#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:46:22 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181093 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217320.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217320_Fobs loop_ _publ_author_name 'Yang, Junli' 'Li, Chengjuan' 'Li, Dacheng' 'Wang, Daqi' _publ_section_title ; catena-Poly[[nickel(II)-\m~3~-1,1-dicyanoethene-2,2-dithiolato-\k^4^S,S':N:N'-bis[(15-crown-5)magnesium(II)]-\m~3~-1,1-dicyanoethene-2,2-dithiolato-\k^4^N:N':S,S'] dichloride] ; _journal_coeditor_code SQ2001 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m174 _journal_volume 64 _journal_year 2008 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.6227 _cell_length_b 20.5907 _cell_length_c 15.1477 _exptl_crystal_F_000 1864.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file sq2001Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 070319b in Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 367.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11191.97 8480.37 153.73 o 6 0 0 49813.00 64373.88 1065.93 o 8 0 0 50068.50 51706.21 869.13 o 10 0 0 14503.95 13932.91 264.85 o 12 0 0 27.17 70.81 37.12 o 14 0 0 1270.30 1694.16 90.49 o 16 0 0 2253.09 2357.61 389.68 o 5 1 0 2300.31 1739.20 32.06 o 7 1 0 5714.14 4270.04 67.44 o 9 1 0 3547.48 2898.76 56.35 o 13 1 0 40.91 -13.56 24.31 o 15 1 0 735.02 633.87 55.81 o 6 2 0 25.62 73.15 11.43 o 8 2 0 36.19 -19.96 13.31 o 10 2 0 0.13 -17.23 15.93 o 12 2 0 260.84 143.59 25.83 o 14 2 0 0.05 -35.47 23.64 o 16 2 0 0.03 -8.61 37.48 o 3 3 0 4203.05 5846.02 83.30 o 5 3 0 5005.24 5523.58 74.98 o 7 3 0 5034.73 4263.70 74.58 o 9 3 0 8946.96 8562.38 135.16 o 11 3 0 619.19 850.00 37.61 o 13 3 0 1.71 -25.40 21.27 o 15 3 0 752.20 780.72 65.99 o 0 4 0 56863.02 65527.11 1081.73 o 2 4 0 15329.50 15306.26 229.74 o 4 4 0 9153.98 10737.36 147.90 o 6 4 0 27858.46 33015.11 381.06 o 8 4 0 284.54 375.59 24.47 o 10 4 0 844.56 794.34 35.46 o 14 4 0 507.22 602.49 77.89 o 3 5 0 44457.80 42580.35 544.47 o 5 5 0 14594.65 13478.43 185.30 o 7 5 0 4027.76 4273.16 66.80 o 9 5 0 516.69 510.55 28.99 o 13 5 0 554.91 481.86 44.23 o 15 5 0 68.64 3.99 29.85 o 0 6 0 80602.88 73442.19 1203.58 o 6 6 0 744.11 824.70 30.26 o 8 6 0 977.23 1035.06 30.14 o 10 6 0 183.47 236.61 25.10 o 12 6 0 102.07 180.28 33.11 o 14 6 0 120.82 61.23 33.65 o 1 7 0 540.98 355.52 14.82 o 3 7 0 5516.74 4971.76 78.37 o 5 7 0 17257.36 19403.86 301.43 o 7 7 0 4.27 17.68 11.51 o 11 7 0 3016.04 3057.33 85.03 o 13 7 0 1428.51 1617.38 67.25 o 15 7 0 122.35 24.78 40.91 o 2 8 0 90.66 202.01 13.75 o 4 8 0 16563.31 17225.25 269.48 o 6 8 0 882.47 1007.84 41.90 o 8 8 0 4780.76 4256.38 80.86 o 10 8 0 794.12 784.16 37.51 o 12 8 0 3150.91 2589.19 81.50 o 14 8 0 196.97 136.39 57.82 o 3 9 0 6533.59 5217.23 85.15 o 5 9 0 476.87 455.90 41.36 o 7 9 0 3297.73 3128.20 76.68 o 9 9 0 72.35 9.55 18.14 o 11 9 0 882.02 1181.08 55.84 o 13 9 0 42.41 125.46 34.83 o 15 9 0 0.37 -39.93 26.62 o 0 10 0 32.27 113.24 23.19 o 2 10 0 0.90 13.27 11.74 o 4 10 0 421.07 309.57 40.73 o 6 10 0 4068.58 3188.05 76.38 o 8 10 0 441.52 322.79 32.40 o 10 10 0 1008.23 1342.86 47.73 o 12 10 0 10.55 54.48 32.88 o 14 10 0 27.31 0.12 31.14 o 1 11 0 154.34 136.25 15.04 o 3 11 0 1223.81 1317.50 35.79 o 5 11 0 8813.28 8683.02 155.99 o 7 11 0 376.19 348.16 31.68 o 9 11 0 1451.41 1584.89 50.55 o 11 11 0 970.90 864.66 43.70 o 13 11 0 734.52 788.02 56.91 o 0 12 0 6034.67 5316.41 147.52 o 2 12 0 2052.94 2169.72 47.89 o 4 12 0 3527.27 3087.27 73.72 o 6 12 0 2410.54 2202.91 63.97 o 8 12 0 35.17 73.41 25.54 o 10 12 0 901.85 696.35 42.99 o 12 12 0 1377.58 1447.21 60.60 o 14 12 0 227.62 206.03 41.23 o 1 13 0 21.47 15.65 16.40 o 3 13 0 1262.85 1528.51 48.33 o 5 13 0 1668.93 1615.13 53.47 o 7 13 0 1.52 32.99 23.56 o 9 13 0 205.18 143.77 32.59 o 11 13 0 212.86 272.54 34.91 o 13 13 0 11.24 -34.40 29.04 o 0 14 0 5.08 19.81 30.03 o 2 14 0 1649.92 1463.88 40.66 o 4 14 0 211.12 276.93 28.57 o 6 14 0 8.12 15.68 21.57 o 10 14 0 84.25 41.83 27.17 o 12 14 0 221.50 151.73 31.09 o 1 15 0 7687.60 7684.30 146.30 o 3 15 0 776.05 666.18 36.83 o 5 15 0 1295.64 1231.60 49.44 o 7 15 0 4468.42 4236.08 103.16 o 9 15 0 1200.22 1047.04 54.95 o 11 15 0 22.46 -26.77 25.14 o 0 16 0 4978.70 4685.75 146.51 o 2 16 0 824.37 847.95 54.39 o 4 16 0 1399.16 1581.81 54.80 o 6 16 0 206.93 198.70 31.27 o 8 16 0 2973.00 3266.54 92.56 o 10 16 0 247.31 213.54 38.61 o 12 16 0 159.53 58.55 31.96 o 1 17 0 2407.36 2389.94 83.86 o 3 17 0 93.31 31.26 28.19 o 5 17 0 2043.45 2057.45 65.71 o 7 17 0 1192.11 1362.79 58.58 o 9 17 0 131.30 156.13 35.62 o 11 17 0 91.34 52.68 30.99 o 0 18 0 3488.31 4405.13 222.09 o 2 18 0 44.11 60.88 30.86 o 4 18 0 0.46 -35.89 23.93 o 6 18 0 150.61 90.23 36.52 o 8 18 0 487.33 471.64 56.51 o 10 18 0 159.66 325.52 43.07 o 1 19 0 4244.19 3978.82 118.38 o 3 19 0 543.23 620.22 73.37 o 5 19 0 17.85 -14.06 29.92 o 7 19 0 1481.39 1380.01 74.18 o 9 19 0 537.55 725.09 66.47 o 0 20 0 668.65 830.46 113.90 o 2 20 0 1084.06 1294.52 76.53 o 4 20 0 187.81 168.71 40.31 o 6 20 0 95.69 81.68 39.24 o 8 20 0 673.73 657.56 64.49 o 1 21 0 97.13 73.13 45.09 o 3 21 0 222.11 132.26 38.96 o 5 21 0 0.15 -45.84 32.06 o 7 21 0 13.39 -35.86 34.06 o 0 22 0 33.38 41.29 64.62 o 2 22 0 16.31 2.38 42.06 o 4 22 0 487.33 513.34 57.75 o 6 22 0 74.19 91.40 59.16 o 1 23 0 20.53 -57.57 38.38 o 3 23 0 226.37 316.48 65.52 o 5 23 0 583.38 674.44 66.04 o 0 24 0 64.68 54.99 77.35 o 2 24 0 133.08 139.84 57.86 o 5 1 1 1535.94 1569.47 22.35 o 7 1 1 6358.13 6572.84 83.21 o 9 1 1 3921.98 3646.43 48.27 o 11 1 1 155.23 232.49 17.85 o 13 1 1 214.55 262.48 22.80 o 15 1 1 1076.87 1171.67 48.58 o 0 2 1 22416.25 20582.82 345.77 o 4 2 1 9270.86 10726.05 93.14 o 6 2 1 575.76 568.76 15.12 o 8 2 1 9540.70 8893.85 91.55 o 12 2 1 1167.45 611.06 28.29 o 14 2 1 402.35 387.24 31.43 o 16 2 1 884.32 963.47 73.21 o 3 3 1 9537.08 8405.45 109.10 o 5 3 1 3184.82 4257.41 65.43 o 7 3 1 5847.07 5636.77 61.83 o 9 3 1 4103.22 3881.63 50.40 o 13 3 1 28.87 -23.42 15.62 o 15 3 1 518.17 598.47 67.88 o 0 4 1 45452.45 35408.37 460.49 o 4 4 1 26661.59 21827.24 215.16 o 6 4 1 5150.59 4276.92 43.50 o 8 4 1 94.97 82.55 10.88 o 10 4 1 751.46 911.45 25.96 o 12 4 1 684.39 592.93 29.29 o 14 4 1 195.49 399.23 33.22 o 1 5 1 45259.77 47987.43 463.63 o 3 5 1 1104.83 1143.15 19.53 o 5 5 1 1852.90 1821.38 46.19 o 7 5 1 889.10 1383.94 24.81 o 9 5 1 1182.87 1174.37 29.52 o 11 5 1 1284.28 1173.64 33.43 o 13 5 1 118.00 82.07 22.52 o 15 5 1 80.86 20.89 26.26 o 0 6 1 14107.34 11815.73 255.90 o 2 6 1 7249.99 6937.71 70.54 o 4 6 1 57981.43 63473.88 606.96 o 6 6 1 7474.66 6470.13 71.88 o 8 6 1 506.17 493.20 36.41 o 10 6 1 3974.00 4016.95 61.73 o 12 6 1 3130.63 3391.66 65.07 o 14 6 1 778.21 715.10 38.13 o 1 7 1 5642.83 5833.16 61.41 o 3 7 1 24947.02 21274.41 211.74 o 5 7 1 8771.51 7455.01 85.35 o 7 7 1 317.56 177.57 13.06 o 9 7 1 384.76 348.75 17.85 o 11 7 1 2075.14 1691.52 45.40 o 13 7 1 1149.90 1240.54 41.49 o 15 7 1 12.69 2.24 26.35 o 0 8 1 120.74 81.03 10.60 o 2 8 1 4915.59 4477.19 47.56 o 4 8 1 4190.23 4176.65 53.04 o 6 8 1 6.09 -13.01 8.68 o 8 8 1 1028.66 985.69 25.42 o 10 8 1 557.45 437.49 24.75 o 14 8 1 9.04 -28.58 19.05 o 1 9 1 7344.95 7244.85 122.16 o 3 9 1 28136.15 30402.15 288.04 o 5 9 1 22125.85 23522.46 238.37 o 9 9 1 356.04 370.21 20.78 o 11 9 1 4248.32 4465.01 70.82 o 13 9 1 2445.80 2705.11 61.74 o 15 9 1 13.48 -37.14 24.76 o 0 10 1 2875.18 3028.11 90.10 o 2 10 1 6988.80 6065.50 87.50 o 4 10 1 32490.88 32318.15 324.50 o 6 10 1 4337.33 3657.32 59.06 o 8 10 1 1724.24 1670.95 36.87 o 10 10 1 1342.34 1392.33 34.42 o 12 10 1 2671.34 2778.37 61.18 o 14 10 1 312.43 236.01 31.04 o 1 11 1 2661.27 2495.79 34.68 o 3 11 1 2183.71 1846.11 30.44 o 5 11 1 1538.52 1532.62 35.57 o 7 11 1 272.56 375.03 23.20 o 9 11 1 986.75 1028.68 33.04 o 11 11 1 767.20 668.63 31.27 o 13 11 1 46.34 57.00 22.95 o 0 12 1 17659.91 17902.62 249.23 o 2 12 1 1032.60 838.00 22.17 o 4 12 1 1745.16 1840.28 38.43 o 6 12 1 683.82 666.66 27.27 o 8 12 1 803.57 863.61 31.93 o 10 12 1 1147.58 1201.69 33.97 o 12 12 1 138.90 164.81 22.00 o 14 12 1 25.34 3.97 26.31 o 1 13 1 1919.31 1699.92 39.87 o 3 13 1 2834.21 2870.50 49.03 o 5 13 1 339.82 468.64 24.35 o 7 13 1 931.13 830.30 30.53 o 9 13 1 915.54 940.55 37.47 o 11 13 1 302.26 325.48 25.15 o 13 13 1 106.75 52.92 23.33 o 0 14 1 6404.11 6537.00 107.03 o 2 14 1 2781.34 2625.02 43.45 o 4 14 1 1061.17 1169.80 44.59 o 6 14 1 1973.91 1954.55 57.95 o 8 14 1 2453.04 2472.13 53.95 o 10 14 1 648.50 769.73 37.56 o 12 14 1 30.91 49.98 20.61 o 1 15 1 285.26 358.49 30.17 o 3 15 1 701.55 820.07 41.43 o 5 15 1 270.73 255.07 25.66 o 7 15 1 126.88 167.91 21.73 o 9 15 1 128.00 91.23 22.94 o 11 15 1 82.02 40.17 20.99 o 0 16 1 5035.24 5611.21 117.99 o 2 16 1 66.10 16.56 15.80 o 4 16 1 570.30 404.65 27.13 o 6 16 1 632.16 602.10 33.49 o 8 16 1 646.48 895.40 42.16 o 10 16 1 57.81 44.00 23.43 o 12 16 1 143.40 126.59 25.35 o 1 17 1 3761.77 3739.81 77.16 o 3 17 1 194.40 204.13 25.52 o 5 17 1 218.99 256.79 34.31 o 7 17 1 1673.68 1771.03 50.93 o 9 17 1 1263.92 1343.98 51.95 o 11 17 1 52.88 12.42 22.19 o 0 18 1 3282.99 3762.83 142.81 o 2 18 1 976.03 1025.81 40.78 o 4 18 1 97.62 30.25 21.36 o 6 18 1 176.01 137.30 31.56 o 8 18 1 1980.17 2020.36 57.01 o 10 18 1 314.10 336.65 33.96 o 1 19 1 339.68 313.29 34.41 o 3 19 1 114.88 95.56 24.59 o 5 19 1 16.35 -18.59 20.99 o 7 19 1 166.69 155.62 26.68 o 9 19 1 63.48 99.42 26.66 o 0 20 1 575.74 474.80 65.19 o 2 20 1 75.02 80.27 24.97 o 4 20 1 60.24 37.48 24.09 o 6 20 1 55.63 50.41 25.89 o 8 20 1 89.19 68.98 25.21 o 1 21 1 801.63 880.83 59.31 o 3 21 1 38.07 20.86 22.50 o 5 21 1 218.50 154.01 30.08 o 7 21 1 213.77 197.27 33.39 o 0 22 1 6.95 -43.11 37.58 o 2 22 1 251.10 179.94 38.51 o 4 22 1 357.08 353.99 35.94 o 6 22 1 154.15 144.70 32.96 o 1 23 1 229.85 265.74 43.02 o 3 23 1 58.44 35.81 33.44 o 5 23 1 66.68 58.97 29.18 o 0 24 1 88.43 75.17 51.42 o 2 24 1 6.69 -28.22 31.49 o 4 0 2 23119.64 29824.44 437.74 o 6 0 2 11376.05 12787.68 202.65 o 8 0 2 15047.18 17506.11 243.17 o 10 0 2 487.29 352.39 29.73 o 12 0 2 1285.94 1388.22 54.48 o 14 0 2 301.51 239.16 43.66 o 16 0 2 1210.20 1625.04 115.52 o 1 1 2 26006.46 20182.21 294.99 o 3 1 2 12647.21 17579.28 169.51 o 5 1 2 4855.48 4078.81 65.00 o 7 1 2 11929.21 10125.65 111.15 o 9 1 2 5646.47 5930.96 75.90 o 13 1 2 310.93 262.31 29.04 o 15 1 2 874.70 1045.25 55.64 o 4 2 2 7600.55 9437.88 96.67 o 6 2 2 2504.19 1700.23 27.45 o 8 2 2 10317.98 9537.08 108.04 o 10 2 2 641.59 587.48 24.28 o 12 2 2 383.08 376.81 27.69 o 14 2 2 19.28 45.76 24.26 o 16 2 2 249.43 299.66 51.26 o 3 3 2 19395.75 23022.47 233.06 o 5 3 2 876.99 838.47 17.22 o 7 3 2 8324.04 8552.52 92.19 o 9 3 2 2388.72 2672.28 42.36 o 11 3 2 724.29 1045.51 32.64 o 13 3 2 64.45 12.34 19.20 o 15 3 2 542.89 580.44 50.60 o 0 4 2 95698.50 105617.91 1730.05 o 2 4 2 28403.08 31463.75 302.75 o 4 4 2 12742.50 12736.38 122.69 o 6 4 2 4819.24 5816.97 63.05 o 8 4 2 2351.58 2741.35 41.12 o 10 4 2 4347.61 3540.83 56.09 o 12 4 2 859.83 901.37 36.83 o 14 4 2 611.80 596.93 47.06 o 1 5 2 5832.57 4492.75 56.54 o 3 5 2 13102.56 13743.16 155.83 o 5 5 2 725.74 705.19 15.53 o 7 5 2 1907.37 2590.06 69.21 o 9 5 2 3609.88 4094.27 76.12 o 13 5 2 254.57 306.95 32.55 o 15 5 2 293.84 219.06 36.52 o 0 6 2 40135.34 39319.41 653.66 o 2 6 2 1436.81 1155.27 18.99 o 4 6 2 6696.61 7863.02 92.99 o 6 6 2 394.67 393.85 16.28 o 8 6 2 4600.73 4402.64 56.88 o 10 6 2 201.45 279.06 20.53 o 12 6 2 430.26 471.15 33.53 o 14 6 2 18.19 44.15 29.96 o 1 7 2 866.83 559.46 36.66 o 3 7 2 8502.59 9275.24 98.39 o 5 7 2 7946.29 6956.74 81.16 o 7 7 2 123.18 88.99 11.57 o 9 7 2 317.48 478.69 22.10 o 11 7 2 2823.75 3023.28 59.79 o 13 7 2 923.79 1056.19 47.46 o 15 7 2 48.97 -22.39 27.83 o 0 8 2 1639.04 2264.45 103.38 o 2 8 2 5596.23 5765.78 84.69 o 4 8 2 24394.76 26582.61 262.36 o 6 8 2 2399.21 2884.93 91.63 o 8 8 2 606.67 711.04 25.45 o 10 8 2 2520.00 2292.42 45.52 o 12 8 2 2662.03 2303.75 58.22 o 14 8 2 298.42 417.56 41.05 o 1 9 2 1401.31 1314.82 29.18 o 3 9 2 13138.41 15518.41 171.21 o 5 9 2 8916.75 10438.54 113.68 o 9 9 2 688.03 683.81 25.70 o 11 9 2 932.83 1145.87 37.42 o 13 9 2 333.15 407.02 38.05 o 0 10 2 3670.81 3550.66 62.63 o 2 10 2 120.85 138.57 9.25 o 4 10 2 3151.06 3961.22 56.47 o 6 10 2 888.46 858.90 30.00 o 8 10 2 596.90 664.90 25.82 o 10 10 2 818.73 938.52 31.11 o 12 10 2 431.94 413.11 33.08 o 14 10 2 12.49 -9.61 26.29 o 1 11 2 519.00 792.04 18.48 o 3 11 2 11813.06 12602.06 135.92 o 5 11 2 7443.00 7846.83 110.92 o 7 11 2 1475.27 1306.95 38.03 o 9 11 2 16.47 -20.99 13.99 o 11 11 2 1780.73 1725.14 42.53 o 13 11 2 698.40 725.59 46.42 o 0 12 2 3513.56 3233.46 83.53 o 2 12 2 319.93 296.23 25.04 o 4 12 2 3367.02 3699.97 58.00 o 6 12 2 1414.69 1635.29 42.23 o 8 12 2 5.25 -19.43 16.60 o 10 12 2 216.79 237.71 24.25 o 12 12 2 541.33 587.43 36.93 o 14 12 2 136.09 98.13 34.62 o 1 13 2 6790.69 6705.95 76.45 o 3 13 2 1389.69 1542.83 34.62 o 5 13 2 760.58 845.18 32.65 o 7 13 2 3003.64 2911.44 60.87 o 9 13 2 1219.19 1313.95 40.68 o 11 13 2 237.48 220.83 25.12 o 13 13 2 33.39 6.32 23.12 o 0 14 2 1537.17 1297.79 38.18 o 2 14 2 36.77 -16.26 11.75 o 4 14 2 1642.02 1648.65 41.52 o 6 14 2 816.36 870.13 34.14 o 8 14 2 523.86 468.39 32.00 o 10 14 2 107.48 181.39 32.79 o 12 14 2 420.15 352.04 31.42 o 1 15 2 4565.08 4393.88 62.87 o 3 15 2 116.21 44.28 16.68 o 5 15 2 96.13 51.67 17.94 o 7 15 2 1548.19 1548.82 55.95 o 9 15 2 1294.70 1321.97 46.27 o 11 15 2 42.92 37.23 21.26 o 0 16 2 13846.54 14147.45 286.20 o 2 16 2 1869.48 1623.44 41.49 o 4 16 2 640.35 659.57 50.98 o 6 16 2 2739.06 2916.29 65.26 o 8 16 2 3095.78 3378.79 72.39 o 10 16 2 716.27 674.55 44.49 o 12 16 2 105.52 84.87 26.68 o 1 17 2 412.09 503.10 32.73 o 3 17 2 6.25 -3.55 18.77 o 5 17 2 130.25 133.71 22.53 o 7 17 2 325.99 388.72 31.42 o 9 17 2 72.79 33.36 23.68 o 11 17 2 4.42 -36.80 24.53 o 0 18 2 2002.12 1871.77 75.18 o 2 18 2 68.99 30.60 21.37 o 4 18 2 900.25 817.21 39.99 o 6 18 2 214.29 237.61 27.22 o 8 18 2 310.64 339.28 36.58 o 10 18 2 59.87 41.65 26.55 o 1 19 2 1723.37 1668.63 58.11 o 3 19 2 579.60 557.28 50.49 o 5 19 2 337.79 332.62 32.38 o 7 19 2 1024.69 1021.60 43.21 o 9 19 2 647.30 704.94 43.09 o 0 20 2 452.32 649.22 72.19 o 2 20 2 494.84 569.65 42.54 o 4 20 2 99.58 63.97 25.25 o 8 20 2 474.76 572.42 39.98 o 1 21 2 333.99 480.58 47.67 o 3 21 2 514.05 460.15 37.22 o 5 21 2 181.47 100.62 35.58 o 7 21 2 227.04 228.20 35.37 o 0 22 2 309.42 231.33 57.35 o 2 22 2 102.68 79.83 35.70 o 4 22 2 527.13 716.41 45.36 o 6 22 2 45.50 23.45 26.06 o 1 23 2 36.45 32.80 31.69 o 3 23 2 230.56 244.29 43.15 o 5 23 2 499.36 477.90 46.73 o 0 24 2 0.76 -63.16 42.11 o 2 24 2 200.90 186.93 41.35 o 5 1 3 8175.43 9547.97 108.81 o 7 1 3 6834.14 8199.17 118.89 o 9 1 3 5347.29 4442.14 66.03 o 11 1 3 1279.31 1019.82 31.61 o 15 1 3 547.26 507.81 47.47 o 0 2 3 134812.48 160151.17 2113.53 o 4 2 3 11002.07 12536.19 146.17 o 6 2 3 24405.36 25110.06 267.25 o 8 2 3 9975.29 9482.01 115.31 o 10 2 3 3685.33 4512.75 69.15 o 12 2 3 91.28 48.55 20.04 o 14 2 3 912.86 1116.26 59.40 o 1 3 3 99431.38 102773.82 1088.44 o 3 3 3 12453.69 11315.45 120.16 o 5 3 3 4709.37 4308.77 62.49 o 9 3 3 962.72 901.03 27.88 o 11 3 3 1498.90 1700.48 44.31 o 13 3 3 646.87 477.40 35.20 o 15 3 3 210.96 225.25 46.77 o 0 4 3 73174.59 81891.88 1341.13 o 2 4 3 4257.66 3445.59 45.39 o 4 4 3 29716.84 34689.81 349.83 o 6 4 3 409.53 466.84 16.28 o 8 4 3 6415.97 5228.79 72.17 o 10 4 3 15.15 16.30 15.74 o 12 4 3 2014.06 1860.55 48.44 o 14 4 3 37.54 23.41 26.66 o 1 5 3 2385.17 3160.95 42.70 o 3 5 3 7171.15 7497.83 85.35 o 5 5 3 12581.40 13257.57 136.11 o 7 5 3 3212.06 3224.72 45.36 o 9 5 3 1063.84 1218.31 34.38 o 11 5 3 1620.94 1492.67 42.63 o 13 5 3 591.42 609.31 44.07 o 15 5 3 299.63 216.07 41.05 o 0 6 3 2213.33 1986.80 189.18 o 2 6 3 187.58 402.75 36.20 o 4 6 3 9011.07 7978.07 95.04 o 6 6 3 1568.03 1621.72 27.31 o 10 6 3 1169.74 1505.11 40.31 o 12 6 3 485.67 538.59 38.26 o 14 6 3 93.29 113.01 32.16 o 1 7 3 73.40 96.01 8.27 o 3 7 3 16011.16 16796.01 178.90 o 5 7 3 23807.09 23720.50 248.18 o 7 7 3 1354.82 1422.44 29.82 o 9 7 3 296.89 302.11 21.26 o 11 7 3 2231.69 2429.95 61.72 o 13 7 3 1445.86 1304.18 54.80 o 15 7 3 50.70 15.62 34.09 o 0 8 3 3940.36 4636.20 95.30 o 2 8 3 1968.81 1954.67 29.41 o 4 8 3 7418.15 7081.61 80.60 o 6 8 3 540.74 498.48 19.65 o 8 8 3 248.16 254.38 19.68 o 10 8 3 1201.76 1006.40 33.30 o 12 8 3 260.86 317.97 35.02 o 14 8 3 41.28 2.63 27.19 o 1 9 3 2080.73 2282.56 38.61 o 3 9 3 1821.64 2488.80 82.01 o 5 9 3 1560.79 1730.12 30.37 o 7 9 3 1427.09 1273.01 32.60 o 9 9 3 1409.90 1210.32 38.44 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