#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/72/2217227.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217227_Fobs loop_ _publ_author_name 'Abbasi, Alireza' 'Badiei, Alireza' 'Tarighi, Sara' _publ_section_title ; 5,6-Dioxo-1,10-phenanthrolin-1-ium nitrate ; _journal_coeditor_code NG2405 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o290 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.720 _cell_angle_gamma 90.000 _cell_length_a 14.4860 _cell_length_b 12.5177 _cell_length_c 13.4535 _exptl_crystal_F_000 1120.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file ng2405Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' RTHDATA2 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 664.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 454.65 614.54 52.41 o 6 0 0 15458.12 15207.06 495.53 o 8 0 0 10.63 0.00 2015.36 o 10 0 0 2896.35 2734.01 193.25 o 12 0 0 486.74 270.52 248.25 o 14 0 0 6.33 8.03 294.95 o 16 0 0 581.68 865.06 284.53 o 3 1 0 602.73 448.34 26.98 o 5 1 0 4214.05 3659.45 128.62 o 7 1 0 105.35 144.37 67.90 o 9 1 0 1.90 44.00 86.17 o 11 1 0 3459.05 3146.57 151.59 o 13 1 0 2667.91 2553.72 169.07 o 15 1 0 3.84 28.45 193.46 o 2 2 0 33863.96 31451.08 134.08 o 4 2 0 1195.78 1762.43 97.71 o 6 2 0 869.61 768.76 45.36 o 8 2 0 178.03 313.13 89.74 o 10 2 0 164.21 206.92 98.53 o 12 2 0 1025.73 955.96 155.12 o 14 2 0 485.49 635.33 183.60 o 16 2 0 102.64 129.65 230.91 o 1 3 0 428.63 624.36 41.23 o 3 3 0 3204.07 3368.36 66.17 o 5 3 0 8986.36 9917.54 114.39 o 7 3 0 4.84 0.00 52.54 o 9 3 0 88.18 65.39 79.79 o 11 3 0 26.33 100.57 118.96 o 13 3 0 14.93 42.77 162.59 o 15 3 0 35.92 51.44 222.27 o 0 4 0 301.37 143.45 54.35 o 2 4 0 1460.02 1239.43 47.05 o 4 4 0 5843.21 6035.91 71.30 o 6 4 0 7593.10 7496.61 100.06 o 8 4 0 452.43 457.75 69.36 o 10 4 0 2560.90 2697.44 144.02 o 12 4 0 31.17 140.20 165.76 o 14 4 0 27.09 71.53 193.97 o 16 4 0 2.30 3.15 169.27 o 1 5 0 262.17 454.92 53.64 o 3 5 0 423.27 520.15 46.79 o 5 5 0 453.25 300.86 46.87 o 7 5 0 0.11 0.00 56.02 o 9 5 0 34.14 63.41 69.59 o 11 5 0 11.62 15.23 32.67 o 13 5 0 115.51 63.30 171.26 o 15 5 0 67.17 81.35 254.37 o 0 6 0 5719.04 5806.13 208.16 o 2 6 0 11.82 70.11 60.43 o 4 6 0 730.04 814.02 56.60 o 6 6 0 354.99 354.60 54.18 o 8 6 0 15.92 16.13 62.23 o 10 6 0 9.31 72.10 89.92 o 12 6 0 0.17 109.38 170.38 o 14 6 0 0.00 0.00 25.00 o 1 7 0 1.06 5.25 51.13 o 3 7 0 5.51 61.08 69.70 o 5 7 0 67.39 46.89 56.01 o 7 7 0 86.55 84.51 67.22 o 9 7 0 8.99 6.19 30.50 o 11 7 0 67.60 30.77 174.66 o 13 7 0 7.55 77.39 311.01 o 0 8 0 11.73 43.07 135.06 o 2 8 0 4.01 45.70 86.99 o 4 8 0 405.65 376.36 78.97 o 6 8 0 55.06 135.37 85.47 o 8 8 0 0.16 23.96 66.18 o 10 8 0 302.22 232.39 137.94 o 12 8 0 1.35 0.00 195.10 o 14 8 0 0.89 72.28 415.77 o 1 9 0 101.69 79.31 126.16 o 3 9 0 499.38 530.81 86.46 o 5 9 0 1063.86 992.85 87.21 o 7 9 0 0.01 0.00 133.04 o 9 9 0 23.19 0.00 155.26 o 11 9 0 80.56 25.98 236.86 o 13 9 0 76.61 235.82 404.46 o 0 10 0 724.95 656.81 200.07 o 2 10 0 53.82 20.63 113.67 o 4 10 0 1612.53 1513.27 101.28 o 6 10 0 87.34 0.00 72.08 o 8 10 0 64.76 59.25 140.72 o 10 10 0 158.44 262.40 203.92 o 12 10 0 40.09 73.15 378.97 o 1 11 0 25.01 15.58 132.41 o 3 11 0 8.94 45.29 114.14 o 5 11 0 2.17 0.00 31.24 o 7 11 0 168.60 232.42 151.49 o 9 11 0 4.39 62.85 171.92 o 11 11 0 8.31 0.00 38.24 o 0 12 0 56.13 4.38 234.72 o 2 12 0 606.64 770.13 145.64 o 4 12 0 4.78 80.44 130.02 o 6 12 0 47.53 20.98 75.57 o 8 12 0 24.88 40.42 178.27 o 1 13 0 79.45 0.00 112.96 o 3 13 0 438.81 524.91 170.86 o 5 13 0 31.77 43.23 173.14 o 7 13 0 49.75 21.33 190.40 o 0 14 0 417.81 555.62 294.60 o 2 14 0 107.39 193.60 198.26 o 4 14 0 2.38 70.37 225.05 o -17 1 1 41.35 0.00 76.43 o -15 1 1 0.43 37.41 189.43 o -13 1 1 162.20 142.61 162.49 o -11 1 1 560.88 388.07 151.01 o -9 1 1 66.63 55.19 115.38 o -7 1 1 147.60 154.42 126.67 o -5 1 1 161.23 169.64 41.19 o -3 1 1 229.56 274.52 33.52 o 3 1 1 2.66 29.58 24.93 o 5 1 1 201.56 188.01 47.94 o 7 1 1 374.93 300.84 71.05 o 9 1 1 15.10 32.60 92.15 o 11 1 1 264.27 181.67 124.03 o 13 1 1 103.37 115.93 169.18 o 15 1 1 63.18 123.72 233.77 o -16 2 1 16.62 31.79 186.05 o -14 2 1 373.18 464.73 172.06 o -12 2 1 649.87 457.64 144.78 o -10 2 1 364.08 267.57 146.17 o -8 2 1 715.98 756.08 60.46 o -6 2 1 391.89 407.22 45.31 o -4 2 1 1444.33 1409.56 38.61 o -2 2 1 21.06 27.38 26.71 o 2 2 1 9754.05 9732.31 77.42 o 4 2 1 0.25 0.00 27.15 o 6 2 1 200.41 129.03 37.92 o 8 2 1 5.56 0.00 16.43 o 10 2 1 245.21 237.48 71.85 o 12 2 1 55.00 6.32 118.75 o 14 2 1 10.50 0.00 182.86 o 16 2 1 211.23 146.72 262.74 o -15 3 1 44.17 189.16 199.34 o -13 3 1 194.43 214.46 165.33 o -11 3 1 70.00 98.69 156.98 o -9 3 1 28.73 99.52 71.92 o -7 3 1 4346.96 4693.38 204.84 o -5 3 1 7070.38 7509.84 155.75 o -3 3 1 3093.35 3093.85 49.04 o -1 3 1 2213.25 2279.85 117.84 o 1 3 1 1357.55 1491.86 45.30 o 3 3 1 815.68 832.65 39.89 o 5 3 1 2612.66 2713.67 60.87 o 7 3 1 141.65 161.45 50.47 o 9 3 1 1269.58 1272.15 54.85 o 11 3 1 12.58 5.19 108.43 o 13 3 1 30.18 75.89 178.19 o 15 3 1 78.61 221.17 224.17 o -16 4 1 2.54 70.94 218.48 o -14 4 1 0.23 58.53 202.28 o -12 4 1 13.00 21.30 187.73 o -10 4 1 490.88 482.67 87.30 o -8 4 1 257.53 244.53 67.71 o -6 4 1 278.06 247.73 50.93 o -4 4 1 1968.16 1953.06 47.75 o -2 4 1 6231.82 6058.68 108.14 o 0 4 1 667.47 693.31 38.70 o 2 4 1 437.17 475.30 42.31 o 4 4 1 328.16 372.58 43.28 o 6 4 1 3750.20 3881.63 75.53 o 8 4 1 8.00 0.00 9.38 o 10 4 1 33.62 23.65 65.91 o 12 4 1 145.26 58.36 134.97 o 14 4 1 102.03 51.99 120.66 o -15 5 1 357.12 597.33 243.69 o -13 5 1 25.87 83.78 210.65 o -11 5 1 25.85 45.54 168.74 o -9 5 1 11.25 14.13 83.37 o -7 5 1 176.25 214.03 62.41 o -5 5 1 23.31 39.36 47.14 o -3 5 1 183.23 244.96 34.86 o -1 5 1 1325.92 1430.30 53.45 o 1 5 1 7175.01 7572.41 120.85 o 3 5 1 677.78 700.55 48.10 o 5 5 1 59.92 85.68 55.20 o 7 5 1 1521.36 1590.77 62.13 o 9 5 1 382.62 494.76 78.85 o 11 5 1 343.84 241.54 110.08 o 13 5 1 151.64 129.07 186.66 o 15 5 1 1.44 148.55 284.39 o -14 6 1 58.63 360.66 367.59 o -12 6 1 858.31 579.97 154.51 o -10 6 1 0.02 0.00 27.29 o -8 6 1 143.41 121.34 77.12 o -6 6 1 1067.47 1096.41 57.80 o -4 6 1 6772.17 6596.82 74.49 o -2 6 1 481.49 415.74 64.16 o 0 6 1 13777.28 14347.31 132.53 o 2 6 1 423.33 459.85 56.68 o 4 6 1 13.62 1.24 43.73 o 6 6 1 1588.86 1543.93 92.92 o 8 6 1 12.53 50.46 75.96 o 10 6 1 37.43 105.46 106.71 o 12 6 1 1228.26 1019.06 257.78 o 14 6 1 100.33 124.91 250.70 o -15 7 1 90.10 192.51 345.62 o -13 7 1 11.27 54.39 342.04 o -11 7 1 513.65 357.86 136.17 o -9 7 1 195.88 198.85 110.96 o -7 7 1 1571.17 1496.85 63.67 o -5 7 1 155.86 134.63 45.26 o -3 7 1 123.87 108.42 78.10 o -1 7 1 678.12 784.79 68.69 o 1 7 1 3414.55 3822.02 114.79 o 3 7 1 580.77 501.90 66.41 o 5 7 1 2623.24 2437.38 78.54 o 7 7 1 575.68 480.96 81.53 o 9 7 1 2.74 42.49 112.45 o 11 7 1 670.53 579.01 166.14 o 13 7 1 3.94 51.47 361.75 o -14 8 1 0.36 126.61 294.77 o -12 8 1 2.45 0.00 44.72 o -10 8 1 20.60 123.32 135.28 o -8 8 1 448.78 444.63 111.93 o -6 8 1 800.15 735.42 83.29 o -4 8 1 2390.44 2367.58 80.55 o -2 8 1 1024.59 1087.85 84.17 o 0 8 1 1097.00 1025.48 86.27 o 2 8 1 22.51 57.35 75.48 o 4 8 1 359.95 340.12 77.11 o 6 8 1 5126.01 5043.96 111.20 o 8 8 1 915.85 707.23 95.98 o 10 8 1 41.28 47.94 179.94 o 12 8 1 37.13 61.33 339.48 o -13 9 1 373.15 356.88 221.88 o -11 9 1 92.06 59.98 267.53 o -9 9 1 741.09 532.35 136.53 o -7 9 1 6630.05 6223.99 280.97 o -5 9 1 8606.46 8254.41 141.21 o -3 9 1 570.63 623.45 93.32 o -1 9 1 52.78 57.06 84.16 o 1 9 1 324.08 285.80 97.97 o 3 9 1 310.79 398.24 88.44 o 5 9 1 2587.19 2453.00 91.62 o 7 9 1 2730.48 2627.51 97.61 o 9 9 1 5.12 52.45 136.02 o 11 9 1 30.08 22.79 139.45 o 13 9 1 16.07 0.00 507.40 o -12 10 1 80.24 38.32 242.56 o -10 10 1 398.00 431.60 166.22 o -8 10 1 61.05 172.06 142.94 o -6 10 1 44.33 23.16 34.54 o -4 10 1 153.40 138.22 93.77 o -2 10 1 317.03 229.43 139.35 o 0 10 1 1010.80 885.50 134.23 o 2 10 1 118.69 194.60 99.52 o 4 10 1 85.29 125.46 107.53 o 6 10 1 3947.86 3732.53 111.49 o 8 10 1 7.73 0.00 102.55 o 10 10 1 0.06 56.62 206.54 o 12 10 1 46.37 0.00 323.06 o -11 11 1 4.42 0.00 189.79 o -9 11 1 1.80 8.09 204.63 o -7 11 1 259.25 131.25 140.69 o -5 11 1 115.59 89.57 112.43 o -3 11 1 9.68 133.61 128.08 o -1 11 1 395.52 425.85 145.89 o 1 11 1 305.32 231.75 148.71 o 3 11 1 305.77 222.56 118.14 o 5 11 1 7.00 0.00 12.22 o 7 11 1 56.65 23.43 141.32 o 9 11 1 30.02 92.48 171.64 o 11 11 1 24.62 48.62 252.16 o -10 12 1 30.20 27.37 190.93 o -8 12 1 33.73 2.49 160.20 o -6 12 1 8.96 12.10 179.92 o -4 12 1 0.21 87.82 134.03 o -2 12 1 127.98 120.53 169.67 o 0 12 1 81.14 63.75 172.94 o 2 12 1 152.44 216.45 147.09 o 4 12 1 20.16 37.08 143.51 o 6 12 1 47.22 52.02 138.25 o 8 12 1 35.62 35.68 92.04 o -7 13 1 104.56 229.60 196.59 o -5 13 1 17.57 44.32 180.34 o -3 13 1 0.75 36.71 104.93 o -1 13 1 46.85 25.03 152.71 o 1 13 1 20.91 1.58 33.31 o 3 13 1 70.70 112.78 166.00 o 5 13 1 13.16 91.30 175.80 o 7 13 1 109.81 150.68 199.19 o -4 14 1 21.82 17.95 210.95 o -2 14 1 50.62 57.70 103.05 o 0 14 1 0.03 0.00 144.89 o 2 14 1 22.75 4.33 214.01 o 4 14 1 4.97 45.81 249.33 o -16 0 2 245.58 135.56 271.45 o -14 0 2 0.44 0.00 150.17 o -12 0 2 15966.66 16145.50 337.92 o -10 0 2 276.88 333.36 153.91 o -8 0 2 2679.10 2300.62 193.46 o -6 0 2 6943.75 7725.14 259.96 o -4 0 2 29737.87 30701.45 385.86 o -2 0 2 10999.88 10165.55 112.53 o 2 0 2 8061.18 7474.69 154.72 o 4 0 2 24258.34 24050.60 451.17 o 6 0 2 2194.81 2043.22 94.02 o 8 0 2 103.65 119.42 106.19 o 10 0 2 31.13 65.88 132.40 o 12 0 2 10662.23 9923.43 360.38 o 14 0 2 70.25 79.94 295.68 o 16 0 2 345.10 214.29 393.53 o -17 1 2 9.87 95.11 256.41 o -15 1 2 4.29 77.23 182.35 o -13 1 2 608.61 567.44 141.99 o -11 1 2 282.86 260.74 115.97 o -9 1 2 3733.12 4048.45 196.27 o -7 1 2 207.44 184.23 84.90 o -5 1 2 185.83 186.72 48.89 o -3 1 2 5413.58 5751.33 126.60 o 1 1 2 5893.07 5595.02 48.24 o 3 1 2 13337.27 12873.74 189.27 o 5 1 2 2491.51 2539.23 45.20 o 7 1 2 1768.76 1679.56 41.39 o 9 1 2 401.62 333.31 43.53 o 11 1 2 439.93 383.33 127.89 o 13 1 2 575.96 463.44 183.70 o 15 1 2 20.71 0.00 317.09 o -16 2 2 161.72 137.85 206.80 o -14 2 2 18.26 34.06 131.33 o -12 2 2 75.39 120.68 128.64 o -10 2 2 107.25 118.52 128.32 o -8 2 2 65.53 108.48 72.92 o -6 2 2 4258.45 4724.85 98.28 o -4 2 2 7207.34 7258.49 153.34 o -2 2 2 16625.80 16586.10 209.98 o 0 2 2 0.64 14.72 20.65 o 2 2 2 16117.32 15675.76 211.95 o 4 2 2 8703.05 8548.44 72.67 o 6 2 2 5837.68 5510.72 123.35 o 8 2 2 245.37 265.52 55.66 o 10 2 2 11.16 19.80 87.34 o 12 2 2 61.33 94.61 138.90 o 14 2 2 0.11 70.17 218.12 o 16 2 2 213.22 119.07 275.71 o -15 3 2 73.52 33.19 65.30 o -13 3 2 81.97 30.44 115.58 o -11 3 2 577.55 646.14 144.15 o -9 3 2 71.82 82.09 92.87 o -7 3 2 11386.20 11713.36 423.36 o -5 3 2 374.15 422.15 39.57 o -3 3 2 2129.93 2335.55 100.70 o -1 3 2 6971.07 6771.27 163.98 o 1 3 2 12807.83 12716.67 94.89 o 3 3 2 9836.74 9485.35 96.14 o 5 3 2 1042.83 1075.55 51.02 o 7 3 2 4116.33 4353.89 66.30 o 9 3 2 24.14 3.88 11.22 o 11 3 2 212.01 169.87 133.51 o 13 3 2 7.27 40.84 105.39 o 15 3 2 30.43 7.61 296.02 o -16 4 2 11.17 85.81 204.77 o -14 4 2 550.14 467.79 171.84 o -12 4 2 1186.51 1046.01 162.49 o -10 4 2 17.83 29.52 143.59 o -8 4 2 578.86 596.95 59.61 o -6 4 2 3429.74 3658.90 125.13 o -4 4 2 1067.85 1119.76 40.00 o -2 4 2 8613.82 8218.84 251.91 o 0 4 2 41.02 13.69 20.29 o 2 4 2 7889.34 7766.09 97.38 o 4 4 2 60.19 27.24 31.42 o 6 4 2 6296.52 6392.67 93.16 o 8 4 2 753.11 843.91 61.98 o 10 4 2 7.72 0.00 10.06 o 12 4 2 675.43 605.02 151.17 o 14 4 2 313.43 181.89 234.34 o -15 5 2 0.07 0.91 128.60 o -13 5 2 115.54 113.45 189.39 o -11 5 2 735.09 588.04 119.34 o -9 5 2 29.72 22.35 69.89 o -7 5 2 12.60 43.89 58.46 o -5 5 2 11.58 6.26 35.97 o -3 5 2 71.16 74.07 44.46 o -1 5 2 5363.93 5537.22 111.01 o 1 5 2 6733.00 7086.63 183.41 o 3 5 2 661.30 708.37 51.52 o 5 5 2 410.64 430.82 58.84 o 7 5 2 89.28 69.47 67.03 o 9 5 2 10.07 0.00 53.83 o 11 5 2 235.24 201.98 141.53 o 13 5 2 13.52 19.61 168.60 o 15 5 2 0.23 35.38 220.50 o -14 6 2 27.32 111.52 269.88 o -12 6 2 623.88 720.24 174.38 o -10 6 2 82.88 114.71 118.54 o -8 6 2 91.48 94.26 72.42 o -6 6 2 171.20 150.60 56.45 o -4 6 2 556.02 528.95 46.48 o -2 6 2 35.59 5.64 70.48 o 0 6 2 16.54 45.73 45.20 o 2 6 2 29.35 32.94 62.03 o 4 6 2 69.42 72.19 72.00 o 6 6 2 235.14 179.34 68.71 o 8 6 2 108.46 116.04 83.74 o 10 6 2 63.60 16.72 92.93 o 12 6 2 314.37 469.90 193.39 o 14 6 2 4.60 90.49 254.19 o -15 7 2 9.70 6.56 157.33 o -13 7 2 14.85 0.00 129.86 o -11 7 2 29.52 25.50 129.86 o -9 7 2 7.01 9.68 100.34 o -7 7 2 0.31 51.58 83.71 o -5 7 2 17.65 41.30 56.52 o -3 7 2 46.11 49.97 69.86 o -1 7 2 130.82 155.04 66.86 o 1 7 2 207.63 382.41 66.45 o 3 7 2 57.55 76.52 69.46 o 5 7 2 0.85 28.39 80.52 o 7 7 2 15.85 0.00 71.43 o 9 7 2 6.88 5.31 71.64 o 11 7 2 29.95 0.00 158.79 o 13 7 2 10.36 30.74 250.83 o -14 8 2 72.04 3.40 263.93 o -12 8 2 34.31 43.07 109.44 o -10 8 2 17.36 51.44 132.86 o -8 8 2 331.40 397.29 107.47 o -6 8 2 658.91 602.80 78.92 o -4 8 2 104.22 131.32 81.90 o -2 8 2 136.61 154.71 69.99 o 0 8 2 17.17 42.97 100.03 o 2 8 2 231.34 250.62 78.33 o 4 8 2 1.71 18.86 45.11 o 6 8 2 524.91 516.04 88.17 o 8 8 2 233.42 269.74 101.95 o 10 8 2 4.67 47.31 148.78 o 12 8 2 55.81 123.38 314.66 o -13 9 2 97.98 82.98 225.29 o -11 9 2 15.30 84.20 153.55 o -9 9 2 479.82 425.47 125.61 o -7 9 2 297.77 248.98 109.38 o -5 9 2 0.43 26.70 86.42 o -3 9 2 4.62 30.60 111.26 o -1 9 2 0.01 22.35 31.76 o 1 9 2 81.75 125.09 88.26 o 3 9 2 300.59 241.53 89.61 o 5 9 2 52.59 113.23 97.87 o 7 9 2 330.53 328.89 105.52 o 9 9 2 401.55 424.80 146.96 o 11 9 2 9.55 62.01 228.85 o -12 10 2 4.59 0.00 229.38 o -10 10 2 161.79 154.57 153.80 o -8 10 2 282.47 274.99 130.29 o -6 10 2 526.56 410.92 116.62 o -4 10 2 82.11 88.91 95.11 o -2 10 2 0.14 6.30 83.22 o 0 10 2 29.03 49.29 140.35 o 2 10 2 23.07 97.04 104.81 o 4 10 2 226.18 187.65 109.19 o 6 10 2 88.63 41.64 86.32 o 8 10 2 350.71 305.07 129.64 o 10 10 2 140.59 96.91 212.31 o -11 11 2 42.16 48.21 178.30 o -9 11 2 222.72 236.82 155.27 o -7 11 2 282.36 309.19 139.85 o -5 11 2 138.68 159.93 111.53 o -3 11 2 339.85 417.20 152.23 o -1 11 2 337.89 354.57 152.39 o 1 11 2 587.54 656.36 132.69 o 3 11 2 784.91 880.83 119.39 o 5 11 2 0.35 0.00 110.54 o 7 11 2 91.35 112.75 138.50 o 9 11 2 81.52 108.36 214.50 o -10 12 2 2.68 27.06 178.15 o -8 12 2 20.80 61.20 161.20 o -6 12 2 193.04 173.74 168.80 o -4 12 2 16.43 44.34 153.56 o -2 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