#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/71/2217176.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217176_Fobs loop_ _publ_author_name 'Du, Jian-Long' 'Zhang, Shu-Ming' _publ_section_title ; Bis[\m-2,3-bis(imidazol-1-ylmethyl)quinoxaline]disilver(I) bis(tetrafluoridoborate) ; _journal_coeditor_code LH2577 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m181 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.350 _cell_angle_beta 76.603 _cell_angle_gamma 73.208 _cell_length_a 8.5398 _cell_length_b 9.3110 _cell_length_c 12.1040 _exptl_crystal_F_000 479.90 _reflns_d_resolution_high 0.7988 _[local]_cod_data_source_file lh2577Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 181.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 185.16 224.45 8.91 o 2 0 0 2775.11 2925.90 44.14 o 3 0 0 36.54 23.18 6.44 o 4 0 0 40.48 53.07 8.49 o 5 0 0 853.92 847.25 38.92 o 6 0 0 21.35 6.24 10.49 o 7 0 0 11.83 5.24 12.43 o 8 0 0 227.97 244.31 22.31 o 9 0 0 0.17 12.35 16.07 o 10 0 0 116.45 76.85 34.58 o -9 1 0 0.10 -3.58 17.72 o -8 1 0 130.34 127.51 19.01 o -7 1 0 63.66 45.26 13.21 o -6 1 0 1.08 -9.78 9.78 o -5 1 0 954.92 894.65 26.40 o -4 1 0 642.76 614.41 19.90 o -3 1 0 2198.44 2145.40 38.03 o -2 1 0 16129.70 17352.94 256.43 o -1 1 0 119.86 78.73 8.15 o 0 1 0 15931.63 16116.37 304.27 o 1 1 0 30.92 61.03 6.56 o 2 1 0 782.15 847.29 18.89 o 3 1 0 2507.47 2462.58 42.01 o 4 1 0 169.99 184.25 14.18 o 5 1 0 2324.54 2469.21 119.22 o 6 1 0 285.66 302.01 18.81 o 7 1 0 222.97 206.26 19.56 o 8 1 0 187.37 207.92 20.97 o 9 1 0 13.63 43.52 17.26 o 10 1 0 34.24 49.19 21.18 o -9 2 0 2.69 8.87 34.64 o -8 2 0 121.63 135.14 19.36 o -7 2 0 141.34 172.98 19.34 o -6 2 0 14.90 17.54 19.93 o -5 2 0 760.97 722.43 25.29 o -4 2 0 1517.03 1573.41 33.10 o -3 2 0 3711.46 3752.42 59.85 o -2 2 0 6021.45 6060.36 85.54 o -1 2 0 455.20 408.65 18.79 o 0 2 0 30.89 23.56 8.35 o 1 2 0 17.86 40.49 8.52 o 2 2 0 2560.04 2766.14 66.60 o 3 2 0 7396.27 7497.50 254.41 o 4 2 0 48.64 44.82 9.08 o 5 2 0 685.31 686.09 30.43 o 6 2 0 788.21 753.49 30.68 o 7 2 0 40.29 42.68 14.50 o 8 2 0 296.03 300.24 23.97 o 9 2 0 21.24 30.08 16.32 o 10 2 0 2.76 -16.81 16.81 o -9 3 0 0.06 -10.44 27.80 o -8 3 0 124.50 106.28 19.65 o -7 3 0 123.27 107.08 17.48 o -6 3 0 0.41 -10.58 11.00 o -5 3 0 1094.77 1030.94 41.85 o -4 3 0 376.71 349.02 12.55 o -3 3 0 1444.60 1454.45 31.69 o -2 3 0 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