#------------------------------------------------------------------------------
#$Date: 2016-04-03 01:45:55 +0300 (Sun, 03 Apr 2016) $
#$Revision: 181092 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/72/2217242.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2217242_Fobs
loop_
_publ_author_name
'Daszkiewicz, M.'
'Gulay, L. D.'
'Shemet, V. Ya.'
'Pietraszko, A.'
_publ_section_title
;
 Dy~8~SnS~13.61~O~0.39~ from single-crystal data
;
_journal_coeditor_code           PK2066
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              i2
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           36
_symmetry_space_group_name_Hall  'C 2c -2'
_symmetry_space_group_name_H-M   'C m c 21'
_cell_angle_alpha                90.000
_cell_angle_beta                 90.000
_cell_angle_gamma                90.000
_cell_length_a                   3.7822
_cell_length_b                   23.6202
_cell_length_c                   21.2708
_exptl_crystal_F_000             3195.52
_reflns_d_resolution_high        0.7903
_cod_data_source_file            pk2066Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' Dy8SnS14 in Cmc2(1)'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            1719.04
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x, -y, z+1/2'
'-x, y, z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 3 -26 18160.71 17866.74 15035.40 o
0 4 -26 53690.29 54650.74 12411.04 o
0 6 -26 13292.59 8865.03 8345.62 o
1 3 -25 13055.59 11848.67 9532.83 o
1 5 -25 142356.67 133287.83 16687.34 o
0 6 -25 50324.43 41458.65 10997.32 o
1 7 -25 4530.36 4639.49 7970.71 o
0 8 -25 10456.49 7806.69 10083.48 o
1 9 -25 45775.34 53155.02 17237.99 o
0 10 -25 33366.97 34151.83 15410.31 o
1 1 -24 53505.41 54978.79 16089.83 o
1 3 -24 80613.34 66706.41 16292.90 o
2 4 -24 8732.54 8841.59 8201.13 o
1 5 -24 8252.67 6049.31 6803.03 o
0 6 -24 25684.70 21975.11 10809.87 o
1 7 -24 83420.37 70205.55 15746.16 o
0 8 -24 115.28 1519.16 6076.64 o
1 9 -24 39778.99 48085.94 17608.99 o
0 10 -24 26685.66 37311.22 13082.75 o
1 11 -24 6729.80 5654.87 9501.59 o
0 12 -24 72581.72 57903.86 15785.21 o
1 1 -23 92061.99 82292.45 15488.41 o
2 2 -23 109296.33 114847.01 10735.67 o
1 3 -23 107354.08 107708.12 14879.19 o
2 4 -23 9276.27 8878.09 5656.06 o
1 5 -23 48325.84 47851.62 13840.38 o
2 6 -23 1791.00 2013.02 4211.73 o
1 7 -23 1091.77 2350.99 5912.62 o
0 8 -23 11326.55 10657.56 11415.19 o
2 8 -23 9082.47 12377.10 6965.17 o
1 9 -23 4621.04 3917.85 4784.47 o
0 10 -23 30739.58 38619.49 14562.86 o
1 11 -23 26806.57 32333.60 7964.86 o
0 12 -23 112785.07 110355.91 15789.12 o
1 13 -23 22393.96 8854.80 4774.28 o
0 14 -23 27971.90 30570.67 13020.26 o
2 0 -22 578.94 2651.70 3659.26 o
1 1 -22 70713.76 68132.70 10741.92 o
2 2 -22 3636.98 4748.84 4311.45 o
1 3 -22 66488.46 57704.68 17054.44 o
2 4 -22 36712.18 39505.59 9329.50 o
1 5 -22 13199.55 20198.20 12731.27 o
2 6 -22 60686.76 63184.61 8249.94 o
1 7 -22 46564.18 45644.07 7449.35 o
0 8 -22 72532.16 67674.91 12785.95 o
2 8 -22 59979.49 62701.36 8326.10 o
1 9 -22 6963.58 7018.04 4884.14 o
0 10 -22 47460.29 50983.67 13410.79 o
2 10 -22 37990.60 38337.36 8607.52 o
1 11 -22 178026.89 195377.08 10501.85 o
0 12 -22 36666.08 19893.59 8997.81 o
1 13 -22 9633.98 6654.56 4884.87 o
0 14 -22 41044.20 47055.50 8925.67 o
1 15 -22 64308.12 66176.51 7924.10 o
0 16 -22 9164.91 7379.07 4495.43 o
1 1 -21 121847.41 121304.43 12452.05 o
2 2 -21 19908.75 18886.68 4682.04 o
1 3 -21 71963.03 74970.01 14082.51 o
2 4 -21 32912.91 37975.53 8037.10 o
1 5 -21 20217.06 21415.66 5776.47 o
2 6 -21 416742.81 444914.72 11439.57 o
1 7 -21 35455.32 38337.66 5830.14 o
0 8 -21 93552.33 82604.87 10063.95 o
2 8 -21 73102.63 75637.80 9270.17 o
1 9 -21 41202.87 41941.61 7232.50 o
0 10 -21 22935.98 13402.98 8302.66 o
2 10 -21 18295.63 9119.78 4744.24 o
1 11 -21 12654.06 10622.29 5492.80 o
0 12 -21 6221.68 7477.94 5074.52 o
2 12 -21 5288.78 4173.87 4803.26 o
1 13 -21 43135.01 35719.72 7599.87 o
0 14 -21 18262.72 17168.54 5942.44 o
1 15 -21 10835.85 7054.04 5606.88 o
0 16 -21 5525.13 7204.83 5135.65 o
1 17 -21 11060.27 9983.86 5191.84 o
0 18 -21 7359.48 6785.32 4525.86 o
2 0 -20 4590.24 3018.80 3647.55 o
1 1 -20 5655.90 4830.06 4573.96 o
3 1 -20 3647.95 5026.49 4244.14 o
2 2 -20 4112.06 3544.24 2401.14 o
1 3 -20 21919.98 11628.14 6406.64 o
3 3 -20 12057.68 6244.01 4184.36 o
2 4 -20 56044.52 54688.99 6892.42 o
1 5 -20 40232.15 39138.10 5897.00 o
3 5 -20 26148.71 23480.22 5701.09 o
2 6 -20 45348.79 41977.67 5274.66 o
1 7 -20 5684.90 4938.23 3611.40 o
3 7 -20 2853.40 5058.44 4881.60 o
2 8 -20 114992.68 122500.48 9809.43 o
1 9 -20 122220.66 127629.72 7798.26 o
0 10 -20 41739.10 45792.73 6765.09 o
2 10 -20 34542.49 41179.95 6924.52 o
1 11 -20 16821.38 14396.78 5057.96 o
0 12 -20 59929.57 56875.13 9179.40 o
2 12 -20 48693.29 55943.62 8783.56 o
1 13 -20 68021.33 70008.31 8414.77 o
0 14 -20 65844.01 68322.41 7957.75 o
2 14 -20 51556.97 57401.94 11764.71 o
1 15 -20 15871.68 16249.96 5701.34 o
0 16 -20 2111.83 3110.33 4756.85 o
1 17 -20 19649.43 24288.14 6311.44 o
0 18 -20 116581.73 113619.19 11047.83 o
1 19 -20 6278.04 5350.19 3672.11 o
0 20 -20 12106.78 5106.92 6378.71 o
1 1 -19 4686.93 5513.08 2265.82 o
3 1 -19 3650.71 2582.15 3352.03 o
2 2 -19 30468.51 33423.48 4721.93 o
1 3 -19 38376.97 40030.64 5495.22 o
3 3 -19 19554.88 14957.23 4450.77 o
2 4 -19 6170.44 4436.76 2768.33 o
1 5 -19 91073.87 88034.87 5523.67 o
3 5 -19 51237.55 51414.44 7216.99 o
2 6 -19 25222.41 23665.95 4623.23 o
1 7 -19 5414.98 3679.22 3099.92 o
3 7 -19 2417.83 3593.16 4800.43 o
0 8 -19 21754.34 21678.31 5842.33 o
2 8 -19 16914.45 15069.87 4688.19 o
1 9 -19 77718.21 78899.95 5705.25 o
3 9 -19 48655.82 41321.43 7163.80 o
0 10 -19 36009.50 40490.20 5702.18 o
2 10 -19 29091.40 34025.96 7381.12 o
1 11 -19 46908.82 49605.79 5752.08 o
0 12 -19 184950.27 183976.30 8143.34 o
2 12 -19 145133.92 154618.42 20676.60 o
1 13 -19 56367.91 61968.97 7734.15 o
0 14 -19 17432.72 14365.48 5975.46 o
2 14 -19 14068.86 15474.46 5816.14 o
1 15 -19 5288.68 3655.36 3125.62 o
0 16 -19 5729.74 3137.20 5348.77 o
2 16 -19 4207.54 3358.42 4964.33 o
1 17 -19 155324.52 153329.25 6893.37 o
0 18 -19 84500.66 100805.01 9782.88 o
1 19 -19 12006.46 11611.96 3745.89 o
0 20 -19 8175.88 3484.92 5461.42 o
2 0 -18 777739.25 812630.13 14703.45 o
1 1 -18 143570.39 145186.55 4339.17 o
3 1 -18 92237.12 97184.05 6953.32 o
2 2 -18 29302.36 32682.07 4291.73 o
1 3 -18 101346.43 100498.70 4289.32 o
3 3 -18 63242.35 60862.20 6726.96 o
2 4 -18 4234.02 5365.82 2981.57 o
1 5 -18 10250.03 12306.83 3701.43 o
3 5 -18 6487.81 5032.63 3695.91 o
0 6 -18 7453.01 11036.37 4655.12 o
2 6 -18 5813.08 5504.47 3271.72 o
1 7 -18 76786.65 74173.59 5957.15 o
3 7 -18 45607.81 46403.65 7317.99 o
0 8 -18 3363.28 2089.33 2612.64 o
2 8 -18 2511.16 3320.74 2478.98 o
1 9 -18 47526.13 53939.58 7472.79 o
3 9 -18 33389.93 30855.56 7051.30 o
0 10 -18 11499.22 12861.20 4368.08 o
2 10 -18 7703.67 5162.28 2626.44 o
1 11 -18 3852.81 1808.72 2835.21 o
3 11 -18 1375.38 5256.92 3480.69 o
0 12 -18 177595.52 185420.64 6836.93 o
2 12 -18 134218.23 147457.95 9931.97 o
1 13 -18 46893.79 49546.84 6282.29 o
0 14 -18 14075.28 11160.56 4393.73 o
2 14 -18 10697.04 12053.36 5435.02 o
1 15 -18 19196.83 17944.65 4720.35 o
0 16 -18 62728.82 72868.13 9071.92 o
2 16 -18 49922.41 41666.00 7182.53 o
1 17 -18 35896.77 35943.01 4937.05 o
0 18 -18 15067.45 16535.67 5273.59 o
2 18 -18 12032.50 9483.92 5842.48 o
1 19 -18 435.65 2769.68 2669.74 o
0 20 -18 29495.07 26630.72 6931.45 o
1 21 -18 12660.65 9081.84 3799.91 o
0 22 -18 2692.07 2315.95 4839.08 o
1 1 -17 140406.31 140145.77 4074.15 o
3 1 -17 82416.95 84240.01 6199.64 o
2 2 -17 44042.42 43157.90 4092.27 o
1 3 -17 126678.90 133090.52 4529.76 o
3 3 -17 70650.36 76428.91 6643.57 o
0 4 -17 26675.94 25868.70 5584.58 o
2 4 -17 23324.52 24566.90 4077.00 o
1 5 -17 43246.02 41372.24 3473.10 o
3 5 -17 23579.71 23938.44 5175.92 o
0 6 -17 33757.60 35920.93 5057.36 o
2 6 -17 24152.06 21687.20 4499.83 o
1 7 -17 4180.48 2874.89 2225.87 o
3 7 -17 3120.40 3339.93 3839.96 o
0 8 -17 8857.69 7771.54 4151.33 o
2 8 -17 6249.82 6903.40 3168.71 o
1 9 -17 21869.35 15782.21 4625.24 o
3 9 -17 12356.94 8198.79 4417.45 o
0 10 -17 16933.14 16575.56 4012.91 o
2 10 -17 13310.46 13482.59 3885.91 o
1 11 -17 70839.10 66057.56 5569.74 o
3 11 -17 47638.55 51414.45 5720.83 o
0 12 -17 98940.75 104397.98 6317.27 o
2 12 -17 75522.19 78748.37 6395.76 o
1 13 -17 860.17 2185.12 1960.36 o
3 13 -17 170.72 2812.68 2948.22 o
0 14 -17 32309.17 37118.25 6707.42 o
2 14 -17 23014.88 31928.40 7625.68 o
1 15 -17 120128.96 122617.78 5430.54 o
0 16 -17 35784.41 39920.67 5837.30 o
2 16 -17 28124.45 30031.64 8113.25 o
1 17 -17 11444.86 11772.29 3451.74 o
0 18 -17 158140.03 160793.52 7089.63 o
2 18 -17 128813.61 141554.23 12124.92 o
1 19 -17 88800.49 94216.55 6323.50 o
0 20 -17 12178.70 8634.12 4196.84 o
1 21 -17 9040.35 8115.93 3789.32 o
0 22 -17 1617.83 4740.64 3831.37 o
2 0 -16 64552.04 59588.31 5303.98 o
1 1 -16 116575.41 120506.99 3823.58 o
3 1 -16 60448.17 57327.88 5424.61 o
0 2 -16 2202.10 3905.30 3374.18 o
2 2 -16 1093.34 800.27 1714.44 o
1 3 -16 86876.97 93569.98 3653.13 o
3 3 -16 46844.09 47949.08 5408.80 o
0 4 -16 13928.79 16328.05 5479.13 o
2 4 -16 10352.80 11529.42 3378.28 o
1 5 -16 14340.87 14875.60 2944.10 o
3 5 -16 8444.02 9642.23 3878.88 o
0 6 -16 250309.59 273831.69 7599.71 o
2 6 -16 186171.98 193421.58 6806.08 o
1 7 -16 181599.89 179930.08 4693.87 o
3 7 -16 109149.02 117123.52 6079.39 o
0 8 -16 26371.58 28375.90 4850.38 o
2 8 -16 22402.13 23128.51 4201.04 o
1 9 -16 53314.08 48962.33 4625.22 o
3 9 -16 27000.09 25229.20 4678.45 o
0 10 -16 33155.86 30309.18 4497.61 o
2 10 -16 24392.72 21578.47 4247.53 o
1 11 -16 381363.97 385924.19 5726.56 o
3 11 -16 223729.53 224807.64 7730.32 o
0 12 -16 79439.50 88389.30 6178.48 o
2 12 -16 59287.82 66130.01 5139.06 o
1 13 -16 48709.86 48815.65 4296.58 o
3 13 -16 33387.76 28780.15 5141.51 o
0 14 -16 42614.69 41703.09 4913.64 o
2 14 -16 32600.03 36100.08 4961.40 o
1 15 -16 74998.03 82329.88 5684.32 o
3 15 -16 48654.47 50562.06 5798.48 o
0 16 -16 58865.86 61737.61 5900.04 o
2 16 -16 47884.25 58336.26 9187.21 o
1 17 -16 43824.58 55636.66 4602.45 o
0 18 -16 226351.53 220295.33 7016.42 o
2 18 -16 177010.86 186879.41 11420.69 o
1 19 -16 42820.53 47650.49 5504.55 o
0 20 -16 20663.98 17675.06 5330.26 o
2 20 -16 17616.72 24014.18 8184.20 o
1 21 -16 36201.85 37624.79 5758.09 o
0 22 -16 9833.74 6226.82 3701.93 o
1 23 -16 51233.88 51200.10 6922.59 o
0 24 -16 87306.51 101221.48 21731.03 o
1 1 -15 234303.16 237397.98 4954.35 o
3 1 -15 131345.88 142969.70 14119.61 o
0 2 -15 7714.12 6310.96 2975.84 o
2 2 -15 5067.46 7809.85 2952.39 o
1 3 -15 127759.21 131828.08 3307.34 o
3 3 -15 77383.89 78543.66 6340.43 o
0 4 -15 48600.82 51905.32 4819.14 o
2 4 -15 35186.73 36883.63 4419.21 o
1 5 -15 30430.21 31491.37 3051.47 o
3 5 -15 19897.05 21211.72 3858.73 o
0 6 -15 899456.44 941914.94 13063.22 o
2 6 -15 649716.63 669737.88 9210.03 o
1 7 -15 111116.31 111617.72 3068.79 o
3 7 -15 68254.07 79023.64 4778.64 o
0 8 -15 50714.17 44758.62 5147.18 o
2 8 -15 38123.77 38110.80 3374.83 o
1 9 -15 197911.44 196700.73 3431.13 o
3 9 -15 119137.29 118403.03 5706.37 o
0 10 -15 16047.72 19101.75 4664.99 o
2 10 -15 12228.54 12130.45 3040.69 o
1 11 -15 3507.96 5542.99 2445.91 o
3 11 -15 1896.97 3418.98 2849.25 o
0 12 -15 20339.57 20505.69 3389.35 o
2 12 -15 16167.63 18461.45 3551.78 o
1 13 -15 113295.69 123599.08 4543.01 o
3 13 -15 65156.32 61451.06 6227.89 o
0 14 -15 18402.76 16657.54 3396.31 o
2 14 -15 13242.71 13780.47 3926.78 o
1 15 -15 30694.15 32298.90 3816.07 o
3 15 -15 22397.81 23579.49 4931.98 o
0 16 -15 23050.40 20949.07 4370.28 o
2 16 -15 16057.63 13002.35 4316.24 o
1 17 -15 43032.49 45759.17 4408.77 o
0 18 -15 1581.34 2127.65 2299.71 o
2 18 -15 1378.06 2357.63 3404.11 o
1 19 -15 19784.56 22511.84 4134.85 o
0 20 -15 92.47 3270.46 3054.94 o
2 20 -15 110.37 1599.92 4410.94 o
1 21 -15 23909.90 22824.05 3992.05 o
0 22 -15 54660.77 59699.22 7201.38 o
1 23 -15 54965.14 45821.27 4886.57 o
0 24 -15 11259.97 11771.52 5792.93 o
0 0 -14 5375.67 4924.58 2749.33 o
2 0 -14 4997.87 4933.88 3249.86 o
4 0 -14 4195.29 3651.45 5611.91 o
1 1 -14 100138.60 104379.37 3575.74 o
3 1 -14 52759.63 50093.73 4652.46 o
0 2 -14 1621.66 1025.96 1037.46 o
2 2 -14 1359.97 1544.49 1503.26 o
4 2 -14 1431.33 2122.41 4085.98 o
1 3 -14 49110.66 46453.38 2611.21 o
3 3 -14 23400.52 20475.39 3200.11 o
0 4 -14 110981.91 114062.05 5330.73 o
2 4 -14 80162.24 84683.18 4430.14 o
4 4 -14 38608.24 42143.90 6081.36 o
1 5 -14 177860.58 177046.86 4420.39 o
3 5 -14 100668.52 101204.09 4710.10 o
0 6 -14 214413.83 214654.72 6564.81 o
2 6 -14 154233.42 153424.52 3861.01 o
1 7 -14 102627.38 104612.63 3386.48 o
3 7 -14 57809.29 58842.68 4569.71 o
0 8 -14 49917.23 50905.57 6049.31 o
2 8 -14 33249.91 33171.90 3726.33 o
1 9 -14 330950.28 337072.03 6198.67 o
3 9 -14 185094.13 177970.08 5453.11 o
0 10 -14 33203.08 32194.95 3801.05 o
2 10 -14 25442.42 25514.21 3201.39 o
1 11 -14 129127.18 134918.86 3799.44 o
3 11 -14 73573.91 67931.60 4969.38 o
0 12 -14 31792.14 32855.43 3471.50 o
2 12 -14 23898.62 25815.26 3808.18 o
1 13 -14 124824.70 126894.23 5062.75 o
3 13 -14 78197.68 77200.20 5314.01 o
0 14 -14 31142.16 30684.53 4341.84 o
2 14 -14 22944.04 20876.74 4018.86 o
1 15 -14 749.06 1027.00 1940.89 o
3 15 -14 781.26 3749.28 3334.06 o
0 16 -14 4495.44 2429.65 2320.14 o
2 16 -14 3794.96 4643.15 2489.66 o
1 17 -14 34982.09 36462.95 4539.62 o
3 17 -14 22621.77 19676.14 4711.66 o
0 18 -14 279642.84 292632.84 10548.54 o
2 18 -14 216452.66 228593.97 6610.48 o
1 19 -14 4003.34 3637.59 2286.40 o
0 20 -14 25154.49 23477.39 5219.95 o
2 20 -14 19285.36 18503.80 5589.24 o
1 21 -14 124252.20 123152.30 6393.00 o
0 22 -14 29652.94 27422.91 5918.91 o
2 22 -14 23333.59 17562.92 6422.06 o
1 23 -14 20748.47 21986.90 5019.52 o
0 24 -14 193628.31 201933.95 15706.91 o
1 1 -13 115284.67 114142.64 3389.01 o
3 1 -13 63115.65 61531.02 4175.19 o
0 2 -13 101197.54 101496.26 2993.29 o
2 2 -13 73739.77 80358.78 3614.31 o
4 2 -13 37723.13 39708.81 5175.39 o
1 3 -13 110251.87 112515.34 3377.32 o
3 3 -13 52778.62 50326.09 3974.43 o
0 4 -13 28613.37 30780.60 2605.62 o
2 4 -13 20137.37 20256.99 3053.51 o
4 4 -13 10259.39 11000.27 4162.83 o
1 5 -13 310846.88 319230.75 4096.22 o
3 5 -13 160578.03 169772.56 5010.02 o
0 6 -13 3010.94 2417.38 2190.87 o
2 6 -13 1786.83 2687.36 1550.48 o
4 6 -13 1046.00 2190.99 2774.02 o
1 7 -13 1136.78 805.07 999.57 o
3 7 -13 1694.04 1885.41 2108.64 o
0 8 -13 69236.41 70275.84 5264.34 o
2 8 -13 49829.05 52575.89 3340.83 o
1 9 -13 114871.59 117245.90 3155.77 o
3 9 -13 65266.68 62018.02 5289.98 o
0 10 -13 33843.53 36151.44 3064.73 o
2 10 -13 25832.08 27327.31 2887.33 o
1 11 -13 72653.10 74135.04 2892.63 o
3 11 -13 42873.73 44460.77 4780.43 o
0 12 -13 284690.91 290534.72 5657.82 o
2 12 -13 209995.13 211478.73 4695.48 o
1 13 -13 119733.31 122016.59 4758.94 o
3 13 -13 73808.32 73490.21 5468.47 o
0 14 -13 60051.50 61449.06 4445.99 o
2 14 -13 49207.04 52848.05 4455.69 o
1 15 -13 23899.36 22512.25 3772.15 o
3 15 -13 14928.21 12157.33 4098.87 o
0 16 -13 4178.72 4206.21 2454.42 o
2 16 -13 2580.24 2244.73 1974.22 o
1 17 -13 98484.57 97399.96 3804.42 o
3 17 -13 57691.55 53831.71 6405.40 o
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