#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/72/2217281.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217281_Fobs loop_ _publ_author_name 'Srinivasan, Krishnan' 'Govindarajan, Subbaiah' 'Harrison, William T. A.' _publ_section_title ; Tris(ethyl carbazate-\k^2^N,O)nickel(II) dinitrate ; _journal_coeditor_code SG2208 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m222 _journal_page_last m223 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.652 _cell_angle_gamma 90.000 _cell_length_a 14.0580 _cell_length_b 8.6571 _cell_length_c 33.6639 _exptl_crystal_F_000 2064.00 _reflns_d_resolution_high 0.7069 _[local]_cod_data_source_file sg2208Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ksni in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 8404.96 9122.97 111.04 o 6 0 0 773.94 721.78 43.67 o 8 0 0 2495.96 2779.19 86.09 o 10 0 0 52.06 69.25 42.42 o 12 0 0 614.22 728.02 57.39 o 14 0 0 483.84 356.21 74.24 o 16 0 0 866.06 501.56 76.73 o 18 0 0 48.37 -15.60 56.77 o 3 1 0 7635.64 8291.33 72.68 o 4 1 0 962.27 785.01 24.22 o 5 1 0 3266.46 3617.55 47.36 o 6 1 0 1978.97 1897.77 45.85 o 7 1 0 223.93 243.62 28.66 o 8 1 0 21.90 5.50 26.73 o 9 1 0 40.79 -11.83 28.31 o 10 1 0 8441.30 7665.07 151.59 o 11 1 0 29.83 38.05 45.54 o 12 1 0 1219.61 1086.97 161.57 o 13 1 0 93.98 109.40 76.11 o 14 1 0 4.07 -16.62 37.77 o 15 1 0 18.01 13.37 40.22 o 16 1 0 241.51 183.68 43.41 o 17 1 0 12.05 -0.24 39.84 o 18 1 0 24.47 0.24 40.57 o 19 1 0 2.26 -33.16 43.45 o 0 2 0 14694.96 15307.05 144.11 o 1 2 0 615.19 649.32 32.75 o 2 2 0 5085.50 5486.62 80.47 o 3 2 0 11.78 23.52 32.75 o 4 2 0 116.77 112.19 17.10 o 5 2 0 4313.04 4316.68 64.29 o 6 2 0 5893.81 5901.20 208.58 o 7 2 0 4752.49 5290.52 82.23 o 8 2 0 85.18 53.51 23.09 o 9 2 0 16.94 48.05 34.55 o 10 2 0 523.17 535.29 35.12 o 11 2 0 15.18 1.58 27.33 o 12 2 0 555.22 519.90 43.44 o 13 2 0 47.96 -28.78 28.78 o 14 2 0 194.66 172.49 43.62 o 15 2 0 17.76 24.96 38.53 o 16 2 0 754.33 481.85 65.50 o 17 2 0 0.98 4.51 38.97 o 18 2 0 35.36 -0.43 41.73 o 19 2 0 3.95 -41.63 41.63 o 1 3 0 4879.95 4348.76 86.09 o 2 3 0 1485.18 1390.46 39.69 o 3 3 0 19995.47 20774.08 234.87 o 4 3 0 18764.90 20166.34 112.48 o 5 3 0 473.77 623.45 36.08 o 6 3 0 25524.40 26129.65 149.10 o 7 3 0 1235.17 1015.77 34.46 o 8 3 0 71.59 20.33 69.64 o 9 3 0 1611.81 1453.71 82.01 o 10 3 0 4746.64 4575.11 73.19 o 11 3 0 45.09 -10.44 29.66 o 12 3 0 664.99 700.54 39.69 o 13 3 0 32.54 6.05 22.28 o 14 3 0 62.43 48.75 35.93 o 15 3 0 632.31 507.88 70.81 o 16 3 0 97.72 72.75 38.79 o 17 3 0 20.69 -15.37 40.36 o 18 3 0 7.90 33.72 44.13 o 19 3 0 8.60 -27.83 43.79 o 0 4 0 2788.73 2325.03 72.99 o 1 4 0 1192.95 1074.17 41.44 o 2 4 0 1469.20 1453.43 38.94 o 3 4 0 107.14 64.01 22.48 o 4 4 0 10057.93 10466.75 70.40 o 5 4 0 4.02 19.87 16.10 o 6 4 0 2487.47 2585.52 60.96 o 7 4 0 2300.61 2281.66 118.30 o 8 4 0 639.54 709.95 72.64 o 9 4 0 55.76 30.38 31.26 o 10 4 0 35.17 20.98 23.96 o 11 4 0 318.93 287.90 31.49 o 12 4 0 14.03 10.58 48.67 o 13 4 0 45.48 35.40 26.58 o 14 4 0 502.75 419.12 49.06 o 15 4 0 1.40 -17.17 28.27 o 16 4 0 271.11 246.35 47.34 o 17 4 0 26.02 -62.38 62.38 o 18 4 0 16.09 55.52 66.13 o 1 5 0 1.79 23.76 28.75 o 2 5 0 5.22 -17.61 17.61 o 3 5 0 2127.31 2151.83 75.38 o 4 5 0 4173.01 3799.07 61.78 o 5 5 0 749.44 701.15 27.82 o 6 5 0 2207.83 2074.57 49.17 o 7 5 0 953.45 1006.64 40.48 o 8 5 0 618.34 603.82 38.65 o 9 5 0 266.85 292.57 39.56 o 10 5 0 1062.79 1024.18 67.69 o 11 5 0 2.56 22.22 37.12 o 12 5 0 534.84 385.37 39.65 o 13 5 0 1.57 63.71 40.23 o 14 5 0 207.53 150.92 74.55 o 15 5 0 168.10 137.65 60.51 o 16 5 0 90.97 65.30 42.62 o 17 5 0 3.73 17.47 68.00 o 18 5 0 1.65 139.12 74.24 o 0 6 0 1485.78 1416.73 84.22 o 1 6 0 186.04 130.53 37.73 o 2 6 0 3357.39 3377.65 105.43 o 3 6 0 677.61 706.98 51.80 o 4 6 0 627.20 593.42 100.44 o 5 6 0 1202.45 1184.93 60.87 o 6 6 0 383.18 392.37 48.74 o 7 6 0 564.07 656.85 67.69 o 8 6 0 12.09 15.46 25.50 o 9 6 0 15.55 -11.77 24.80 o 10 6 0 3.53 -11.12 25.52 o 11 6 0 70.16 49.13 29.81 o 12 6 0 1.43 28.31 31.13 o 13 6 0 32.94 41.24 34.57 o 14 6 0 149.89 167.05 35.89 o 15 6 0 16.25 39.84 43.98 o 16 6 0 93.34 93.40 78.29 o 17 6 0 60.02 13.41 45.24 o 1 7 0 91.96 97.82 54.59 o 2 7 0 291.22 322.65 58.33 o 3 7 0 102.01 142.79 44.76 o 4 7 0 669.29 691.66 56.90 o 5 7 0 660.77 703.69 68.93 o 6 7 0 1221.45 1139.59 63.08 o 7 7 0 598.86 615.56 54.37 o 8 7 0 437.72 345.66 50.03 o 9 7 0 475.17 469.84 53.37 o 10 7 0 1320.18 1351.08 73.60 o 11 7 0 304.17 404.89 55.44 o 12 7 0 408.83 368.15 53.24 o 13 7 0 1.96 0.32 41.29 o 14 7 0 0.55 28.11 42.43 o 15 7 0 76.50 109.39 47.96 o 16 7 0 111.42 164.27 50.77 o 0 8 0 2432.18 2358.72 119.78 o 1 8 0 1230.88 1227.88 68.36 o 2 8 0 1074.38 1277.12 70.12 o 3 8 0 1733.10 1739.07 78.04 o 4 8 0 237.37 216.56 49.41 o 5 8 0 1109.58 1113.98 67.93 o 6 8 0 638.19 742.09 62.41 o 7 8 0 18.19 50.08 46.02 o 8 8 0 474.82 589.20 59.27 o 9 8 0 53.32 86.33 45.03 o 10 8 0 32.78 45.49 43.66 o 11 8 0 5.44 28.27 45.30 o 12 8 0 5.20 21.89 46.01 o 13 8 0 0.56 -3.92 47.59 o 14 8 0 5.24 -2.89 47.77 o 15 8 0 0.13 10.61 59.89 o 1 9 0 14.70 34.47 47.86 o 2 9 0 30.15 -29.69 42.99 o 3 9 0 25.21 18.84 54.90 o 4 9 0 38.85 24.36 49.55 o 5 9 0 141.17 151.52 54.90 o 6 9 0 413.79 372.94 59.24 o 7 9 0 32.32 77.12 48.56 o 8 9 0 48.14 35.92 46.79 o 9 9 0 125.90 115.46 49.54 o 10 9 0 163.47 200.73 52.66 o 11 9 0 88.03 112.92 51.25 o 12 9 0 84.97 131.90 50.90 o 13 9 0 0.05 -33.77 48.56 o 0 10 0 121.03 168.44 73.61 o 1 10 0 796.41 885.63 72.11 o 2 10 0 39.16 119.68 57.33 o 3 10 0 10.33 -14.53 52.49 o 4 10 0 0.08 -14.70 52.20 o 5 10 0 214.05 182.28 55.80 o 6 10 0 141.00 165.61 63.32 o 7 10 0 1.05 19.49 50.88 o 8 10 0 44.78 51.10 53.55 o 9 10 0 241.26 279.38 57.90 o 10 10 0 37.15 7.36 58.95 o 11 10 0 1.95 43.62 52.89 o 1 11 0 78.14 108.21 59.09 o 2 11 0 363.28 509.29 75.20 o 3 11 0 72.89 37.10 59.07 o 4 11 0 132.93 88.20 60.87 o 5 11 0 26.28 61.54 58.30 o 6 11 0 42.89 95.62 58.71 o 7 11 0 13.41 46.41 60.51 o 8 11 0 12.63 7.36 55.32 o 0 12 0 25.93 33.06 87.96 o 1 12 0 67.07 62.24 64.62 o 2 12 0 78.07 86.05 60.75 o 3 12 0 58.02 60.24 88.90 o -19 0 1 0.16 -4.37 68.00 o -17 0 1 4.93 -56.77 56.77 o -15 0 1 8.66 -28.70 61.76 o -13 0 1 3516.30 3571.46 122.27 o -9 0 1 586.66 515.91 56.77 o -7 0 1 3387.57 3481.00 90.46 o -5 0 1 312.74 294.45 34.93 o 3 0 1 3070.09 3321.30 60.51 o 5 0 1 14.98 32.44 26.82 o 9 0 1 7488.99 7464.81 143.48 o 15 0 1 1687.83 1748.61 106.05 o 17 0 1 76.06 -4.37 55.52 o 19 0 1 0.14 -33.69 59.89 o -19 1 1 103.12 41.16 43.17 o -18 1 1 1.40 -21.48 41.84 o -17 1 1 564.68 371.44 71.43 o -16 1 1 51.17 31.18 39.96 o -15 1 1 57.85 2.75 38.72 o -14 1 1 166.67 126.83 38.62 o -13 1 1 355.25 279.78 57.08 o -12 1 1 7.53 -24.01 29.98 o -11 1 1 447.47 421.09 56.15 o -10 1 1 128.07 103.19 69.25 o -9 1 1 1959.31 2026.84 83.59 o -8 1 1 946.69 1003.15 53.23 o -7 1 1 2399.72 2428.73 258.09 o -6 1 1 5790.97 6734.74 142.29 o -5 1 1 6064.38 5638.42 56.46 o -4 1 1 8392.24 8141.19 62.16 o -3 1 1 92781.41 91585.80 405.76 o 3 1 1 71821.18 74660.34 340.73 o 4 1 1 880.40 773.10 94.80 o 5 1 1 4929.35 4668.68 243.23 o 6 1 1 950.63 884.11 81.87 o 7 1 1 1393.81 1478.39 98.57 o 8 1 1 618.68 930.77 72.64 o 9 1 1 76.39 62.28 28.87 o 10 1 1 907.42 711.71 135.37 o 11 1 1 23.61 2.50 52.40 o 12 1 1 36.60 -31.02 31.02 o 13 1 1 35.31 28.21 33.30 o 14 1 1 4.96 45.89 39.52 o 15 1 1 915.74 794.88 91.70 o 16 1 1 25.47 -0.36 37.56 o 17 1 1 0.65 -3.77 38.89 o 18 1 1 0.03 -5.38 41.21 o 19 1 1 126.23 94.28 47.79 o -19 2 1 0.55 -27.61 42.87 o -18 2 1 2.05 -16.16 44.19 o -17 2 1 9.10 -35.97 35.97 o -16 2 1 121.19 46.96 40.69 o -15 2 1 21.03 9.24 37.62 o -14 2 1 319.36 354.46 105.43 o -13 2 1 552.13 428.01 180.91 o -12 2 1 270.75 201.31 39.39 o -11 2 1 1643.25 1405.99 132.22 o -10 2 1 751.32 692.34 33.08 o -9 2 1 801.32 692.62 36.65 o -8 2 1 1526.94 1602.52 53.03 o -7 2 1 17796.70 18506.78 157.15 o -6 2 1 1565.94 1671.16 58.95 o -5 2 1 5812.88 5782.51 103.24 o -4 2 1 675.11 517.60 77.39 o -3 2 1 6104.30 6887.85 69.37 o -2 2 1 11117.00 11621.43 133.50 o -1 2 1 59158.50 57230.88 397.07 o 0 2 1 10963.12 11940.82 220.84 o 1 2 1 264.78 238.85 36.18 o 2 2 1 2911.81 2886.93 47.42 o 3 2 1 6582.42 6833.62 112.60 o 4 2 1 3768.09 3999.21 44.84 o 5 2 1 9993.45 10596.28 80.60 o 6 2 1 1057.27 1128.52 50.58 o 7 2 1 4574.11 4552.23 164.51 o 8 2 1 86.08 59.20 28.25 o 9 2 1 4051.74 3924.69 193.68 o 10 2 1 185.49 158.44 34.40 o 11 2 1 1452.48 1293.40 106.56 o 12 2 1 349.01 303.54 35.52 o 13 2 1 200.51 119.57 38.97 o 14 2 1 311.52 242.81 43.76 o 15 2 1 634.69 677.46 52.49 o 16 2 1 11.00 12.14 40.91 o 17 2 1 0.66 -39.27 39.27 o 18 2 1 9.52 32.86 42.36 o 19 2 1 18.27 -22.56 45.20 o -19 3 1 39.10 9.56 43.81 o -18 3 1 15.22 45.37 42.27 o -17 3 1 265.62 260.05 48.73 o -16 3 1 0.09 -28.63 36.78 o -15 3 1 10.97 22.66 36.12 o -14 3 1 11.41 2.41 31.17 o -13 3 1 458.51 403.83 34.68 o -12 3 1 143.71 140.67 28.19 o -11 3 1 599.26 620.83 56.78 o -10 3 1 64.50 72.46 63.54 o -9 3 1 242.51 238.08 32.70 o -8 3 1 1135.36 1024.66 123.00 o -7 3 1 138.62 97.61 30.95 o -6 3 1 5122.12 5393.48 125.70 o -5 3 1 57.06 46.67 18.55 o -4 3 1 634.98 700.54 20.79 o -3 3 1 62.67 65.75 17.17 o -2 3 1 125.84 167.19 25.89 o -1 3 1 3240.58 2719.78 73.92 o 0 3 1 377.90 392.23 27.99 o 1 3 1 1005.77 817.67 32.06 o 2 3 1 2913.30 2899.07 52.93 o 3 3 1 12844.86 13325.45 123.30 o 4 3 1 5993.90 5779.83 87.64 o 5 3 1 9044.27 9462.23 100.31 o 6 3 1 514.52 516.37 69.51 o 7 3 1 804.03 869.22 32.67 o 8 3 1 4093.94 4072.71 62.74 o 9 3 1 1311.23 1131.16 44.88 o 10 3 1 1438.02 1398.64 60.14 o 11 3 1 1.10 16.45 26.13 o 12 3 1 13.36 14.09 23.99 o 13 3 1 253.03 194.01 32.73 o 14 3 1 589.59 538.90 49.31 o 15 3 1 293.40 254.10 42.07 o 16 3 1 11.98 15.85 37.47 o 17 3 1 14.81 -20.01 49.59 o 18 3 1 9.95 30.05 40.40 o 19 3 1 103.71 64.17 66.13 o -18 4 1 0.16 -17.47 66.75 o -17 4 1 19.87 -55.52 55.52 o -16 4 1 0.61 -6.86 67.37 o -15 4 1 1.94 -13.78 29.53 o -14 4 1 10.37 -0.22 36.18 o -13 4 1 514.87 499.43 36.45 o -12 4 1 683.17 665.91 38.17 o -11 4 1 1735.42 1612.28 103.58 o -10 4 1 15.78 28.92 30.88 o -9 4 1 1530.56 1349.02 48.60 o -8 4 1 1.96 7.39 28.16 o -7 4 1 6193.66 6089.24 119.69 o -6 4 1 390.59 414.68 24.47 o -5 4 1 171.06 161.02 15.14 o -4 4 1 29.36 17.34 27.17 o -3 4 1 1424.67 1315.36 51.39 o -2 4 1 2183.70 2218.59 55.63 o -1 4 1 1980.36 1868.39 71.74 o 0 4 1 18363.38 17743.74 145.67 o 1 4 1 1361.59 1268.01 42.04 o 2 4 1 395.20 386.74 32.68 o 3 4 1 7495.96 7256.98 68.00 o 4 4 1 551.22 502.67 32.27 o 5 4 1 6050.21 5981.20 136.26 o 6 4 1 526.95 575.64 29.17 o 7 4 1 36.07 44.34 40.30 o 8 4 1 1632.51 1657.26 73.02 o 9 4 1 1152.70 1240.18 42.39 o 10 4 1 145.53 160.64 28.07 o 11 4 1 89.53 104.16 56.75 o 12 4 1 416.96 350.12 32.70 o 13 4 1 854.79 854.78 54.44 o 14 4 1 14.91 45.94 39.84 o 15 4 1 135.45 111.35 31.93 o 16 4 1 40.65 -1.83 44.83 o 17 4 1 7.21 26.20 64.26 o 18 4 1 5.24 -47.41 60.51 o -18 5 1 42.94 140.99 74.24 o -17 5 1 139.86 171.55 73.61 o -16 5 1 61.51 27.65 40.80 o -15 5 1 64.97 69.94 44.25 o -14 5 1 67.47 71.81 45.85 o -13 5 1 310.33 375.32 42.01 o -12 5 1 15.31 43.51 34.27 o -11 5 1 312.24 272.08 40.40 o -10 5 1 6.43 51.64 34.16 o -9 5 1 7.29 28.93 35.46 o -8 5 1 15.02 -4.86 34.44 o -7 5 1 1093.21 1074.37 41.40 o -6 5 1 160.87 175.00 32.13 o -5 5 1 328.44 266.48 22.27 o -4 5 1 9925.69 9964.67 90.48 o -3 5 1 262.57 350.61 30.74 o -2 5 1 215.39 179.73 21.68 o -1 5 1 7245.60 6824.82 125.70 o 0 5 1 1217.32 1131.33 46.52 o 1 5 1 51.86 17.53 26.24 o 2 5 1 118.14 128.85 33.52 o 3 5 1 4475.22 4569.61 92.02 o 4 5 1 54.00 73.93 60.80 o 5 5 1 6105.08 5901.93 80.64 o 6 5 1 22.59 36.79 24.98 o 7 5 1 30.15 -10.59 26.09 o 8 5 1 895.20 887.33 42.99 o 9 5 1 1091.51 1058.98 55.83 o 10 5 1 25.63 13.70 31.82 o 11 5 1 98.71 109.41 33.45 o 12 5 1 10.67 11.98 35.46 o 13 5 1 243.36 197.20 44.23 o 14 5 1 23.34 37.37 60.20 o 15 5 1 61.74 43.12 39.88 o 16 5 1 58.21 22.17 59.58 o 17 5 1 0.90 -23.71 58.02 o 18 5 1 2.13 50.53 69.25 o -17 6 1 0.62 -25.84 47.16 o -16 6 1 42.19 19.75 43.22 o -15 6 1 52.84 101.26 43.17 o -14 6 1 0.44 -29.75 33.06 o -13 6 1 408.43 435.04 42.58 o -12 6 1 634.37 713.04 55.60 o -11 6 1 861.83 856.88 45.34 o -10 6 1 5.83 -25.27 25.27 o -9 6 1 46.65 34.30 27.40 o -8 6 1 788.45 787.35 57.11 o -7 6 1 2807.77 2889.50 129.13 o -6 6 1 813.96 824.75 55.12 o -5 6 1 651.31 818.27 54.47 o -4 6 1 737.42 641.77 49.40 o -3 6 1 821.24 872.28 51.17 o -2 6 1 1423.87 1579.42 99.19 o -1 6 1 456.02 418.50 43.37 o 0 6 1 238.10 232.18 56.15 o 1 6 1 628.93 587.17 48.73 o 2 6 1 149.56 184.02 39.34 o 3 6 1 322.82 349.22 45.64 o 4 6 1 681.07 713.62 52.93 o 5 6 1 271.87 315.84 64.88 o 6 6 1 65.57 51.88 42.53 o 7 6 1 1382.51 1455.00 66.59 o 8 6 1 544.88 578.63 49.62 o 9 6 1 653.64 698.25 52.47 o 10 6 1 169.88 186.76 33.17 o 11 6 1 19.34 29.06 31.63 o 12 6 1 39.79 23.12 31.91 o 13 6 1 167.02 206.01 35.90 o 14 6 1 39.95 61.07 33.57 o 15 6 1 178.92 136.07 52.09 o 16 6 1 2.55 0.34 45.62 o 17 6 1 3.43 -8.58 43.64 o -16 7 1 14.49 25.49 46.16 o -15 7 1 12.63 15.08 43.95 o -14 7 1 49.26 79.54 45.36 o -13 7 1 45.07 71.73 42.97 o -12 7 1 6.37 50.33 41.23 o -11 7 1 338.02 399.88 55.59 o -10 7 1 14.74 180.67 50.93 o -9 7 1 343.38 434.69 52.80 o -8 7 1 1.30 55.85 53.65 o -7 7 1 4.05 13.14 41.16 o -6 7 1 50.56 106.46 43.17 o -5 7 1 74.00 45.88 48.35 o -4 7 1 629.71 691.30 62.38 o -3 7 1 1527.76 1500.17 70.14 o -2 7 1 4858.16 4936.94 109.35 o -1 7 1 6309.86 6358.31 118.42 o 0 7 1 1550.18 1571.60 70.57 o 1 7 1 185.29 192.18 53.34 o 2 7 1 233.65 218.13 46.36 o 3 7 1 1864.06 2009.03 75.86 o 4 7 1 1741.68 1775.09 72.56 o 5 7 1 1761.13 1799.93 74.28 o 6 7 1 412.08 378.73 44.77 o 7 7 1 139.44 147.02 47.72 o 8 7 1 231.76 295.46 49.17 o 9 7 1 14.79 -13.58 42.07 o 10 7 1 14.94 114.43 71.43 o 11 7 1 11.49 62.72 44.89 o 12 7 1 27.01 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