#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:45:29 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181091 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/71/2217111.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217111_Fobs loop_ _publ_author_name 'Li, Zongxiao' 'Zhang, Xinli' 'Pu, Xiaohua' _publ_section_title ; Bis(4-chloro-2-formylphenolato)nickel(II) ; _journal_coeditor_code HK2368 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m215 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.896 _cell_angle_gamma 90.000 _cell_length_a 15.7653 _cell_length_b 5.6921 _cell_length_c 7.8869 _exptl_crystal_F_000 372.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file hk2368Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070612a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 188.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1045.09 1111.87 8.06 o 3 0 0 1390.55 1472.64 10.42 o 4 0 0 846.28 920.31 9.67 o 5 0 0 1324.06 1485.34 11.32 o 6 0 0 121.46 137.65 2.86 o 7 0 0 4455.59 4632.31 30.31 o 8 0 0 2.28 3.52 1.66 o 9 0 0 4100.74 4340.98 29.86 o 10 0 0 46.96 66.20 2.86 o 11 0 0 1220.73 1263.79 17.26 o 12 0 0 973.14 1037.95 16.01 o 13 0 0 239.14 238.03 7.77 o 14 0 0 17.73 11.87 3.01 o 15 0 0 3.36 3.30 5.55 o 16 0 0 524.84 510.78 19.40 o 17 0 0 5.45 4.35 5.67 o 18 0 0 256.98 293.99 14.38 o 1 1 0 508.50 483.72 4.57 o 2 1 0 237.39 317.30 3.64 o 3 1 0 2420.37 2262.15 11.87 o 4 1 0 931.17 1144.74 6.33 o 5 1 0 2194.11 2077.99 10.29 o 6 1 0 52.35 65.65 1.56 o 7 1 0 872.20 866.41 9.71 o 8 1 0 799.73 824.39 6.20 o 9 1 0 3.48 6.14 1.05 o 10 1 0 213.86 199.87 3.76 o 11 1 0 65.98 74.08 2.71 o 12 1 0 397.55 387.88 5.73 o 13 1 0 474.02 470.52 7.97 o 14 1 0 26.80 26.22 2.63 o 15 1 0 1.40 1.48 2.07 o 16 1 0 0.19 1.25 2.30 o 17 1 0 15.17 6.99 3.42 o 18 1 0 12.30 21.29 4.81 o 0 2 0 647.15 577.89 11.12 o 1 2 0 578.63 712.34 16.16 o 2 2 0 1089.22 1288.40 11.62 o 3 2 0 1156.34 1246.31 13.05 o 4 2 0 396.16 416.14 4.85 o 5 2 0 1940.20 2093.58 18.77 o 6 2 0 4599.89 4990.43 24.73 o 7 2 0 301.06 282.13 3.42 o 8 2 0 420.28 376.55 4.07 o 9 2 0 485.70 482.05 4.94 o 10 2 0 876.07 898.05 9.89 o 11 2 0 439.29 437.15 9.33 o 12 2 0 498.61 513.26 10.01 o 13 2 0 608.49 643.92 9.14 o 14 2 0 267.22 284.15 9.72 o 15 2 0 221.76 260.25 9.68 o 16 2 0 18.82 19.88 4.36 o 17 2 0 125.24 152.33 9.04 o 1 3 0 23.66 19.90 2.48 o 2 3 0 732.11 767.58 11.07 o 3 3 0 60.28 47.09 3.01 o 4 3 0 176.98 157.89 4.18 o 5 3 0 0.68 -0.89 1.04 o 6 3 0 11.95 5.45 1.38 o 7 3 0 12.17 8.60 1.38 o 8 3 0 118.38 110.76 2.77 o 9 3 0 6.74 5.14 1.59 o 10 3 0 24.51 23.62 3.27 o 11 3 0 77.75 66.59 3.91 o 12 3 0 1.73 0.13 1.93 o 13 3 0 4.93 2.85 2.33 o 14 3 0 7.26 7.55 3.62 o 15 3 0 4.86 0.66 3.30 o 16 3 0 10.40 14.32 4.46 o 0 4 0 100.13 82.16 6.60 o 1 4 0 1411.61 1434.40 18.30 o 2 4 0 578.12 585.69 17.92 o 3 4 0 1399.55 1374.84 24.47 o 4 4 0 1481.12 1481.32 56.89 o 5 4 0 460.71 418.99 7.74 o 6 4 0 378.52 344.38 6.09 o 7 4 0 226.67 208.61 4.51 o 8 4 0 1100.43 1060.65 12.02 o 9 4 0 6.15 1.57 1.81 o 10 4 0 69.12 59.72 3.73 o 11 4 0 33.19 23.12 3.23 o 12 4 0 42.79 50.12 6.56 o 13 4 0 176.37 144.63 6.05 o 14 4 0 65.46 42.55 6.67 o 15 4 0 121.72 106.12 7.52 o 1 5 0 0.02 -0.63 2.41 o 2 5 0 12.11 11.01 3.06 o 3 5 0 16.30 21.10 2.88 o 4 5 0 621.21 649.54 10.57 o 5 5 0 22.61 17.46 3.26 o 6 5 0 0.05 0.32 2.55 o 7 5 0 14.94 8.98 2.93 o 8 5 0 32.82 23.00 3.00 o 9 5 0 35.10 24.76 3.15 o 10 5 0 23.54 26.30 3.18 o 11 5 0 21.58 22.19 3.71 o 12 5 0 12.95 11.86 3.40 o 0 6 0 271.61 271.80 13.44 o 1 6 0 121.86 108.26 6.41 o 2 6 0 214.84 194.11 8.47 o 3 6 0 79.89 63.14 7.99 o 4 6 0 57.23 50.67 10.37 o 5 6 0 50.10 44.18 4.84 o 6 6 0 27.79 23.62 4.64 o 7 6 0 159.10 171.06 8.01 o 8 6 0 78.83 80.08 5.25 o -18 1 1 178.11 185.35 7.07 o -17 1 1 29.14 36.58 4.07 o -16 1 1 115.57 125.07 6.61 o -15 1 1 128.37 129.34 5.45 o -14 1 1 39.49 42.87 3.82 o -13 1 1 147.66 143.71 4.59 o -12 1 1 285.79 284.04 5.83 o -11 1 1 2251.25 2279.02 34.46 o -10 1 1 267.79 263.67 4.61 o -9 1 1 2346.27 2352.26 16.40 o -8 1 1 240.71 204.44 3.30 o -7 1 1 162.80 115.90 3.22 o -6 1 1 2963.48 3023.79 21.47 o -5 1 1 764.24 738.67 7.68 o -4 1 1 2636.79 2570.95 31.00 o -3 1 1 625.15 583.33 4.06 o -2 1 1 4016.83 4044.18 20.91 o -1 1 1 230.79 217.50 2.52 o 0 1 1 15486.31 15630.85 110.53 o 1 1 1 6115.28 6460.63 39.73 o 2 1 1 67.96 81.13 2.79 o 3 1 1 2657.09 2652.85 14.17 o 4 1 1 6.83 4.41 0.69 o 5 1 1 2548.00 2499.90 12.79 o 6 1 1 1938.12 2066.73 11.38 o 7 1 1 2553.98 2611.66 13.97 o 8 1 1 160.44 125.76 2.51 o 9 1 1 741.59 696.88 6.28 o 10 1 1 1041.18 1037.38 11.26 o 11 1 1 210.01 209.82 4.14 o 12 1 1 1607.65 1634.24 13.06 o 13 1 1 35.68 40.48 3.80 o 14 1 1 61.56 67.42 4.11 o 15 1 1 80.98 82.27 4.54 o 16 1 1 152.59 152.63 7.47 o 17 1 1 85.69 94.40 6.44 o 18 1 1 62.61 85.66 14.83 o -17 2 1 4.77 2.88 3.51 o -16 2 1 105.08 96.58 6.60 o -15 2 1 6.62 6.75 2.73 o -14 2 1 61.52 70.88 4.97 o -13 2 1 440.53 440.11 9.30 o -12 2 1 48.93 46.00 3.20 o -11 2 1 1.19 -1.10 1.94 o -10 2 1 113.45 113.17 3.39 o -9 2 1 161.70 147.37 3.62 o -8 2 1 274.42 277.47 3.44 o -7 2 1 977.45 951.94 12.14 o -6 2 1 58.75 50.25 2.04 o -5 2 1 1097.27 1075.44 8.79 o -4 2 1 491.50 568.29 5.83 o -3 2 1 401.09 438.07 5.60 o -2 2 1 328.07 383.99 3.98 o -1 2 1 2989.10 3251.55 18.90 o 0 2 1 1640.49 1714.43 10.01 o 1 2 1 361.24 397.29 4.51 o 2 2 1 1827.91 1764.18 11.93 o 3 2 1 1.73 7.08 4.40 o 4 2 1 745.93 716.38 6.61 o 5 2 1 5.84 4.23 1.10 o 6 2 1 553.44 625.49 5.99 o 7 2 1 12.98 4.95 1.11 o 8 2 1 1119.88 1192.29 8.61 o 9 2 1 183.29 152.75 3.96 o 10 2 1 63.78 64.56 2.56 o 11 2 1 217.70 208.34 5.88 o 12 2 1 10.23 4.16 2.16 o 13 2 1 8.17 6.29 2.42 o 14 2 1 66.98 61.26 5.72 o 15 2 1 88.59 96.49 6.34 o 16 2 1 4.15 3.82 3.37 o 17 2 1 91.32 96.40 7.31 o -16 3 1 41.90 52.67 6.45 o -15 3 1 122.35 122.37 7.34 o -14 3 1 306.94 319.83 10.98 o -13 3 1 110.44 110.86 4.32 o -12 3 1 354.46 367.53 6.07 o -11 3 1 10.85 3.81 1.90 o -10 3 1 378.19 387.44 6.48 o -9 3 1 2.00 -2.43 1.69 o -8 3 1 1123.36 1130.58 13.34 o -7 3 1 954.71 954.34 19.56 o -6 3 1 898.67 945.46 15.43 o -5 3 1 2938.45 3083.12 44.72 o -4 3 1 79.29 66.85 4.28 o -3 3 1 1835.98 1779.56 13.68 o -2 3 1 361.37 420.22 5.36 o -1 3 1 2373.09 2564.49 16.88 o 0 3 1 2.94 9.88 1.66 o 1 3 1 538.34 505.20 7.02 o 2 3 1 3411.75 3641.55 28.70 o 3 3 1 836.68 878.35 8.63 o 4 3 1 3154.95 3204.53 20.76 o 5 3 1 280.46 263.73 3.87 o 6 3 1 1843.47 1859.78 12.15 o 7 3 1 163.47 153.75 4.57 o 8 3 1 485.51 472.88 6.97 o 9 3 1 385.14 376.62 6.36 o 10 3 1 150.86 146.62 6.03 o 11 3 1 439.08 456.09 9.20 o 12 3 1 2.87 1.25 2.03 o 13 3 1 462.54 478.34 10.06 o 14 3 1 140.17 128.36 5.71 o 15 3 1 141.07 152.22 8.05 o 16 3 1 18.97 14.51 6.24 o -15 4 1 2.92 -4.05 3.84 o -14 4 1 24.64 24.28 5.05 o -13 4 1 28.30 19.32 3.39 o -12 4 1 15.75 11.97 2.50 o -11 4 1 10.64 8.03 2.17 o -10 4 1 116.52 105.50 4.03 o -9 4 1 76.57 60.13 5.63 o -8 4 1 12.54 11.42 2.71 o -7 4 1 325.47 333.83 7.46 o -6 4 1 12.58 7.81 1.82 o -5 4 1 85.23 84.97 5.66 o -4 4 1 121.20 114.31 4.21 o -3 4 1 133.94 139.14 4.55 o -2 4 1 2.75 -0.71 1.78 o -1 4 1 156.75 148.03 5.67 o 0 4 1 32.96 36.42 3.51 o 1 4 1 5.48 2.85 2.70 o 2 4 1 7.60 4.72 1.65 o 3 4 1 0.11 -1.67 1.34 o 4 4 1 644.03 676.91 8.55 o 5 4 1 41.11 42.35 3.52 o 6 4 1 132.01 122.43 3.96 o 7 4 1 3.06 0.99 1.49 o 8 4 1 249.31 258.05 5.74 o 9 4 1 4.64 4.25 2.29 o 10 4 1 54.65 40.24 3.92 o 11 4 1 66.69 67.53 4.87 o 12 4 1 0.19 -0.37 2.27 o 13 4 1 7.27 6.20 2.82 o 14 4 1 3.25 -3.50 2.33 o -12 5 1 98.97 106.13 4.72 o -11 5 1 133.60 138.49 5.14 o -10 5 1 148.66 146.73 5.20 o -9 5 1 116.63 120.91 5.38 o -8 5 1 197.00 188.70 11.48 o -7 5 1 292.70 304.25 8.42 o -6 5 1 47.56 56.38 4.37 o -5 5 1 101.21 110.73 9.51 o -4 5 1 584.60 599.32 13.32 o -3 5 1 650.32 718.71 13.85 o -2 5 1 346.37 346.27 9.57 o -1 5 1 241.93 225.66 10.97 o 0 5 1 259.68 263.90 12.40 o 1 5 1 159.45 165.48 5.83 o 2 5 1 116.54 124.04 4.84 o 3 5 1 222.40 242.09 7.20 o 4 5 1 602.80 628.22 9.02 o 5 5 1 357.50 362.03 6.94 o 6 5 1 43.16 45.49 3.73 o 7 5 1 192.33 192.18 6.32 o 8 5 1 404.91 419.16 11.70 o 9 5 1 118.49 116.72 6.70 o 10 5 1 24.81 33.72 5.03 o 11 5 1 73.37 87.53 9.64 o 12 5 1 98.52 100.42 5.87 o -8 6 1 0.08 2.59 2.81 o -7 6 1 1.64 2.26 4.04 o -6 6 1 3.59 1.99 4.58 o -5 6 1 17.80 14.80 5.76 o -4 6 1 81.73 74.21 6.30 o -3 6 1 51.91 57.63 5.80 o -2 6 1 58.41 69.03 4.94 o -1 6 1 20.81 16.27 3.13 o 0 6 1 12.89 15.95 3.05 o 1 6 1 0.04 -0.28 2.42 o 2 6 1 0.01 -2.56 2.36 o 3 6 1 9.41 9.85 3.07 o 4 6 1 4.46 3.67 2.60 o 5 6 1 0.07 -1.90 2.41 o 6 6 1 4.96 5.47 2.78 o 7 6 1 1.43 0.67 3.69 o 8 6 1 13.92 16.37 6.45 o -18 0 2 66.74 95.63 9.55 o -17 0 2 189.19 210.29 12.57 o -16 0 2 9.53 14.86 3.74 o -15 0 2 572.05 573.89 13.21 o -14 0 2 1.10 -2.05 2.02 o -13 0 2 657.80 643.57 13.15 o -12 0 2 14.81 17.09 5.09 o -11 0 2 1267.06 1343.31 27.19 o -10 0 2 409.35 427.49 13.93 o -9 0 2 463.70 519.45 6.98 o -8 0 2 1626.34 1635.59 27.70 o -7 0 2 1396.82 1481.33 17.53 o -6 0 2 4143.10 4429.39 34.94 o -5 0 2 16.30 28.16 5.24 o -4 0 2 1499.10 1682.59 15.47 o -3 0 2 224.71 259.56 4.76 o -2 0 2 154.41 178.28 4.03 o -1 0 2 254.05 282.07 4.96 o 0 0 2 5907.54 5968.35 87.78 o 1 0 2 35557.08 30137.69 319.52 o 2 0 2 9.59 28.52 2.56 o 3 0 2 6547.91 6099.06 48.17 o 4 0 2 753.92 623.69 6.79 o 5 0 2 1390.29 1163.50 10.60 o 6 0 2 2572.79 2472.29 18.82 o 7 0 2 1010.25 938.33 9.97 o 8 0 2 2813.30 2738.41 21.42 o 9 0 2 344.57 319.61 7.10 o 10 0 2 2333.33 2308.02 31.23 o 11 0 2 114.64 109.24 4.37 o 12 0 2 2069.68 2106.12 27.47 o 13 0 2 280.70 272.67 8.21 o 14 0 2 213.90 229.85 12.36 o 15 0 2 32.47 21.34 5.85 o 16 0 2 33.90 24.44 6.42 o 17 0 2 176.15 179.85 12.39 o 18 0 2 14.73 4.64 5.73 o -18 1 2 75.24 76.47 5.82 o -17 1 2 26.45 38.21 4.34 o -16 1 2 74.15 71.00 5.11 o -15 1 2 2.04 -0.67 2.73 o -14 1 2 9.90 11.45 5.17 o -13 1 2 456.49 423.06 11.15 o -12 1 2 535.18 519.72 9.14 o -11 1 2 321.06 309.14 6.70 o -10 1 2 500.95 476.44 5.77 o -9 1 2 173.46 166.00 4.27 o -8 1 2 9.91 10.52 1.90 o -7 1 2 1117.39 1257.40 14.70 o -6 1 2 72.53 76.09 2.76 o -5 1 2 284.53 278.42 3.53 o -4 1 2 281.58 254.01 3.36 o -3 1 2 677.17 755.05 6.38 o -2 1 2 552.14 490.13 4.89 o -1 1 2 2535.64 2835.71 20.60 o 0 1 2 8202.85 8314.32 44.07 o 1 1 2 6181.59 6299.35 34.61 o 2 1 2 65.30 51.07 4.83 o 3 1 2 121.66 117.82 3.52 o 4 1 2 14.41 9.92 1.29 o 5 1 2 439.40 479.50 4.23 o 6 1 2 2183.68 2162.62 12.14 o 7 1 2 0.67 -0.50 0.74 o 8 1 2 291.54 259.75 3.65 o 9 1 2 1.02 1.43 1.03 o 10 1 2 1.38 2.34 1.14 o 11 1 2 64.34 61.85 2.84 o 12 1 2 75.71 77.97 3.64 o 13 1 2 144.86 149.96 4.72 o 14 1 2 2.73 4.17 2.25 o 15 1 2 83.22 94.17 4.91 o 16 1 2 6.55 4.64 5.27 o 17 1 2 0.95 0.54 4.85 o -17 2 2 79.05 66.64 5.52 o -16 2 2 70.78 89.39 5.90 o -15 2 2 32.53 36.01 4.13 o -14 2 2 210.74 224.85 8.80 o -13 2 2 29.18 30.22 6.65 o -12 2 2 479.14 454.84 16.08 o -11 2 2 652.43 630.16 12.97 o -10 2 2 682.20 669.93 9.87 o -9 2 2 623.74 573.09 8.79 o -8 2 2 831.33 756.07 10.77 o -7 2 2 1498.94 1386.34 10.78 o -6 2 2 1132.54 1083.52 18.95 o -5 2 2 4302.26 4455.99 25.98 o -4 2 2 1324.21 1269.50 11.58 o -3 2 2 1762.77 1674.42 24.40 o -2 2 2 2844.69 2879.92 46.59 o -1 2 2 2108.12 2224.29 18.57 o 0 2 2 1179.89 1191.67 9.09 o 1 2 2 219.69 225.86 3.34 o 2 2 2 906.72 947.77 13.80 o 3 2 2 156.30 173.13 4.05 o 4 2 2 663.80 705.69 12.36 o 5 2 2 246.36 264.12 3.51 o 6 2 2 1390.79 1489.14 10.34 o 7 2 2 1291.65 1387.52 12.35 o 8 2 2 12.16 11.15 1.72 o 9 2 2 218.91 221.44 4.32 o 10 2 2 273.43 274.43 8.37 o 11 2 2 344.76 351.17 6.62 o 12 2 2 73.82 77.59 4.17 o 13 2 2 235.80 252.96 7.12 o 14 2 2 325.89 354.70 8.60 o 15 2 2 177.74 194.69 8.50 o 16 2 2 106.25 121.24 7.23 o 17 2 2 45.09 75.91 14.21 o -16 3 2 5.02 6.30 3.88 o -15 3 2 2.84 1.68 2.90 o -14 3 2 0.83 3.56 4.64 o -13 3 2 6.27 9.11 3.79 o -12 3 2 0.08 -0.19 1.77 o -11 3 2 19.85 18.10 4.02 o -10 3 2 0.33 -2.40 1.60 o -9 3 2 303.24 296.33 6.95 o -8 3 2 23.88 21.50 3.06 o -7 3 2 292.20 270.69 9.36 o -6 3 2 33.44 43.06 2.42 o -5 3 2 45.43 59.17 2.21 o -4 3 2 3.12 -0.68 1.05 o -3 3 2 318.06 257.42 4.26 o -2 3 2 91.99 73.24 2.07 o -1 3 2 483.14 469.30 6.04 o 0 3 2 108.07 75.76 2.18 o 1 3 2 183.80 138.67 3.89 o 2 3 2 8.09 2.52 1.42 o 3 3 2 105.19 125.11 4.01 o 4 3 2 237.52 205.17 5.06 o 5 3 2 26.94 17.97 2.27 o 6 3 2 11.58 17.49 2.33 o 7 3 2 62.23 69.92 3.15 o 8 3 2 22.65 13.34 2.46 o 9 3 2 0.31 -0.76 1.43 o 10 3 2 9.06 15.24 2.80 o 11 3 2 0.12 0.92 2.02 o 12 3 2 65.87 66.51 4.66 o 13 3 2 4.80 4.98 2.62 o 14 3 2 15.03 24.28 3.67 o 15 3 2 0.03 -3.97 3.20 o 16 3 2 5.20 4.94 3.62 o -14 4 2 226.25 214.63 13.62 o -13 4 2 91.15 88.99 4.42 o -12 4 2 179.53 170.40 5.26 o -11 4 2 35.49 39.38 8.76 o -10 4 2 35.11 28.22 4.42 o -9 4 2 40.56 42.31 3.87 o -8 4 2 64.29 58.40 4.15 o -7 4 2 964.18 972.49 14.46 o -6 4 2 87.64 77.29 4.15 o -5 4 2 678.80 670.48 8.04 o -4 4 2 256.90 247.47 4.86 o -3 4 2 438.27 422.29 6.29 o -2 4 2 441.43 446.41 6.51 o -1 4 2 236.54 233.69 5.55 o 0 4 2 508.84 516.41 8.24 o 1 4 2 78.64 78.20 3.11 o 2 4 2 1315.84 1387.06 31.98 o 3 4 2 567.09 582.24 11.14 o 4 4 2 1972.14 2019.83 19.58 o 5 4 2 1242.29 1281.83 31.78 o 6 4 2 203.85 202.10 5.80 o 7 4 2 301.52 310.75 7.25 o 8 4 2 293.43 313.14 7.43 o 9 4 2 509.70 499.25 12.33 o 10 4 2 34.71 37.02 3.88 o 11 4 2 204.79 193.97 6.73 o 12 4 2 53.69 60.25 4.97 o 13 4 2 100.67 99.58 8.38 o 14 4 2 137.43 119.62 5.99 o -12 5 2 15.18 9.63 3.17 o -11 5 2 41.06 29.78 7.73 o -10 5 2 7.11 4.21 2.70 o -9 5 2 24.90 28.89 3.69 o -8 5 2 0.11 -0.37 2.43 o -7 5 2 31.12 31.21 10.08 o -6 5 2 13.42 11.91 2.73 o -5 5 2 6.69 3.95 2.71 o -4 5 2 27.55 22.74 2.57 o -3 5 2 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