#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217291.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217291_Fobs loop_ _publ_author_name 'Li, Yang' 'Hua, Guoxiong' 'Slawin, Alexandra M. Z.' 'Woollins, J. Derek' _publ_section_title ; 5-Benzylidene-2,3-diphenyl-1,2-selenaphosphole-2-selenide ; _journal_coeditor_code SI2054 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o4 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.847 _cell_angle_gamma 90.000 _cell_length_a 22.3854 _cell_length_b 14.4348 _cell_length_c 12.4433 _exptl_crystal_F_000 1920.00 _reflns_d_resolution_high 0.7763 _[local]_cod_data_source_file si2054Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2c in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 358.31 355.51 60.97 o 8 0 0 153393.98 161706.47 304.38 o 10 0 0 58331.55 60059.54 155.76 o 12 0 0 4309.76 3427.51 73.51 o 14 0 0 12456.87 10930.15 297.99 o 16 0 0 2986.94 2647.66 62.46 o 18 0 0 1151.30 1191.50 68.38 o 20 0 0 16958.36 17091.05 507.38 o 22 0 0 14410.19 14639.34 282.07 o 24 0 0 3539.62 3350.63 262.74 o 3 1 0 407.15 481.34 35.70 o 5 1 0 496.62 571.40 36.32 o 7 1 0 4071.99 4035.11 190.69 o 9 1 0 9949.20 9760.75 124.09 o 11 1 0 9453.09 8900.04 170.56 o 13 1 0 24183.19 25970.49 360.92 o 15 1 0 2682.50 2629.82 47.56 o 17 1 0 438.11 275.09 79.14 o 19 1 0 27387.34 27046.86 330.57 o 21 1 0 13896.57 13270.15 506.14 o 23 1 0 1779.20 1773.05 189.14 o 25 1 0 1494.09 1591.27 179.47 o 0 2 0 3597.24 3659.96 50.56 o 2 2 0 9313.04 9010.15 85.20 o 4 2 0 15197.65 16016.90 216.30 o 6 2 0 45079.59 46670.25 325.62 o 8 2 0 23001.16 23558.30 303.17 o 10 2 0 4902.54 5801.62 70.26 o 12 2 0 1034.28 877.34 68.45 o 14 2 0 21193.67 20555.30 215.73 o 16 2 0 11840.78 11535.97 232.40 o 18 2 0 22458.28 22423.97 740.39 o 20 2 0 6126.34 6075.98 108.69 o 22 2 0 1378.50 1441.12 317.02 o 24 2 0 6216.46 6078.79 193.58 o 1 3 0 3919.80 4323.23 109.19 o 3 3 0 876.82 1273.20 121.12 o 5 3 0 90.00 153.67 46.16 o 7 3 0 3548.57 3526.16 45.96 o 9 3 0 3292.13 2918.94 102.18 o 11 3 0 1540.07 1392.62 71.31 o 13 3 0 204.30 419.82 105.25 o 15 3 0 14833.84 14461.11 187.94 o 17 3 0 17131.82 16228.30 109.87 o 19 3 0 9516.07 9557.08 149.90 o 21 3 0 154.23 183.67 168.77 o 23 3 0 861.44 635.84 183.78 o 25 3 0 3384.62 3192.58 406.25 o 0 4 0 54494.95 57923.30 519.36 o 2 4 0 56716.17 55733.26 727.38 o 4 4 0 27368.84 27519.21 344.37 o 6 4 0 1350.57 1600.97 92.08 o 8 4 0 13807.03 13128.61 211.75 o 10 4 0 69407.31 70140.45 711.97 o 12 4 0 50091.37 51055.74 405.70 o 14 4 0 6206.19 6373.72 78.19 o 16 4 0 7047.97 6810.07 102.38 o 18 4 0 3465.09 3632.70 143.95 o 20 4 0 1634.19 1750.34 108.07 o 22 4 0 1030.75 896.05 188.51 o 24 4 0 519.26 355.11 208.72 o 1 5 0 32429.50 34506.18 542.98 o 3 5 0 39948.60 40663.55 481.60 o 5 5 0 13822.36 14060.32 330.70 o 7 5 0 1692.72 1838.94 63.58 o 9 5 0 24594.04 23397.43 259.70 o 11 5 0 71079.24 74034.45 535.93 o 13 5 0 28282.90 27878.62 242.92 o 15 5 0 270.73 255.96 92.72 o 17 5 0 1378.95 1259.17 121.73 o 19 5 0 1028.93 1492.98 148.43 o 21 5 0 1023.83 986.27 226.80 o 23 5 0 1003.01 941.17 389.89 o 25 5 0 1520.96 1112.41 261.25 o 0 6 0 2190.43 1707.89 130.89 o 2 6 0 7620.22 7287.07 166.86 o 4 6 0 1541.84 1542.04 73.23 o 6 6 0 401.98 317.38 50.78 o 8 6 0 5.08 69.04 42.12 o 10 6 0 947.27 1036.50 93.04 o 12 6 0 538.34 579.71 41.71 o 14 6 0 540.76 778.12 87.86 o 16 6 0 8561.58 8796.85 141.03 o 18 6 0 297.23 203.97 146.82 o 20 6 0 14.07 186.70 258.77 o 22 6 0 2570.76 2604.36 417.16 o 24 6 0 807.26 1461.41 323.21 o 1 7 0 66395.45 70031.63 629.25 o 3 7 0 30024.74 29682.43 424.59 o 5 7 0 2537.06 2955.21 101.93 o 7 7 0 8715.47 8531.00 971.13 o 9 7 0 10072.38 9900.39 140.41 o 11 7 0 7778.09 7278.72 161.11 o 13 7 0 8423.17 7972.24 208.09 o 15 7 0 7189.70 7529.55 791.84 o 17 7 0 4032.40 3881.92 178.71 o 19 7 0 206.83 226.93 148.27 o 21 7 0 1424.23 1483.02 206.72 o 23 7 0 4989.55 5169.45 270.67 o 25 7 0 2760.72 2929.26 302.39 o 0 8 0 1843.01 2221.06 88.75 o 2 8 0 50.92 60.31 96.17 o 4 8 0 4807.71 5197.99 84.72 o 6 8 0 1075.08 1106.45 72.03 o 8 8 0 136.32 113.45 100.97 o 10 8 0 2260.72 2355.95 78.70 o 12 8 0 296.64 258.32 59.56 o 14 8 0 3117.35 3093.66 66.01 o 16 8 0 1350.09 1275.79 137.46 o 18 8 0 218.73 204.16 232.74 o 20 8 0 100.24 79.10 154.65 o 22 8 0 128.68 200.83 173.31 o 24 8 0 65.58 421.37 240.43 o 1 9 0 10665.59 9733.72 167.51 o 3 9 0 4108.15 3664.47 90.96 o 5 9 0 25.35 3.32 57.93 o 7 9 0 1562.50 1860.33 60.48 o 9 9 0 21.56 102.15 56.43 o 11 9 0 516.58 565.43 71.28 o 13 9 0 11400.72 10428.75 418.41 o 15 9 0 13886.47 13815.63 160.08 o 17 9 0 14135.53 13978.09 224.57 o 19 9 0 168.67 170.44 159.79 o 21 9 0 144.77 51.85 185.75 o 23 9 0 4519.73 5127.31 269.18 o 0 10 0 3518.90 3477.13 177.11 o 2 10 0 12.11 15.40 100.88 o 4 10 0 801.41 959.24 106.04 o 6 10 0 35.15 104.43 57.82 o 8 10 0 736.27 852.71 98.65 o 10 10 0 13104.88 12912.62 214.31 o 12 10 0 1509.45 1602.83 158.20 o 14 10 0 9214.45 8729.37 151.40 o 16 10 0 13976.62 13750.30 248.61 o 18 10 0 1909.32 2046.30 427.32 o 20 10 0 359.78 314.42 173.53 o 22 10 0 985.45 1019.22 284.55 o 1 11 0 30565.27 30374.48 262.01 o 3 11 0 24101.43 23687.97 309.25 o 5 11 0 4361.95 4219.33 115.72 o 7 11 0 3972.41 3808.07 89.93 o 9 11 0 41038.02 41538.73 547.60 o 11 11 0 52177.54 51294.17 1184.37 o 13 11 0 12733.14 12318.73 159.88 o 15 11 0 2521.72 2438.42 154.61 o 17 11 0 1828.18 1786.56 232.74 o 19 11 0 7087.21 6768.05 214.81 o 21 11 0 565.41 549.27 246.87 o 23 11 0 752.01 851.66 300.91 o 0 12 0 28565.89 31337.36 1479.15 o 2 12 0 21467.50 21027.20 204.50 o 4 12 0 11349.60 11030.63 90.04 o 6 12 0 72.42 173.07 108.60 o 8 12 0 18905.50 19119.68 287.64 o 10 12 0 22471.03 22829.35 393.90 o 12 12 0 25022.39 23937.41 444.92 o 14 12 0 2865.71 3059.53 169.96 o 16 12 0 7.96 218.07 175.77 o 18 12 0 4272.27 4297.69 207.71 o 20 12 0 2904.93 2746.33 265.21 o 1 13 0 3122.09 3541.12 626.18 o 3 13 0 374.99 160.59 88.19 o 5 13 0 143.73 319.31 110.01 o 7 13 0 9076.04 9543.95 745.57 o 9 13 0 3022.07 3123.04 135.54 o 11 13 0 478.78 751.32 145.22 o 13 13 0 57.70 351.29 235.72 o 15 13 0 2627.03 2802.00 184.41 o 17 13 0 4423.86 4853.18 282.07 o 0 14 0 13846.46 14840.61 279.59 o 2 14 0 324.27 158.08 131.37 o 4 14 0 1518.05 1536.94 153.46 o 6 14 0 14526.39 15052.14 313.93 o 8 14 0 4011.89 3883.42 163.59 o 10 14 0 117.03 203.35 201.79 o 12 14 0 4631.56 4813.61 169.58 o 14 14 0 3812.13 4457.29 197.07 o 16 14 0 4711.88 5014.78 253.81 o 1 15 0 19057.24 20372.09 850.87 o 3 15 0 678.94 711.51 108.51 o 5 15 0 847.33 1063.94 141.96 o 7 15 0 4641.99 4882.43 224.46 o 9 15 0 8864.08 9162.72 363.62 o 11 15 0 1351.52 1505.96 285.04 o 13 15 0 2273.57 2200.04 284.05 o 0 16 0 41371.84 40377.54 352.46 o 2 16 0 21261.68 21551.35 1347.92 o 4 16 0 2219.21 2487.49 149.33 o 6 16 0 2360.21 2657.93 225.70 o 8 16 0 10422.68 9942.78 824.44 o 10 16 0 12593.46 11916.31 295.95 o 12 16 0 8653.31 8930.54 328.17 o 1 17 0 4521.20 5194.08 424.93 o 3 17 0 3610.56 3639.10 149.62 o 5 17 0 1.50 154.18 267.94 o 7 17 0 717.11 632.84 200.85 o 9 17 0 2551.93 2275.84 205.44 o -25 1 1 78.20 -149.51 192.36 o -23 1 1 7.40 115.36 172.63 o -21 1 1 3588.43 3835.83 219.11 o -19 1 1 8976.90 8277.41 190.05 o -17 1 1 26749.14 26331.87 170.18 o -15 1 1 12047.85 12659.88 217.81 o -13 1 1 560.55 638.47 85.16 o -11 1 1 196.94 91.10 68.26 o -9 1 1 10015.11 9456.84 243.06 o -7 1 1 61519.09 65841.72 708.83 o -5 1 1 61649.86 64673.70 688.33 o -3 1 1 185.42 165.10 29.93 o -1 1 1 13667.03 13887.73 502.92 o 1 1 1 17.57 61.47 11.80 o 3 1 1 16522.11 16851.27 69.90 o 5 1 1 649.51 1005.09 92.58 o 7 1 1 3471.83 3430.66 74.04 o 9 1 1 12051.25 12245.70 132.94 o 11 1 1 43229.13 44228.26 455.09 o 13 1 1 21658.33 21285.43 365.27 o 15 1 1 1102.85 1076.12 87.39 o 17 1 1 6480.92 6514.59 231.17 o 19 1 1 14497.12 15208.36 414.89 o 21 1 1 14426.06 14198.25 176.67 o 23 1 1 2997.04 3084.83 187.32 o 25 1 1 53.20 -176.14 176.14 o -24 2 1 8.47 -118.94 183.72 o -22 2 1 3392.62 3203.28 183.42 o -20 2 1 1712.30 1793.54 123.62 o -18 2 1 7182.50 6645.28 141.59 o -16 2 1 5857.58 5559.47 214.40 o -14 2 1 5096.60 5200.81 105.79 o -12 2 1 13788.48 13303.00 155.45 o -10 2 1 104.28 121.83 27.68 o -8 2 1 1301.91 1374.68 68.21 o -6 2 1 1115.95 1196.55 32.51 o -4 2 1 3517.41 3578.11 26.56 o -2 2 1 21950.76 22247.09 487.12 o 0 2 1 22930.13 24354.37 448.57 o 2 2 1 8403.21 8635.26 54.45 o 4 2 1 3688.93 3647.38 43.39 o 6 2 1 2264.65 2678.44 168.59 o 8 2 1 52.86 251.25 41.32 o 10 2 1 4775.20 5028.25 57.62 o 12 2 1 6543.82 6743.40 69.06 o 14 2 1 5185.86 4414.13 71.32 o 16 2 1 3153.91 3014.22 137.52 o 18 2 1 424.47 433.22 89.91 o 20 2 1 7304.86 7190.84 411.95 o 22 2 1 1273.68 1277.42 191.30 o 24 2 1 1697.53 1826.60 434.75 o 26 2 1 19.19 130.38 251.83 o -25 3 1 647.68 711.82 187.68 o -23 3 1 1313.99 1299.09 170.54 o -21 3 1 2065.04 2097.86 167.33 o -19 3 1 2112.59 2035.27 164.40 o -17 3 1 2450.33 2520.96 120.62 o -15 3 1 27777.40 27708.35 275.83 o -13 3 1 52713.23 53846.36 363.49 o -11 3 1 16924.76 16446.07 88.55 o -9 3 1 404.26 145.56 69.17 o -7 3 1 92796.51 96856.90 1014.16 o -5 3 1 74544.78 75089.34 809.38 o -3 3 1 118157.14 111784.34 183.42 o -1 3 1 1818.01 1912.82 48.99 o 1 3 1 35567.35 37890.38 452.87 o 3 3 1 11278.24 11425.24 140.78 o 5 3 1 57092.04 60581.09 1114.78 o 7 3 1 78895.64 81279.79 246.14 o 9 3 1 69784.87 70570.39 541.65 o 11 3 1 15985.44 16122.73 195.19 o 13 3 1 5091.68 5386.58 91.76 o 15 3 1 22883.88 22145.94 315.40 o 17 3 1 16590.21 16211.56 106.46 o 19 3 1 1853.31 1888.62 103.27 o 21 3 1 676.12 856.21 163.34 o 23 3 1 396.41 117.40 177.22 o 25 3 1 141.65 113.03 294.96 o -24 4 1 1932.35 1775.00 464.25 o -22 4 1 431.66 655.57 173.09 o -20 4 1 336.80 -107.47 153.10 o -18 4 1 206.57 442.19 144.23 o -16 4 1 14930.61 14372.89 145.85 o -14 4 1 16034.90 15398.50 288.80 o -12 4 1 34614.85 34031.42 618.50 o -10 4 1 14326.27 16267.75 223.62 o -8 4 1 10387.28 9779.50 116.92 o -6 4 1 91690.41 95226.94 1264.35 o -4 4 1 74424.91 73028.70 637.67 o -2 4 1 92767.09 99671.06 243.40 o 0 4 1 9988.79 11201.47 249.93 o 2 4 1 810.45 728.87 32.25 o 4 4 1 16590.89 16591.45 175.20 o 6 4 1 98149.99 104388.48 557.39 o 8 4 1 49303.41 49792.38 502.72 o 10 4 1 43249.68 44389.77 348.53 o 12 4 1 192.40 217.75 57.27 o 14 4 1 12049.35 12221.99 120.53 o 16 4 1 32992.80 33356.76 589.66 o 18 4 1 2332.32 2565.75 104.70 o 20 4 1 5418.70 5410.33 142.68 o 22 4 1 300.54 332.05 180.44 o 24 4 1 8.56 -342.03 430.54 o 26 4 1 42.46 -43.13 241.92 o -25 5 1 39.50 217.13 300.91 o -23 5 1 6321.79 6251.31 188.58 o -21 5 1 6040.68 6282.83 240.43 o -19 5 1 18289.34 18313.01 184.71 o -17 5 1 1706.31 1831.58 142.27 o -15 5 1 912.37 953.61 91.76 o -13 5 1 6083.12 6366.29 96.38 o -11 5 1 13495.90 14027.99 139.67 o -9 5 1 14478.50 15523.07 181.38 o -7 5 1 17.51 147.15 50.78 o -5 5 1 1283.80 1368.28 72.86 o -3 5 1 8858.11 9508.53 198.04 o -1 5 1 2333.32 2613.68 73.13 o 1 5 1 27.81 -42.51 53.98 o 3 5 1 7000.46 7286.81 110.63 o 5 5 1 3663.67 3618.63 101.01 o 7 5 1 763.74 898.24 52.38 o 9 5 1 199.76 248.26 60.29 o 11 5 1 5700.58 5316.54 124.00 o 13 5 1 6073.35 5993.25 244.21 o 15 5 1 11342.04 11251.59 200.35 o 17 5 1 900.13 806.45 207.84 o 19 5 1 128.40 172.68 107.13 o 21 5 1 2525.72 2564.17 363.12 o 23 5 1 10868.42 10070.98 215.15 o 25 5 1 4745.33 4472.95 292.98 o -24 6 1 2279.61 2678.91 268.68 o -22 6 1 13587.54 13767.25 437.48 o -20 6 1 16367.24 16012.95 529.69 o -18 6 1 11196.04 10535.31 197.55 o -16 6 1 1002.82 1161.32 145.65 o -14 6 1 143.34 317.99 88.76 o -12 6 1 2945.01 2994.14 110.05 o -10 6 1 17960.96 17768.15 237.84 o -8 6 1 28094.09 26961.05 349.61 o -6 6 1 28575.44 28352.26 298.04 o -4 6 1 1862.91 1802.65 62.08 o -2 6 1 8013.39 9115.11 199.99 o 0 6 1 37122.53 41085.75 727.59 o 2 6 1 1554.12 1523.77 103.74 o 4 6 1 47233.45 48992.60 435.22 o 6 6 1 4776.94 4668.69 56.24 o 8 6 1 60.15 204.69 91.17 o 10 6 1 30427.42 31629.97 543.27 o 12 6 1 33517.19 32462.22 407.24 o 14 6 1 8356.87 8111.25 138.38 o 16 6 1 1764.83 1775.08 106.83 o 18 6 1 148.02 223.18 105.46 o 20 6 1 2893.50 2985.13 175.07 o 22 6 1 10831.66 10167.06 446.90 o 24 6 1 10733.17 10404.34 302.89 o -23 7 1 9372.59 9369.33 226.91 o -21 7 1 11602.64 10970.73 201.88 o -19 7 1 1191.13 1148.28 287.03 o -17 7 1 8281.79 8253.71 167.82 o -15 7 1 14355.35 14506.87 208.70 o -13 7 1 9617.21 9962.61 130.79 o -11 7 1 11814.68 11511.35 162.44 o -9 7 1 48.44 87.03 56.64 o -7 7 1 578.67 747.79 60.31 o -5 7 1 8466.73 7483.71 126.32 o -3 7 1 40479.13 38150.04 513.52 o -1 7 1 38300.36 39155.07 298.48 o 1 7 1 13556.12 14990.93 189.90 o 3 7 1 42219.45 44368.59 497.29 o 5 7 1 32368.35 30752.81 285.06 o 7 7 1 33865.23 32581.54 3450.33 o 9 7 1 108.73 182.66 51.30 o 11 7 1 49.99 322.76 104.00 o 13 7 1 445.55 354.64 86.20 o 15 7 1 1635.70 1541.31 132.29 o 17 7 1 16908.56 15481.37 1109.19 o 19 7 1 6761.93 6491.16 188.45 o 21 7 1 1483.93 1603.11 201.27 o 23 7 1 2499.54 2878.69 252.33 o 25 7 1 9825.04 8666.81 301.40 o -24 8 1 3727.00 3868.66 296.45 o -22 8 1 5752.24 5695.40 639.49 o -20 8 1 129.72 188.34 189.50 o -18 8 1 3982.11 3712.18 328.42 o -16 8 1 32679.65 32033.80 595.86 o -14 8 1 27085.49 27150.99 272.65 o -12 8 1 26064.60 25094.46 526.54 o -10 8 1 3107.02 2851.08 65.75 o -8 8 1 8460.90 9041.38 130.32 o -6 8 1 31497.31 29989.01 163.38 o -4 8 1 98024.37 94382.16 667.54 o -2 8 1 146713.44 144711.78 1296.14 o 0 8 1 32857.64 31367.79 833.80 o 2 8 1 1172.19 1199.65 138.35 o 4 8 1 90476.74 89851.84 1030.35 o 6 8 1 91189.34 86916.05 1119.84 o 8 8 1 63175.59 62654.20 289.91 o 10 8 1 5889.27 5502.83 129.81 o 12 8 1 750.66 953.65 67.81 o 14 8 1 252.46 246.55 57.75 o 16 8 1 21883.00 21497.66 789.70 o 18 8 1 19763.79 18904.38 1334.25 o 20 8 1 12728.04 12994.26 197.62 o 22 8 1 224.26 407.98 264.22 o 24 8 1 1340.04 1183.80 241.42 o -23 9 1 3052.86 3062.61 260.75 o -21 9 1 591.91 597.96 171.64 o -19 9 1 824.95 957.76 221.84 o -17 9 1 524.50 764.54 197.55 o -15 9 1 7772.66 7985.60 436.49 o -13 9 1 14895.33 14316.67 713.09 o -11 9 1 3087.34 2866.68 397.98 o -9 9 1 643.57 723.87 60.49 o -7 9 1 2342.04 2394.57 89.50 o -5 9 1 9922.54 9232.34 128.07 o -3 9 1 42667.56 42908.99 372.86 o -1 9 1 23302.88 23581.90 277.47 o 1 9 1 1784.48 2007.18 72.19 o 3 9 1 8341.10 7964.33 99.14 o 5 9 1 26532.50 25077.65 132.14 o 7 9 1 28352.63 28600.92 258.09 o 9 9 1 7711.62 8500.60 230.97 o 11 9 1 834.04 833.31 98.92 o 13 9 1 566.61 528.93 65.81 o 15 9 1 2800.84 2926.68 134.32 o 17 9 1 8658.76 9213.86 160.06 o 19 9 1 2658.21 2854.82 191.00 o 21 9 1 25.76 211.53 173.41 o 23 9 1 1370.95 1658.21 288.02 o -22 10 1 1627.28 2196.57 261.74 o -20 10 1 5589.15 5945.46 392.37 o -18 10 1 20967.20 21460.23 520.51 o -16 10 1 6518.28 6248.56 380.22 o -14 10 1 790.44 917.21 210.19 o -12 10 1 5724.05 5298.81 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