#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217316_Fobs loop_ _publ_author_name 'Yohei, Sato' 'Kazuya, Uta' 'Mizuguchi, Jin' _publ_section_title ; Diacetonitriletetrakis{\m~2~-3-anilinocarbonyl-1-[(5-chloro-2-oxidophenyl)diazenyl]-2-naphtholato}tetraaquadiiron(III)disodium(I) dihydrate ; _journal_coeditor_code SJ2453 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m240 _journal_page_last m241 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.396 _cell_angle_beta 76.285 _cell_angle_gamma 83.015 _cell_length_a 11.4416 _cell_length_b 14.1161 _cell_length_c 15.0105 _exptl_crystal_F_000 1034.00 _reflns_d_resolution_high 0.8301 _[local]_cod_data_source_file sj2453Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' T77_Na_acetonitril_new3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 336.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 70.33 89.39 7.25 o 3 0 0 43.85 94.29 14.21 o 4 0 0 2569.11 2142.75 55.17 o 5 0 0 0.56 -8.72 14.44 o 6 0 0 298.23 281.33 24.74 o 7 0 0 150.53 173.64 26.60 o 8 0 0 1868.09 2171.16 77.21 o 9 0 0 317.28 441.47 115.00 o 10 0 0 9.64 -7.30 22.90 o 11 0 0 11.75 -6.00 21.37 o 12 0 0 55.36 37.03 31.46 o 13 0 0 2.87 14.77 30.38 o -13 1 0 21.77 19.30 48.33 o -12 1 0 170.10 108.24 56.18 o -11 1 0 473.94 712.88 114.51 o -10 1 0 145.85 152.31 51.83 o -9 1 0 346.93 381.34 49.36 o -8 1 0 151.98 176.66 34.93 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385.57 452.30 98.07 o -7 8 0 0.05 30.25 45.54 o -6 8 0 382.76 531.76 80.66 o -5 8 0 2.63 -2.36 10.50 o -4 8 0 1399.19 1596.79 62.78 o -3 8 0 638.56 725.81 43.48 o -2 8 0 1100.60 1138.40 54.76 o -1 8 0 2950.07 3051.61 81.44 o 0 8 0 128.55 118.78 23.83 o 1 8 0 491.34 558.80 31.28 o 2 8 0 1271.14 1495.32 45.19 o 3 8 0 1946.05 2017.45 73.16 o 4 8 0 365.60 332.50 24.98 o 5 8 0 83.25 77.06 15.40 o 6 8 0 67.91 73.76 20.46 o 7 8 0 133.04 144.67 28.22 o 8 8 0 156.88 126.49 31.35 o 9 8 0 177.55 139.90 49.67 o 10 8 0 8.10 6.34 17.49 o 11 8 0 8.47 23.49 28.74 o -10 9 0 3.76 42.71 73.21 o -9 9 0 1.11 53.38 60.98 o -8 9 0 1871.63 2155.30 236.44 o -7 9 0 890.93 1199.56 163.93 o -6 9 0 21.84 73.74 70.83 o -5 9 0 125.75 114.78 33.67 o -4 9 0 399.46 363.69 68.55 o -3 9 0 4.69 16.32 21.69 o -2 9 0 169.99 195.78 32.30 o -1 9 0 194.23 265.48 32.83 o 0 9 0 433.56 462.30 36.89 o 1 9 0 105.24 95.55 30.79 o 2 9 0 24.78 44.70 18.43 o 3 9 0 195.77 199.58 26.58 o 4 9 0 127.44 144.47 32.99 o 5 9 0 14.87 12.36 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