#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/71/2217189.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217189_Fobs loop_ _publ_author_name 'Nayak, Susanta K.' 'Chandrasekhar, S.' 'Row, T. N. Guru' _publ_section_title ; 1,1'-Binaphthalene-2,2'-diyl hydrogen phosphate ; _journal_coeditor_code LN2013 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o256 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 87.710 _cell_angle_beta 88.074 _cell_angle_gamma 83.952 _cell_length_a 14.2152 _cell_length_b 14.6480 _cell_length_c 15.6397 _exptl_crystal_F_000 1440.00 _reflns_d_resolution_high 0.8201 _[local]_cod_data_source_file ln2013Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' skn19_m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 311.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8598.69 -6.28 6.28 o 2 0 0 6054.39 6482.95 78.83 o 3 0 0 667.52 652.07 20.86 o 4 0 0 97101.04 103344.41 646.14 o 5 0 0 301.93 259.79 19.19 o 6 0 0 6674.13 6733.77 96.73 o 7 0 0 1574.37 1641.67 44.73 o 8 0 0 2646.20 2551.38 89.47 o 9 0 0 41.63 76.75 13.90 o 10 0 0 227.61 195.88 32.39 o 11 0 0 452.41 485.02 49.58 o 12 0 0 1363.59 1326.19 71.90 o 13 0 0 356.92 296.33 42.72 o 14 0 0 11.63 27.78 18.70 o 15 0 0 195.26 272.11 57.53 o 16 0 0 250.98 362.16 61.33 o 17 0 0 3.86 26.39 29.93 o -17 1 0 58.44 69.79 51.32 o -16 1 0 1.23 -22.63 30.10 o -15 1 0 235.73 165.64 49.26 o -14 1 0 1051.75 1075.25 79.34 o -13 1 0 797.56 790.79 63.98 o -12 1 0 3655.28 3526.38 196.86 o -11 1 0 895.33 861.32 61.09 o -10 1 0 80.49 61.85 23.02 o -9 1 0 1665.87 1589.40 217.53 o -8 1 0 25969.42 26954.47 180.63 o -7 1 0 923.56 953.72 43.10 o -6 1 0 1246.21 1263.39 34.79 o -5 1 0 1566.12 1537.85 34.71 o -4 1 0 64854.16 72547.81 237.13 o -3 1 0 3122.89 2867.09 53.01 o -2 1 0 24741.70 26797.86 135.09 o -1 1 0 3001.06 3467.21 37.67 o 1 1 0 201.43 174.94 11.24 o 2 1 0 31130.04 33484.38 143.76 o 3 1 0 7217.34 6815.31 59.84 o 4 1 0 55379.66 54138.63 325.58 o 5 1 0 11827.08 12809.15 126.84 o 6 1 0 673.66 724.51 35.49 o 7 1 0 5546.61 5423.04 95.83 o 8 1 0 6914.14 7557.35 119.14 o 9 1 0 556.98 558.69 33.24 o 10 1 0 2371.42 2159.30 61.57 o 11 1 0 2044.25 1628.56 68.57 o 12 1 0 246.13 251.54 36.91 o 13 1 0 728.85 749.52 64.16 o 14 1 0 112.52 73.79 48.91 o 15 1 0 100.95 165.29 49.33 o 16 1 0 5.39 10.78 26.97 o 17 1 0 0.40 61.82 39.12 o -16 2 0 36.76 39.51 25.16 o -15 2 0 2.64 -18.76 18.76 o -14 2 0 403.46 421.07 51.71 o -13 2 0 96.30 122.27 27.52 o -12 2 0 86.69 72.05 26.30 o -11 2 0 17.50 44.96 19.76 o -10 2 0 135.62 119.32 33.31 o -9 2 0 5374.45 5272.70 119.92 o -8 2 0 63.23 67.42 10.44 o -7 2 0 3333.24 3283.83 54.89 o -6 2 0 9664.42 9766.99 131.72 o -5 2 0 5.95 10.11 5.25 o -4 2 0 14439.23 14000.20 93.26 o -3 2 0 75208.38 76456.14 232.71 o -2 2 0 2017.91 2231.54 34.10 o -1 2 0 3776.78 4177.27 48.95 o 0 2 0 5211.18 5529.69 51.46 o 1 2 0 22705.53 24373.41 122.08 o 2 2 0 27.02 45.28 10.83 o 3 2 0 1507.46 1333.84 30.31 o 4 2 0 1000.74 890.68 27.56 o 5 2 0 3219.23 3193.30 54.18 o 6 2 0 0.85 -7.60 9.03 o 7 2 0 0.56 -2.38 10.47 o 8 2 0 0.48 7.68 10.57 o 9 2 0 876.22 836.32 39.61 o 10 2 0 432.51 490.71 37.34 o 11 2 0 2.42 -13.06 15.22 o 12 2 0 1281.04 1185.47 68.67 o 13 2 0 34.25 84.48 32.88 o 14 2 0 56.76 75.77 39.85 o 15 2 0 393.01 333.28 61.50 o 16 2 0 6.53 -10.82 29.94 o 17 2 0 59.49 -2.14 40.79 o -16 3 0 22.95 52.35 30.50 o -15 3 0 234.64 193.28 35.64 o -14 3 0 9.12 -20.07 37.07 o -13 3 0 314.00 351.66 59.60 o -12 3 0 2.86 10.73 17.96 o -11 3 0 1489.24 1445.81 73.38 o -10 3 0 901.25 851.66 59.92 o -9 3 0 14.04 -4.39 14.55 o -8 3 0 997.01 1052.40 55.27 o -7 3 0 2253.27 2132.75 43.18 o -6 3 0 538.14 550.24 22.33 o -5 3 0 771.15 703.07 27.78 o -4 3 0 14594.32 15177.89 108.15 o -3 3 0 4263.10 4249.03 55.15 o -2 3 0 6299.14 6729.55 79.00 o -1 3 0 586.25 517.47 49.52 o 0 3 0 45163.14 48960.81 206.49 o 1 3 0 73517.01 75338.71 307.86 o 2 3 0 7702.46 8064.16 63.05 o 3 3 0 3668.19 3361.70 45.00 o 4 3 0 2006.55 2107.41 40.56 o 5 3 0 87.03 55.93 13.68 o 6 3 0 50.02 34.17 12.99 o 7 3 0 62.24 45.91 15.21 o 8 3 0 336.48 338.31 28.25 o 9 3 0 130.65 118.26 19.96 o 10 3 0 11.95 6.93 12.39 o 11 3 0 444.92 491.53 39.81 o 12 3 0 766.70 826.24 87.41 o 13 3 0 576.04 478.49 69.89 o 14 3 0 0.03 26.48 31.21 o 15 3 0 18.59 78.64 38.44 o 16 3 0 0.35 35.89 42.52 o 17 3 0 173.66 96.41 40.93 o -16 4 0 91.58 69.31 34.56 o -15 4 0 31.36 45.53 50.69 o -14 4 0 70.41 94.42 26.91 o -13 4 0 581.69 661.65 66.18 o -12 4 0 434.16 453.38 52.64 o -11 4 0 51.85 79.07 23.24 o -10 4 0 417.78 384.29 48.24 o -9 4 0 854.09 928.66 58.63 o -8 4 0 1040.38 1015.01 55.76 o -7 4 0 268.59 267.83 21.69 o -6 4 0 440.29 397.61 24.39 o -5 4 0 428.32 454.10 26.29 o -4 4 0 22.04 35.03 11.32 o -3 4 0 1869.98 2221.02 53.65 o -2 4 0 160.19 177.51 22.09 o -1 4 0 857.79 736.28 46.07 o 0 4 0 18448.86 19648.88 120.55 o 1 4 0 1065.48 1010.45 29.09 o 2 4 0 245.32 223.38 15.58 o 3 4 0 1333.69 1423.49 31.89 o 4 4 0 8.23 -1.24 8.81 o 5 4 0 4892.60 4823.59 66.29 o 6 4 0 34.61 104.92 17.32 o 7 4 0 1403.69 1474.63 45.25 o 8 4 0 329.07 301.76 28.23 o 9 4 0 689.40 706.44 38.65 o 10 4 0 163.59 195.76 33.05 o 11 4 0 916.17 900.79 64.16 o 12 4 0 50.37 54.23 33.76 o 13 4 0 107.76 244.86 84.83 o 14 4 0 2.29 -25.11 25.11 o 15 4 0 52.31 27.20 32.16 o 16 4 0 178.50 294.49 54.19 o 17 4 0 19.43 28.89 50.53 o -16 5 0 14.10 40.79 31.87 o -15 5 0 5.50 92.48 30.56 o -14 5 0 22.91 82.30 38.33 o -13 5 0 148.23 132.56 30.36 o -12 5 0 62.25 39.12 27.17 o -11 5 0 64.08 16.98 31.43 o -10 5 0 36.14 35.10 20.28 o -9 5 0 964.79 921.67 59.33 o -8 5 0 1382.75 1254.17 61.08 o -7 5 0 207.56 203.77 30.31 o -6 5 0 2619.97 2507.23 56.19 o -5 5 0 241.27 289.05 25.15 o -4 5 0 4265.78 4222.44 70.74 o -3 5 0 2589.29 2221.12 50.55 o -2 5 0 18.80 -1.35 8.88 o -1 5 0 284.53 251.45 21.14 o 0 5 0 8.09 -2.72 10.10 o 1 5 0 8500.77 8469.32 83.39 o 2 5 0 6957.68 6869.29 73.47 o 3 5 0 554.06 621.93 23.39 o 4 5 0 467.04 414.98 23.69 o 5 5 0 6884.13 6794.91 76.93 o 6 5 0 2002.95 2198.14 48.89 o 7 5 0 1157.86 1260.57 41.00 o 8 5 0 23.32 49.72 13.85 o 9 5 0 527.91 574.64 49.19 o 10 5 0 84.30 118.35 28.98 o 11 5 0 1.92 21.07 20.55 o 12 5 0 761.92 759.90 63.33 o 13 5 0 7.23 -7.02 22.90 o 14 5 0 0.42 28.08 31.75 o 15 5 0 58.76 251.56 89.23 o 16 5 0 20.29 44.67 39.16 o 17 5 0 5.01 50.32 40.53 o -15 6 0 2.26 25.14 35.61 o -14 6 0 0.01 -37.81 41.89 o -13 6 0 94.46 51.83 52.42 o -12 6 0 686.55 609.59 61.52 o -11 6 0 725.76 708.06 66.53 o -10 6 0 147.86 123.92 33.18 o -9 6 0 553.90 585.36 55.85 o -8 6 0 249.37 287.27 45.15 o -7 6 0 207.45 225.69 35.45 o -6 6 0 677.55 678.37 36.57 o -5 6 0 552.36 655.38 37.15 o -4 6 0 41.48 77.85 18.38 o -3 6 0 6688.24 6593.74 93.69 o -2 6 0 1959.13 1980.38 61.24 o -1 6 0 498.68 506.90 29.89 o 0 6 0 9768.70 9780.75 99.45 o 1 6 0 574.56 509.37 26.66 o 2 6 0 1440.53 1329.84 37.14 o 3 6 0 1054.44 1050.65 31.84 o 4 6 0 789.02 869.14 29.20 o 5 6 0 5232.15 5654.17 74.47 o 6 6 0 800.61 757.09 30.03 o 7 6 0 165.58 165.02 20.93 o 8 6 0 140.65 155.22 31.87 o 9 6 0 3304.67 3188.15 98.40 o 10 6 0 12.50 -1.20 20.06 o 11 6 0 1157.97 1164.49 70.04 o 12 6 0 700.34 777.91 66.67 o 13 6 0 121.81 166.82 51.01 o 14 6 0 0.09 -27.58 27.58 o 15 6 0 4.99 -25.16 25.16 o 16 6 0 0.10 44.31 32.53 o -15 7 0 22.74 11.86 38.33 o -14 7 0 37.62 41.89 30.01 o -13 7 0 98.61 98.01 39.26 o -12 7 0 0.83 22.43 28.43 o -11 7 0 270.30 280.77 35.72 o -10 7 0 63.35 38.55 23.73 o -9 7 0 413.02 467.08 58.25 o -8 7 0 1980.24 1919.11 85.30 o -7 7 0 522.29 462.33 49.02 o -6 7 0 14.36 46.94 17.10 o -5 7 0 473.95 516.51 35.45 o -4 7 0 1167.97 1211.62 46.86 o -3 7 0 1714.21 1783.41 54.18 o -2 7 0 2483.69 2466.07 60.09 o -1 7 0 243.46 266.80 26.55 o 0 7 0 1307.55 1478.51 46.05 o 1 7 0 5246.84 5161.74 79.17 o 2 7 0 860.71 879.11 34.34 o 3 7 0 2363.72 2706.41 56.16 o 4 7 0 1091.25 1225.09 36.59 o 5 7 0 1432.20 1320.87 38.76 o 6 7 0 2.57 23.35 16.52 o 7 7 0 184.84 172.54 28.23 o 8 7 0 244.75 262.06 39.83 o 9 7 0 1.89 -15.83 15.83 o 10 7 0 64.41 94.45 27.20 o 11 7 0 1226.11 1227.72 78.62 o 12 7 0 237.21 285.82 54.41 o 13 7 0 286.30 249.13 41.07 o 14 7 0 0.31 -17.50 29.71 o 15 7 0 102.57 159.89 46.63 o 16 7 0 52.86 81.12 66.50 o -14 8 0 0.02 65.44 38.89 o -13 8 0 285.40 275.10 57.58 o -12 8 0 95.86 74.56 33.84 o -11 8 0 27.19 15.44 26.59 o -10 8 0 411.10 375.92 51.24 o -9 8 0 26.03 43.65 27.26 o -8 8 0 164.16 168.84 38.61 o -7 8 0 276.17 281.42 43.49 o -6 8 0 3157.15 3050.64 100.45 o -5 8 0 536.45 525.52 38.74 o -4 8 0 1942.18 1933.43 59.48 o -3 8 0 537.11 455.61 34.22 o -2 8 0 1182.37 947.28 42.30 o -1 8 0 51.00 83.12 26.47 o 0 8 0 606.81 667.97 37.74 o 1 8 0 1288.20 1468.82 47.96 o 2 8 0 6953.45 7744.69 101.39 o 3 8 0 75.70 87.37 14.89 o 4 8 0 1937.27 1900.12 49.00 o 5 8 0 1916.69 1859.86 68.91 o 6 8 0 2208.13 2193.53 76.68 o 7 8 0 18.10 10.78 16.06 o 8 8 0 465.63 450.86 50.74 o 9 8 0 85.53 59.57 32.94 o 10 8 0 0.16 -0.82 23.00 o 11 8 0 226.11 240.97 39.19 o 12 8 0 121.71 149.05 33.87 o 13 8 0 41.26 107.44 34.32 o 14 8 0 1.33 -18.78 26.91 o 15 8 0 52.13 80.64 39.07 o 16 8 0 148.91 254.72 61.38 o -13 9 0 79.38 63.61 30.92 o -12 9 0 153.56 151.14 44.62 o -11 9 0 182.25 271.37 57.65 o -10 9 0 28.52 54.20 29.33 o -9 9 0 6.83 -0.04 20.02 o -8 9 0 489.77 538.21 58.89 o -7 9 0 199.98 168.79 40.75 o -6 9 0 466.17 501.80 59.43 o -5 9 0 50.51 120.10 23.61 o -4 9 0 182.86 217.16 29.58 o -3 9 0 1045.82 984.78 57.75 o -2 9 0 7902.78 8275.41 123.30 o -1 9 0 269.76 297.07 31.05 o 0 9 0 374.04 413.23 33.74 o 1 9 0 64.12 55.09 24.93 o 2 9 0 238.54 240.47 25.39 o 3 9 0 24.17 40.63 12.25 o 4 9 0 55.61 70.99 21.76 o 5 9 0 408.28 387.83 41.05 o 6 9 0 333.47 359.71 41.13 o 7 9 0 98.36 84.12 23.34 o 8 9 0 386.09 369.67 43.64 o 9 9 0 2.07 -18.30 18.30 o 10 9 0 151.04 143.36 33.19 o 11 9 0 61.10 137.59 31.59 o 12 9 0 731.10 787.53 71.67 o 13 9 0 88.69 165.05 60.35 o 14 9 0 1.66 11.29 51.21 o 15 9 0 6.54 -26.60 26.60 o -13 10 0 35.39 16.45 60.59 o -12 10 0 100.36 105.08 41.39 o -11 10 0 266.99 360.30 63.67 o -10 10 0 224.45 199.67 49.39 o -9 10 0 238.85 240.77 54.17 o -8 10 0 148.46 166.78 36.36 o -7 10 0 500.12 554.41 76.69 o -6 10 0 157.71 139.58 33.51 o -5 10 0 878.64 811.31 63.93 o -4 10 0 180.41 193.78 28.78 o -3 10 0 298.75 318.10 41.18 o -2 10 0 45.45 60.07 19.09 o -1 10 0 1177.16 1196.44 51.85 o 0 10 0 934.23 929.49 44.82 o 1 10 0 1.07 22.48 13.42 o 2 10 0 361.78 332.83 30.83 o 3 10 0 96.68 44.30 32.04 o 4 10 0 454.79 424.94 44.83 o 5 10 0 0.07 19.27 26.73 o 6 10 0 147.21 126.57 27.52 o 7 10 0 828.03 783.75 60.02 o 8 10 0 166.16 144.63 30.60 o 9 10 0 10.23 8.12 18.92 o 10 10 0 9.24 11.47 29.19 o 11 10 0 187.79 231.60 39.89 o 12 10 0 226.25 231.30 44.11 o 13 10 0 0.20 0.03 22.86 o 14 10 0 10.25 -14.68 22.16 o 15 10 0 8.13 37.27 33.05 o -12 11 0 0.13 15.14 31.58 o -11 11 0 40.72 57.43 30.55 o -10 11 0 2.07 49.00 27.18 o -9 11 0 3.45 -1.18 21.92 o -8 11 0 437.72 427.02 67.46 o -7 11 0 494.25 446.06 65.83 o -6 11 0 455.13 500.24 54.91 o -5 11 0 779.30 846.78 67.48 o -4 11 0 569.44 564.36 47.50 o -3 11 0 287.31 333.23 37.20 o -2 11 0 250.93 274.25 32.91 o -1 11 0 29.30 30.96 18.43 o 0 11 0 100.93 97.38 21.45 o 1 11 0 13.16 3.55 17.25 o 2 11 0 3.67 5.47 16.38 o 3 11 0 2.84 15.11 15.72 o 4 11 0 25.84 26.03 18.37 o 5 11 0 622.56 662.42 55.89 o 6 11 0 95.10 93.24 24.89 o 7 11 0 428.91 455.56 48.80 o 8 11 0 33.30 28.84 20.45 o 9 11 0 2.48 28.42 18.65 o 10 11 0 193.74 235.51 39.75 o 11 11 0 227.34 225.39 37.76 o 12 11 0 143.22 174.34 36.76 o 13 11 0 30.61 69.20 29.65 o 14 11 0 2.19 10.33 43.52 o -11 12 0 11.08 12.22 44.41 o -10 12 0 85.33 31.84 27.96 o -9 12 0 152.50 163.98 46.68 o -8 12 0 33.18 20.54 24.36 o -7 12 0 1.01 16.49 23.87 o -6 12 0 71.72 156.32 37.83 o -5 12 0 177.52 248.62 37.01 o -4 12 0 27.37 51.38 23.30 o -3 12 0 689.58 757.25 52.97 o -2 12 0 1919.54 1724.13 65.22 o -1 12 0 110.27 103.75 23.68 o 0 12 0 429.50 409.75 39.39 o 1 12 0 26.02 36.72 22.60 o 2 12 0 7.67 25.91 18.72 o 3 12 0 4.76 4.23 18.75 o 4 12 0 0.32 -7.92 17.94 o 5 12 0 225.03 287.46 40.94 o 6 12 0 280.55 324.47 43.53 o 7 12 0 0.82 40.67 18.77 o 8 12 0 6.20 52.19 20.73 o 9 12 0 222.55 222.90 35.32 o 10 12 0 9.66 51.22 26.25 o 11 12 0 32.27 76.92 41.68 o 12 12 0 117.43 76.22 31.13 o 13 12 0 55.92 74.31 59.85 o -10 13 0 359.35 324.88 61.29 o -9 13 0 18.11 36.72 28.55 o -8 13 0 245.13 254.12 50.49 o -7 13 0 83.28 76.69 46.29 o -6 13 0 53.94 53.61 25.93 o -5 13 0 5.17 -4.26 23.80 o -4 13 0 17.30 5.24 26.88 o -3 13 0 16.62 43.15 17.31 o -2 13 0 799.69 754.30 53.62 o -1 13 0 4.06 32.59 15.95 o 0 13 0 45.87 52.12 26.22 o 1 13 0 395.25 378.16 47.65 o 2 13 0 23.79 31.47 22.65 o 3 13 0 86.70 87.53 25.46 o 4 13 0 27.20 22.59 19.92 o 5 13 0 809.17 910.91 69.70 o 6 13 0 329.75 354.07 46.72 o 7 13 0 22.33 62.31 29.43 o 8 13 0 58.13 79.71 30.42 o 9 13 0 36.59 30.82 25.76 o 10 13 0 0.08 38.99 47.65 o 11 13 0 105.44 92.58 38.35 o 12 13 0 254.88 326.39 59.99 o 13 13 0 0.01 7.24 47.23 o -9 14 0 30.84 151.70 81.11 o -8 14 0 197.52 152.86 77.97 o -7 14 0 4.57 25.91 40.37 o -6 14 0 261.14 280.38 53.87 o -5 14 0 143.50 102.94 35.16 o -4 14 0 183.32 249.82 46.63 o -3 14 0 1.11 0.83 19.61 o -2 14 0 47.43 72.61 21.09 o -1 14 0 238.92 288.24 41.19 o 0 14 0 1194.30 1271.35 80.17 o 1 14 0 18.53 68.02 26.87 o 2 14 0 45.58 135.64 28.78 o 3 14 0 574.86 470.39 69.79 o 4 14 0 62.28 108.18 36.60 o 5 14 0 459.47 476.39 74.23 o 6 14 0 853.34 754.32 87.22 o 7 14 0 279.16 216.85 49.92 o 8 14 0 0.40 45.75 28.54 o 9 14 0 16.36 58.94 59.75 o 10 14 0 18.34 112.67 35.18 o 11 14 0 158.93 139.34 87.50 o 12 14 0 11.95 67.42 28.95 o -7 15 0 3.38 -24.56 24.56 o -6 15 0 427.61 528.00 134.89 o -5 15 0 0.42 45.88 25.88 o -4 15 0 0.47 -3.10 18.94 o -3 15 0 1.05 22.52 32.36 o -2 15 0 3.76 22.94 39.48 o -1 15 0 291.89 298.21 59.49 o 0 15 0 198.99 157.92 47.97 o 1 15 0 966.88 945.61 92.42 o 2 15 0 62.37 97.21 36.68 o 3 15 0 77.99 171.69 42.48 o 4 15 0 22.76 93.48 35.63 o 5 15 0 15.22 39.25 32.30 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