#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217315.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217315_Fobs loop_ _publ_author_name 'Chantrapromma, Suchada' 'Fun, Hoong-Kun' 'Chanawanno, Kullapa' 'Ruanwas, Pumsak' _publ_section_title ; Bis[(E)-2-(3-hydroxy-4-methoxyphenyl)ethenyl]-1-methylquinolinium tetraiodidozincate(II) methanol solvate ; _journal_coeditor_code SJ2450 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m126 _journal_page_last m127 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.724 _cell_angle_gamma 90.000 _cell_length_a 8.6449 _cell_length_b 23.4312 _cell_length_c 19.7763 _exptl_crystal_F_000 2280.00 _reflns_d_resolution_high 0.6046 _[local]_cod_data_source_file sj2450Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' znk7b_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1137.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 96549.12 97660.59 5966.71 o 2 0 0 14043.44 15173.10 187.16 o 3 0 0 49064.06 50306.81 563.15 o 4 0 0 220168.94 222588.22 2362.60 o 5 0 0 30976.24 33340.07 374.86 o 6 0 0 35542.43 35236.19 393.02 o 7 0 0 16935.08 16486.06 244.02 o 8 0 0 8778.18 8619.29 194.18 o 9 0 0 1000.24 865.26 70.67 o 10 0 0 24375.62 25226.91 429.94 o 11 0 0 3436.21 3555.89 171.08 o 12 0 0 4042.02 3669.23 203.09 o 13 0 0 2621.96 2551.03 170.69 o 14 0 0 1292.30 1138.66 235.37 o 1 1 0 819.80 497.28 23.75 o 2 1 0 185.13 42.64 10.04 o 3 1 0 3800.35 3580.98 45.69 o 4 1 0 6.07 -20.33 10.17 o 5 1 0 8.88 16.99 10.81 o 6 1 0 2174.42 2188.62 51.89 o 7 1 0 520.76 582.74 29.58 o 8 1 0 2838.22 2775.72 66.70 o 9 1 0 3650.37 3572.78 87.04 o 10 1 0 6484.16 6654.28 127.99 o 11 1 0 395.55 376.69 39.87 o 12 1 0 1258.48 1220.70 70.90 o 13 1 0 7.74 42.38 43.67 o 14 1 0 22.79 28.75 54.31 o 0 2 0 80488.16 3.89 10.37 o 1 2 0 16718.46 17754.21 159.17 o 2 2 0 210293.08 221465.05 1488.54 o 3 2 0 125.10 189.17 24.98 o 4 2 0 79626.92 80363.55 586.55 o 5 2 0 8925.69 8503.69 95.88 o 6 2 0 25858.69 26491.40 210.71 o 7 2 0 4184.51 4349.59 70.68 o 8 2 0 35344.93 35199.82 344.43 o 9 2 0 8663.70 8713.63 140.39 o 10 2 0 6617.16 6276.90 113.75 o 11 2 0 1462.31 1619.97 76.92 o 12 2 0 9682.86 9520.92 222.41 o 13 2 0 2837.64 3097.76 139.28 o 14 2 0 437.85 478.13 75.00 o 1 3 0 215.64 171.46 11.30 o 2 3 0 4449.92 3959.55 45.45 o 3 3 0 11.70 -15.33 7.67 o 4 3 0 4806.76 4516.03 59.12 o 5 3 0 1351.09 1312.64 32.43 o 6 3 0 1608.35 1596.18 36.03 o 7 3 0 406.27 435.09 27.21 o 8 3 0 32.34 64.75 27.91 o 9 3 0 69.62 84.71 29.65 o 10 3 0 1.88 -53.97 26.98 o 11 3 0 1391.50 1199.47 114.25 o 12 3 0 75.30 114.53 52.74 o 13 3 0 153.24 153.02 48.71 o 14 3 0 1.01 -13.04 43.54 o 0 4 0 535.57 456.87 38.88 o 1 4 0 75334.24 82445.13 683.77 o 2 4 0 549974.00 541734.88 4058.92 o 3 4 0 72427.23 75847.76 552.12 o 4 4 0 32207.39 32744.66 251.05 o 5 4 0 504.80 468.45 25.86 o 6 4 0 24867.04 25155.20 197.75 o 7 4 0 309.72 499.13 41.85 o 8 4 0 44126.21 44137.89 403.44 o 9 4 0 22286.58 22338.95 245.16 o 10 4 0 4011.23 3685.63 105.25 o 11 4 0 564.23 510.27 59.18 o 12 4 0 6910.11 6806.36 186.04 o 13 4 0 4517.29 4800.26 165.52 o 14 4 0 494.23 373.65 61.24 o 1 5 0 564.58 302.35 20.71 o 2 5 0 3536.99 3097.07 48.79 o 3 5 0 777.82 760.57 22.82 o 4 5 0 850.65 731.94 24.43 o 5 5 0 9383.94 9786.34 90.80 o 6 5 0 21.13 47.24 13.71 o 7 5 0 11231.89 11187.67 136.30 o 8 5 0 4882.87 4983.31 94.90 o 9 5 0 4741.74 4665.81 111.71 o 10 5 0 6003.98 6148.79 126.38 o 11 5 0 4385.71 4599.01 140.63 o 12 5 0 2793.85 3122.91 130.71 o 13 5 0 437.77 458.11 70.51 o 14 5 0 214.67 106.34 50.22 o 0 6 0 150109.14 159687.45 1854.14 o 1 6 0 27155.09 29627.51 286.79 o 2 6 0 62162.84 62735.38 540.84 o 3 6 0 4913.34 5083.78 65.67 o 4 6 0 46588.60 47708.19 364.82 o 5 6 0 11248.06 12962.46 122.71 o 6 6 0 70113.59 70491.47 480.12 o 7 6 0 18893.15 18217.96 215.60 o 8 6 0 4010.10 3987.31 112.21 o 9 6 0 1.11 63.14 44.32 o 10 6 0 17584.89 17269.86 238.36 o 11 6 0 12489.95 13023.34 228.77 o 12 6 0 634.42 452.22 83.03 o 13 6 0 1285.33 1147.20 115.33 o 14 6 0 2596.65 2587.78 137.41 o 1 7 0 1328.67 1345.02 34.02 o 2 7 0 135.72 2.54 15.82 o 3 7 0 61.14 98.51 11.72 o 4 7 0 774.09 789.96 28.59 o 5 7 0 4226.73 4308.87 61.26 o 6 7 0 572.45 651.32 42.40 o 7 7 0 68.48 76.16 23.89 o 8 7 0 179.49 126.94 30.98 o 9 7 0 74.78 70.05 33.37 o 10 7 0 190.23 231.37 42.57 o 11 7 0 385.17 571.89 63.46 o 12 7 0 248.12 167.90 45.62 o 13 7 0 6.74 -9.79 49.26 o 14 7 0 71.31 101.77 59.90 o 0 8 0 341726.03 344800.84 4176.93 o 1 8 0 16841.39 17512.29 182.39 o 2 8 0 31146.40 31951.19 286.91 o 3 8 0 1709.18 1649.90 35.70 o 4 8 0 42799.63 44112.26 344.40 o 5 8 0 764.32 1001.64 43.52 o 6 8 0 57765.16 57015.77 480.19 o 7 8 0 28359.14 27134.34 295.43 o 8 8 0 286.57 427.69 60.73 o 9 8 0 357.39 363.07 46.12 o 10 8 0 24168.46 23937.29 302.56 o 11 8 0 10993.89 11127.25 213.31 o 12 8 0 185.40 151.12 45.23 o 13 8 0 457.44 277.35 80.39 o 1 9 0 1265.46 1064.32 37.41 o 2 9 0 346.67 271.52 19.84 o 3 9 0 1320.52 1234.43 38.10 o 4 9 0 519.47 420.33 25.16 o 5 9 0 493.64 564.40 24.90 o 6 9 0 5547.46 5628.77 91.52 o 7 9 0 3485.23 3519.31 83.13 o 8 9 0 2385.37 2251.54 75.81 o 9 9 0 7588.68 8098.74 156.63 o 10 9 0 5665.13 6122.45 149.43 o 11 9 0 2008.10 2065.27 96.20 o 12 9 0 824.37 976.07 69.82 o 13 9 0 1189.89 1220.13 99.37 o 0 10 0 20758.89 24264.78 346.95 o 1 10 0 47575.18 48512.96 443.53 o 2 10 0 217322.83 219837.94 2464.09 o 3 10 0 46146.77 49810.91 412.09 o 4 10 0 17346.86 17120.77 162.43 o 5 10 0 2912.81 2533.46 48.50 o 6 10 0 19560.08 19216.88 204.86 o 7 10 0 1622.30 1763.08 63.40 o 8 10 0 30607.70 30180.87 348.37 o 9 10 0 12236.33 12431.41 204.48 o 10 10 0 1804.66 1694.17 87.20 o 11 10 0 368.03 348.54 57.27 o 12 10 0 5879.69 5750.06 148.10 o 13 10 0 3027.69 3280.87 146.32 o 1 11 0 4421.52 4417.81 72.35 o 2 11 0 924.87 983.19 35.87 o 3 11 0 1458.60 1382.56 41.63 o 4 11 0 6.50 7.34 12.09 o 5 11 0 1437.73 1344.36 41.60 o 6 11 0 709.68 670.04 40.24 o 7 11 0 57.83 51.63 24.93 o 8 11 0 128.92 158.82 36.71 o 9 11 0 140.92 185.34 44.34 o 10 11 0 1311.06 1305.38 80.69 o 11 11 0 14.43 93.29 42.31 o 12 11 0 2.58 138.71 43.85 o 13 11 0 150.42 283.85 62.99 o 0 12 0 25192.17 24793.29 329.89 o 1 12 0 9624.43 9587.71 112.20 o 2 12 0 135145.63 140171.02 1066.47 o 3 12 0 2496.49 2390.38 53.78 o 4 12 0 40191.22 39457.35 305.36 o 5 12 0 7203.10 7045.39 110.97 o 6 12 0 4892.42 4788.77 124.26 o 7 12 0 16.67 65.78 26.57 o 8 12 0 30366.00 29609.20 366.80 o 9 12 0 12545.65 12379.11 218.41 o 10 12 0 2018.03 1813.85 91.29 o 11 12 0 327.48 298.76 51.97 o 12 12 0 5267.64 5286.56 164.83 o 13 12 0 2742.37 2708.11 157.04 o 1 13 0 3137.75 2893.06 56.85 o 2 13 0 585.28 488.26 30.36 o 3 13 0 88.53 93.54 17.26 o 4 13 0 14.97 22.72 15.28 o 5 13 0 627.37 572.46 36.01 o 6 13 0 210.69 157.19 29.38 o 7 13 0 2617.76 2580.22 121.94 o 8 13 0 8207.71 8459.93 175.93 o 9 13 0 858.69 787.65 66.29 o 10 13 0 1430.49 1580.98 88.21 o 11 13 0 907.38 1052.85 76.67 o 12 13 0 1090.91 1266.49 106.77 o 13 13 0 132.11 219.39 64.55 o 0 14 0 321834.69 326928.88 3553.60 o 1 14 0 93500.16 94864.19 721.73 o 2 14 0 2201.35 2562.16 60.00 o 3 14 0 20134.98 20868.80 202.98 o 4 14 0 103840.88 105972.83 783.20 o 5 14 0 12013.93 12403.39 155.87 o 6 14 0 11333.13 10989.61 171.76 o 7 14 0 5063.98 5161.80 135.79 o 8 14 0 5998.73 5998.85 155.58 o 9 14 0 455.54 422.42 59.68 o 10 14 0 10802.81 10722.60 230.73 o 11 14 0 5614.51 5667.71 168.25 o 12 14 0 500.05 571.98 79.63 o 13 14 0 1121.94 796.58 99.32 o 1 15 0 487.37 628.13 53.79 o 2 15 0 6.25 -2.72 14.13 o 3 15 0 4011.32 3832.68 68.55 o 4 15 0 508.91 535.82 33.34 o 5 15 0 212.77 186.76 31.53 o 6 15 0 398.08 383.83 42.56 o 7 15 0 102.37 71.85 34.60 o 8 15 0 1919.85 1825.36 87.22 o 9 15 0 985.67 900.60 77.52 o 10 15 0 1152.69 1240.02 91.45 o 11 15 0 46.22 100.00 46.84 o 12 15 0 73.46 142.56 51.83 o 13 15 0 39.30 -0.63 50.86 o 0 16 0 63877.09 66297.72 852.59 o 1 16 0 12833.68 12823.83 192.85 o 2 16 0 19337.76 18923.73 215.92 o 3 16 0 1683.25 1623.38 49.54 o 4 16 0 31130.91 30899.75 310.35 o 5 16 0 17501.20 17400.60 222.04 o 6 16 0 10341.98 10005.16 168.12 o 7 16 0 448.01 478.06 51.21 o 8 16 0 6619.65 6652.93 155.61 o 9 16 0 3699.51 3611.92 121.27 o 10 16 0 1860.36 1583.63 92.52 o 11 16 0 2612.90 2747.35 114.38 o 12 16 0 1765.80 1815.52 99.38 o 13 16 0 1452.90 1395.44 111.91 o 1 17 0 641.69 678.68 35.41 o 2 17 0 878.90 867.39 43.67 o 3 17 0 2118.52 2047.57 57.48 o 4 17 0 7846.57 7466.20 123.06 o 5 17 0 537.59 516.49 44.79 o 6 17 0 304.23 337.97 42.56 o 7 17 0 1599.17 1494.05 80.18 o 8 17 0 194.49 173.29 45.91 o 9 17 0 730.85 769.95 70.48 o 10 17 0 2152.95 2082.42 103.07 o 11 17 0 511.46 584.73 65.11 o 12 17 0 1.76 68.29 44.76 o 0 18 0 6241.69 6963.29 180.37 o 1 18 0 42240.46 44798.34 419.37 o 2 18 0 112997.19 116705.38 951.02 o 3 18 0 56607.88 56627.80 491.08 o 4 18 0 3660.72 3337.00 89.22 o 5 18 0 1643.69 1621.54 71.99 o 6 18 0 4711.12 4772.20 121.63 o 7 18 0 67.93 140.01 54.90 o 8 18 0 12014.33 11888.24 223.58 o 9 18 0 10376.87 10308.92 210.87 o 10 18 0 56.92 40.40 40.90 o 11 18 0 92.04 -4.95 39.77 o 12 18 0 2653.07 2771.99 127.50 o 1 19 0 533.06 820.84 67.95 o 2 19 0 2037.22 2162.33 80.12 o 3 19 0 879.11 834.32 49.78 o 4 19 0 59.90 68.81 28.25 o 5 19 0 218.35 182.58 37.55 o 6 19 0 19.69 3.67 34.06 o 7 19 0 3766.99 3717.31 155.62 o 8 19 0 5741.94 5603.34 150.95 o 9 19 0 1361.28 1278.54 87.76 o 10 19 0 778.74 611.24 66.76 o 11 19 0 1669.58 1789.48 120.24 o 12 19 0 2129.20 2137.64 111.06 o 0 20 0 8289.40 9323.70 232.11 o 1 20 0 49.47 101.02 39.78 o 2 20 0 10701.24 10710.28 169.72 o 3 20 0 3730.04 3655.23 101.41 o 4 20 0 4792.62 4921.36 103.98 o 5 20 0 0.18 92.01 35.01 o 6 20 0 11657.65 11048.61 210.02 o 7 20 0 7488.54 7710.39 176.42 o 8 20 0 1528.75 1605.96 101.37 o 9 20 0 1.78 17.99 43.42 o 10 20 0 2794.49 2761.80 147.31 o 11 20 0 3373.43 3488.82 133.50 o 12 20 0 94.82 136.51 57.70 o 1 21 0 767.97 793.67 90.31 o 2 21 0 932.87 938.67 70.01 o 3 21 0 210.56 144.99 40.51 o 4 21 0 57.70 80.04 35.18 o 5 21 0 439.78 318.55 48.43 o 6 21 0 160.71 126.55 62.46 o 7 21 0 398.94 393.62 59.07 o 8 21 0 1512.81 1524.87 93.58 o 9 21 0 760.38 795.51 74.65 o 10 21 0 64.22 189.85 54.18 o 11 21 0 212.12 483.23 66.27 o 12 21 0 800.27 853.28 90.61 o 0 22 0 72423.59 75364.54 1079.17 o 1 22 0 12508.91 12670.49 369.52 o 2 22 0 45.03 112.22 43.06 o 3 22 0 18.82 85.42 37.62 o 4 22 0 11025.05 11068.63 217.79 o 5 22 0 149.95 234.54 48.39 o 6 22 0 17146.67 16297.54 274.98 o 7 22 0 12733.59 12623.66 388.56 o 8 22 0 307.45 377.88 60.53 o 9 22 0 930.81 977.33 103.49 o 10 22 0 7314.59 7376.30 188.06 o 11 22 0 5697.96 5838.05 197.49 o 1 23 0 672.68 678.20 65.44 o 2 23 0 496.79 311.22 55.37 o 3 23 0 424.86 495.84 66.27 o 4 23 0 360.10 168.37 51.52 o 5 23 0 858.17 799.45 79.08 o 6 23 0 2362.15 2218.66 117.40 o 7 23 0 460.84 490.34 71.81 o 8 23 0 1004.06 959.00 104.88 o 9 23 0 2345.81 2531.42 141.88 o 10 23 0 3612.50 3647.14 159.34 o 11 23 0 893.93 843.15 93.01 o 0 24 0 464.07 886.01 131.04 o 1 24 0 1662.08 1995.17 119.83 o 2 24 0 30199.80 31324.26 479.58 o 3 24 0 6989.53 6906.03 190.12 o 4 24 0 1207.12 1098.73 87.62 o 5 24 0 263.74 189.56 55.51 o 6 24 0 3812.28 3518.04 154.60 o 7 24 0 565.32 569.22 91.04 o 8 24 0 2032.68 1926.24 118.64 o 9 24 0 1554.31 1274.68 105.17 o 10 24 0 62.90 135.38 82.27 o 11 24 0 303.85 272.47 67.55 o 1 25 0 558.02 563.05 79.90 o 2 25 0 110.03 289.96 55.54 o 3 25 0 702.15 843.39 88.73 o 4 25 0 611.59 527.40 87.79 o 5 25 0 523.80 455.91 69.38 o 6 25 0 316.90 90.38 51.76 o 7 25 0 237.51 83.20 72.08 o 8 25 0 102.91 119.43 55.30 o 9 25 0 313.88 247.58 65.91 o 10 25 0 1099.37 1069.10 104.31 o 0 26 0 35.05 163.40 127.09 o 1 26 0 4605.97 4496.98 209.31 o 2 26 0 21235.64 21553.04 575.57 o 3 26 0 2434.42 2411.89 164.34 o 4 26 0 3831.84 3916.45 171.61 o 5 26 0 2999.71 3043.64 137.04 o 6 26 0 229.40 180.05 120.84 o 7 26 0 1550.62 1462.07 107.51 o 8 26 0 4967.91 4893.33 175.26 o 9 26 0 6282.58 6574.81 244.97 o 10 26 0 51.26 62.80 60.36 o 1 27 0 1230.56 1307.90 151.17 o 2 27 0 1322.28 1530.51 131.32 o 3 27 0 0.00 -56.04 49.13 o 4 27 0 42.59 43.50 62.69 o 5 27 0 38.12 52.40 54.81 o 6 27 0 83.32 52.11 53.46 o 7 27 0 414.82 373.39 69.01 o 8 27 0 2014.88 1983.09 159.87 o 9 27 0 1123.69 1091.87 102.46 o 10 27 0 376.44 569.00 102.99 o 0 28 0 42295.20 42161.44 1386.28 o 1 28 0 18396.75 18681.09 564.75 o 2 28 0 2957.26 2905.11 254.17 o 3 28 0 2241.99 2127.34 132.74 o 4 28 0 12276.53 12891.64 485.48 o 5 28 0 2942.50 2978.25 157.90 o 6 28 0 784.53 803.36 101.21 o 7 28 0 852.21 799.42 89.14 o 8 28 0 469.02 458.61 79.20 o 9 28 0 72.20 146.25 63.62 o 1 29 0 668.26 1243.73 156.80 o 2 29 0 257.95 247.34 128.38 o 3 29 0 7.65 76.31 62.10 o 4 29 0 81.35 31.64 56.00 o 5 29 0 198.02 69.66 59.20 o 6 29 0 117.91 89.71 58.56 o 7 29 0 11.76 -38.95 49.90 o 8 29 0 293.49 248.68 67.97 o 9 29 0 0.87 -6.36 55.80 o 0 30 0 17922.00 18998.07 820.87 o 1 30 0 5171.01 5567.04 288.78 o 2 30 0 592.05 379.69 142.65 o 3 30 0 1537.33 1648.53 148.33 o 4 30 0 3003.99 3166.92 194.57 o 5 30 0 826.27 932.06 107.44 o 6 30 0 1122.94 1213.18 181.75 o 7 30 0 1143.70 1264.79 109.89 o 8 30 0 143.22 102.32 63.19 o 9 30 0 2.30 89.69 71.86 o 1 31 0 167.82 253.38 134.87 o 2 31 0 3.03 -13.89 62.33 o 3 31 0 193.08 159.64 84.03 o 4 31 0 341.07 504.27 130.17 o 5 31 0 28.54 -34.51 61.70 o 6 31 0 617.08 682.09 124.29 o 7 31 0 88.31 120.99 84.79 o 8 31 0 1.11 60.35 59.57 o 0 32 0 7110.39 7280.21 483.71 o 1 32 0 5652.40 5589.86 294.72 o 2 32 0 13586.09 13204.63 748.90 o 3 32 0 7326.41 8174.04 298.25 o 4 32 0 119.06 272.90 84.00 o 5 32 0 40.64 2.83 73.11 o 6 32 0 84.13 -9.67 73.91 o 7 32 0 1.16 16.33 74.30 o 8 32 0 2329.60 2713.44 199.74 o 1 33 0 141.92 377.53 101.25 o 2 33 0 435.68 919.87 145.25 o 3 33 0 11.73 52.88 75.86 o 4 33 0 998.30 912.63 126.09 o 5 33 0 63.55 9.84 68.16 o 6 33 0 9.39 5.01 73.89 o 7 33 0 445.31 205.19 86.18 o 0 34 0 18.85 59.65 105.04 o 1 34 0 1370.25 1557.89 355.32 o 2 34 0 2552.40 2346.73 387.09 o 3 34 0 1911.50 1796.71 335.87 o 4 34 0 236.07 170.78 87.90 o 5 34 0 1.59 3.07 71.58 o 6 34 0 809.44 895.53 130.19 o 1 35 0 117.38 126.51 85.83 o 2 35 0 403.36 313.14 177.66 o 3 35 0 6.10 97.50 88.46 o 4 35 0 359.33 436.15 101.24 o 5 35 0 0.81 -40.61 69.32 o 6 35 0 218.01 267.06 97.47 o 0 36 0 6269.80 6945.64 488.89 o 1 36 0 4121.81 4144.47 283.78 o 2 36 0 266.26 166.00 93.97 o 3 36 0 299.89 393.31 115.78 o 4 36 0 92.71 191.01 86.79 o 5 36 0 168.86 190.41 99.29 o 1 37 0 11.19 93.48 173.77 o 2 37 0 4.27 -73.20 64.80 o 3 37 0 84.35 -64.89 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