#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:45:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181092 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/72/2217218.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217218_Fobs loop_ _publ_author_name 'Lorenzini, Fabio' 'Patrick, Brian O.' 'James, Brian R.' _publ_section_title ; trans-Carbonylchloridobis(ethyldiphenylphosphine-\kP)rhodium(I) ; _journal_coeditor_code NG2391 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m179 _journal_page_last m180 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.216 _cell_angle_gamma 90.000 _cell_length_a 9.8557 _cell_length_b 16.3850 _cell_length_c 16.3811 _exptl_crystal_F_000 1216.00 _reflns_d_resolution_high 0.7563 _cod_data_source_file ng2391Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj455 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 380.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -21 0 330.21 263.16 103.25 o 2 -21 0 568.76 403.29 111.90 o 3 -21 0 0.41 -14.15 183.85 o 0 -20 0 2984.39 3023.18 284.13 o 1 -20 0 286.00 176.44 113.76 o 2 -20 0 1.26 -3.55 73.96 o 3 -20 0 44.14 96.03 83.34 o 4 -20 0 319.15 265.41 98.82 o 1 -19 0 166.54 242.06 91.33 o 2 -19 0 815.62 843.77 125.11 o 3 -19 0 161.28 241.13 90.36 o 4 -19 0 46.53 88.51 80.10 o 5 -19 0 2.35 -47.70 72.47 o 6 -19 0 1053.45 833.69 141.49 o 0 -18 0 4594.00 4759.58 322.68 o 1 -18 0 857.68 895.22 241.82 o 2 -18 0 45.41 -17.56 129.12 o 3 -18 0 15.92 -27.60 108.79 o 4 -18 0 1005.45 1136.57 402.93 o 5 -18 0 200.72 361.83 124.75 o 6 -18 0 47.37 -28.40 76.99 o 7 -18 0 214.10 113.05 88.84 o 1 -17 0 60.53 10.58 66.85 o 2 -17 0 1601.46 1673.99 145.00 o 3 -17 0 277.44 245.38 83.23 o 4 -17 0 101.57 -11.55 68.95 o 5 -17 0 116.32 152.66 59.54 o 6 -17 0 1340.57 1297.74 133.60 o 7 -17 0 230.92 263.88 113.38 o 8 -17 0 212.91 96.45 98.17 o 0 -16 0 6515.26 6245.27 351.13 o 1 -16 0 955.51 929.75 65.72 o 2 -16 0 23.82 17.86 44.56 o 3 -16 0 174.19 124.04 54.22 o 4 -16 0 228.56 309.29 66.75 o 5 -16 0 118.54 96.12 63.62 o 6 -16 0 59.56 21.99 53.46 o 7 -16 0 7.64 -20.25 58.02 o 8 -16 0 2179.86 2235.12 155.56 o 1 -15 0 247.75 207.74 32.80 o 2 -15 0 2355.13 2299.77 79.07 o 3 -15 0 354.04 344.06 45.07 o 4 -15 0 45.29 8.09 48.25 o 5 -15 0 132.20 71.35 54.88 o 6 -15 0 840.16 848.03 75.52 o 7 -15 0 580.15 368.34 83.02 o 8 -15 0 4.24 -39.50 63.59 o 9 -15 0 40.27 14.04 73.28 o 0 -14 0 20919.42 19822.67 351.00 o 1 -14 0 1937.52 1867.27 64.37 o 2 -14 0 533.15 494.36 41.01 o 3 -14 0 805.53 790.40 57.90 o 4 -14 0 450.31 529.61 61.68 o 5 -14 0 15.95 25.80 53.59 o 6 -14 0 3.16 -15.80 40.19 o 7 -14 0 171.57 156.09 55.44 o 8 -14 0 3179.36 3378.08 149.87 o 9 -14 0 381.86 426.17 79.75 o 1 -13 0 505.76 486.13 40.03 o 2 -13 0 8876.48 8501.87 138.39 o 3 -13 0 99.45 115.34 41.59 o 4 -13 0 736.01 754.48 54.02 o 5 -13 0 385.45 273.96 56.97 o 6 -13 0 2141.17 2283.53 111.30 o 7 -13 0 549.20 468.96 70.33 o 8 -13 0 36.24 194.05 72.98 o 9 -13 0 147.26 174.56 67.87 o 10 -13 0 2028.43 1933.68 187.46 o 0 -12 0 13581.08 13482.67 337.86 o 1 -12 0 492.03 523.16 39.13 o 2 -12 0 23.28 1.69 27.45 o 3 -12 0 1372.81 1359.91 66.62 o 4 -12 0 354.94 479.28 45.96 o 5 -12 0 144.02 139.97 62.65 o 6 -12 0 4.35 -1.72 33.92 o 7 -12 0 73.63 44.47 48.73 o 8 -12 0 4934.62 5150.05 175.48 o 9 -12 0 374.38 523.59 85.24 o 10 -12 0 40.35 134.02 63.85 o 1 -11 0 414.71 521.21 50.59 o 2 -11 0 7816.13 7395.51 158.39 o 3 -11 0 92.79 59.30 32.25 o 4 -11 0 63.63 -7.12 34.79 o 5 -11 0 562.19 483.08 52.66 o 6 -11 0 308.70 305.04 47.73 o 7 -11 0 640.60 710.80 70.84 o 8 -11 0 36.03 74.37 51.96 o 9 -11 0 159.07 252.35 63.64 o 10 -11 0 3009.08 2782.02 288.66 o 11 -11 0 176.27 189.25 80.37 o 0 -10 0 19981.13 20427.86 305.37 o 1 -10 0 24.00 -0.70 21.20 o 2 -10 0 290.00 276.76 36.28 o 3 -10 0 674.66 560.89 42.13 o 4 -10 0 99.37 132.49 36.88 o 5 -10 0 336.40 364.97 47.79 o 6 -10 0 167.93 112.46 41.19 o 7 -10 0 13.70 87.04 39.33 o 8 -10 0 6724.01 6965.07 195.15 o 9 -10 0 624.72 593.51 78.86 o 10 -10 0 73.65 32.99 54.65 o 11 -10 0 5.69 45.66 67.55 o 1 -9 0 4320.08 4355.45 76.35 o 2 -9 0 22748.50 22103.97 257.90 o 3 -9 0 194.50 165.85 33.07 o 4 -9 0 39.00 58.63 32.17 o 5 -9 0 311.75 263.73 49.70 o 6 -9 0 4561.95 4421.54 117.31 o 7 -9 0 693.80 755.73 61.43 o 8 -9 0 42.34 69.51 42.05 o 9 -9 0 29.59 73.13 60.51 o 10 -9 0 2750.10 3052.81 205.73 o 11 -9 0 6.88 67.28 65.57 o 0 -8 0 24073.14 23700.58 460.92 o 1 -8 0 73.38 77.05 23.70 o 2 -8 0 16.06 18.27 20.66 o 3 -8 0 62.34 72.61 24.59 o 4 -8 0 5246.31 5264.84 92.32 o 5 -8 0 149.12 206.67 33.36 o 6 -8 0 141.73 144.75 41.52 o 7 -8 0 314.92 446.86 73.40 o 8 -8 0 6375.50 6553.42 156.53 o 9 -8 0 234.20 95.62 51.92 o 10 -8 0 79.44 83.76 60.23 o 11 -8 0 14.25 -44.78 55.77 o 12 -8 0 161.51 338.79 139.43 o 1 -7 0 1617.52 1595.47 54.70 o 2 -7 0 9706.74 8992.26 126.68 o 3 -7 0 758.57 767.89 38.22 o 4 -7 0 58.84 81.30 22.50 o 5 -7 0 269.68 252.44 33.34 o 6 -7 0 5705.94 5540.84 126.21 o 7 -7 0 154.82 151.21 41.86 o 8 -7 0 55.76 79.20 38.63 o 9 -7 0 37.52 29.81 40.53 o 10 -7 0 3207.24 3445.42 230.62 o 11 -7 0 2.86 -15.79 54.70 o 12 -7 0 5.26 62.54 102.39 o 0 -6 0 14876.25 14204.45 201.81 o 1 -6 0 697.23 658.47 28.72 o 2 -6 0 44.24 29.18 17.93 o 3 -6 0 174.51 207.44 23.07 o 4 -6 0 2975.74 3054.11 90.15 o 5 -6 0 210.70 243.92 31.28 o 6 -6 0 63.25 57.62 33.76 o 7 -6 0 263.72 331.18 47.27 o 8 -6 0 7732.20 7668.31 185.41 o 9 -6 0 147.53 107.51 43.55 o 10 -6 0 102.24 53.06 56.10 o 11 -6 0 46.07 9.76 55.71 o 12 -6 0 13.54 -20.75 126.56 o 1 -5 0 3572.73 3566.70 56.41 o 2 -5 0 17940.18 17279.15 195.03 o 3 -5 0 541.82 541.97 34.59 o 4 -5 0 55.55 47.18 20.05 o 5 -5 0 1156.44 1245.75 49.60 o 6 -5 0 14403.96 14180.88 243.76 o 7 -5 0 152.35 133.28 39.21 o 8 -5 0 304.91 353.26 53.77 o 9 -5 0 129.58 108.37 57.63 o 10 -5 0 6336.38 6343.05 236.39 o 11 -5 0 8.79 -35.21 49.43 o 12 -5 0 6.64 156.33 85.02 o 0 -4 0 55489.22 55099.34 577.63 o 1 -4 0 214.28 213.77 16.91 o 2 -4 0 342.13 304.99 20.59 o 3 -4 0 293.55 304.84 20.57 o 4 -4 0 10596.41 10839.57 149.16 o 5 -4 0 1432.79 1453.76 60.44 o 6 -4 0 309.15 293.95 38.53 o 7 -4 0 862.72 885.45 59.35 o 8 -4 0 19838.80 19563.26 334.67 o 9 -4 0 184.82 183.78 60.07 o 10 -4 0 361.39 501.32 82.96 o 11 -4 0 147.60 218.00 55.89 o 12 -4 0 31.13 118.05 77.52 o 1 -3 0 69.65 44.17 11.10 o 2 -3 0 174.75 249.84 17.65 o 3 -3 0 6483.29 6449.40 81.19 o 4 -3 0 40.64 38.90 17.16 o 5 -3 0 93.80 77.52 25.38 o 6 -3 0 7030.24 6937.20 133.19 o 7 -3 0 110.38 70.33 34.00 o 8 -3 0 160.91 173.24 44.75 o 9 -3 0 22.56 5.05 38.15 o 10 -3 0 9491.81 9824.52 227.17 o 11 -3 0 199.58 217.49 55.17 o 12 -3 0 17.29 100.89 72.78 o 0 -2 0 79322.92 79526.38 934.57 o 1 -2 0 6.81 0.59 5.93 o 2 -2 0 35.11 19.90 11.56 o 3 -2 0 15683.88 15771.77 155.63 o 4 -2 0 12.12 36.44 17.25 o 5 -2 0 1983.95 2038.26 58.40 o 6 -2 0 41.13 22.58 23.52 o 7 -2 0 17.89 -14.92 30.33 o 8 -2 0 6954.24 7000.17 169.12 o 9 -2 0 52.39 17.99 39.27 o 10 -2 0 43.39 -24.11 40.56 o 11 -2 0 61.51 106.52 49.85 o 12 -2 0 312.73 211.46 67.83 o 1 -1 0 130.46 147.76 6.90 o 2 -1 0 26658.23 27504.00 202.26 o 3 -1 0 12339.92 12677.24 121.99 o 4 -1 0 361.89 398.69 23.43 o 5 -1 0 4020.70 4272.70 97.49 o 6 -1 0 2964.47 2659.95 72.77 o 7 -1 0 142.91 77.41 34.16 o 8 -1 0 99.86 21.62 44.40 o 9 -1 0 45.56 -24.92 37.34 o 10 -1 0 7243.98 7565.74 194.58 o 11 -1 0 12.49 17.22 40.82 o 12 -1 0 20.79 -44.75 48.43 o 1 0 0 115.59 119.73 5.45 o 2 0 0 80.18 77.22 9.90 o 3 0 0 2.54 6.73 11.95 o 4 0 0 4035.35 3663.90 79.69 o 5 0 0 176.25 187.35 25.91 o 6 0 0 373.97 349.09 34.19 o 7 0 0 269.83 307.62 62.64 o 8 0 0 4322.23 4018.82 124.39 o 9 0 0 103.72 42.62 40.95 o 10 0 0 108.90 145.59 50.18 o 11 0 0 121.62 127.19 57.15 o 12 0 0 663.04 793.04 99.54 o 1 1 0 130.51 138.81 7.13 o 2 1 0 26655.41 27993.50 256.07 o 3 1 0 12342.66 12609.65 135.50 o 4 1 0 357.10 435.49 27.82 o 5 1 0 4001.50 4116.70 89.54 o 6 1 0 2945.97 2606.68 116.70 o 7 1 0 138.12 193.94 41.05 o 8 1 0 94.51 47.96 38.02 o 9 1 0 45.46 27.24 36.97 o 10 1 0 7217.69 7088.97 187.49 o 11 1 0 13.47 49.45 51.45 o 12 1 0 23.47 115.69 74.76 o 0 2 0 79194.29 79401.13 911.52 o 1 2 0 7.37 -0.70 5.83 o 2 2 0 38.38 27.48 12.35 o 3 2 0 15683.33 15740.79 145.03 o 4 2 0 28.29 85.69 21.81 o 5 2 0 1984.37 2052.32 73.70 o 6 2 0 37.46 -7.64 25.23 o 7 2 0 17.18 5.09 31.70 o 8 2 0 6908.93 6883.35 166.16 o 9 2 0 55.91 56.19 39.22 o 10 2 0 50.76 61.52 46.56 o 11 2 0 67.38 -19.09 45.65 o 12 2 0 307.47 246.73 70.58 o 1 3 0 54.70 39.47 10.90 o 2 3 0 80.77 141.20 15.36 o 3 3 0 6496.45 6671.94 104.90 o 4 3 0 40.69 9.22 17.45 o 5 3 0 97.85 89.28 24.59 o 6 3 0 7051.78 7005.59 148.97 o 7 3 0 115.75 186.36 42.14 o 8 3 0 172.59 80.95 42.38 o 9 3 0 20.45 24.32 36.46 o 10 3 0 9567.31 9186.52 401.47 o 11 3 0 202.42 170.37 63.50 o 12 3 0 15.88 87.89 57.03 o 0 4 0 55391.02 55921.80 830.32 o 1 4 0 216.26 234.46 24.93 o 2 4 0 349.97 351.46 25.57 o 3 4 0 293.51 253.48 25.12 o 4 4 0 10560.42 10484.91 142.15 o 5 4 0 1428.18 1457.53 58.20 o 6 4 0 319.03 262.92 37.59 o 7 4 0 861.34 814.75 62.60 o 8 4 0 19941.63 18880.48 470.22 o 9 4 0 190.38 255.90 51.18 o 10 4 0 358.53 359.18 71.67 o 11 4 0 150.61 107.07 55.47 o 12 4 0 39.34 34.51 54.65 o 1 5 0 3580.38 3763.74 60.15 o 2 5 0 17948.65 17603.46 216.02 o 3 5 0 541.42 528.26 34.86 o 4 5 0 54.37 24.28 22.08 o 5 5 0 1170.76 1234.11 53.75 o 6 5 0 14433.56 14652.02 246.48 o 7 5 0 145.30 178.67 44.79 o 8 5 0 293.40 251.65 50.51 o 9 5 0 138.76 95.83 42.20 o 10 5 0 6329.10 6354.83 207.14 o 11 5 0 8.39 34.54 49.87 o 12 5 0 5.26 38.10 56.99 o 0 6 0 14880.45 14168.71 288.25 o 1 6 0 691.49 693.57 33.76 o 2 6 0 44.20 43.85 19.54 o 3 6 0 175.97 228.84 28.51 o 4 6 0 2999.40 3253.71 80.94 o 5 6 0 197.54 198.73 30.17 o 6 6 0 58.01 89.62 32.39 o 7 6 0 269.69 281.31 50.49 o 8 6 0 7641.29 7469.76 180.45 o 9 6 0 144.09 163.22 54.88 o 10 6 0 103.42 123.15 57.48 o 11 6 0 41.06 9.08 53.96 o 12 6 0 20.66 47.91 59.62 o 1 7 0 1607.02 1635.40 52.07 o 2 7 0 9714.68 9077.35 156.87 o 3 7 0 768.82 726.78 74.91 o 4 7 0 62.41 64.21 26.68 o 5 7 0 258.69 224.39 35.16 o 6 7 0 5687.63 5495.78 143.17 o 7 7 0 161.76 175.17 46.46 o 8 7 0 61.14 67.66 41.85 o 9 7 0 39.91 23.43 47.40 o 10 7 0 3164.02 3199.50 153.72 o 11 7 0 3.87 -37.68 46.05 o 12 7 0 7.54 -40.52 66.04 o 0 8 0 24041.84 23622.87 461.21 o 1 8 0 66.48 86.75 29.37 o 2 8 0 15.25 14.93 25.93 o 3 8 0 64.71 34.45 25.64 o 4 8 0 5243.55 5586.99 116.98 o 5 8 0 154.97 143.79 35.26 o 6 8 0 139.38 150.70 38.55 o 7 8 0 316.79 373.23 50.85 o 8 8 0 6378.06 6457.00 172.74 o 9 8 0 234.70 279.42 65.99 o 10 8 0 83.25 224.97 65.82 o 11 8 0 17.27 49.15 54.58 o 12 8 0 149.21 96.17 77.39 o 1 9 0 4322.69 4378.63 109.76 o 2 9 0 22795.01 23109.47 295.73 o 3 9 0 194.74 180.43 33.21 o 4 9 0 39.76 54.21 31.96 o 5 9 0 305.24 305.36 48.33 o 6 9 0 4563.69 4780.13 136.61 o 7 9 0 688.28 751.27 60.83 o 8 9 0 41.89 4.23 47.56 o 9 9 0 25.70 32.13 58.15 o 10 9 0 2752.43 3016.73 159.05 o 11 9 0 4.89 63.55 74.58 o 0 10 0 19974.74 20389.38 433.15 o 1 10 0 25.03 1.20 34.01 o 2 10 0 290.25 317.37 37.79 o 3 10 0 668.91 688.26 51.84 o 4 10 0 132.89 180.61 39.28 o 5 10 0 328.65 314.19 50.96 o 6 10 0 160.43 199.97 49.16 o 7 10 0 13.20 32.28 45.68 o 8 10 0 6708.85 6599.38 207.42 o 9 10 0 623.53 616.24 85.63 o 10 10 0 68.05 154.80 75.41 o 11 10 0 7.22 55.42 91.85 o 1 11 0 404.17 340.16 52.68 o 2 11 0 7857.82 8005.79 172.03 o 3 11 0 92.04 95.77 35.63 o 4 11 0 65.98 46.09 41.42 o 5 11 0 559.29 517.95 61.01 o 6 11 0 331.73 321.59 53.20 o 7 11 0 647.87 536.77 76.55 o 8 11 0 41.44 13.01 51.07 o 9 11 0 161.25 215.47 120.38 o 10 11 0 2989.58 2685.00 265.31 o 11 11 0 178.36 173.33 91.40 o 0 12 0 13520.21 13461.84 512.32 o 1 12 0 500.74 590.06 60.69 o 2 12 0 25.78 63.86 42.83 o 3 12 0 1379.05 1321.12 68.96 o 4 12 0 322.90 350.08 57.13 o 5 12 0 153.80 155.45 47.20 o 6 12 0 4.53 -43.93 44.78 o 7 12 0 68.72 109.99 55.01 o 8 12 0 4971.05 4974.06 229.11 o 9 12 0 385.50 378.09 93.39 o 10 12 0 37.79 71.50 77.90 o 1 13 0 521.34 480.26 68.98 o 2 13 0 8826.27 9049.94 198.63 o 3 13 0 105.09 49.07 39.09 o 4 13 0 731.51 812.51 72.22 o 5 13 0 382.30 359.80 120.69 o 6 13 0 2169.70 2195.51 201.62 o 7 13 0 530.80 321.50 85.21 o 8 13 0 36.32 72.34 73.65 o 9 13 0 144.01 140.96 84.05 o 10 13 0 2030.31 2024.64 293.39 o 0 14 0 20872.99 20483.56 484.37 o 1 14 0 1932.38 2051.13 100.43 o 2 14 0 532.97 534.20 65.88 o 3 14 0 828.38 737.96 80.72 o 4 14 0 439.24 523.70 74.07 o 5 14 0 12.43 14.11 46.86 o 6 14 0 3.14 -56.26 64.07 o 7 14 0 161.77 89.76 68.87 o 8 14 0 3229.84 3061.58 240.61 o 9 14 0 376.92 403.08 109.04 o 1 15 0 254.82 326.13 66.04 o 2 15 0 2434.26 2508.61 152.93 o 3 15 0 329.01 226.65 74.67 o 4 15 0 46.37 28.85 57.99 o 5 15 0 136.91 126.34 83.72 o 6 15 0 812.82 1084.11 124.75 o 7 15 0 576.54 676.72 113.20 o 8 15 0 3.35 8.06 73.57 o 9 15 0 38.50 9.76 76.24 o 0 16 0 6499.88 7134.40 364.84 o 1 16 0 956.41 1085.34 113.26 o 2 16 0 22.56 -58.58 58.68 o 3 16 0 149.46 192.60 76.24 o 4 16 0 232.86 168.16 81.05 o 5 16 0 137.49 103.75 94.41 o 6 16 0 59.86 57.00 91.17 o 7 16 0 5.62 -41.23 68.08 o 8 16 0 2157.26 2319.00 186.38 o 1 17 0 46.01 45.99 70.14 o 2 17 0 1611.03 1574.83 180.61 o 3 17 0 284.40 421.33 186.11 o 4 17 0 98.10 77.72 74.05 o 5 17 0 126.67 133.84 78.85 o 6 17 0 1298.58 1377.00 271.71 o 7 17 0 247.67 142.08 86.01 o 8 17 0 215.86 323.13 152.53 o 0 18 0 4595.42 4365.98 303.25 o 1 18 0 860.85 806.54 116.64 o 2 18 0 46.82 135.11 79.53 o 3 18 0 21.45 -16.77 66.32 o 4 18 0 983.09 1145.81 135.92 o 5 18 0 218.76 193.23 119.25 o 6 18 0 46.28 33.08 78.08 o 7 18 0 219.66 135.70 93.54 o 1 19 0 155.87 228.99 87.92 o 2 19 0 831.63 718.21 157.42 o 3 19 0 156.46 171.68 91.52 o 4 19 0 44.01 -7.52 79.14 o 5 19 0 2.11 -45.59 72.91 o 6 19 0 1090.47 905.42 157.57 o 0 20 0 3007.61 2799.58 275.25 o 1 20 0 279.27 364.64 103.65 o 2 20 0 1.44 92.55 83.23 o 3 20 0 38.19 -15.81 72.59 o 4 20 0 351.58 381.56 116.27 o 1 21 0 331.30 553.89 121.48 o 2 21 0 554.73 637.42 125.21 o 3 21 0 0.63 -93.96 107.66 o -3 -21 1 26.07 -115.19 115.19 o -2 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