#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/72/2217239.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217239_Fobs loop_ _publ_author_name 'Shustova, Natalia B.' 'Anderson, Oren P.' 'Boltalina, Olga V.' 'Strauss, Steven H.' 'Kareev, Ivan E.' _publ_section_title ; 1,3,7,10,14,17,21,28,31,42,52,55-Dodecakis(trifluoromethyl)- 1,3,7,10,14,17,21,28,31,42,52,55-dodecahydro(C~60~--I~h~)[5,6]fullerene ; _journal_coeditor_code OM2195 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o159 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.288 _cell_angle_gamma 90.000 _cell_length_a 12.2475 _cell_length_b 20.0326 _cell_length_c 20.3782 _exptl_crystal_F_000 3024.00 _reflns_d_resolution_high 0.7897 _[local]_cod_data_source_file om2195Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ss203 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 398.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 36749.82 43735.77 432.30 o 4 0 0 13738.28 13694.37 151.16 o 6 0 0 8260.67 7629.93 111.60 o 8 0 0 6163.30 5920.85 119.03 o 10 0 0 17914.81 17592.37 294.70 o 12 0 0 2052.16 1822.99 107.04 o 14 0 0 19.55 -64.90 64.90 o 1 1 0 5323.48 6776.65 55.40 o 2 1 0 5186.59 5870.33 43.38 o 3 1 0 5551.77 4519.99 40.24 o 4 1 0 1537.38 1551.62 27.62 o 5 1 0 9791.08 10400.35 88.35 o 6 1 0 8349.96 8711.98 80.82 o 7 1 0 10613.49 10736.00 102.64 o 8 1 0 2924.59 3313.85 57.35 o 9 1 0 2926.86 3140.05 80.79 o 10 1 0 5926.46 5455.49 92.47 o 11 1 0 885.54 818.50 61.37 o 12 1 0 1087.56 1019.26 60.86 o 13 1 0 272.51 338.62 47.45 o 14 1 0 424.66 399.57 87.59 o 15 1 0 88.70 108.07 131.57 o 0 2 0 40845.63 41084.55 405.69 o 1 2 0 6654.21 6396.05 45.45 o 2 2 0 19077.14 19261.61 128.73 o 3 2 0 185.62 79.55 9.62 o 4 2 0 13015.83 12662.10 94.03 o 5 2 0 397.83 500.70 20.62 o 6 2 0 4046.21 4509.92 51.47 o 7 2 0 5702.84 5807.24 64.39 o 8 2 0 26.85 -5.38 19.54 o 9 2 0 5344.53 5383.69 79.76 o 10 2 0 2.73 26.50 28.84 o 11 2 0 2503.98 2367.33 83.42 o 12 2 0 330.11 288.86 44.59 o 13 2 0 1709.72 1759.85 90.04 o 14 2 0 15.38 -27.38 55.54 o 15 2 0 418.56 401.71 87.32 o 1 3 0 39677.07 37992.91 236.77 o 2 3 0 1643.67 1771.94 23.10 o 3 3 0 10733.34 10752.14 80.61 o 4 3 0 656.01 1423.59 24.62 o 5 3 0 76.34 174.23 13.77 o 6 3 0 71.37 134.93 16.47 o 7 3 0 1235.83 1407.20 35.76 o 8 3 0 2256.76 2260.55 49.27 o 9 3 0 2484.53 2462.85 57.11 o 10 3 0 1019.92 1026.56 47.68 o 11 3 0 70.40 56.72 40.34 o 12 3 0 1046.35 983.58 57.32 o 13 3 0 17.46 18.89 54.32 o 14 3 0 256.44 299.21 71.73 o 15 3 0 462.92 319.54 89.28 o 0 4 0 916.93 630.66 21.10 o 1 4 0 76360.05 80708.18 496.43 o 2 4 0 7970.59 8581.11 64.30 o 3 4 0 8.23 7.82 8.56 o 4 4 0 9355.51 9031.16 71.99 o 5 4 0 9309.91 8955.11 77.89 o 6 4 0 31.37 59.24 14.17 o 7 4 0 449.82 602.88 25.99 o 8 4 0 2223.40 2156.24 49.22 o 9 4 0 929.02 968.57 39.09 o 10 4 0 0.60 20.98 32.45 o 11 4 0 563.53 566.10 46.76 o 12 4 0 238.12 208.20 47.59 o 13 4 0 16.29 5.79 55.89 o 14 4 0 121.22 114.97 77.52 o 15 4 0 66.22 -100.44 100.44 o 1 5 0 17450.36 19929.35 134.45 o 2 5 0 35077.63 33564.24 231.62 o 3 5 0 787.61 992.13 22.09 o 4 5 0 7517.53 8611.13 78.04 o 5 5 0 237.25 383.74 20.50 o 6 5 0 1706.41 1829.69 36.03 o 7 5 0 201.77 231.06 19.25 o 8 5 0 6181.22 5933.98 79.07 o 9 5 0 242.92 228.05 28.46 o 10 5 0 446.06 505.74 43.04 o 11 5 0 3159.18 3222.29 85.26 o 12 5 0 196.53 139.85 57.70 o 13 5 0 661.56 748.90 84.11 o 14 5 0 1.24 37.62 76.55 o 15 5 0 40.26 11.96 127.66 o 0 6 0 24956.38 25022.57 240.79 o 1 6 0 3451.35 4065.21 40.62 o 2 6 0 336.66 246.44 12.82 o 3 6 0 10660.15 10781.84 82.30 o 4 6 0 11017.65 13011.94 110.35 o 5 6 0 550.63 739.19 23.89 o 6 6 0 5235.40 5343.97 62.68 o 7 6 0 588.71 623.77 24.36 o 8 6 0 475.98 558.81 29.89 o 9 6 0 4848.18 4712.06 80.54 o 10 6 0 1358.11 1350.12 60.56 o 11 6 0 1629.00 1527.54 74.42 o 12 6 0 31.82 -4.15 61.02 o 13 6 0 416.32 623.51 96.81 o 14 6 0 402.08 265.61 90.68 o 15 6 0 0.35 25.55 109.51 o 1 7 0 5824.91 5716.37 53.45 o 2 7 0 24764.91 25170.76 167.74 o 3 7 0 1881.99 1831.91 31.19 o 4 7 0 2993.36 3021.13 39.24 o 5 7 0 269.62 349.22 19.16 o 6 7 0 8882.50 8608.25 83.89 o 7 7 0 2103.18 2194.22 43.39 o 8 7 0 1090.15 1189.79 35.03 o 9 7 0 1475.08 1481.29 51.97 o 10 7 0 4786.89 4375.31 93.37 o 11 7 0 74.20 23.69 42.54 o 12 7 0 1516.55 1463.04 130.42 o 13 7 0 65.74 -73.68 73.68 o 14 7 0 421.83 572.54 103.42 o 0 8 0 976.92 1308.08 43.44 o 1 8 0 1472.23 1587.38 29.98 o 2 8 0 8670.76 8608.00 71.48 o 3 8 0 1320.38 1571.28 34.82 o 4 8 0 481.03 552.79 21.25 o 5 8 0 2300.34 2377.05 44.72 o 6 8 0 11.90 -1.70 18.19 o 7 8 0 62.74 56.30 19.69 o 8 8 0 1248.22 1282.54 41.87 o 9 8 0 5.38 52.13 28.35 o 10 8 0 1527.86 1589.15 70.83 o 11 8 0 2191.92 2308.59 113.37 o 12 8 0 388.71 324.83 72.92 o 13 8 0 57.84 69.74 79.18 o 14 8 0 453.04 766.62 158.68 o 1 9 0 2173.34 1940.24 33.74 o 2 9 0 55.38 100.90 15.31 o 3 9 0 19882.63 21391.94 160.36 o 4 9 0 1066.87 992.13 29.40 o 5 9 0 3274.25 3572.91 53.74 o 6 9 0 304.84 376.47 22.53 o 7 9 0 74.65 75.04 20.20 o 8 9 0 71.43 72.13 25.63 o 9 9 0 302.35 237.43 34.28 o 10 9 0 4257.62 4055.84 99.79 o 11 9 0 326.84 201.40 69.12 o 12 9 0 79.98 92.28 68.31 o 13 9 0 3.68 -23.55 78.53 o 14 9 0 11.70 209.22 124.18 o 0 10 0 4890.70 4488.13 74.12 o 1 10 0 6656.89 6112.20 63.40 o 2 10 0 368.19 475.30 19.65 o 3 10 0 3010.38 3424.41 48.59 o 4 10 0 3179.30 3352.76 53.48 o 5 10 0 726.56 814.53 30.85 o 6 10 0 2293.55 2332.99 53.90 o 7 10 0 2633.90 2735.71 52.44 o 8 10 0 84.06 96.23 25.67 o 9 10 0 26.79 51.97 32.15 o 10 10 0 34.91 52.33 40.76 o 11 10 0 133.12 115.31 85.31 o 12 10 0 0.03 15.08 75.78 o 13 10 0 262.69 229.42 92.04 o 14 10 0 252.57 344.36 126.13 o 1 11 0 4.43 0.48 14.88 o 2 11 0 3740.83 3800.73 46.11 o 3 11 0 450.18 476.36 29.59 o 4 11 0 0.87 17.56 19.59 o 5 11 0 2348.30 2548.01 61.25 o 6 11 0 1714.85 1707.85 46.76 o 7 11 0 88.75 83.18 23.62 o 8 11 0 1500.41 1565.72 51.37 o 9 11 0 38.55 72.32 34.16 o 10 11 0 58.70 92.62 45.74 o 11 11 0 1.08 22.60 67.84 o 12 11 0 101.00 123.32 84.72 o 13 11 0 136.97 224.57 95.65 o 0 12 0 5798.75 6224.47 97.19 o 1 12 0 171.38 189.58 20.63 o 2 12 0 404.85 531.13 21.67 o 3 12 0 2493.56 2432.03 53.57 o 4 12 0 88.41 108.72 22.86 o 5 12 0 440.99 580.09 33.26 o 6 12 0 269.13 284.92 28.49 o 7 12 0 365.61 340.57 33.34 o 8 12 0 711.41 657.11 44.76 o 9 12 0 1373.62 1386.45 68.78 o 10 12 0 32.10 9.85 65.67 o 11 12 0 491.25 584.23 79.94 o 12 12 0 667.08 810.21 114.96 o 13 12 0 463.57 235.87 101.75 o 1 13 0 1564.13 1433.90 37.49 o 2 13 0 1283.68 1428.77 31.74 o 3 13 0 694.19 791.78 34.62 o 4 13 0 15.91 -9.24 21.58 o 5 13 0 1496.72 1418.73 46.14 o 6 13 0 93.84 84.51 28.67 o 7 13 0 228.94 202.81 35.61 o 8 13 0 688.35 574.77 48.98 o 9 13 0 309.63 252.72 56.13 o 10 13 0 1182.56 1310.43 82.11 o 11 13 0 161.13 95.68 84.16 o 12 13 0 6.16 -77.34 77.34 o 13 13 0 291.67 319.06 121.86 o 0 14 0 2672.86 2771.88 90.03 o 1 14 0 269.10 229.95 22.00 o 2 14 0 1051.85 1107.63 31.84 o 3 14 0 22.72 70.32 23.34 o 4 14 0 1115.73 1106.48 42.82 o 5 14 0 1.62 39.59 25.43 o 6 14 0 668.56 803.86 45.75 o 7 14 0 966.57 1084.16 58.96 o 8 14 0 158.70 95.14 40.33 o 9 14 0 348.86 560.96 50.99 o 10 14 0 539.77 529.15 64.84 o 11 14 0 79.93 31.36 84.55 o 12 14 0 30.67 33.00 125.71 o 1 15 0 280.85 299.95 25.20 o 2 15 0 3030.97 3092.78 52.06 o 3 15 0 330.42 258.58 29.53 o 4 15 0 400.04 353.49 33.46 o 5 15 0 645.91 666.79 43.53 o 6 15 0 486.54 512.94 45.17 o 7 15 0 223.68 238.77 41.68 o 8 15 0 670.95 632.53 52.93 o 9 15 0 601.31 534.15 53.42 o 10 15 0 1788.69 1852.02 125.86 o 11 15 0 44.78 60.58 94.65 o 12 15 0 324.62 332.41 127.38 o 0 16 0 1556.46 1622.59 78.99 o 1 16 0 1708.50 1712.93 43.97 o 2 16 0 760.14 927.48 32.29 o 3 16 0 126.86 92.39 28.46 o 4 16 0 2632.76 2413.64 66.61 o 5 16 0 260.06 370.81 43.01 o 6 16 0 34.56 18.72 36.45 o 7 16 0 557.84 507.73 50.11 o 8 16 0 191.54 247.99 45.36 o 9 16 0 173.41 94.07 46.21 o 10 16 0 151.50 59.70 78.71 o 11 16 0 1.34 138.31 96.32 o 12 16 0 429.54 52.82 162.45 o 1 17 0 1237.43 1174.42 41.94 o 2 17 0 259.97 223.47 30.46 o 3 17 0 865.78 991.75 51.26 o 4 17 0 50.47 89.99 35.09 o 5 17 0 373.43 387.25 44.37 o 6 17 0 471.23 441.26 53.04 o 7 17 0 805.08 754.11 57.34 o 8 17 0 0.79 23.05 41.91 o 9 17 0 730.14 655.17 83.74 o 10 17 0 0.02 -50.84 70.62 o 11 17 0 264.43 188.56 125.22 o 0 18 0 1880.53 1678.25 82.48 o 1 18 0 481.92 381.91 36.00 o 2 18 0 700.46 589.85 47.83 o 3 18 0 200.15 136.66 38.56 o 4 18 0 1.52 -3.82 44.25 o 5 18 0 17.14 75.89 37.90 o 6 18 0 15.79 157.97 46.52 o 7 18 0 519.80 424.45 52.81 o 8 18 0 267.35 353.80 53.11 o 9 18 0 1166.75 1345.44 73.41 o 10 18 0 1068.90 1176.71 124.90 o 1 19 0 344.83 322.35 40.06 o 2 19 0 116.99 131.08 41.62 o 3 19 0 2502.68 2429.90 78.71 o 4 19 0 30.05 26.50 40.09 o 5 19 0 17.83 -25.43 40.18 o 6 19 0 567.46 693.72 63.99 o 7 19 0 48.79 -4.03 48.52 o 8 19 0 9.69 -49.99 49.99 o 9 19 0 50.78 57.95 49.09 o 10 19 0 3.76 17.49 100.38 o 0 20 0 3418.70 3349.47 122.58 o 1 20 0 481.42 418.29 46.08 o 2 20 0 168.00 229.73 49.17 o 3 20 0 44.74 62.17 44.07 o 4 20 0 626.42 564.55 57.30 o 5 20 0 953.00 920.40 64.29 o 6 20 0 8.30 8.32 49.73 o 7 20 0 533.43 422.46 64.18 o 8 20 0 9.21 62.90 54.69 o 9 20 0 35.82 67.97 61.50 o 1 21 0 98.74 149.18 55.34 o 2 21 0 30.25 11.61 46.11 o 3 21 0 284.61 272.82 55.60 o 4 21 0 20.73 11.47 45.99 o 5 21 0 17.24 28.75 49.30 o 6 21 0 2.45 -23.15 51.25 o 7 21 0 124.14 146.37 59.72 o 8 21 0 44.32 67.79 77.55 o 0 22 0 116.10 119.37 72.86 o 1 22 0 518.49 503.66 56.81 o 2 22 0 4.98 55.83 55.33 o 3 22 0 83.60 103.73 52.68 o 4 22 0 232.17 201.89 55.40 o 5 22 0 974.42 1038.13 75.42 o 6 22 0 275.28 255.70 75.79 o 7 22 0 42.62 73.64 74.21 o 1 23 0 133.04 224.21 53.70 o 2 23 0 717.82 728.02 97.30 o 3 23 0 18.71 -50.40 50.40 o 4 23 0 449.09 403.24 69.29 o 5 23 0 29.49 -37.54 56.42 o 6 23 0 0.21 2.78 86.57 o 0 24 0 953.86 908.60 116.64 o 1 24 0 1189.34 1228.66 88.30 o 2 24 0 6.02 63.05 55.73 o 3 24 0 86.55 23.67 58.63 o 4 24 0 15.39 49.80 63.08 o 5 24 0 446.95 413.85 105.29 o 1 25 0 368.59 373.12 86.00 o 2 25 0 19.66 28.81 70.98 o -15 0 1 178.01 371.80 208.00 o -13 0 1 84.32 126.51 106.73 o -11 0 1 2479.14 2314.34 97.68 o -9 0 1 3149.68 3373.98 91.97 o -7 0 1 0.37 0.89 21.80 o -5 0 1 4685.21 4986.58 72.13 o -3 0 1 65038.82 66467.39 723.79 o -1 0 1 5405.61 8402.19 207.41 o 1 0 1 22403.43 27979.93 249.03 o 3 0 1 24392.97 24048.86 219.86 o 5 0 1 1187.93 984.01 36.28 o 7 0 1 26223.54 25275.48 281.73 o 9 0 1 19902.65 20004.16 300.67 o 11 0 1 287.78 210.98 67.22 o 13 0 1 5.34 -24.65 72.93 o 15 0 1 149.09 87.96 67.18 o -15 1 1 60.84 17.51 129.04 o -14 1 1 28.45 -81.12 89.14 o -13 1 1 350.70 317.38 54.30 o -12 1 1 1119.93 1039.44 77.13 o -11 1 1 1893.71 1932.38 63.97 o -10 1 1 35.59 -26.95 26.95 o -9 1 1 3199.66 3258.05 62.80 o -8 1 1 896.85 1013.53 32.35 o -7 1 1 2861.29 2898.19 44.08 o -6 1 1 6573.12 7106.02 71.72 o -5 1 1 1747.65 1708.49 28.64 o -4 1 1 167.62 47.84 10.71 o -3 1 1 683.98 893.21 19.88 o -2 1 1 12786.29 15088.77 118.86 o -1 1 1 3963.30 4472.04 48.25 o 1 1 1 8995.47 8874.17 57.31 o 2 1 1 32034.80 37465.86 226.35 o 3 1 1 0.02 19.54 9.76 o 4 1 1 4434.02 4800.11 43.58 o 5 1 1 299.71 238.64 14.52 o 6 1 1 2553.13 3063.23 42.41 o 7 1 1 84.53 -17.75 17.75 o 8 1 1 559.45 612.08 32.58 o 9 1 1 13665.56 13070.27 152.86 o 10 1 1 1672.89 1522.30 57.10 o 11 1 1 5283.51 5068.87 116.76 o 12 1 1 948.10 970.19 62.17 o 13 1 1 514.00 406.53 53.95 o 14 1 1 163.19 136.19 49.03 o 15 1 1 370.20 422.13 78.62 o -15 2 1 1.10 -105.73 259.56 o -14 2 1 68.24 52.89 62.73 o -13 2 1 29.74 -25.46 48.29 o -12 2 1 932.06 876.17 95.72 o -11 2 1 1887.85 1753.44 69.00 o -10 2 1 473.62 441.16 34.13 o -9 2 1 4397.41 4363.00 81.87 o -8 2 1 3926.99 3796.27 55.86 o -7 2 1 1728.80 1858.61 39.74 o -6 2 1 3589.49 3296.32 41.60 o -5 2 1 3084.14 2842.12 36.52 o -4 2 1 9373.92 8868.56 79.77 o -3 2 1 876.19 874.90 20.17 o -2 2 1 7147.00 7511.68 56.63 o -1 2 1 41.67 4.10 5.01 o 0 2 1 264.14 1069.52 11.82 o 1 2 1 7772.09 7328.69 49.36 o 2 2 1 0.66 58.85 8.45 o 3 2 1 22236.85 22392.39 149.04 o 4 2 1 4520.79 4604.56 43.57 o 5 2 1 15928.65 15822.87 114.77 o 6 2 1 2898.38 2712.19 39.36 o 7 2 1 4173.04 4111.82 55.47 o 8 2 1 158.34 167.57 24.66 o 9 2 1 2447.17 2422.52 60.84 o 10 2 1 6709.44 6348.31 103.36 o 11 2 1 3434.72 3246.51 95.21 o 12 2 1 2349.31 1930.33 81.37 o 13 2 1 308.19 302.76 52.23 o 14 2 1 67.12 -34.37 47.48 o 15 2 1 15.83 47.39 95.52 o -15 3 1 2.70 -64.79 121.32 o -14 3 1 5.43 75.09 57.14 o -13 3 1 938.21 668.82 74.64 o -12 3 1 2.74 34.42 48.17 o -11 3 1 112.02 11.81 42.86 o -10 3 1 69.27 25.22 26.82 o -9 3 1 5125.94 4997.32 96.51 o -8 3 1 2108.26 1993.43 43.07 o -7 3 1 3233.98 3059.99 45.78 o -6 3 1 1764.57 1660.21 31.40 o -5 3 1 63.60 132.53 14.99 o -4 3 1 24803.75 27171.54 214.73 o -3 3 1 1838.69 2382.85 28.76 o -2 3 1 9270.89 7575.63 59.43 o -1 3 1 18934.09 21828.89 154.08 o 0 3 1 1318.51 1367.87 15.16 o 1 3 1 655.30 1310.15 17.85 o 2 3 1 1216.18 1194.66 19.17 o 3 3 1 1660.94 1626.43 22.03 o 4 3 1 17382.09 18495.94 136.90 o 5 3 1 8653.63 10052.08 83.22 o 6 3 1 4835.64 4661.90 51.94 o 7 3 1 1566.14 1409.00 37.59 o 8 3 1 2.27 7.29 19.39 o 9 3 1 5925.69 6008.90 95.90 o 10 3 1 2108.63 1898.08 82.94 o 11 3 1 2835.55 2637.30 87.90 o 12 3 1 475.10 525.36 73.88 o 13 3 1 348.61 373.09 56.00 o 14 3 1 115.61 133.47 66.08 o 15 3 1 1954.04 2060.56 214.31 o -15 4 1 488.57 453.91 127.72 o -14 4 1 284.66 193.49 65.47 o -13 4 1 14.60 60.16 59.35 o -12 4 1 17.24 25.93 50.21 o -11 4 1 3653.11 3404.62 125.73 o -10 4 1 1035.37 955.93 55.47 o -9 4 1 147.65 199.27 25.54 o -8 4 1 10867.58 10818.18 112.80 o -7 4 1 1.11 -9.20 16.31 o -6 4 1 3594.13 3744.00 48.95 o -5 4 1 6735.06 6558.21 64.72 o -4 4 1 6891.48 6474.10 57.63 o -3 4 1 20742.70 20345.55 148.65 o -2 4 1 13695.20 15133.82 112.74 o -1 4 1 4799.83 5620.21 45.51 o 0 4 1 65208.01 75229.06 432.59 o 1 4 1 4915.88 3745.37 34.59 o 2 4 1 13.23 31.41 10.00 o 3 4 1 2485.34 2931.25 30.85 o 4 4 1 80.24 43.22 10.76 o 5 4 1 3684.52 4371.73 48.92 o 6 4 1 1909.77 1803.55 33.73 o 7 4 1 1070.78 1202.24 31.89 o 8 4 1 1348.66 1505.94 44.86 o 9 4 1 1097.19 1018.81 56.26 o 10 4 1 181.07 158.59 35.94 o 11 4 1 2244.77 2114.80 81.22 o 12 4 1 212.20 200.80 45.68 o 13 4 1 175.99 127.18 48.65 o 14 4 1 722.06 615.74 91.48 o 15 4 1 34.70 316.36 123.74 o -15 5 1 159.00 203.65 82.95 o -14 5 1 6.90 -71.27 71.27 o -13 5 1 1365.14 1335.35 97.90 o -12 5 1 413.50 417.20 63.16 o -11 5 1 1193.43 1215.42 82.18 o -10 5 1 127.30 158.70 42.88 o -9 5 1 169.39 159.95 27.56 o -8 5 1 2363.86 2450.93 49.44 o -7 5 1 313.59 377.77 21.88 o -6 5 1 8641.94 8350.46 81.87 o -5 5 1 6098.82 5355.06 52.49 o -4 5 1 1586.42 1560.24 30.41 o -3 5 1 54587.14 59334.00 408.42 o -2 5 1 17710.23 17717.96 126.04 o -1 5 1 76734.82 76802.24 499.83 o 0 5 1 54179.94 54122.43 350.28 o 1 5 1 4248.15 4282.17 39.87 o 2 5 1 714.81 868.50 19.17 o 3 5 1 14290.43 16261.67 110.10 o 4 5 1 2718.54 2734.60 34.68 o 5 5 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