#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217348.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217348_Fobs loop_ _publ_author_name 'Amarante, Tatiana R.' 'Coelho, Ana C.' 'Klinowski, Jacek' 'Gon\,calves, Isabel S.' 'Almeida Paz, Filipe A.' _publ_section_title ; 1-Hydroxy-1,1,3,3,3-pentaphenyldisiloxane, [Si~2~O(OH)(Ph)~5~], at 150 K ; _journal_coeditor_code TK2229 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o239 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 65.270 _cell_angle_beta 71.217 _cell_angle_gamma 87.173 _cell_length_a 15.0113 _cell_length_b 19.9930 _cell_length_c 20.1661 _exptl_crystal_F_000 2000.00 _reflns_d_resolution_high 0.8300 _[local]_cod_data_source_file tk2229Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'I in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 580.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l 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o 4 1 0 7962.21 7626.04 167.91 o 5 1 0 448.09 465.40 26.28 o 6 1 0 2751.29 2464.54 62.25 o 7 1 0 5.28 25.69 30.57 o 8 1 0 1563.21 1566.66 50.65 o 9 1 0 0.00 -24.35 29.25 o 10 1 0 3540.81 3696.19 103.92 o 11 1 0 191.08 179.75 44.08 o 12 1 0 290.02 139.12 40.34 o 13 1 0 5.19 -17.05 55.52 o 14 1 0 224.04 357.45 85.65 o 15 1 0 45.34 20.52 103.96 o 16 1 0 1.97 86.32 241.09 o -17 2 0 11.15 -266.36 266.36 o -16 2 0 31.18 96.82 257.03 o -15 2 0 108.20 203.37 223.98 o -14 2 0 1849.93 1961.49 168.88 o -13 2 0 36.98 28.71 64.64 o -12 2 0 1136.95 1200.72 59.75 o -11 2 0 3.30 -27.26 35.42 o -10 2 0 1094.37 1025.43 50.66 o -9 2 0 16.52 -27.85 27.85 o -8 2 0 16761.10 17172.47 390.37 o -7 2 0 509.26 356.43 34.06 o -6 2 0 3673.25 3939.69 98.07 o -5 2 0 17.44 -18.81 18.81 o -4 2 0 97324.33 96488.44 2061.37 o -3 2 0 1104.63 995.88 37.55 o 2 2 0 7350.74 7288.07 206.32 o 3 2 0 382.90 257.92 19.15 o 4 2 0 6124.41 5247.34 117.82 o 5 2 0 10.22 -13.40 13.85 o 6 2 0 4425.06 4107.32 91.55 o 7 2 0 134.23 124.62 17.96 o 8 2 0 21.96 53.94 17.85 o 9 2 0 2276.08 2230.40 71.78 o 10 2 0 15218.00 14548.25 348.00 o 11 2 0 141.78 189.54 36.65 o 12 2 0 1170.35 1235.41 83.24 o 13 2 0 124.13 188.89 74.32 o 14 2 0 709.59 620.87 92.21 o 15 2 0 1.22 -82.50 85.54 o 16 2 0 1402.69 1683.82 146.71 o -17 3 0 40.84 76.99 276.08 o -16 3 0 51.92 -234.09 260.14 o -15 3 0 4.57 -20.22 219.31 o -14 3 0 269.68 423.46 260.92 o -13 3 0 35.82 53.07 67.89 o -12 3 0 0.09 -1.26 44.49 o -11 3 0 72.28 -23.43 38.58 o -10 3 0 1.78 -35.31 35.31 o -9 3 0 15.45 -8.06 32.75 o -8 3 0 17502.17 18594.55 435.25 o -7 3 0 89.95 30.11 27.94 o -6 3 0 2.19 27.16 23.63 o -5 3 0 285.33 210.94 25.20 o -4 3 0 28381.80 28103.70 622.74 o -3 3 0 91.23 41.28 23.35 o -2 3 0 711.47 946.19 34.85 o -1 3 0 342.90 142.86 41.40 o 1 3 0 1041.81 778.32 30.66 o 2 3 0 337446.84 360854.47 8883.08 o 3 3 0 2125.43 1608.39 41.62 o 4 3 0 429.79 310.14 20.58 o 5 3 0 8.00 8.10 23.84 o 6 3 0 6044.23 6131.96 132.79 o 7 3 0 231.08 197.93 30.50 o 8 3 0 4805.26 5147.15 123.05 o 9 3 0 79.57 98.07 32.90 o 10 3 0 3495.94 3691.07 106.19 o 11 3 0 1361.01 1181.43 58.99 o 12 3 0 182.75 88.05 59.70 o 13 3 0 76.80 94.77 68.80 o 14 3 0 71.23 39.09 76.88 o 15 3 0 0.00 -66.14 73.16 o 16 3 0 36.49 -128.70 133.18 o -17 4 0 26.55 87.88 246.14 o -16 4 0 14.40 -38.11 258.97 o -15 4 0 6.37 164.09 232.14 o -14 4 0 1150.06 1179.77 280.36 o -13 4 0 39.19 -17.80 71.52 o -12 4 0 19.66 19.91 50.07 o -11 4 0 72.41 43.81 41.68 o -10 4 0 588.74 683.69 46.99 o -9 4 0 46.16 -31.25 31.25 o -8 4 0 11611.46 11630.91 286.84 o -7 4 0 2561.66 2538.35 83.62 o -6 4 0 650.66 697.53 38.81 o -5 4 0 119.34 84.03 25.75 o -4 4 0 451.22 489.93 28.73 o -3 4 0 8401.12 7253.78 195.53 o -2 4 0 217.47 130.33 23.04 o -1 4 0 1056.20 923.32 34.94 o 0 4 0 841.52 1469.73 49.04 o 1 4 0 3073.95 2269.60 61.59 o 2 4 0 18455.50 19584.50 480.41 o 3 4 0 33.08 -12.80 18.16 o 4 4 0 154.96 200.09 21.33 o 5 4 0 440.65 450.71 30.26 o 6 4 0 15730.71 16324.26 343.06 o 7 4 0 913.74 765.97 35.98 o 8 4 0 2773.59 3078.92 84.29 o 9 4 0 101.92 6.46 34.41 o 10 4 0 10763.45 11034.01 268.17 o 11 4 0 195.61 210.40 44.61 o 12 4 0 1387.88 1569.67 95.09 o 13 4 0 218.39 165.35 66.92 o 14 4 0 153.63 56.99 99.79 o 15 4 0 36.88 -24.12 71.44 o 16 4 0 13.91 -110.54 110.54 o -16 5 0 292.90 1136.61 316.91 o -15 5 0 7.43 24.50 231.37 o -14 5 0 253.52 154.37 237.20 o -13 5 0 1.11 -87.61 87.61 o -12 5 0 132.79 177.11 50.68 o -11 5 0 72.31 44.41 44.07 o -10 5 0 282.99 224.73 36.19 o -9 5 0 721.27 707.80 48.40 o -8 5 0 5922.69 5421.52 146.50 o -7 5 0 3085.14 2923.89 98.05 o -6 5 0 4278.69 4162.09 108.63 o -5 5 0 252.33 285.78 34.42 o -4 5 0 32.63 41.25 24.94 o -3 5 0 2442.51 2075.65 66.87 o -2 5 0 6881.93 6224.90 177.58 o -1 5 0 26.59 48.64 19.61 o 0 5 0 199.26 230.22 26.48 o 1 5 0 1921.62 1633.09 47.63 o 2 5 0 4489.50 4456.41 127.91 o 3 5 0 763.01 734.98 30.76 o 4 5 0 1957.06 2081.00 60.86 o 5 5 0 72.68 45.93 29.57 o 6 5 0 10429.38 10859.29 257.92 o 7 5 0 0.14 -29.04 29.04 o 8 5 0 28.35 53.85 29.65 o 9 5 0 6.79 7.18 34.76 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6 0 23.81 -10.80 55.32 o 13 6 0 0.09 -17.71 59.36 o 14 6 0 626.76 856.50 114.67 o 15 6 0 0.77 77.36 231.56 o -16 7 0 260.99 269.86 290.47 o -15 7 0 28.64 203.76 276.08 o -14 7 0 127.38 -115.88 221.26 o -13 7 0 278.04 360.34 171.33 o -12 7 0 1161.86 1173.79 82.53 o -11 7 0 91.93 -5.66 50.77 o -10 7 0 1.77 -42.13 42.13 o -9 7 0 4.89 -35.19 42.06 o -8 7 0 3713.20 3765.23 114.83 o -7 7 0 654.73 646.31 41.78 o -6 7 0 736.22 792.03 46.91 o -5 7 0 83.56 80.79 29.84 o -4 7 0 1632.23 1834.68 64.94 o -3 7 0 174.64 140.32 31.71 o -2 7 0 2540.92 2957.25 87.77 o -1 7 0 831.66 783.64 38.54 o 0 7 0 130.32 173.41 26.35 o 1 7 0 405.93 392.52 28.48 o 2 7 0 55208.73 59754.18 2003.68 o 3 7 0 366.70 260.03 36.56 o 4 7 0 1505.76 1736.60 58.34 o 5 7 0 862.96 729.95 37.01 o 6 7 0 0.68 28.59 29.15 o 7 7 0 22.10 -20.12 31.59 o 8 7 0 2.04 -26.84 26.84 o 9 7 0 256.82 181.91 46.03 o 10 7 0 1761.94 2236.37 82.38 o 11 7 0 154.33 100.95 73.42 o 12 7 0 948.69 953.29 93.17 o 13 7 0 9.61 14.52 114.08 o 14 7 0 203.97 114.38 91.28 o 15 7 0 40.60 384.18 234.87 o -16 8 0 17.42 -237.20 237.20 o -15 8 0 93.14 -75.83 224.76 o -14 8 0 18.62 26.44 221.26 o -13 8 0 739.53 698.20 162.99 o -12 8 0 1.10 -16.12 73.69 o -11 8 0 668.20 791.46 65.84 o -10 8 0 738.95 680.05 60.87 o -9 8 0 516.19 442.64 49.69 o -8 8 0 652.17 582.26 47.63 o -7 8 0 193.74 206.41 39.93 o -6 8 0 392.54 431.12 43.22 o -5 8 0 131.65 174.63 30.96 o -4 8 0 270.23 301.10 37.66 o -3 8 0 19.50 -1.85 35.35 o -2 8 0 2588.21 2997.01 97.97 o -1 8 0 29.33 30.10 33.01 o 0 8 0 864.18 943.72 48.29 o 1 8 0 232.21 214.17 34.03 o 2 8 0 1420.92 1722.70 62.73 o 3 8 0 697.92 639.29 41.48 o 4 8 0 10318.76 12763.43 322.87 o 5 8 0 426.98 446.05 34.70 o 6 8 0 414.57 319.29 31.92 o 7 8 0 237.08 247.50 43.49 o 8 8 0 4.90 -37.89 37.89 o 9 8 0 7.08 -40.01 40.01 o 10 8 0 96.89 52.28 46.82 o 11 8 0 0.36 26.07 72.23 o 12 8 0 276.96 285.19 76.88 o 13 8 0 347.90 435.60 127.60 o 14 8 0 257.12 339.08 223.20 o 15 8 0 8.52 -121.71 216.98 o -16 9 0 819.97 451.84 257.03 o -15 9 0 5.89 -16.33 227.48 o -14 9 0 43.39 23.72 218.53 o -13 9 0 1.28 46.86 148.75 o -12 9 0 443.57 417.00 87.59 o -11 9 0 853.42 1000.47 76.42 o -10 9 0 909.47 904.37 66.65 o -9 9 0 147.57 -3.06 50.33 o -8 9 0 47.41 67.53 41.33 o -7 9 0 116.69 65.14 35.80 o -6 9 0 688.95 766.24 55.48 o -5 9 0 488.79 586.47 43.88 o -4 9 0 420.45 651.07 42.38 o -3 9 0 102.42 99.89 35.98 o -2 9 0 2042.49 2044.24 74.68 o -1 9 0 0.01 9.19 34.42 o 0 9 0 411.17 338.83 42.05 o 1 9 0 751.75 834.60 54.79 o 2 9 0 5563.79 5914.86 185.81 o 3 9 0 648.24 494.23 39.96 o 4 9 0 422.21 456.57 40.09 o 5 9 0 35.93 48.19 29.98 o 6 9 0 251.59 226.20 38.70 o 7 9 0 77.62 94.43 40.45 o 8 9 0 672.89 682.41 49.23 o 9 9 0 0.87 -26.13 40.41 o 10 9 0 1528.64 1829.16 102.76 o 11 9 0 18.27 54.10 64.02 o 12 9 0 1969.52 2260.92 158.19 o 13 9 0 155.04 131.66 79.13 o 14 9 0 160.63 -139.99 244.20 o -15 10 0 0.18 -101.10 215.42 o -14 10 0 173.94 -25.66 257.42 o -13 10 0 135.96 155.16 257.61 o -12 10 0 167.07 93.81 185.85 o -11 10 0 128.52 49.89 83.50 o -10 10 0 4681.92 4879.57 162.49 o -9 10 0 77.89 75.54 49.64 o -8 10 0 27.90 2.65 41.86 o -7 10 0 103.52 106.72 41.96 o -6 10 0 161.36 137.63 40.80 o -5 10 0 204.13 184.04 37.56 o -4 10 0 118.80 40.85 36.65 o -3 10 0 64.80 41.45 35.28 o -2 10 0 221.81 194.53 36.91 o -1 10 0 37.42 -32.73 32.73 o 0 10 0 7986.76 7260.91 209.49 o 1 10 0 1.91 -31.81 34.49 o 2 10 0 21.09 13.88 39.11 o 3 10 0 114.55 102.40 38.76 o 4 10 0 1844.83 2169.09 80.16 o 5 10 0 64.96 34.91 39.90 o 6 10 0 185.65 182.19 39.11 o 7 10 0 113.05 78.13 40.16 o 8 10 0 22.05 26.54 46.44 o 9 10 0 168.05 165.15 51.14 o 10 10 0 536.82 587.70 117.26 o 11 10 0 38.49 57.63 104.45 o 12 10 0 11.99 -114.32 185.87 o -15 11 0 47.11 -54.83 225.92 o -14 11 0 11.45 -96.05 245.75 o -13 11 0 66.87 100.32 198.31 o -12 11 0 1.70 173.91 106.80 o -11 11 0 1415.20 1305.49 140.67 o -10 11 0 448.25 516.51 79.17 o -9 11 0 3.80 -38.18 38.18 o -8 11 0 14.24 -49.17 49.17 o -7 11 0 112.78 68.20 46.96 o -6 11 0 262.80 338.41 60.72 o -5 11 0 0.58 -37.71 37.71 o -4 11 0 168.94 200.74 41.18 o -3 11 0 4.23 -11.29 37.19 o -2 11 0 0.09 10.84 33.29 o -1 11 0 113.58 61.01 34.30 o 0 11 0 2489.64 2572.05 88.48 o 1 11 0 141.55 184.22 36.66 o 2 11 0 1395.50 1333.60 66.54 o 3 11 0 72.93 75.03 37.26 o 4 11 0 120.57 183.58 40.77 o 5 11 0 7.87 -40.30 41.91 o 6 11 0 118.14 90.47 46.67 o 7 11 0 76.00 55.45 47.86 o 8 11 0 49.16 46.66 63.47 o 9 11 0 22.54 96.54 56.20 o 10 11 0 131.31 129.07 307.97 o 11 11 0 14.42 -139.77 139.77 o 12 11 0 656.66 816.59 225.53 o -15 12 0 133.52 240.70 235.64 o -14 12 0 266.14 -156.59 222.23 o -13 12 0 56.65 -83.21 187.81 o -12 12 0 9.33 -55.81 107.09 o -11 12 0 2.84 -107.18 107.18 o -10 12 0 814.38 854.00 107.25 o -9 12 0 327.25 424.60 69.50 o -8 12 0 1835.93 1665.10 79.61 o -7 12 0 7.10 -46.18 46.18 o -6 12 0 237.25 169.00 50.55 o -5 12 0 83.31 102.45 41.20 o -4 12 0 1851.07 1811.70 76.89 o -3 12 0 101.73 97.30 43.99 o -2 12 0 640.30 683.65 49.03 o -1 12 0 1.61 -35.32 35.32 o 0 12 0 510.67 429.62 42.46 o 1 12 0 7.46 49.33 37.79 o 2 12 0 492.01 463.54 45.52 o 3 12 0 585.88 603.76 52.22 o 4 12 0 0.51 -46.98 46.98 o 5 12 0 222.72 168.61 48.46 o 6 12 0 358.02 316.08 60.58 o 7 12 0 0.38 -50.74 50.74 o 8 12 0 201.88 114.32 61.29 o 9 12 0 7.72 -138.01 223.81 o 10 12 0 4.52 9.50 125.38 o 11 12 0 15.23 253.63 140.18 o 12 12 0 110.00 96.82 265.20 o -13 13 0 22.52 127.15 191.70 o -12 13 0 11.34 -78.15 135.51 o -11 13 0 116.41 -27.05 120.84 o -10 13 0 12.74 -37.85 102.87 o -9 13 0 8.34 -53.93 86.71 o -8 13 0 5824.07 5567.88 188.78 o -7 13 0 966.30 913.65 62.80 o -6 13 0 200.45 100.61 48.08 o -5 13 0 332.50 287.02 46.46 o -4 13 0 2971.60 3173.60 115.25 o -3 13 0 0.76 -39.67 39.67 o -2 13 0 1734.57 1650.04 73.64 o -1 13 0 17.39 -19.90 51.11 o 0 13 0 181.28 156.60 46.02 o 1 13 0 239.89 219.71 46.33 o 2 13 0 452.73 468.16 56.78 o 3 13 0 5.17 17.94 47.13 o 4 13 0 8.71 -8.34 66.91 o 5 13 0 12.04 33.57 48.10 o 6 13 0 3.85 23.44 50.61 o 7 13 0 0.36 -51.37 54.23 o 8 13 0 16.99 61.20 86.57 o 9 13 0 15.58 -134.30 134.30 o 10 13 0 83.76 259.89 128.66 o 11 13 0 230.24 199.51 161.48 o 12 13 0 36.59 -276.08 276.08 o -12 14 0 10.48 307.60 172.65 o -11 14 0 17.67 -102.13 102.13 o -10 14 0 288.74 342.13 105.06 o -9 14 0 179.07 143.06 95.08 o -8 14 0 263.51 318.17 71.54 o -7 14 0 2.25 -46.75 57.33 o -6 14 0 1938.15 2164.53 95.55 o -5 14 0 531.29 505.31 57.38 o -4 14 0 822.06 923.74 61.99 o -3 14 0 560.64 565.71 56.35 o -2 14 0 75.35 58.63 46.23 o -1 14 0 0.07 -48.77 48.77 o 0 14 0 5520.93 5417.45 204.24 o 1 14 0 483.79 373.56 55.72 o 2 14 0 85.34 90.10 51.52 o 3 14 0 1.10 42.89 49.11 o 4 14 0 972.13 1211.66 84.00 o 5 14 0 20.37 25.67 76.52 o 6 14 0 34.61 154.66 64.12 o 7 14 0 4.28 -80.35 80.35 o 8 14 0 132.75 364.30 109.77 o 9 14 0 320.53 189.98 199.29 o 10 14 0 1058.76 1235.08 196.02 o 11 14 0 11.37 -1.63 164.95 o -12 15 0 674.91 842.70 159.20 o -11 15 0 226.46 430.70 120.43 o -10 15 0 0.01 -86.94 86.94 o -9 15 0 585.50 484.94 92.72 o -8 15 0 1255.78 1205.87 162.04 o -7 15 0 1194.30 1371.74 97.24 o -6 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