#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:46:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181093 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217304.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217304_Fobs loop_ _publ_author_name 'Polson, Matthew I. J.' _publ_section_title ; (\h^6^-Benzene)(2,2'-bipyridine-\k^2^N,N')chloridoruthenium(II) chloride methanol sesquisolvate ; _journal_coeditor_code SJ2425 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m256 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 85.597 _cell_angle_beta 84.531 _cell_angle_gamma 75.875 _cell_length_a 6.9027 _cell_length_b 10.2346 _cell_length_c 12.8949 _exptl_crystal_F_000 453.00 _reflns_d_resolution_high 0.8393 _cod_data_source_file sj2425Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3mp28 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 12444.55 11397.14 179.13 o 2 0 0 387.23 381.81 14.27 o 3 0 0 179.81 152.84 5.68 o 4 0 0 5566.09 5199.42 203.93 o 5 0 0 658.06 652.48 18.22 o 6 0 0 327.18 311.00 14.79 o 7 0 0 52.32 62.05 11.00 o -6 1 0 277.84 244.07 13.71 o -5 1 0 1623.76 1615.77 28.32 o -4 1 0 1129.85 1130.88 20.93 o -3 1 0 1672.48 1603.15 21.11 o -2 1 0 25.51 43.29 5.05 o -1 1 0 8782.34 10066.00 64.67 o 1 1 0 1024.88 992.08 6.82 o 2 1 0 0.89 18.02 3.61 o 3 1 0 5376.24 5230.18 31.69 o 4 1 0 699.09 681.52 9.14 o 5 1 0 33.15 44.20 7.58 o 6 1 0 64.76 70.53 9.38 o 7 1 0 1496.27 1483.19 31.39 o 8 1 0 225.57 192.30 15.15 o -7 2 0 16.35 24.17 8.48 o -6 2 0 0.98 5.77 7.40 o -5 2 0 274.72 272.39 14.61 o -4 2 0 2688.75 2598.73 32.47 o -3 2 0 1785.41 1718.06 23.45 o -2 2 0 702.15 824.75 13.71 o -1 2 0 1280.52 1064.24 20.11 o 0 2 0 4094.21 3575.34 113.11 o 1 2 0 11940.55 11484.17 52.79 o 2 2 0 35919.06 40435.83 137.16 o 3 2 0 4824.39 4854.56 94.06 o 4 2 0 3295.63 3184.99 35.97 o 5 2 0 54.25 45.68 4.57 o 6 2 0 895.92 979.89 23.81 o 7 2 0 593.27 562.64 20.20 o 8 2 0 22.48 32.65 9.20 o -7 3 0 127.45 124.47 13.35 o -6 3 0 41.51 44.38 9.20 o -5 3 0 1710.51 1614.51 29.76 o -4 3 0 1904.03 1756.66 27.60 o -3 3 0 4.95 18.76 5.23 o -2 3 0 1222.25 1114.24 36.89 o -1 3 0 3529.04 3458.65 17.18 o 0 3 0 4538.76 4328.99 97.86 o 1 3 0 215.65 150.17 3.52 o 2 3 0 538.16 540.42 6.93 o 3 3 0 4053.52 4311.64 72.52 o 4 3 0 2034.30 1913.16 22.34 o 5 3 0 270.12 324.29 9.09 o 6 3 0 232.27 210.70 12.99 o 7 3 0 302.87 332.28 16.24 o 8 3 0 291.40 266.62 16.60 o -6 4 0 27.84 24.53 8.66 o -5 4 0 153.97 150.63 12.27 o -4 4 0 714.09 670.34 19.30 o -3 4 0 163.87 145.58 10.28 o -2 4 0 1170.52 1050.19 36.35 o -1 4 0 6331.63 6040.57 61.42 o 0 4 0 920.65 814.90 19.75 o 1 4 0 535.33 600.13 31.26 o 2 4 0 2077.61 2052.69 26.79 o 3 4 0 10844.09 11630.56 150.27 o 4 4 0 5596.31 6251.42 30.79 o 5 4 0 356.85 361.07 8.02 o 6 4 0 1255.77 1213.31 21.56 o 7 4 0 466.01 484.71 19.12 o 8 4 0 184.24 192.12 14.61 o -6 5 0 99.99 92.72 11.18 o -5 5 0 262.09 235.59 14.43 o -4 5 0 1690.98 1714.27 30.13 o -3 5 0 1223.42 1192.57 23.27 o -2 5 0 2315.54 2088.68 62.96 o -1 5 0 103.83 81.41 4.91 o 0 5 0 831.04 862.05 54.84 o 1 5 0 1377.46 1315.00 59.33 o 2 5 0 3986.76 3967.09 19.83 o 3 5 0 26.15 46.37 5.59 o 4 5 0 262.72 272.24 7.63 o 5 5 0 724.87 680.44 18.76 o 6 5 0 1193.24 1166.71 17.68 o 7 5 0 45.37 40.41 8.84 o 8 5 0 11.34 0.36 7.58 o -5 6 0 771.14 751.69 23.45 o -4 6 0 7.09 7.04 6.13 o -3 6 0 0.32 2.71 7.04 o -2 6 0 229.31 225.31 12.09 o -1 6 0 1352.25 1367.05 25.62 o 0 6 0 778.72 757.37 11.99 o 1 6 0 2033.59 1942.56 129.66 o 2 6 0 54.75 60.25 7.58 o 3 6 0 1877.33 1973.67 29.58 o 4 6 0 786.32 832.33 21.11 o 5 6 0 2220.74 2095.26 32.11 o 6 6 0 928.84 924.60 17.22 o 7 6 0 13.28 45.64 9.20 o -5 7 0 15.20 11.91 8.30 o -4 7 0 83.20 82.98 10.64 o -3 7 0 269.94 248.04 13.53 o -2 7 0 1858.40 1950.22 31.03 o -1 7 0 651.11 620.55 15.51 o 0 7 0 3.34 4.48 5.14 o 1 7 0 107.12 89.99 6.57 o 2 7 0 521.49 493.55 16.96 o 3 7 0 579.36 570.58 18.22 o 4 7 0 564.28 533.78 18.76 o 5 7 0 116.48 97.41 11.91 o 6 7 0 288.39 294.76 16.60 o 7 7 0 415.10 418.90 16.87 o -4 8 0 93.57 75.04 10.82 o -3 8 0 604.04 565.89 19.48 o -2 8 0 3.77 -1.80 6.31 o -1 8 0 479.02 458.03 11.86 o 0 8 0 504.71 589.20 13.18 o 1 8 0 859.78 857.56 19.84 o 2 8 0 240.25 221.52 14.07 o 3 8 0 117.58 157.66 12.99 o 4 8 0 416.50 402.09 18.04 o 5 8 0 1019.94 1002.08 26.52 o 6 8 0 164.98 161.45 15.15 o 7 8 0 517.59 453.69 14.47 o -3 9 0 1.69 4.51 6.85 o -2 9 0 474.40 454.23 18.40 o -1 9 0 573.94 555.97 18.58 o 0 9 0 1054.31 1022.47 55.65 o 1 9 0 58.35 60.71 6.72 o 2 9 0 215.95 223.87 14.61 o 3 9 0 282.48 269.87 15.69 o 4 9 0 512.65 547.67 20.93 o 5 9 0 128.03 138.00 14.07 o 6 9 0 75.59 66.75 12.09 o -2 10 0 120.86 129.88 12.09 o -1 10 0 255.37 286.28 15.33 o 0 10 0 20.17 22.73 7.58 o 1 10 0 703.58 734.01 41.67 o 2 10 0 213.23 197.35 15.33 o 3 10 0 372.02 369.44 18.76 o 4 10 0 26.53 23.45 9.92 o 5 10 0 1.95 0.00 8.84 o 6 10 0 64.06 50.33 12.81 o -1 11 0 7.44 16.60 7.22 o 0 11 0 786.52 923.61 25.98 o 1 11 0 395.09 389.58 36.80 o 2 11 0 211.97 214.85 16.60 o 3 11 0 11.37 8.84 10.10 o 4 11 0 730.04 723.37 27.24 o 5 11 0 62.60 54.12 12.63 o 1 12 0 8.60 -4.69 9.38 o 2 12 0 5.44 -4.60 9.20 o 3 12 0 648.43 665.83 28.14 o -2 -12 1 101.30 78.11 14.25 o -4 -11 1 384.02 378.64 20.75 o -3 -11 1 1255.65 1241.82 33.73 o -2 -11 1 172.98 186.35 15.69 o -1 -11 1 157.53 170.20 19.84 o 0 -11 1 255.17 329.40 16.96 o 1 -11 1 448.26 471.00 20.02 o -5 -10 1 240.82 224.77 16.42 o -4 -10 1 1410.89 1360.88 33.91 o -3 -10 1 58.99 47.80 10.64 o -2 -10 1 2.07 -1.26 7.40 o -1 -10 1 72.58 78.26 7.22 o 0 -10 1 708.41 704.49 29.76 o 1 -10 1 38.73 40.23 8.66 o 2 -10 1 79.65 93.98 11.55 o -6 -9 1 55.30 50.33 10.64 o -5 -9 1 578.22 563.55 22.37 o -4 -9 1 29.14 23.45 8.66 o -3 -9 1 964.57 901.24 25.80 o -2 -9 1 207.26 228.02 14.79 o -1 -9 1 2284.56 2419.74 33.82 o 0 -9 1 223.21 234.29 9.87 o 1 -9 1 80.73 91.28 9.56 o 2 -9 1 103.17 94.71 11.00 o 3 -9 1 838.02 928.12 27.42 o -7 -8 1 418.06 416.89 20.20 o -6 -8 1 0.75 -3.43 6.85 o -5 -8 1 4.39 4.15 7.40 o -4 -8 1 2114.74 2157.49 36.98 o -3 -8 1 383.47 377.92 16.96 o -2 -8 1 685.81 664.75 20.93 o -1 -8 1 117.18 112.25 7.71 o 0 -8 1 1346.57 1388.52 63.41 o 1 -8 1 29.14 42.26 8.66 o 2 -8 1 255.74 294.22 14.43 o 3 -8 1 119.28 118.70 11.91 o 4 -8 1 76.00 78.83 10.28 o -7 -7 1 389.37 378.95 13.20 o -6 -7 1 66.18 77.39 9.92 o -5 -7 1 997.61 1041.22 25.62 o -4 -7 1 649.30 686.39 21.11 o -3 -7 1 6.71 11.18 6.85 o -2 -7 1 51.58 56.82 8.30 o -1 -7 1 4816.74 5068.32 61.33 o 0 -7 1 1599.19 1676.63 57.82 o 1 -7 1 508.03 492.21 11.54 o 2 -7 1 406.33 389.65 16.24 o 3 -7 1 870.65 840.27 23.09 o 4 -7 1 292.80 291.51 16.05 o 5 -7 1 232.70 242.81 15.87 o -7 -6 1 592.80 595.11 21.47 o -6 -6 1 3081.01 2835.77 38.96 o -5 -6 1 2132.10 2081.73 32.83 o -4 -6 1 1190.75 1282.95 25.62 o -3 -6 1 480.21 517.18 16.42 o -2 -6 1 2480.45 2808.53 34.45 o -1 -6 1 3337.87 3649.43 81.45 o 0 -6 1 44.95 42.95 4.46 o 1 -6 1 10.31 15.89 6.95 o 2 -6 1 1449.80 1422.21 25.44 o 3 -6 1 545.13 561.20 18.22 o 4 -6 1 16.75 17.32 7.40 o 5 -6 1 84.91 97.41 11.91 o -7 -5 1 65.07 57.55 9.02 o -6 -5 1 573.62 543.03 34.82 o -5 -5 1 1491.87 1477.41 25.62 o -4 -5 1 2656.91 2772.27 33.73 o -3 -5 1 183.80 202.94 10.64 o -2 -5 1 2212.89 2292.79 28.50 o -1 -5 1 954.54 906.35 65.98 o 0 -5 1 3527.74 3717.11 60.16 o 1 -5 1 3159.55 3136.18 106.43 o 2 -5 1 2077.26 2078.78 37.79 o 3 -5 1 2.79 5.41 6.49 o 4 -5 1 0.91 6.49 7.22 o 5 -5 1 351.94 342.38 16.78 o 6 -5 1 381.42 399.93 19.12 o -8 -4 1 3.30 1.26 7.76 o -7 -4 1 6.07 15.69 7.76 o -6 -4 1 50.76 46.57 5.35 o -5 -4 1 3940.68 3854.58 108.87 o -4 -4 1 3505.11 3730.87 35.90 o -3 -4 1 2019.26 2212.15 26.34 o -2 -4 1 2184.86 2456.16 14.56 o -1 -4 1 7796.96 8436.85 242.90 o 0 -4 1 2118.61 2027.75 20.84 o 1 -4 1 2514.91 2542.95 63.77 o 2 -4 1 134.39 119.20 4.97 o 3 -4 1 1596.90 1551.91 24.71 o 4 -4 1 1080.00 1009.84 23.09 o 5 -4 1 463.00 473.53 18.04 o 6 -4 1 65.90 64.58 10.46 o -8 -3 1 113.03 115.81 12.81 o -7 -3 1 139.94 131.87 12.81 o -6 -3 1 1172.35 1043.75 24.71 o -5 -3 1 0.76 21.42 4.29 o -4 -3 1 366.99 379.55 11.36 o -3 -3 1 3074.71 3797.62 31.21 o -2 -3 1 9202.05 10049.06 342.66 o -1 -3 1 9.11 61.33 5.59 o 0 -3 1 1.82 20.31 2.47 o 1 -3 1 214.46 169.57 4.93 o 2 -3 1 6805.25 6869.41 122.04 o 3 -3 1 1797.68 1701.10 24.17 o 4 -3 1 319.53 342.20 14.25 o 5 -3 1 0.12 11.73 7.40 o 6 -3 1 42.84 55.38 9.74 o 7 -3 1 166.52 152.07 13.89 o -8 -2 1 71.28 91.10 11.55 o -7 -2 1 707.62 651.94 21.83 o -6 -2 1 39.68 55.74 9.20 o -5 -2 1 1197.43 1041.31 13.34 o -4 -2 1 651.84 646.28 9.88 o -3 -2 1 7798.24 8242.30 42.57 o -2 -2 1 13212.06 13842.40 94.16 o -1 -2 1 1032.52 957.70 12.81 o 0 -2 1 8559.78 8239.69 302.07 o 1 -2 1 6971.86 7328.31 110.94 o 2 -2 1 1312.07 1025.33 34.82 o 4 -2 1 529.42 496.98 14.61 o 5 -2 1 1242.67 1268.70 26.52 o 6 -2 1 527.65 492.29 17.86 o 7 -2 1 87.49 87.31 11.36 o -8 -1 1 1.93 1.44 7.40 o -7 -1 1 0.40 -2.16 6.67 o -6 -1 1 617.29 516.46 18.22 o -5 -1 1 705.73 696.67 18.58 o -4 -1 1 399.00 398.13 7.31 o -3 -1 1 60.26 72.98 5.68 o -2 -1 1 2184.62 2538.66 18.76 o -1 -1 1 9628.41 10373.64 71.44 o 0 -1 1 6110.21 7229.56 95.88 o 1 -1 1 186.53 281.53 3.43 o 2 -1 1 88.60 42.92 3.25 o 3 -1 1 1211.26 1102.44 45.10 o 4 -1 1 2818.94 2765.95 31.39 o 5 -1 1 347.62 312.98 14.07 o 6 -1 1 0.02 9.38 6.85 o 7 -1 1 80.76 103.18 12.45 o -7 0 1 431.20 368.00 17.86 o -6 0 1 440.14 422.12 16.42 o -5 0 1 161.59 206.55 11.73 o -4 0 1 125.89 135.40 4.45 o -3 0 1 3985.10 3928.84 37.88 o -2 0 1 2398.79 2100.04 39.24 o -1 0 1 2903.87 3277.75 70.62 o 1 0 1 3264.87 2943.76 92.63 o 2 0 1 7129.32 7009.81 78.46 o 3 0 1 2150.07 2007.44 38.27 o 4 0 1 9.94 20.55 3.82 o 5 0 1 56.20 58.99 7.58 o 6 0 1 527.83 545.87 18.76 o 7 0 1 1237.96 1129.62 28.14 o -7 1 1 120.85 136.02 12.81 o -6 1 1 115.30 80.82 9.74 o -5 1 1 197.09 193.02 12.27 o -4 1 1 1281.31 1182.83 21.47 o -3 1 1 1664.65 1595.93 21.47 o -2 1 1 347.87 362.23 8.84 o -1 1 1 3007.16 3600.09 21.65 o 0 1 1 9972.18 8147.23 129.61 o 1 1 1 12304.08 13411.88 59.38 o 2 1 1 5685.89 6094.97 77.48 o 3 1 1 959.31 928.14 27.89 o 4 1 1 1453.55 1269.64 35.79 o 5 1 1 455.99 459.96 21.29 o 6 1 1 1945.47 1776.14 30.49 o 7 1 1 1.18 1.98 7.04 o 8 1 1 169.63 165.60 14.43 o -7 2 1 536.68 495.00 20.75 o -6 2 1 418.82 415.62 17.50 o -5 2 1 497.74 458.92 16.60 o -4 2 1 195.71 198.43 11.36 o -3 2 1 79.01 134.75 8.66 o -2 2 1 502.89 528.01 11.73 o -1 2 1 9086.97 7976.31 124.74 o 0 2 1 783.96 944.52 19.21 o 1 2 1 1086.42 1184.88 36.17 o 2 2 1 1316.55 1698.48 12.45 o 3 2 1 4875.37 4416.39 64.88 o 4 2 1 1794.12 1836.10 16.31 o 5 2 1 1075.23 1043.81 31.03 o 6 2 1 3.39 3.43 6.85 o 7 2 1 644.72 581.95 20.38 o 8 2 1 170.84 166.86 14.07 o -7 3 1 317.68 342.93 18.40 o -6 3 1 209.42 240.82 14.79 o -5 3 1 0.47 3.79 6.67 o -4 3 1 1384.66 1380.00 24.89 o -3 3 1 441.82 438.71 13.35 o -2 3 1 1629.19 1214.73 48.35 o -1 3 1 262.45 245.40 10.64 o 0 3 1 1578.85 1560.53 63.14 o 1 3 1 28.03 56.46 11.55 o 2 3 1 4103.12 4070.47 30.67 o 3 3 1 1529.00 2147.63 16.39 o 4 3 1 304.57 361.88 9.57 o 5 3 1 33.17 25.09 3.54 o 6 3 1 1055.39 1008.39 23.81 o 7 3 1 126.38 135.29 12.63 o 8 3 1 169.24 168.67 13.53 o -6 4 1 41.06 23.27 8.30 o -5 4 1 1154.65 1094.62 25.07 o -4 4 1 555.64 596.74 18.04 o -3 4 1 86.92 91.64 9.20 o -2 4 1 248.83 256.48 26.43 o -1 4 1 978.46 730.22 9.54 o 0 4 1 144.59 121.89 11.73 o 1 4 1 3722.20 3258.62 151.07 o 2 4 1 102.20 122.67 5.41 o 3 4 1 3218.18 3229.52 127.54 o 4 4 1 57.29 69.35 5.16 o 5 4 1 1337.97 1268.45 28.50 o 6 4 1 990.64 996.09 13.01 o 7 4 1 197.02 194.28 13.53 o 8 4 1 10.40 10.28 7.94 o -6 5 1 427.31 395.96 18.94 o -5 5 1 681.24 700.64 22.01 o -4 5 1 70.79 76.13 9.38 o -3 5 1 217.65 237.94 12.45 o -2 5 1 3747.92 3514.15 25.98 o -1 5 1 916.46 814.30 30.94 o 0 5 1 240.02 306.29 11.00 o 1 5 1 405.78 358.18 22.89 o 2 5 1 3795.28 3583.52 19.98 o 3 5 1 1588.27 1789.77 35.72 o 4 5 1 325.23 322.95 24.53 o 5 5 1 2028.20 2208.75 63.32 o 6 5 1 107.90 107.83 14.97 o 7 5 1 129.64 133.49 12.27 o 8 5 1 228.58 241.18 15.69 o -5 6 1 83.01 102.82 11.91 o -4 6 1 427.08 408.59 16.78 o -3 6 1 1005.70 919.46 21.83 o -2 6 1 1540.28 1548.31 25.44 o -1 6 1 569.47 603.03 12.36 o 0 6 1 11.21 7.87 3.29 o 1 6 1 544.08 472.83 18.11 o 2 6 1 2926.60 2845.84 71.25 o 3 6 1 0.73 -0.36 4.87 o 4 6 1 23.83 14.25 7.22 o 5 6 1 946.25 916.39 23.45 o 6 6 1 335.32 374.17 30.85 o 7 6 1 27.12 36.80 8.48 o -5 7 1 276.54 301.44 16.42 o -4 7 1 207.71 178.23 12.99 o -3 7 1 1053.63 1061.07 24.89 o -2 7 1 239.65 279.97 14.07 o -1 7 1 1833.38 1690.70 18.62 o 0 7 1 898.13 891.25 49.34 o 1 7 1 2313.12 2322.39 54.93 o 2 7 1 223.67 219.36 12.63 o 3 7 1 139.08 133.13 11.55 o 4 7 1 423.41 402.09 17.32 o 5 7 1 2068.26 2190.50 36.44 o 6 7 1 0.67 -1.08 7.58 o 7 7 1 158.35 169.34 23.36 o -4 8 1 3.42 4.33 6.85 o -3 8 1 33.66 40.95 8.30 o -2 8 1 1316.27 1230.64 26.16 o -1 8 1 40.28 54.81 6.27 o 0 8 1 318.25 312.35 10.29 o 1 8 1 109.50 126.58 7.76 o 2 8 1 739.84 752.42 21.83 o 3 8 1 83.45 78.83 10.64 o 4 8 1 769.88 829.44 24.71 o 5 8 1 9.78 12.81 8.84 o 6 8 1 474.63 494.64 21.83 o 7 8 1 66.93 85.66 10.37 o -3 9 1 550.29 513.04 19.84 o -2 9 1 173.34 179.31 12.63 o -1 9 1 6.02 3.97 5.95 o 0 9 1 136.40 139.94 8.27 o 1 9 1 2879.53 3109.80 135.47 o 2 9 1 265.90 280.51 16.05 o 3 9 1 6.92 9.02 8.12 o 4 9 1 69.15 62.05 11.18 o 5 9 1 1075.35 1087.58 29.40 o 6 9 1 153.72 171.37 15.87 o -2 10 1 264.29 298.01 15.87 o -1 10 1 34.97 36.62 7.94 o 0 10 1 842.89 897.86 33.37 o 1 10 1 192.36 205.91 19.30 o 2 10 1 170.11 165.42 14.79 o 3 10 1 41.81 35.54 10.64 o 4 10 1 711.95 697.58 25.80 o 5 10 1 35.17 48.16 11.18 o 6 10 1 7.14 -4.42 8.84 o -1 11 1 108.82 126.09 11.91 o 0 11 1 270.85 304.86 15.51 o 1 11 1 160.14 186.24 36.53 o 2 11 1 261.84 281.05 18.04 o 3 11 1 847.91 841.89 28.68 o 4 11 1 321.60 321.28 20.02 o 5 11 1 104.41 92.00 15.15 o 1 12 1 193.41 181.11 17.68 o 2 12 1 123.05 117.44 15.51 o 3 12 1 101.34 87.31 14.61 o -4 -11 2 230.41 228.92 17.50 o -3 -11 2 13.42 1.26 8.84 o -2 -11 2 173.37 223.87 16.60 o -1 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