#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217330.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217330_Fobs loop_ _publ_author_name 'Aghabozorg, Hossein' 'Motyeian, Elham' 'Soleimannejad, Janet' 'Ghadermazi, Mohammad' 'Attar Gharamaleki, Jafar' _publ_section_title ; Aqua(4-hydroxypyridine-2,6-dicarboxylato)(1,10-phenanothroline)copper(II) 4.5-hydrate ; _journal_coeditor_code SU2032 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m252 _journal_page_last m253 _journal_volume 64 _journal_year 2008 _space_group_IT_number 43 _symmetry_space_group_name_Hall 'F 2 -2d' _symmetry_space_group_name_H-M 'F d d 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.68600 _cell_length_b 44.0330 _cell_length_c 10.3812 _exptl_crystal_F_000 4336.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file su2032Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' fdd2 Fdd2 R = 0.03 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1016.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz x,y,z -x,-y,z 1/4-x,1/4+y,1/4+z 3/4+x,3/4-y,1/4+z x,1/2+y,1/2+z -x,1/2-y,1/2+z 1/4-x,3/4+y,3/4+z 3/4+x,1/4-y,3/4+z 1/2+x,y,1/2+z 1/2-x,-y,1/2+z 3/4-x,1/4+y,3/4+z 1/4+x,3/4-y,3/4+z 1/2+x,1/2+y,z 1/2-x,1/2-y,z 3/4-x,3/4+y,1/4+z 1/4+x,1/4-y,1/4+z loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status _refln_sint/lambda 4 0 0 5533.27 5533.27 74.39 o 0.10703 8 0 0 108030.01 108030.01 328.68 o 0.21406 12 0 0 58536.30 58536.30 241.94 o 0.32110 16 0 0 43119.19 43119.19 207.65 o 0.42813 20 0 0 404.15 404.15 20.10 o 0.53516 24 0 0 1692.06 1692.06 41.13 o 0.64219 2 2 0 260162.28 260162.28 510.06 o 0.05814 4 2 0 17408.27 17408.27 131.94 o 0.10941 6 2 0 404.36 404.36 20.11 o 0.16215 8 2 0 1050.55 1050.55 32.41 o 0.21527 10 2 0 9358.81 9358.81 96.74 o 0.26854 12 2 0 8039.19 8039.19 89.66 o 0.32190 14 2 0 30220.59 30220.59 173.84 o 0.37530 16 2 0 16882.65 16882.65 129.93 o 0.42873 18 2 0 9054.00 9054.00 95.15 o 0.48218 20 2 0 184.43 184.43 13.58 o 0.53564 22 2 0 5206.93 5206.93 72.16 o 0.58911 24 2 0 4531.02 4531.02 67.31 o 0.64259 0 4 0 59273.00 59273.00 243.46 o 0.04542 2 4 0 14865.17 14865.17 121.92 o 0.07019 4 4 0 30993.04 30993.04 176.05 o 0.11627 6 4 0 71219.39 71219.39 266.87 o 0.16685 8 4 0 7396.56 7396.56 86.00 o 0.21883 10 4 0 47770.58 47770.58 218.56 o 0.27141 12 4 0 20801.04 20801.04 144.23 o 0.32429 14 4 0 40695.49 40695.49 201.73 o 0.37736 16 4 0 1373.79 1373.79 37.06 o 0.43053 18 4 0 13329.71 13329.71 115.45 o 0.48378 20 4 0 30.36 30.36 5.51 o 0.53708 22 4 0 28877.62 28877.62 169.93 o 0.59043 24 4 0 229.89 229.89 15.16 o 0.64380 2 6 0 3364.38 3364.38 58.00 o 0.08664 4 6 0 311380.25 311380.25 558.01 o 0.12688 6 6 0 162871.25 162871.25 403.57 o 0.17441 8 6 0 56430.06 56430.06 237.55 o 0.22464 10 6 0 32579.37 32579.37 180.50 o 0.27612 12 6 0 25236.55 25236.55 158.86 o 0.32824 14 6 0 12793.13 12793.13 113.11 o 0.38076 16 6 0 10985.74 10985.74 104.81 o 0.43352 18 6 0 3024.59 3024.59 55.00 o 0.48644 20 6 0 19304.95 19304.95 138.94 o 0.53948 22 6 0 43.28 43.28 6.58 o 0.59261 24 6 0 12168.36 12168.36 110.31 o 0.64580 0 8 0 17393.03 17393.03 131.88 o 0.09084 2 8 0 14379.62 14379.62 119.92 o 0.10543 4 8 0 1032388.25 1032388.25 1016.07 o 0.14038 6 8 0 56961.80 56961.80 238.67 o 0.18447 8 8 0 149200.09 149200.09 386.26 o 0.23254 10 8 0 18451.41 18451.41 135.84 o 0.28258 12 8 0 35236.30 35236.30 187.71 o 0.33370 14 8 0 266.96 266.96 16.34 o 0.38547 16 8 0 7491.03 7491.03 86.55 o 0.43766 18 8 0 628.26 628.26 25.07 o 0.49014 20 8 0 1122.50 1122.50 33.50 o 0.54282 22 8 0 9624.12 9624.12 98.10 o 0.59564 24 8 0 518.71 518.71 22.78 o 0.64859 2 10 0 240731.55 240731.55 490.64 o 0.12553 4 10 0 174024.66 174024.66 417.16 o 0.15604 6 10 0 196931.84 196931.84 443.77 o 0.19665 8 10 0 17262.86 17262.86 131.39 o 0.24232 10 10 0 62984.20 62984.20 250.97 o 0.29068 12 10 0 192.09 192.09 13.86 o 0.34058 14 10 0 44249.57 44249.57 210.36 o 0.39144 16 10 0 12610.01 12610.01 112.29 o 0.44293 18 10 0 21689.83 21689.83 147.27 o 0.49485 20 10 0 1318.62 1318.62 36.31 o 0.54707 22 10 0 3291.21 3291.21 57.37 o 0.59953 24 10 0 984.92 984.92 31.38 o 0.65215 0 12 0 4794.75 4794.75 69.24 o 0.13626 2 12 0 940.30 940.30 30.66 o 0.14639 4 12 0 865706.75 865706.75 930.43 o 0.17327 6 12 0 701.31 701.31 26.48 o 0.21058 8 12 0 670.42 670.42 25.89 o 0.25375 10 12 0 13314.89 13314.89 115.39 o 0.30028 12 12 0 38285.57 38285.57 195.67 o 0.34881 14 12 0 69804.45 69804.45 264.21 o 0.39862 16 12 0 984.35 984.35 31.37 o 0.44929 18 12 0 38123.52 38123.52 195.25 o 0.50055 20 12 0 1058.32 1058.32 32.53 o 0.55223 22 12 0 1228.57 1228.57 35.05 o 0.60424 24 12 0 1880.71 1880.71 43.37 o 0.65649 2 14 0 20396.63 20396.63 142.82 o 0.16774 4 14 0 7730.28 7730.28 87.92 o 0.19165 6 14 0 946.99 946.99 30.77 o 0.22594 8 14 0 83903.48 83903.48 289.66 o 0.26664 10 14 0 6648.61 6648.61 81.54 o 0.31124 12 14 0 41708.39 41708.39 204.23 o 0.35829 14 14 0 1654.04 1654.04 40.67 o 0.40695 16 14 0 11452.12 11452.12 107.01 o 0.45669 18 14 0 6495.95 6495.95 80.60 o 0.50720 20 14 0 32489.24 32489.24 180.25 o 0.55827 22 14 0 140.31 140.31 11.85 o 0.60976 24 14 0 6861.03 6861.03 82.83 o 0.66158 0 16 0 7656.70 7656.70 87.50 o 0.18168 2 16 0 495.70 495.70 22.26 o 0.18940 4 16 0 154433.50 154433.50 392.98 o 0.21087 6 16 0 42704.66 42704.66 206.65 o 0.24245 8 16 0 212858.25 212858.25 461.37 o 0.28077 10 16 0 25236.87 25236.87 158.86 o 0.32343 12 16 0 26785.04 26785.04 163.66 o 0.36893 14 16 0 6079.45 6079.45 77.97 o 0.41634 16 16 0 567.21 567.21 23.82 o 0.46508 18 16 0 43583.21 43583.21 208.77 o 0.51477 20 16 0 1748.02 1748.02 41.81 o 0.56516 22 16 0 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28.22 o 0.58135 22 20 0 4434.94 4434.94 66.60 o 0.63096 24 20 0 136.18 136.18 11.67 o 0.68117 2 22 0 393.86 393.86 19.85 o 0.25548 4 22 0 1633.51 1633.51 40.42 o 0.27178 6 22 0 1485.20 1485.20 38.54 o 0.29695 8 22 0 1070.68 1070.68 32.72 o 0.32898 10 22 0 5520.73 5520.73 74.30 o 0.36607 12 22 0 72577.01 72577.01 269.40 o 0.40683 14 22 0 14044.08 14044.08 118.51 o 0.45027 16 22 0 35187.97 35187.97 187.58 o 0.49568 18 22 0 1496.44 1496.44 38.68 o 0.54257 20 22 0 7142.09 7142.09 84.51 o 0.59060 22 22 0 1317.86 1317.86 36.30 o 0.63949 24 22 0 3731.88 3731.88 61.09 o 0.68907 0 24 0 940.48 940.48 30.67 o 0.27252 2 24 0 49.85 49.85 7.06 o 0.27773 4 24 0 294.50 294.50 17.16 o 0.29279 6 24 0 128.64 128.64 11.34 o 0.31630 8 24 0 32205.80 32205.80 179.46 o 0.34654 10 24 0 5630.27 5630.27 75.04 o 0.38193 12 24 0 26350.22 26350.22 162.33 o 0.42115 14 24 0 144165.38 144165.38 379.69 o 0.46325 16 24 0 235.41 235.41 15.34 o 0.50751 18 24 0 19197.43 19197.43 138.55 o 0.55340 20 24 0 28.04 28.04 5.30 o 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4753.62 4753.62 68.95 o 0.77413 19 55 1 1618.71 1618.71 40.23 o 0.80674 21 55 1 3357.47 3357.47 57.94 o 0.84149 23 55 1 716.78 716.78 26.77 o 0.87813 25 55 1 677.11 677.11 26.02 o 0.91644 1 57 1 187.36 187.36 13.69 o 0.64958 3 57 1 771.79 771.79 27.78 o 0.65398 5 57 1 1536.57 1536.57 39.20 o 0.66268 7 57 1 2688.18 2688.18 51.85 o 0.67552 9 57 1 1770.86 1770.86 42.08 o 0.69227 11 57 1 2075.89 2075.89 45.56 o 0.71265 13 57 1 7413.60 7413.60 86.10 o 0.73637 15 57 1 9076.44 9076.44 95.27 o 0.76311 17 57 1 1149.17 1149.17 33.90 o 0.79257 19 57 1 2359.13 2359.13 48.57 o 0.82445 21 57 1 1408.92 1408.92 37.54 o 0.85848 23 57 1 510.91 510.91 22.60 o 0.89443 25 57 1 753.95 753.95 27.46 o 0.93206 2 0 2 407126.28 407126.28 638.06 o 0.11020 6 0 2 57680.95 57680.95 240.17 o 0.18723 10 0 2 104430.70 104430.70 323.16 o 0.28439 14 0 2 30226.85 30226.85 173.86 o 0.38680 18 0 2 8124.45 8124.45 90.14 o 0.49118 22 0 2 6395.88 6395.88 79.97 o 0.59651 0 2 2 114612.24 114612.24 338.54 o 0.09897 2 2 2 5866.37 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2954.34 54.35 o 0.46823 17 17 3 9499.81 9499.81 97.47 o 0.51484 19 17 3 14266.59 14266.59 119.44 o 0.56268 21 17 3 9655.32 9655.32 98.26 o 0.61147 23 17 3 4107.59 4107.59 64.09 o 0.66098 25 17 3 1629.49 1629.49 40.37 o 0.71108 1 19 3 2218.07 2218.07 47.10 o 0.26104 3 19 3 14086.06 14086.06 118.68 o 0.27179 5 19 3 20670.90 20670.90 143.77 o 0.29210 7 19 3 28308.27 28308.27 168.25 o 0.32017 9 19 3 4280.68 4280.68 65.43 o 0.35415 11 19 3 16560.71 16560.71 128.69 o 0.39250 13 19 3 7734.12 7734.12 87.94 o 0.43408 15 19 3 2815.76 2815.76 53.06 o 0.47804 17 19 3 16718.68 16718.68 129.30 o 0.52378 19 19 3 10718.31 10718.31 103.53 o 0.57087 21 19 3 8448.38 8448.38 91.92 o 0.61901 23 19 3 4423.56 4423.56 66.51 o 0.66797 25 19 3 2590.45 2590.45 50.90 o 0.71758 1 21 3 14277.55 14277.55 119.49 o 0.28010 3 21 3 20299.07 20299.07 142.47 o 0.29014 5 21 3 18725.61 18725.61 136.84 o 0.30926 7 21 3 48223.92 48223.92 219.60 o 0.33589 9 21 3 31156.11 31156.11 176.51 o 0.36842 11 21 3 2900.90 2900.90 53.86 o 0.40543 13 21 3 29079.26 29079.26 170.53 o 0.44581 15 21 3 26563.98 26563.98 162.98 o 0.48871 17 21 3 19295.27 19295.27 138.91 o 0.53354 19 21 3 2879.47 2879.47 53.66 o 0.57984 21 21 3 716.66 716.66 26.77 o 0.62729 23 21 3 1565.24 1565.24 39.56 o 0.67565 25 21 3 1851.07 1851.07 43.02 o 0.72473 1 23 3 28955.81 28955.81 170.16 o 0.29967 3 23 3 43740.30 43740.30 209.14 o 0.30908 5 23 3 35688.96 35688.96 188.92 o 0.32709 7 23 3 11144.26 11144.26 105.57 o 0.35238 9 23 3 11262.75 11262.75 106.13 o 0.38351 11 23 3 6907.80 6907.80 83.11 o 0.41919 13 23 3 27702.02 27702.02 166.44 o 0.45835 15 23 3 14986.46 14986.46 122.42 o 0.50018 17 23 3 2833.27 2833.27 53.23 o 0.54407 19 23 3 1994.74 1994.74 44.66 o 0.58954 21 23 3 765.15 765.15 27.66 o 0.63627 23 23 3 179.36 179.36 13.39 o 0.68399 25 23 3 119.22 119.22 10.92 o 0.73252 1 25 3 30831.07 30831.07 175.59 o 0.31966 3 25 3 40604.11 40604.11 201.50 o 0.32849 5 25 3 25881.22 25881.22 160.88 o 0.34549 7 25 3 25866.54 25866.54 160.83 o 0.36952 9 25 3 29460.96 29460.96 171.64 o 0.39932 11 25 3 784.92 784.92 28.02 o 0.43370 13 25 3 14439.13 14439.13 120.16 o 0.47166 15 25 3 13323.19 13323.19 115.43 o 0.51241 17 25 3 3657.99 3657.99 60.48 o 0.55533 19 25 3 2649.66 2649.66 51.47 o 0.59995 21 25 3 1644.70 1644.70 40.55 o 0.64592 23 25 3 237.53 237.53 15.41 o 0.69298 25 25 3 545.66 545.66 23.36 o 0.74092 1 27 3 8576.86 8576.86 92.61 o 0.33999 3 27 3 2110.22 2110.22 45.94 o 0.34831 5 27 3 23271.41 23271.41 152.55 o 0.36438 7 27 3 32948.53 32948.53 181.52 o 0.38724 9 27 3 15661.63 15661.63 125.15 o 0.41578 11 27 3 2702.32 2702.32 51.98 o 0.44890 13 27 3 4203.24 4203.24 64.83 o 0.48567 15 27 3 11261.92 11261.92 106.12 o 0.52533 17 27 3 7806.43 7806.43 88.35 o 0.56727 19 27 3 2901.45 2901.45 53.87 o 0.61102 21 27 3 661.01 661.01 25.71 o 0.65622 23 27 3 1709.46 1709.46 41.35 o 0.70259 25 27 3 3348.14 3348.14 57.86 o 0.74991 1 29 3 7847.08 7847.08 88.58 o 0.36060 3 29 3 1894.86 1894.86 43.53 o 0.36846 5 29 3 8784.55 8784.55 93.73 o 0.38369 7 29 3 2057.83 2057.83 45.36 o 0.40546 9 29 3 22705.52 22705.52 150.68 o 0.43279 11 29 3 11306.40 11306.40 106.33 o 0.46470 13 29 3 8584.37 8584.37 92.65 o 0.50032 15 29 3 14541.90 14541.90 120.59 o 0.53890 17 29 3 7580.86 7580.86 87.07 o 0.57986 19 29 3 4422.10 4422.10 66.50 o 0.62273 21 29 3 8340.20 8340.20 91.32 o 0.66713 23 29 3 3001.62 3001.62 54.79 o 0.71279 25 29 3 1644.41 1644.41 40.55 o 0.75948 1 31 3 16801.94 16801.94 129.62 o 0.38145 3 31 3 7737.72 7737.72 87.96 o 0.38889 5 31 3 2762.19 2762.19 52.56 o 0.40335 7 31 3 20408.96 20408.96 142.86 o 0.42411 9 31 3 2740.77 2740.77 52.35 o 0.45031 11 31 3 5620.17 5620.17 74.97 o 0.48106 13 31 3 6040.07 6040.07 77.72 o 0.51555 15 31 3 6613.14 6613.14 81.32 o 0.55307 17 31 3 1754.04 1754.04 41.88 o 0.59305 19 31 3 1935.49 1935.49 43.99 o 0.63503 21 31 3 2330.37 2330.37 48.27 o 0.67863 23 31 3 614.44 614.44 24.79 o 0.72357 25 31 3 2227.03 2227.03 47.19 o 0.76960 1 33 3 96992.26 96992.26 311.44 o 0.40250 3 33 3 58834.84 58834.84 242.56 o 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137.71 o 0.44510 3 37 3 4411.87 4411.87 66.42 o 0.45149 5 37 3 6327.72 6327.72 79.55 o 0.46400 7 37 3 2140.45 2140.45 46.26 o 0.48216 9 37 3 11489.47 11489.47 107.19 o 0.50536 11 37 3 13540.56 13540.56 116.36 o 0.53294 13 37 3 11085.07 11085.07 105.29 o 0.56427 15 37 3 4206.82 4206.82 64.86 o 0.59874 17 37 3 5949.53 5949.53 77.13 o 0.63586 19 37 3 2338.18 2338.18 48.35 o 0.67518 21 37 3 2806.02 2806.02 52.97 o 0.71634 23 37 3 3998.84 3998.84 63.24 o 0.75905 25 37 3 4896.72 4896.72 69.98 o 0.80305 1 39 3 8469.91 8469.91 92.03 o 0.46659 3 39 3 1822.99 1822.99 42.70 o 0.47269 5 39 3 3142.42 3142.42 56.06 o 0.48466 7 39 3 5415.94 5415.94 73.59 o 0.50207 9 39 3 6189.65 6189.65 78.67 o 0.52439 11 39 3 12786.84 12786.84 113.08 o 0.55103 13 39 3 4174.54 4174.54 64.61 o 0.58137 15 39 3 4089.26 4089.26 63.95 o 0.61489 17 39 3 2377.39 2377.39 48.76 o 0.65109 19 39 3 2254.37 2254.37 47.48 o 0.68954 21 39 3 6312.89 6312.89 79.45 o 0.72989 23 39 3 5328.40 5328.40 73.00 o 0.77185 25 39 3 1291.75 1291.75 35.94 o 0.81516 1 41 3 2098.04 2098.04 45.80 o 0.48820 3 41 3 5358.21 5358.21 73.20 o 0.49403 5 41 3 12591.88 12591.88 112.21 o 0.50549 7 41 3 15562.48 15562.48 124.75 o 0.52221 9 41 3 13750.43 13750.43 117.26 o 0.54371 11 41 3 6292.75 6292.75 79.33 o 0.56944 13 41 3 2765.79 2765.79 52.59 o 0.59885 15 41 3 2791.54 2791.54 52.83 o 0.63144 17 41 3 871.06 871.06 29.51 o 0.66674 19 41 3 1597.29 1597.29 39.97 o 0.70434 21 41 3 1315.99 1315.99 36.28 o 0.74389 23 41 3 1539.99 1539.99 39.24 o 0.78510 25 41 3 2678.78 2678.78 51.76 o 0.82772 1 43 3 4751.24 4751.24 68.93 o 0.50990 3 43 3 22668.49 22668.49 150.56 o 0.51549 5 43 3 10626.13 10626.13 103.08 o 0.52648 7 43 3 18224.94 18224.94 135.00 o 0.54256 9 43 3 6364.62 6364.62 79.78 o 0.56328 11 43 3 5478.10 5478.10 74.01 o 0.58815 13 43 3 5765.77 5765.77 75.93 o 0.61668 15 43 3 650.39 650.39 25.50 o 0.64837 17 43 3 1449.45 1449.45 38.07 o 0.68279 19 43 3 3747.21 3747.21 61.21 o 0.71955 21 43 3 816.28 816.28 28.57 o 0.75831 23 43 3 216.50 216.50 14.71 o 0.79878 25 43 3 73.14 73.14 8.55 o 0.84070 1 45 3 25851.84 25851.84 160.79 o 0.53169 3 45 3 3083.60 3083.60 55.53 o 0.53705 5 45 3 7238.91 7238.91 85.08 o 0.54761 7 45 3 5306.60 5306.60 72.85 o 0.56308 9 45 3 4565.01 4565.01 67.56 o 0.58307 11 45 3 5321.99 5321.99 72.95 o 0.60714 13 45 3 2420.61 2420.61 49.20 o 0.63481 15 45 3 1149.00 1149.00 33.90 o 0.66564 17 45 3 3632.78 3632.78 60.27 o 0.69921 19 45 3 3891.68 3891.68 62.38 o 0.73515 21 45 3 3137.10 3137.10 56.01 o 0.77313 23 45 3 919.18 919.18 30.32 o 0.81286 25 45 3 17.29 17.29 4.16 o 0.85409 1 47 3 5023.44 5023.44 70.88 o 0.55355 3 47 3 65.36 65.36 8.08 o 0.55870 5 47 3 1368.53 1368.53 36.99 o 0.56886 7 47 3 2591.88 2591.88 50.91 o 0.58377 9 47 3 2712.55 2712.55 52.08 o 0.60307 11 47 3 646.16 646.16 25.42 o 0.62637 13 47 3 1579.97 1579.97 39.75 o 0.65323 15 47 3 2866.05 2866.05 53.54 o 0.68323 17 47 3 4017.66 4017.66 63.38 o 0.71598 19 47 3 5393.90 5393.90 73.44 o 0.75112 21 47 3 588.86 588.86 24.27 o 0.78832 23 47 3 2480.59 2480.59 49.81 o 0.82732 25 47 3 1916.39 1916.39 43.78 o 0.86787 1 49 3 846.24 846.24 29.09 o 0.57548 3 49 3 9349.51 9349.51 96.69 o 0.58043 5 49 3 6293.76 6293.76 79.33 o 0.59022 7 49 3 7231.57 7231.57 85.04 o 0.60460 9 49 3 4279.00 4279.00 65.41 o 0.62326 11 49 3 3659.54 3659.54 60.49 o 0.64583 13 49 3 1377.51 1377.51 37.11 o 0.67191 15 49 3 929.49 929.49 30.49 o 0.70111 17 49 3 2257.04 2257.04 47.51 o 0.73306 19 49 3 2845.30 2845.30 53.34 o 0.76742 21 49 3 3456.11 3456.11 58.79 o 0.80387 23 49 3 3561.15 3561.15 59.68 o 0.84215 25 49 3 468.75 468.75 21.65 o 0.88202 1 51 3 3240.59 3240.59 56.93 o 0.59746 3 51 3 14118.99 14118.99 118.82 o 0.60224 5 51 3 8549.57 8549.57 92.46 o 0.61168 7 51 3 10647.59 10647.59 103.19 o 0.62556 9 51 3 3559.17 3559.17 59.66 o 0.64362 11 51 3 611.17 611.17 24.72 o 0.66549 13 51 3 54.11 54.11 7.36 o 0.69083 15 51 3 971.11 971.11 31.16 o 0.71927 17 51 3 5856.19 5856.19 76.53 o 0.75045 19 51 3 1255.41 1255.41 35.43 o 0.78404 21 51 3 234.99 234.99 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39.06 o 0.85245 23 55 3 513.72 513.72 22.67 o 0.88864 25 55 3 344.81 344.81 18.57 o 0.92651 1 57 3 1557.44 1557.44 39.46 o 0.66371 3 57 3 2285.05 2285.05 47.80 o 0.66801 5 57 3 4089.53 4089.53 63.95 o 0.67654 7 57 3 132.02 132.02 11.49 o 0.68912 9 57 3 1634.50 1634.50 40.43 o 0.70555 11 57 3 2454.44 2454.44 49.54 o 0.72556 13 57 3 5991.44 5991.44 77.40 o 0.74887 15 57 3 8707.53 8707.53 93.31 o 0.77518 17 57 3 5163.51 5163.51 71.86 o 0.80419 19 57 3 1975.61 1975.61 44.45 o 0.83563 21 57 3 172.74 172.74 13.14 o 0.86922 23 57 3 634.74 634.74 25.19 o 0.90474 25 57 3 575.54 575.54 23.99 o 0.94196 0 0 4 494988.47 494988.47 703.55 o 0.19266 4 0 4 46103.96 46103.96 214.72 o 0.22039 8 0 4 15193.45 15193.45 123.26 o 0.28799 12 0 4 55285.34 55285.34 235.13 o 0.37446 16 0 4 5349.97 5349.97 73.14 o 0.46948 20 0 4 8119.28 8119.28 90.11 o 0.56878 24 0 4 2203.46 2203.46 46.94 o 0.67047 2 2 4 248384.33 248384.33 498.38 o 0.20124 4 2 4 4419.32 4419.32 66.48 o 0.22156 6 2 4 89824.06 89824.06 299.71 o 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3856.66 62.10 o 0.30058 6 18 4 153949.72 153949.72 392.36 o 0.32352 8 18 4 638.23 638.23 25.26 o 0.35315 10 18 4 31270.94 31270.94 176.84 o 0.38793 12 18 4 3290.84 3290.84 57.37 o 0.42661 14 18 4 4331.30 4331.30 65.81 o 0.46822 16 18 4 5921.39 5921.39 76.95 o 0.51204 18 18 4 1611.83 1611.83 40.15 o 0.55756 20 18 4 3121.69 3121.69 55.87 o 0.60439 22 18 4 937.89 937.89 30.62 o 0.65225 24 18 4 1109.83 1109.83 33.31 o 0.70093 0 20 4 42166.78 42166.78 205.35 o 0.29781 2 20 4 15106.17 15106.17 122.91 o 0.30258 4 20 4 31838.85 31838.85 178.43 o 0.31646 6 20 4 16592.48 16592.48 128.81 o 0.33833 8 20 4 42581.47 42581.47 206.35 o 0.36676 10 20 4 5825.63 5825.63 76.33 o 0.40036 12 20 4 12550.02 12550.02 112.03 o 0.43794 14 20 4 7449.01 7449.01 86.31 o 0.47857 16 20 4 12128.08 12128.08 110.13 o 0.52152 18 20 4 6454.75 6454.75 80.34 o 0.56628 20 20 4 3003.74 3003.74 54.81 o 0.61244 22 20 4 3948.74 3948.74 62.84 o 0.65972 24 20 4 5.03 5.03 2.24 o 0.70789 2 22 4 57566.09 57566.09 239.93 o 0.31998 4 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12 2412.53 2412.53 49.12 o 0.75680 12 36 12 4315.29 4315.29 65.69 o 0.77734 14 36 12 124.23 124.23 11.15 o 0.80093 16 36 12 1066.99 1066.99 32.66 o 0.82731 18 36 12 1970.41 1970.41 44.39 o 0.85623 20 36 12 58.04 58.04 7.62 o 0.88744 22 36 12 853.46 853.46 29.21 o 0.92070 24 36 12 198.94 198.94 14.10 o 0.95580 2 38 12 6941.43 6941.43 83.32 o 0.72326 4 38 12 2054.90 2054.90 45.33 o 0.72917 6 38 12 10172.25 10172.25 100.86 o 0.73892 8 38 12 158.71 158.71 12.60 o 0.75237 10 38 12 1592.76 1592.76 39.91 o 0.76931 12 38 12 721.10 721.10 26.85 o 0.78952 14 38 12 3551.28 3551.28 59.59 o 0.81275 16 38 12 582.57 582.57 24.14 o 0.83877 18 38 12 64.83 64.83 8.05 o 0.86730 20 38 12 165.65 165.65 12.87 o 0.89813 22 38 12 113.31 113.31 10.64 o 0.93101 24 38 12 83.20 83.20 9.12 o 0.96574 0 40 12 2302.35 2302.35 47.98 o 0.73508 2 40 12 180.74 180.74 13.44 o 0.73703 4 40 12 7430.11 7430.11 86.20 o 0.74284 6 40 12 10.22 10.22 3.20 o 0.75241 8 40 12 2928.19 2928.19 54.11 o 0.76562 10 40 12 176.63 176.63 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14 941.50 941.50 30.68 o 0.77437 16 6 14 33.59 33.59 5.80 o 0.80163 18 6 14 2819.68 2819.68 53.10 o 0.83144 20 6 14 0.92 0.92 0.96 o 0.86355 22 6 14 1879.31 1879.31 43.35 o 0.89769 24 6 14 226.18 226.18 15.04 o 0.93366 2 8 14 12063.80 12063.80 109.84 o 0.68249 4 8 14 1970.75 1970.75 44.39 o 0.68875 6 8 14 5624.72 5624.72 75.00 o 0.69907 8 8 14 2002.16 2002.16 44.75 o 0.71327 10 8 14 13264.41 13264.41 115.17 o 0.73111 12 8 14 3041.14 3041.14 55.15 o 0.75235 14 8 14 803.08 803.08 28.34 o 0.77670 16 8 14 2239.03 2239.03 47.32 o 0.80388 18 8 14 805.48 805.48 28.38 o 0.83361 20 8 14 845.09 845.09 29.07 o 0.86563 22 8 14 184.29 184.29 13.58 o 0.89970 24 8 14 640.18 640.18 25.30 o 0.93559 0 10 14 17539.46 17539.46 132.44 o 0.68379 2 10 14 3271.02 3271.02 57.19 o 0.68588 4 10 14 9199.67 9199.67 95.91 o 0.69212 6 10 14 164.11 164.11 12.81 o 0.70238 8 10 14 6346.92 6346.92 79.67 o 0.71651 10 10 14 899.60 899.60 29.99 o 0.73428 12 10 14 3974.70 3974.70 63.05 o 0.75543 14 10 14 896.68 896.68 29.94 o 0.77968 16 10 14 642.97 642.97 25.36 o 0.80676 18 10 14 149.05 149.05 12.21 o 0.83639 20 10 14 420.41 420.41 20.50 o 0.86831 22 10 14 172.10 172.10 13.12 o 0.90228 24 10 14 69.62 69.62 8.34 o 0.93807 2 12 14 7459.04 7459.04 86.37 o 0.69000 4 12 14 3008.93 3008.93 54.85 o 0.69620 6 12 14 1804.45 1804.45 42.48 o 0.70641 8 12 14 205.91 205.91 14.35 o 0.72046 10 12 14 4141.43 4141.43 64.35 o 0.73813 12 12 14 2102.09 2102.09 45.85 o 0.75917 14 12 14 675.78 675.78 26.00 o 0.78331 16 12 14 3604.69 3604.69 60.04 o 0.81027 18 12 14 2325.29 2325.29 48.22 o 0.83978 20 12 14 1153.32 1153.32 33.96 o 0.87157 22 12 14 68.53 68.53 8.28 o 0.90542 24 12 14 1320.95 1320.95 36.34 o 0.94109 0 14 14 2408.09 2408.09 49.07 o 0.69278 2 14 14 2887.32 2887.32 53.73 o 0.69485 4 14 14 638.00 638.00 25.26 o 0.70100 6 14 14 109.85 109.85 10.48 o 0.71114 8 14 14 7.54 7.54 2.75 o 0.72510 10 14 14 1987.86 1987.86 44.59 o 0.74266 12 14 14 14.87 14.87 3.86 o 0.76358 14 14 14 4482.40 4482.40 66.95 o 0.78758 16 14 14 321.47 321.47 17.93 o 0.81440 18 14 14 1535.23 1535.23 39.18 o 0.84376 20 14 14 15.79 15.79 3.97 o 0.87541 22 14 14 2263.32 2263.32 47.57 o 0.90911 24 14 14 106.12 106.12 10.30 o 0.94465 2 16 14 2946.77 2946.77 54.28 o 0.70039 4 16 14 2737.95 2737.95 52.33 o 0.70650 6 16 14 4938.37 4938.37 70.27 o 0.71656 8 16 14 4218.95 4218.95 64.95 o 0.73042 10 16 14 1189.93 1189.93 34.50 o 0.74785 12 16 14 3361.48 3361.48 57.98 o 0.76863 14 16 14 1298.90 1298.90 36.04 o 0.79248 16 16 14 4552.07 4552.07 67.47 o 0.81913 18 16 14 398.33 398.33 19.96 o 0.84833 20 16 14 2594.14 2594.14 50.93 o 0.87982 22 16 14 204.87 204.87 14.31 o 0.91336 24 16 14 1826.75 1826.75 42.74 o 0.94873 0 18 14 4683.52 4683.52 68.44 o 0.70459 2 18 14 2385.03 2385.03 48.84 o 0.70662 4 18 14 12087.55 12087.55 109.94 o 0.71268 6 18 14 247.97 247.97 15.75 o 0.72265 8 18 14 6374.49 6374.49 79.84 o 0.73639 10 18 14 474.57 474.57 21.78 o 0.75369 12 18 14 2305.48 2305.48 48.02 o 0.77431 14 18 14 839.22 839.22 28.97 o 0.79799 16 18 14 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146.19 12.09 o 0.83688 18 22 14 3594.82 3594.82 59.96 o 0.86548 20 22 14 260.06 260.06 16.13 o 0.89637 22 22 14 833.80 833.80 28.88 o 0.92931 24 22 14 197.36 197.36 14.05 o 0.96410 2 24 14 2101.59 2101.59 45.84 o 0.72925 4 24 14 746.15 746.15 27.32 o 0.73512 6 24 14 510.29 510.29 22.59 o 0.74479 8 24 14 1700.63 1700.63 41.24 o 0.75813 10 24 14 38.34 38.34 6.19 o 0.77495 12 24 14 1574.10 1574.10 39.67 o 0.79501 14 24 14 84.57 84.57 9.20 o 0.81809 16 24 14 3214.99 3214.99 56.70 o 0.84394 18 24 14 410.58 410.58 20.26 o 0.87231 20 24 14 3420.86 3420.86 58.49 o 0.90296 22 24 14 342.98 342.98 18.52 o 0.93567 24 24 14 1025.67 1025.67 32.03 o 0.97023 0 26 14 3469.36 3469.36 58.90 o 0.73610 2 26 14 161.68 161.68 12.72 o 0.73804 4 26 14 4460.79 4460.79 66.79 o 0.74384 6 26 14 2930.35 2930.35 54.13 o 0.75340 8 26 14 3393.82 3393.82 58.26 o 0.76659 10 26 14 322.87 322.87 17.97 o 0.78322 12 26 14 787.86 787.86 28.07 o 0.80308 14 26 14 317.26 317.26 17.81 o 0.82594 16 26 14 578.81 578.81 24.06 o 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18 30 14 274.42 274.42 16.57 o 0.89594 20 30 14 212.64 212.64 14.58 o 0.92581 22 30 14 1062.73 1062.73 32.60 o 0.95774 24 30 14 315.80 315.80 17.77 o 0.99153 2 32 14 1012.24 1012.24 31.82 o 0.76784 4 32 14 2205.63 2205.63 46.96 o 0.77341 6 32 14 977.23 977.23 31.26 o 0.78261 8 32 14 1286.00 1286.00 35.86 o 0.79532 10 32 14 70.99 70.99 8.43 o 0.81136 12 32 14 3086.40 3086.40 55.56 o 0.83055 14 32 14 489.96 489.96 22.14 o 0.85267 16 32 14 1942.98 1942.98 44.08 o 0.87750 18 32 14 1169.98 1169.98 34.20 o 0.90481 20 32 14 781.43 781.43 27.95 o 0.93440 22 32 14 20.89 20.89 4.57 o 0.96605 24 32 14 2486.37 2486.37 49.86 o 0.99956 0 34 14 3140.79 3140.79 56.04 o 0.77700 2 34 14 296.91 296.91 17.23 o 0.77884 4 34 14 26.04 26.04 5.10 o 0.78434 6 34 14 695.31 695.31 26.37 o 0.79341 8 34 14 593.58 593.58 24.36 o 0.80595 10 34 14 2454.73 2454.73 49.55 o 0.82178 12 34 14 1610.97 1610.97 40.14 o 0.84073 14 34 14 2900.56 2900.56 53.86 o 0.86259 16 34 14 417.94 417.94 20.44 o 0.88714 18 34 14 1140.01 1140.01 33.76 o 0.91417 20 34 14 15.66 15.66 3.96 o 0.94346 22 34 14 2706.28 2706.28 52.02 o 0.97482 24 34 14 336.32 336.32 18.34 o 1.00804 2 36 14 5192.90 5192.90 72.06 o 0.79034 4 36 14 420.91 420.91 20.52 o 0.79576 6 36 14 332.61 332.61 18.24 o 0.80471 8 36 14 1523.97 1523.97 39.04 o 0.81707 10 36 14 4531.22 4531.22 67.31 o 0.83269 12 36 14 1601.42 1601.42 40.02 o 0.85140 14 36 14 1266.51 1266.51 35.59 o 0.87299 16 36 14 1555.73 1555.73 39.44 o 0.89726 18 36 14 55.46 55.46 7.45 o 0.92399 20 36 14 540.71 540.71 23.25 o 0.95298 22 36 14 527.79 527.79 22.97 o 0.98403 24 36 14 658.15 658.15 25.65 o 1.01695 0 38 14 6971.96 6971.96 83.50 o 0.80054 2 38 14 15.92 15.92 3.99 o 0.80233 4 38 14 5816.22 5816.22 76.26 o 0.80766 6 38 14 1487.55 1487.55 38.57 o 0.81648 8 38 14 3964.67 3964.67 62.97 o 0.82867 10 38 14 118.63 118.63 10.89 o 0.84407 12 38 14 3650.42 3650.42 60.42 o 0.86253 14 38 14 1383.64 1383.64 37.20 o 0.88385 16 38 14 256.37 256.37 16.01 o 0.90783 18 38 14 38.09 38.09 6.17 o 0.93426 20 38 14 381.67 381.67 19.54 o 0.96294 22 38 14 86.51 86.51 9.30 o 0.99368 24 38 14 67.27 67.27 8.20 o 1.02629 2 40 14 2975.77 2975.77 54.55 o 0.81476 4 40 14 952.14 952.14 30.86 o 0.82002 6 40 14 1953.65 1953.65 44.20 o 0.82871 8 40 14 205.76 205.76 14.34 o 0.84071 10 40 14 2465.73 2465.73 49.66 o 0.85591 12 40 14 236.92 236.92 15.39 o 0.87412 14 40 14 677.72 677.72 26.03 o 0.89516 16 40 14 434.33 434.33 20.84 o 0.91884 18 40 14 145.56 145.56 12.06 o 0.94496 20 40 14 559.16 559.16 23.65 o 0.97333 22 40 14 18.79 18.79 4.34 o 1.00375 24 40 14 323.94 323.94 18.00 o 1.03604 0 42 14 515.83 515.83 22.71 o 0.82591 2 42 14 2.76 2.76 1.66 o 0.82764 4 42 14 17.57 17.57 4.19 o 0.83281 6 42 14 572.53 572.53 23.93 o 0.84137 8 42 14 17.46 17.46 4.18 o 0.85320 10 42 14 791.06 791.06 28.13 o 0.86817 12 42 14 851.08 851.08 29.17 o 0.88613 14 42 14 3179.74 3179.74 56.39 o 0.90689 16 42 14 62.33 62.33 7.89 o 0.93028 18 42 14 1888.97 1888.97 43.46 o 0.95609 20 42 14 192.41 192.41 13.87 o 0.98413 22 42 14 846.90 846.90 29.10 o 1.01423 24 42 14 12.94 12.94 3.60 o 1.04620 2 44 14 896.51 896.51 29.94 o 0.84093 4 44 14 94.99 94.99 9.75 o 0.84602 6 44 14 3075.73 3075.73 55.46 o 0.85444 8 44 14 513.48 513.48 22.66 o 0.86610 10 44 14 400.81 400.81 20.02 o 0.88085 12 44 14 2594.69 2594.69 50.94 o 0.89856 14 44 14 125.78 125.78 11.22 o 0.91904 16 44 14 1348.74 1348.74 36.73 o 0.94212 18 44 14 43.76 43.76 6.62 o 0.96762 20 44 14 813.73 813.73 28.53 o 0.99534 22 44 14 48.20 48.20 6.94 o 1.02510 24 44 14 1070.29 1070.29 32.72 o 1.05675 0 46 14 3068.72 3068.72 55.40 o 0.85294 2 46 14 15.43 15.43 3.93 o 0.85462 4 46 14 3464.19 3464.19 58.86 o 0.85963 6 46 14 153.36 153.36 12.38 o 0.86792 8 46 14 1679.27 1679.27 40.98 o 0.87939 10 46 14 245.00 245.00 15.65 o 0.89393 12 46 14 826.46 826.46 28.75 o 0.91138 14 46 14 715.40 715.40 26.75 o 0.93158 16 46 14 1137.02 1137.02 33.72 o 0.95436 18 46 14 54.04 54.04 7.35 o 0.97954 20 46 14 186.42 186.42 13.65 o 1.00693 22 46 14 111.18 111.18 10.54 o 1.03636 24 46 14 86.98 86.98 9.33 o 1.06767 2 48 14 2936.87 2936.87 54.19 o 0.86869 4 48 14 2.01 2.01 1.42 o 0.87362 6 48 14 4159.51 4159.51 64.49 o 0.88177 8 48 14 36.59 36.59 6.05 o 0.89307 10 48 14 1024.98 1024.98 32.02 o 0.90739 12 48 14 8.32 8.32 2.88 o 0.92458 14 48 14 1380.07 1380.07 37.15 o 0.94450 16 48 14 149.44 149.44 12.22 o 0.96698 18 48 14 658.43 658.43 25.66 o 0.99183 20 48 14 184.82 184.82 13.59 o 1.01889 22 48 14 62.68 62.68 7.92 o 1.04799 24 48 14 33.51 33.51 5.79 o 1.07896 0 50 14 256.09 256.09 16.00 o 0.88149 2 50 14 145.14 145.14 12.05 o 0.88311 4 50 14 845.69 845.69 29.08 o 0.88796 6 50 14 498.48 498.48 22.33 o 0.89599 8 50 14 1114.19 1114.19 33.38 o 0.90711 10 50 14 3113.11 3113.11 55.80 o 0.92121 12 50 14 280.89 280.89 16.76 o 0.93815 14 50 14 383.17 383.17 19.57 o 0.95779 16 50 14 539.73 539.73 23.23 o 0.97996 18 50 14 1726.32 1726.32 41.55 o 1.00449 20 50 14 36.51 36.51 6.04 o 1.03122 22 50 14 869.55 869.55 29.49 o 1.05998 24 50 14 54.12 54.12 7.36 o 1.09061 2 52 14 47.12 47.12 6.86 o 0.89788 4 52 14 332.62 332.62 18.24 o 0.90265 6 52 14 613.18 613.18 24.76 o 0.91055 8 52 14 1919.60 1919.60 43.81 o 0.92149 10 52 14 1160.54 1160.54 34.07 o 0.93537 12 52 14 181.84 181.84 13.48 o 0.95207 14 52 14 142.11 142.11 11.92 o 0.97142 16 52 14 1500.42 1500.42 38.74 o 0.99329 18 52 14 324.55 324.55 18.02 o 1.01750 20 52 14 1928.20 1928.20 43.91 o 1.04390 22 52 14 55.87 55.87 7.47 o 1.07232 24 52 14 380.62 380.62 19.51 o 1.10260 0 54 14 905.70 905.70 30.09 o 0.91141 2 54 14 192.31 192.31 13.87 o 0.91298 4 54 14 1388.36 1388.36 37.26 o 0.91767 6 54 14 325.16 325.16 18.03 o 0.92544 8 54 14 1317.05 1317.05 36.29 o 0.93621 10 54 14 154.07 154.07 12.41 o 0.94987 12 54 14 590.23 590.23 24.29 o 0.96631 14 54 14 397.97 397.97 19.95 o 0.98539 16 54 14 248.62 248.62 15.77 o 1.00695 18 54 14 1033.13 1033.13 32.14 o 1.03084 20 54 14 93.67 93.67 9.68 o 1.05691 22 54 14 643.33 643.33 25.36 o 1.08499 24 54 14 4.07 4.07 2.02 o 1.11493 2 56 14 3083.30 3083.30 55.53 o 0.92838 4 56 14 141.40 141.40 11.89 o 0.93300 6 56 14 1881.26 1881.26 43.37 o 0.94064 8 56 14 97.74 97.74 9.89 o 0.95124 10 56 14 2124.76 2124.76 46.10 o 0.96469 12 56 14 150.70 150.70 12.28 o 0.98088 14 56 14 122.34 122.34 11.06 o 0.99968 16 56 14 132.39 132.39 11.51 o 1.02094 18 56 14 116.78 116.78 10.81 o 1.04451 20 56 14 346.41 346.41 18.61 o 1.07024 22 56 14 21.19 21.19 4.60 o 1.09798 24 56 14 54.20 54.20 7.36 o 1.12758 0 58 14 2237.57 2237.57 47.30 o 0.94256 2 58 14 33.43 33.43 5.78 o 0.94408 4 58 14 1889.82 1889.82 43.47 o 0.94862 6 58 14 142.45 142.45 11.94 o 0.95614 8 58 14 1260.21 1260.21 35.50 o 0.96657 10 58 14 215.38 215.38 14.68 o 0.97981 12 58 14 824.80 824.80 28.72 o 0.99575 14 58 14 455.85 455.85 21.35 o 1.01428 16 58 14 284.90 284.90 16.88 o 1.03524 18 58 14 32.09 32.09 5.66 o 1.05849 20 58 14 93.27 93.27 9.66 o 1.08389 22 58 14 164.40 164.40 12.82 o 1.11129 24 58 14 39.83 39.83 6.31 o 1.14054