o 8 4 1 112.70 76.99 17.87 o 9 4 1 600.85 565.64 44.92 o 10 4 1 1377.33 1207.82 58.49 o 11 4 1 1268.98 1188.58 62.25 o 12 4 1 278.58 245.43 47.51 o -13 5 1 678.95 622.52 66.03 o -12 5 1 875.59 872.59 61.97 o -11 5 1 981.59 820.47 50.35 o -10 5 1 2580.32 2429.28 74.42 o -9 5 1 740.85 801.25 36.20 o -8 5 1 1519.42 1490.11 53.36 o -7 5 1 648.19 666.82 22.58 o -6 5 1 368.04 390.44 27.53 o -5 5 1 338.24 367.56 16.94 o -4 5 1 5549.06 5823.01 59.83 o -3 5 1 307.81 314.48 17.77 o -2 5 1 14646.20 14496.73 114.38 o -1 5 1 1379.85 1440.04 22.23 o 0 5 1 24982.94 25410.34 158.47 o 1 5 1 506.37 550.72 15.96 o 2 5 1 49303.60 48963.71 180.87 o 3 5 1 37608.12 38517.52 210.36 o 4 5 1 5451.91 4843.38 71.36 o 5 5 1 50013.42 51806.51 380.92 o 6 5 1 16340.30 16380.92 173.41 o 7 5 1 473.75 460.61 40.37 o 8 5 1 2022.46 1915.16 45.65 o 9 5 1 9250.46 9609.24 187.36 o 10 5 1 386.50 350.85 46.59 o 11 5 1 4203.01 4458.53 93.65 o 12 5 1 284.35 206.69 37.33 o -13 6 1 84.59 70.17 24.19 o -12 6 1 681.50 637.70 53.95 o -11 6 1 168.51 169.09 27.72 o -10 6 1 304.52 243.20 28.35 o -9 6 1 1187.40 1372.95 52.15 o -8 6 1 2098.18 2090.81 51.51 o -7 6 1 14447.32 14971.20 103.48 o -6 6 1 314.63 316.58 29.27 o -5 6 1 4077.65 3822.39 37.86 o -4 6 1 9560.88 9502.69 94.92 o -3 6 1 5361.67 5187.75 61.95 o -2 6 1 6698.17 6480.38 69.86 o -1 6 1 30516.11 31079.13 190.83 o 0 6 1 8994.98 9187.04 109.40 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