#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217287.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217287_Fobs loop_ _publ_author_name 'Grigoriev, Mikhail S.' 'Krot, Nikolai N.' _publ_section_title ; Reinvestigation of trisodium dihydroxidotetraoxidoneptunate(VII) dihydrate ; _journal_coeditor_code SG2217 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i6 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.914 _cell_angle_gamma 90.000 _cell_length_a 7.8166 _cell_length_b 7.7703 _cell_length_c 6.8211 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.5529 _[local]_cod_data_source_file sg2217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' n in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 213.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 12108.21 11616.81 164.85 o 4 0 0 10577.35 10804.61 179.04 o 5 0 0 13701.21 13904.76 197.67 o 6 0 0 14173.36 14681.11 209.12 o 7 0 0 5962.22 6170.79 84.71 o 8 0 0 9190.74 9168.96 102.76 o 9 0 0 6023.83 6010.77 81.05 o 10 0 0 2702.50 2727.00 58.75 o 11 0 0 3078.85 3049.63 59.30 o 12 0 0 1851.02 1817.91 41.27 o 13 0 0 2119.99 1999.03 56.16 o 1 1 0 432.83 421.84 7.54 o 3 1 0 1660.71 1744.95 20.36 o 4 1 0 344.65 323.41 6.42 o 5 1 0 567.24 529.03 8.66 o 6 1 0 12.74 16.31 3.40 o 7 1 0 17.05 18.59 4.03 o 8 1 0 105.86 107.51 4.44 o 9 1 0 130.62 135.69 8.11 o 10 1 0 4.27 1.89 4.86 o 11 1 0 17.14 24.93 5.47 o 12 1 0 43.27 49.89 8.71 o 0 2 0 28895.52 27914.70 558.01 o 1 2 0 21343.50 21219.65 272.24 o 2 2 0 24455.42 24233.25 281.33 o 3 2 0 10874.21 10815.68 125.90 o 4 2 0 24357.10 23922.34 323.74 o 5 2 0 13720.04 13117.78 140.89 o 6 2 0 10182.95 9804.06 103.44 o 7 2 0 8466.61 8469.08 90.06 o 8 2 0 4768.27 4822.00 45.01 o 9 2 0 3893.79 3906.06 39.25 o 10 2 0 3623.37 3586.97 59.83 o 11 2 0 2692.13 2675.69 39.82 o 12 2 0 2628.05 2625.17 37.65 o 3 3 0 28.51 26.42 2.54 o 4 3 0 36.94 31.24 5.15 o 5 3 0 343.48 319.93 7.40 o 6 3 0 44.80 45.45 3.94 o 7 3 0 82.80 89.16 4.59 o 8 3 0 4.80 18.19 4.95 o 9 3 0 5.39 -4.81 4.81 o 10 3 0 94.52 92.90 7.44 o 11 3 0 17.56 22.42 6.73 o 12 3 0 0.60 -3.27 6.76 o 0 4 0 17924.53 17644.57 350.98 o 1 4 0 19934.27 19979.94 281.04 o 2 4 0 19608.24 19784.51 249.97 o 3 4 0 12378.28 12680.34 161.38 o 4 4 0 10170.28 10404.72 133.30 o 5 4 0 7784.56 7824.52 82.02 o 6 4 0 8505.20 8412.78 84.23 o 7 4 0 8014.41 7877.77 77.88 o 8 4 0 5446.68 5359.99 58.78 o 9 4 0 4107.27 4117.82 46.08 o 10 4 0 3526.96 3496.13 43.36 o 11 4 0 2624.59 2662.51 40.87 o 12 4 0 1993.61 2046.94 31.95 o 1 5 0 391.06 408.81 8.72 o 2 5 0 11.74 5.55 3.03 o 3 5 0 15.05 8.36 3.63 o 4 5 0 0.16 -1.23 3.39 o 5 5 0 313.86 300.91 7.15 o 6 5 0 231.01 240.54 6.44 o 7 5 0 0.01 1.62 4.21 o 8 5 0 32.56 37.59 5.60 o 9 5 0 1.90 -3.58 6.90 o 10 5 0 1.01 5.83 6.44 o 11 5 0 73.84 75.69 7.72 o 12 5 0 1.81 0.67 8.58 o 0 6 0 10089.61 10007.73 201.68 o 1 6 0 8781.06 8781.53 107.50 o 2 6 0 11885.67 11953.38 145.69 o 3 6 0 16411.54 16390.60 181.09 o 4 6 0 6078.11 6228.57 70.97 o 5 6 0 7532.77 7613.32 70.89 o 6 6 0 6982.46 7073.04 66.22 o 7 6 0 4324.41 4365.83 45.43 o 8 6 0 4581.42 4537.06 59.89 o 9 6 0 3123.09 3104.91 45.56 o 10 6 0 2620.48 2674.38 34.31 o 11 6 0 2860.37 2959.18 39.23 o 1 7 0 235.38 221.22 6.10 o 2 7 0 324.42 329.49 6.71 o 3 7 0 2.32 2.47 2.71 o 4 7 0 4.38 8.74 3.01 o 5 7 0 4.23 4.15 3.26 o 6 7 0 92.23 99.94 5.57 o 7 7 0 2.27 -0.22 4.90 o 8 7 0 154.63 150.68 7.72 o 9 7 0 49.34 53.54 7.43 o 10 7 0 0.29 10.08 7.06 o 11 7 0 2.88 -4.97 11.07 o 0 8 0 3762.82 3760.33 51.19 o 1 8 0 8744.55 8744.41 80.46 o 2 8 0 7697.67 7664.19 71.06 o 3 8 0 7231.43 7192.32 64.97 o 4 8 0 7629.72 7615.83 80.69 o 5 8 0 5130.21 5116.96 52.88 o 6 8 0 3234.77 3241.05 35.84 o 7 8 0 4285.05 4315.97 46.71 o 8 8 0 2819.93 2868.06 34.09 o 9 8 0 2778.36 2808.80 38.89 o 10 8 0 2896.08 2871.00 37.14 o 1 9 0 0.45 1.45 2.93 o 2 9 0 48.20 54.54 3.77 o 3 9 0 79.45 81.85 5.83 o 4 9 0 48.40 50.98 4.92 o 5 9 0 57.54 63.74 5.12 o 6 9 0 5.73 -4.74 4.74 o 7 9 0 0.51 -1.92 5.22 o 8 9 0 0.08 0.85 6.00 o 9 9 0 9.19 5.98 6.78 o 10 9 0 3.75 5.80 9.84 o 0 10 0 5492.12 5470.60 82.61 o 1 10 0 5278.77 5239.92 56.17 o 2 10 0 4030.30 3973.01 43.80 o 3 10 0 4982.26 4932.53 53.63 o 4 10 0 4073.80 4020.38 44.96 o 5 10 0 3753.88 3776.24 42.94 o 6 10 0 2631.21 2603.01 30.75 o 7 10 0 2334.09 2329.95 28.81 o 8 10 0 2696.61 2707.44 33.31 o 9 10 0 2725.60 2724.30 41.99 o 1 11 0 28.35 29.97 4.82 o 2 11 0 94.17 102.69 6.13 o 3 11 0 2.19 -4.54 4.54 o 4 11 0 4.29 9.84 4.92 o 5 11 0 39.06 35.22 6.56 o 6 11 0 18.16 15.48 5.89 o 7 11 0 0.73 -6.05 6.05 o 8 11 0 12.48 30.92 8.66 o 0 12 0 3434.42 3417.66 55.71 o 1 12 0 2754.49 2732.15 32.66 o 2 12 0 2621.09 2615.69 31.68 o 3 12 0 3457.64 3470.91 40.33 o 4 12 0 3117.68 3091.83 36.86 o 5 12 0 3171.80 3243.34 38.97 o 6 12 0 2072.12 2132.91 33.26 o 1 13 0 0.37 -0.43 5.18 o 2 13 0 26.61 22.42 5.68 o 3 13 0 2.54 1.48 6.73 o 4 13 0 0.61 4.54 7.08 o 0 14 0 2336.27 2338.96 48.89 o 1 14 0 2644.42 2623.39 37.98 o -13 1 1 1637.63 1620.66 34.93 o -12 1 1 2347.02 2301.04 35.94 o -11 1 1 1378.31 1340.37 19.21 o -10 1 1 3539.92 3509.42 35.76 o -9 1 1 4600.02 4587.97 44.66 o -8 1 1 7334.76 7238.62 65.23 o -7 1 1 6094.99 6128.04 61.37 o -6 1 1 6243.10 6189.39 75.68 o -4 1 1 16425.38 15500.29 227.90 o -3 1 1 11832.93 11637.25 133.21 o -2 1 1 17842.94 18088.27 227.88 o -1 1 1 22066.24 21293.11 900.37 o 0 1 1 18989.38 19149.37 310.98 o 1 1 1 16780.05 16963.11 195.87 o 2 1 1 8527.05 8399.43 89.96 o 3 1 1 7307.91 7408.29 80.03 o 4 1 1 10513.69 10398.05 197.70 o 5 1 1 13316.14 13316.21 164.14 o 6 1 1 4630.70 4663.30 47.33 o 7 1 1 5338.50 5529.52 50.22 o 8 1 1 2611.41 2687.69 28.13 o 9 1 1 4033.97 4084.11 38.31 o 10 1 1 3102.37 3134.47 34.08 o 11 1 1 2481.48 2407.68 32.64 o 12 1 1 1263.92 1268.63 22.90 o -13 2 1 35.44 47.28 11.34 o -12 2 1 4.30 -4.02 7.21 o -11 2 1 11.72 14.95 5.91 o -10 2 1 0.32 -2.05 4.57 o -9 2 1 160.50 162.12 5.90 o -8 2 1 22.36 27.07 4.07 o -7 2 1 226.68 241.15 9.29 o -6 2 1 113.64 112.27 4.81 o -5 2 1 58.83 58.24 3.60 o -4 2 1 7.39 0.82 2.75 o -3 2 1 373.32 365.99 6.83 o -2 2 1 3100.90 3212.39 41.59 o -1 2 1 805.75 801.38 11.76 o 0 2 1 0.77 -1.89 1.89 o 1 2 1 427.77 428.30 6.45 o 3 2 1 936.64 957.87 13.38 o 4 2 1 21.30 17.10 3.46 o 5 2 1 126.01 132.13 8.29 o 6 2 1 553.61 534.27 12.84 o 7 2 1 116.39 117.27 4.53 o 8 2 1 181.11 194.80 6.41 o 9 2 1 10.61 16.39 4.81 o 10 2 1 5.11 -1.71 7.62 o 11 2 1 0.05 -0.60 6.16 o 12 2 1 6.95 -2.40 9.06 o -13 3 1 1574.72 1590.49 33.07 o -12 3 1 1829.62 1897.14 31.63 o -11 3 1 2719.95 2749.97 35.55 o -10 3 1 2818.85 2907.03 34.25 o -9 3 1 2801.38 2825.72 35.37 o -8 3 1 6269.96 6205.57 57.02 o -7 3 1 3764.85 3660.21 39.62 o -6 3 1 7573.06 7439.41 82.89 o -5 3 1 10404.05 10498.51 122.43 o -4 3 1 6356.25 6527.46 94.78 o -3 3 1 14038.01 14369.10 204.90 o -2 3 1 17742.01 17499.30 221.13 o -1 3 1 6303.36 6311.60 80.64 o 0 3 1 15000.63 14571.00 184.56 o 1 3 1 8684.08 8691.09 110.50 o 2 3 1 6291.01 6378.58 81.94 o 3 3 1 18360.20 18404.06 259.49 o 4 3 1 7464.47 7474.19 98.25 o 5 3 1 7372.98 7337.29 75.46 o 6 3 1 7134.36 6916.70 87.75 o 7 3 1 3283.03 3242.44 34.58 o 8 3 1 3047.13 3034.83 37.49 o 9 3 1 3597.85 3561.23 41.49 o 10 3 1 1864.26 1888.84 38.60 o 11 3 1 2778.38 2685.91 42.87 o 12 3 1 1769.93 1760.87 34.81 o -12 4 1 21.43 24.22 7.93 o -11 4 1 0.11 3.35 6.23 o -10 4 1 290.54 315.79 9.55 o -9 4 1 1.39 -5.19 5.19 o -8 4 1 9.44 16.43 5.15 o -7 4 1 67.11 72.55 4.61 o -6 4 1 945.45 923.41 12.33 o -5 4 1 436.87 472.82 10.87 o -4 4 1 87.56 97.43 4.34 o -3 4 1 23.95 20.09 2.76 o -2 4 1 371.46 376.96 7.06 o -1 4 1 156.66 153.96 4.41 o 0 4 1 1888.48 1811.17 24.55 o 2 4 1 1597.13 1677.90 23.39 o 3 4 1 271.49 262.00 6.95 o 4 4 1 549.04 537.72 9.46 o 5 4 1 61.05 64.63 3.92 o 6 4 1 34.92 28.45 3.92 o 7 4 1 18.87 14.62 3.93 o 8 4 1 14.41 -0.01 6.52 o 9 4 1 79.52 94.03 7.12 o 10 4 1 0.08 -5.11 6.17 o 11 4 1 101.05 111.52 9.15 o -12 5 1 1612.53 1638.26 26.78 o -11 5 1 2142.06 2194.95 30.57 o -10 5 1 3410.85 3490.44 40.89 o -9 5 1 3596.78 3533.35 46.12 o -8 5 1 2760.53 2742.49 30.88 o -7 5 1 6403.56 6433.34 60.85 o -6 5 1 5963.71 6060.53 63.91 o -5 5 1 4629.23 4744.92 54.79 o -4 5 1 6634.40 6762.67 82.09 o -3 5 1 5334.98 5414.33 70.44 o -2 5 1 9364.89 9379.05 119.81 o -1 5 1 16351.34 16404.94 207.84 o 0 5 1 7103.95 7092.82 91.10 o 1 5 1 9231.03 9222.54 117.90 o 2 5 1 11555.61 11712.28 149.35 o 3 5 1 5214.12 5344.38 62.16 o 4 5 1 5681.64 5728.06 60.47 o 5 5 1 4044.79 4053.93 42.38 o 6 5 1 3721.16 3723.23 33.93 o 7 5 1 6172.17 6109.63 62.14 o 8 5 1 4441.38 4310.29 62.91 o 9 5 1 2215.42 2247.06 31.78 o 10 5 1 2268.89 2313.04 32.51 o 11 5 1 1448.94 1457.37 27.33 o -12 6 1 0.09 -1.25 9.11 o -11 6 1 10.51 14.31 7.14 o -10 6 1 8.24 5.73 9.00 o -9 6 1 11.36 13.42 6.76 o -8 6 1 0.02 11.74 5.06 o -7 6 1 6.36 2.96 3.84 o -6 6 1 15.30 17.20 3.70 o -5 6 1 0.11 0.47 2.99 o -4 6 1 9.98 7.02 2.81 o -3 6 1 147.32 153.50 4.74 o -2 6 1 472.22 447.74 8.46 o -1 6 1 8.85 6.74 2.88 o 0 6 1 96.04 89.03 3.89 o 1 6 1 46.52 44.13 3.77 o 2 6 1 222.20 216.98 6.27 o 3 6 1 304.43 304.58 6.09 o 4 6 1 85.00 83.27 3.88 o 5 6 1 0.03 5.96 3.39 o 6 6 1 138.32 140.70 5.56 o 7 6 1 47.80 56.90 5.67 o 8 6 1 10.37 4.97 6.08 o 9 6 1 21.48 29.38 6.61 o 10 6 1 44.63 45.13 7.66 o 11 6 1 12.09 20.89 9.54 o -11 7 1 2515.60 2563.01 36.22 o -10 7 1 1968.88 1936.22 37.59 o -9 7 1 2074.07 2116.59 44.91 o -8 7 1 1658.90 1718.78 21.92 o -7 7 1 3628.20 3624.34 38.59 o -6 7 1 5214.42 5224.75 52.94 o -5 7 1 7151.77 7013.34 69.14 o -4 7 1 5809.86 5778.17 54.29 o -3 7 1 6186.03 6125.97 64.73 o -2 7 1 5171.73 5247.31 55.57 o -1 7 1 4992.69 5081.92 50.19 o 0 7 1 4645.27 4651.19 49.48 o 1 7 1 5792.34 5762.86 56.77 o 2 7 1 7701.77 7750.01 72.96 o 3 7 1 6916.60 6959.15 65.87 o 4 7 1 5504.29 5525.80 53.37 o 5 7 1 3178.83 3189.81 32.82 o 6 7 1 3851.04 3823.69 49.76 o 7 7 1 3159.92 3105.20 35.41 o 8 7 1 2968.25 2922.30 36.41 o 9 7 1 1696.91 1681.16 29.30 o 10 7 1 1640.97 1689.27 29.03 o -11 8 1 39.66 47.92 9.64 o -10 8 1 2.40 -4.19 6.93 o -9 8 1 0.07 -4.61 6.16 o -8 8 1 0.36 3.75 5.46 o -7 8 1 5.24 6.43 4.95 o -6 8 1 17.88 19.22 4.57 o -5 8 1 94.01 102.34 4.77 o -4 8 1 0.53 3.24 3.15 o -3 8 1 379.77 370.26 7.33 o -2 8 1 24.07 25.44 3.02 o -1 8 1 0.03 2.32 2.66 o 0 8 1 42.19 48.22 3.23 o 1 8 1 38.20 44.21 3.24 o 2 8 1 4.98 1.37 2.88 o 3 8 1 14.86 15.70 3.25 o 4 8 1 73.94 69.94 4.77 o 5 8 1 74.44 88.49 4.96 o 6 8 1 58.13 63.26 5.59 o 7 8 1 18.86 13.25 5.57 o 8 8 1 2.47 8.32 6.40 o 9 8 1 38.57 29.52 7.34 o 10 8 1 0.22 16.70 12.12 o -10 9 1 1578.62 1559.54 28.76 o -9 9 1 2217.17 2206.05 30.07 o -8 9 1 2610.14 2633.04 31.84 o -7 9 1 2534.49 2559.23 31.50 o -6 9 1 2641.87 2634.09 31.57 o -5 9 1 4415.55 4358.16 47.94 o -4 9 1 2897.06 2815.90 30.38 o -3 9 1 4256.15 4200.83 43.06 o -2 9 1 3830.44 3841.52 37.18 o -1 9 1 3574.35 3610.04 37.22 o 0 9 1 6812.66 6748.56 66.49 o 1 9 1 5716.63 5700.06 60.75 o 2 9 1 3973.30 3942.20 40.62 o 3 9 1 3637.45 3588.32 37.61 o 4 9 1 2365.56 2380.61 27.24 o 5 9 1 2211.43 2211.44 26.34 o 6 9 1 3527.96 3571.51 46.39 o 7 9 1 2242.64 2271.25 35.71 o 8 9 1 3040.60 3041.69 38.30 o 9 9 1 2056.33 2104.96 40.77 o -9 10 1 50.31 61.12 10.99 o -8 10 1 13.53 13.08 6.21 o -7 10 1 127.39 133.46 7.08 o -6 10 1 0.00 2.64 4.92 o -5 10 1 4.96 -0.55 4.59 o -4 10 1 8.08 2.90 4.36 o -3 10 1 137.15 141.81 5.29 o -2 10 1 17.18 12.54 3.93 o -1 10 1 35.55 29.20 4.05 o 0 10 1 0.70 1.25 3.65 o 1 10 1 192.24 188.87 5.86 o 2 10 1 3.24 -4.01 4.01 o 3 10 1 7.43 7.62 4.42 o 4 10 1 1.24 0.10 4.83 o 5 10 1 63.70 74.60 5.79 o 6 10 1 13.09 11.60 5.41 o 7 10 1 6.96 -2.89 6.02 o 8 10 1 36.24 42.56 9.16 o -8 11 1 1286.50 1252.24 33.80 o -7 11 1 2094.26 2133.41 28.30 o -6 11 1 1926.89 1960.01 25.98 o -5 11 1 2696.95 2718.98 32.97 o -4 11 1 4285.37 4227.08 44.30 o -3 11 1 2821.18 2810.49 33.03 o -2 11 1 1947.58 1920.71 24.17 o -1 11 1 2842.28 2840.41 33.11 o 0 11 1 2566.62 2553.88 30.34 o 1 11 1 3509.88 3481.18 39.48 o 2 11 1 3459.45 3431.70 39.26 o 3 11 1 1915.41 1909.62 26.41 o 4 11 1 3033.13 3028.60 35.96 o 5 11 1 2734.18 2763.59 33.86 o 6 11 1 1762.93 1783.60 26.09 o 7 11 1 1592.80 1614.31 28.16 o -7 12 1 5.39 -0.55 11.08 o -6 12 1 26.00 21.83 7.52 o -5 12 1 3.37 4.81 5.22 o -4 12 1 1.68 -2.70 5.03 o -3 12 1 2.96 -0.31 4.88 o -2 12 1 4.19 4.98 4.77 o -1 12 1 35.21 26.98 5.17 o 0 12 1 81.65 84.24 5.87 o 1 12 1 52.55 55.99 5.54 o 2 12 1 7.22 4.22 4.86 o 3 12 1 26.32 40.44 5.93 o 4 12 1 3.49 -3.39 5.66 o 5 12 1 29.37 31.84 7.49 o 6 12 1 14.49 14.22 8.68 o -5 13 1 1579.22 1646.93 29.15 o -4 13 1 1677.52 1659.04 28.62 o -3 13 1 2044.74 2068.87 28.84 o -2 13 1 2028.28 2041.98 26.51 o -1 13 1 1937.25 1963.22 25.61 o 0 13 1 2427.15 2416.69 30.02 o 1 13 1 2126.76 2107.15 27.09 o 2 13 1 1671.80 1684.19 23.21 o 3 13 1 1723.77 1737.36 29.74 o 4 13 1 1596.49 1593.98 28.42 o 0 14 1 40.25 35.13 7.36 o -13 0 2 1705.25 1676.68 37.68 o -12 0 2 2446.52 2400.16 42.72 o -11 0 2 4105.31 3938.00 63.38 o -10 0 2 5439.84 5312.82 72.54 o -9 0 2 5970.50 5874.83 78.85 o -8 0 2 11618.58 11598.24 136.88 o -7 0 2 8265.16 8219.37 122.53 o -6 0 2 4537.02 4587.22 78.28 o -5 0 2 17082.67 17510.20 284.12 o -4 0 2 12948.50 12807.83 208.10 o -3 0 2 39149.19 40393.45 569.53 o -2 0 2 27638.41 26306.41 1033.39 o -1 0 2 16805.30 16808.82 468.89 o 0 0 2 19490.46 19344.95 535.83 o 1 0 2 45613.93 45305.58 638.06 o 2 0 2 10586.06 10473.24 170.04 o 3 0 2 20016.42 18885.49 485.15 o 4 0 2 7928.65 7745.80 116.72 o 5 0 2 7553.48 7434.67 195.23 o 6 0 2 9960.37 10149.90 131.55 o 7 0 2 5700.62 5951.57 69.42 o 8 0 2 4535.99 4687.38 67.58 o 9 0 2 5715.77 5805.94 82.53 o 10 0 2 3179.13 3223.75 49.63 o 11 0 2 1799.73 1814.46 36.29 o -13 1 2 31.52 24.91 8.99 o -12 1 2 14.49 19.92 6.32 o -11 1 2 64.29 62.90 6.24 o -10 1 2 3.94 14.99 4.73 o -9 1 2 1.24 3.54 3.76 o -8 1 2 7.71 5.71 3.29 o -7 1 2 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4 4781.18 4825.62 53.06 o -7 6 4 5427.25 5446.89 58.32 o -6 6 4 4412.12 4391.45 50.35 o -5 6 4 10171.39 10152.72 98.90 o -4 6 4 10745.97 10658.44 98.81 o -3 6 4 6665.71 6732.33 63.55 o -2 6 4 7834.63 7864.51 74.96 o -1 6 4 7709.80 7832.60 83.76 o 0 6 4 6533.34 6583.00 67.33 o 1 6 4 10809.59 10778.11 100.71 o 2 6 4 5450.25 5401.41 52.08 o 3 6 4 6181.67 6069.50 62.31 o 4 6 4 6755.38 6682.82 68.08 o 5 6 4 3808.06 3742.95 46.17 o 6 6 4 2895.87 2877.93 40.68 o 7 6 4 2832.26 2814.59 32.84 o 8 6 4 2142.36 2076.66 37.71 o 9 6 4 2638.57 2709.86 45.29 o -12 7 4 1.63 -0.58 11.35 o -11 7 4 38.34 34.87 8.57 o -10 7 4 48.80 48.28 7.01 o -9 7 4 17.79 15.26 5.61 o -8 7 4 47.93 45.05 5.66 o -7 7 4 1.71 7.32 4.37 o -6 7 4 21.96 23.23 3.81 o -5 7 4 80.81 83.87 3.96 o -4 7 4 81.24 76.50 3.47 o -3 7 4 29.65 27.14 2.91 o -2 7 4 2.18 1.36 2.45 o -1 7 4 316.55 306.33 7.69 o 0 7 4 131.79 135.21 4.39 o 1 7 4 68.82 71.04 3.92 o 2 7 4 20.42 19.53 3.43 o 3 7 4 2.37 1.82 3.83 o 4 7 4 30.85 22.14 4.89 o 5 7 4 18.35 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25.90 45.38 10.77 o -7 12 4 2663.14 2758.11 56.63 o -6 12 4 2475.97 2442.59 73.89 o -5 12 4 2754.81 2838.15 42.91 o -4 12 4 2566.46 2538.21 38.88 o -3 12 4 2523.16 2509.72 35.17 o -2 12 4 2835.65 2822.21 38.63 o -1 12 4 2303.96 2337.15 33.03 o 0 12 4 1862.29 1808.62 27.25 o 1 12 4 2859.78 2852.32 39.30 o 2 12 4 2801.72 2770.62 48.34 o 3 12 4 2617.52 2589.98 66.73 o -4 13 4 61.21 38.41 10.33 o -3 13 4 12.95 13.68 9.59 o -2 13 4 22.25 22.64 9.67 o -1 13 4 1.95 -3.26 9.24 o 0 13 4 8.91 7.53 9.43 o -14 1 5 1921.49 1954.18 31.05 o -13 1 5 1208.71 1208.78 18.93 o -12 1 5 2132.92 2124.00 27.30 o -11 1 5 2984.00 2988.24 33.56 o -10 1 5 4607.51 4585.35 48.19 o -9 1 5 4150.44 4168.53 46.65 o -8 1 5 6017.46 5968.07 64.22 o -7 1 5 3816.18 3778.32 41.55 o -6 1 5 7954.53 7827.89 102.82 o -5 1 5 5020.72 5040.40 54.89 o -4 1 5 6216.87 6332.43 75.32 o -3 1 5 10268.78 10239.39 194.60 o -2 1 5 12405.67 12858.42 235.81 o -1 1 5 8301.52 8361.28 126.38 o 0 1 5 6482.65 6573.24 104.63 o 1 1 5 3940.96 3999.79 52.62 o 2 1 5 5452.40 5521.34 58.12 o 3 1 5 8462.76 8577.79 87.92 o 4 1 5 4018.96 4071.90 57.09 o 5 1 5 4393.60 4314.10 52.65 o 6 1 5 2541.28 2431.61 51.04 o 7 1 5 2759.82 2698.14 30.51 o 8 1 5 1986.31 2070.45 28.30 o 9 1 5 1993.46 2024.69 29.26 o -13 2 5 12.08 18.02 6.60 o -12 2 5 0.17 1.30 6.51 o -11 2 5 27.32 36.04 6.18 o -10 2 5 7.44 6.74 4.93 o -9 2 5 94.81 93.71 7.20 o -8 2 5 72.07 77.17 4.90 o -7 2 5 23.16 24.00 3.82 o -6 2 5 166.42 160.47 4.46 o -5 2 5 99.93 100.89 3.25 o -4 2 5 140.24 144.67 6.72 o -3 2 5 96.94 98.31 4.38 o -2 2 5 74.67 79.06 4.82 o -1 2 5 399.95 391.83 8.94 o 0 2 5 104.99 98.98 5.49 o 1 2 5 615.41 614.43 13.26 o 2 2 5 8.38 11.35 2.84 o 3 2 5 117.33 121.23 5.07 o 4 2 5 103.82 96.41 4.65 o 5 2 5 115.20 114.05 5.10 o 6 2 5 22.21 23.49 5.22 o 7 2 5 4.92 0.92 6.12 o 8 2 5 2.10 7.63 6.93 o 9 2 5 26.64 31.40 7.02 o -13 3 5 2027.79 2084.84 30.30 o -12 3 5 2346.76 2322.32 32.39 o -11 3 5 1767.10 1773.02 24.50 o -10 3 5 4042.92 4056.45 43.75 o -9 3 5 3314.22 3256.90 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