#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217356.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217356_Fobs loop_ _publ_author_name 'Atalay, \,Sehriman' 'Erdem, Talip Kaya' 'Er\,sahin, Ferda' 'T\?ink\?il\?i\,c, Nihat' _publ_section_title ; (E)-4-Bromo-2-[(4-ethylphenyl)iminomethyl]phenol ; _journal_coeditor_code WN2219 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o92 _journal_volume 64 _journal_year 2008 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.2280 _cell_length_b 7.0292 _cell_length_c 30.2369 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.8103 _[local]_cod_data_source_file wn2219Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TEST STRUCTURE D:\DATA\F51_D\F51' _shelx_refln_list_code 4 _shelx_f_calc_maximum 309.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5795.65 5207.67 148.07 o 4 0 0 88.34 107.21 17.63 o 6 0 0 339.31 338.11 20.38 o 1 1 0 10554.06 10638.18 601.25 o 2 1 0 1950.43 1916.35 94.34 o 3 1 0 97.43 115.49 12.76 o 4 1 0 69.24 66.87 12.19 o 5 1 0 641.49 575.79 44.14 o 7 1 0 7.68 29.04 29.22 o 0 2 0 95703.86 95859.13 243.31 o 1 2 0 13119.35 13262.63 387.30 o 2 2 0 1543.59 1535.83 52.72 o 3 2 0 570.92 518.33 29.18 o 4 2 0 66.89 91.31 12.64 o 5 2 0 13.00 34.27 14.52 o 6 2 0 148.72 157.59 16.01 o 7 2 0 29.02 34.78 30.19 o 1 3 0 2192.23 2379.59 83.19 o 2 3 0 4814.04 5217.76 101.95 o 3 3 0 2.42 29.88 14.16 o 4 3 0 201.28 225.15 15.84 o 5 3 0 80.65 79.90 13.86 o 6 3 0 39.26 41.02 22.11 o 7 3 0 2.88 -1.32 22.19 o 0 4 0 1311.42 1249.33 130.98 o 1 4 0 5822.03 6354.65 148.08 o 2 4 0 23.30 29.32 15.63 o 3 4 0 202.79 230.84 16.08 o 4 4 0 29.18 11.98 16.32 o 5 4 0 5.17 19.70 22.55 o 6 4 0 7.78 -10.79 27.85 o 1 5 0 75.97 65.39 19.30 o 2 5 0 1415.97 1533.02 67.84 o 3 5 0 29.58 42.35 18.12 o 4 5 0 40.35 54.49 20.65 o 5 5 0 0.39 -12.50 19.59 o 6 5 0 15.07 5.81 28.70 o 0 6 0 434.69 471.27 66.30 o 1 6 0 546.81 609.54 23.70 o 2 6 0 123.87 158.12 18.58 o 3 6 0 0.55 16.36 19.92 o 4 6 0 11.93 1.25 18.59 o 5 6 0 0.17 -6.51 23.38 o 1 7 0 0.57 12.55 23.49 o 2 7 0 114.44 106.05 24.26 o 3 7 0 6.50 10.49 22.78 o 4 7 0 1.24 -8.30 28.30 o 0 8 0 171.30 151.01 44.26 o 1 8 0 12.11 18.84 35.64 o 2 8 0 15.64 12.15 32.52 o 2 0 1 11009.56 10925.28 342.56 o 4 0 1 1942.54 1910.57 75.49 o 6 0 1 362.12 333.63 20.57 o 0 1 1 1491.99 1676.84 81.29 o 1 1 1 2909.59 3617.35 294.16 o 2 1 1 557.44 515.99 29.73 o 3 1 1 2512.20 2438.36 118.13 o 4 1 1 18.18 25.69 9.30 o 5 1 1 39.11 63.79 9.95 o 6 1 1 0.63 -6.27 27.10 o 7 1 1 21.76 33.11 14.81 o 1 2 1 6058.46 6610.86 103.85 o 2 2 1 2864.88 3032.55 59.40 o 3 2 1 1420.89 1369.52 52.49 o 4 2 1 580.43 582.53 31.84 o 5 2 1 388.27 389.54 21.91 o 6 2 1 157.33 146.83 16.29 o 7 2 1 15.43 -9.98 21.28 o 0 3 1 3608.68 3502.83 57.86 o 1 3 1 207.03 358.33 34.80 o 2 3 1 1634.46 1595.89 122.34 o 3 3 1 290.65 319.89 19.59 o 4 3 1 43.57 67.54 13.99 o 5 3 1 25.81 23.98 9.80 o 6 3 1 1.30 15.98 12.65 o 7 3 1 1.54 -10.02 17.41 o 1 4 1 2428.12 2834.93 76.74 o 2 4 1 26.08 24.00 11.53 o 3 4 1 539.96 652.36 20.46 o 4 4 1 94.63 98.06 12.92 o 5 4 1 228.37 250.71 15.12 o 6 4 1 13.60 10.45 14.37 o 0 5 1 834.10 820.69 79.11 o 1 5 1 145.00 162.04 13.83 o 2 5 1 473.82 479.19 38.50 o 3 5 1 36.52 43.53 12.05 o 4 5 1 15.89 27.70 12.00 o 5 5 1 10.52 14.87 12.32 o 6 5 1 1.39 -1.61 16.33 o 1 6 1 314.83 341.89 16.05 o 2 6 1 105.89 131.87 15.16 o 3 6 1 1.92 10.14 12.87 o 4 6 1 77.45 86.47 13.71 o 5 6 1 13.84 11.67 16.25 o 0 7 1 54.12 50.68 23.77 o 1 7 1 34.67 50.65 17.57 o 2 7 1 83.76 67.53 17.01 o 3 7 1 27.44 20.19 18.05 o 4 7 1 7.22 20.39 19.16 o 1 8 1 16.63 11.23 23.90 o 2 8 1 19.38 27.11 22.68 o 0 0 2 4047.78 4692.21 1066.65 o 2 0 2 11735.89 12267.32 132.79 o 4 0 2 521.93 591.74 41.59 o 6 0 2 90.09 130.55 28.16 o 1 1 2 5316.67 5723.91 160.21 o 2 1 2 166.41 145.33 9.73 o 3 1 2 5484.80 5305.76 189.32 o 4 1 2 343.94 371.25 10.09 o 5 1 2 836.22 838.04 20.64 o 6 1 2 35.96 16.36 12.07 o 7 1 2 79.29 47.61 21.36 o 0 2 2 2174.91 2554.41 241.21 o 1 2 2 8542.53 9319.26 231.98 o 2 2 2 3289.63 3341.44 85.72 o 3 2 2 598.35 616.88 15.47 o 4 2 2 229.90 245.86 10.15 o 5 2 2 6.45 31.45 9.66 o 6 2 2 49.35 30.63 13.79 o 7 2 2 16.96 34.31 17.54 o 1 3 2 1106.45 1193.44 46.84 o 2 3 2 349.66 327.04 23.24 o 3 3 2 409.30 442.40 10.60 o 4 3 2 874.77 968.99 31.85 o 5 3 2 159.85 172.94 11.07 o 6 3 2 98.97 87.81 17.55 o 7 3 2 10.55 21.88 16.62 o 0 4 2 158.95 167.46 21.03 o 1 4 2 3737.37 4331.82 176.27 o 2 4 2 146.20 131.97 11.79 o 3 4 2 442.99 522.40 18.97 o 4 4 2 21.68 26.17 12.29 o 5 4 2 3.41 25.81 11.73 o 6 4 2 7.87 8.88 15.12 o 1 5 2 205.00 190.85 14.41 o 2 5 2 33.49 59.46 13.36 o 3 5 2 91.18 103.22 12.49 o 4 5 2 163.46 185.00 14.88 o 5 5 2 67.10 47.75 12.93 o 6 5 2 26.06 26.30 17.75 o 0 6 2 68.35 94.06 23.06 o 1 6 2 322.45 369.18 16.75 o 2 6 2 177.34 200.75 14.84 o 3 6 2 69.03 72.05 12.25 o 4 6 2 4.83 12.37 15.84 o 5 6 2 0.18 6.46 15.79 o 1 7 2 23.17 35.27 18.28 o 2 7 2 7.69 31.26 21.46 o 3 7 2 62.06 67.03 17.00 o 4 7 2 1.77 -3.14 14.51 o 0 8 2 14.78 18.30 38.96 o 1 8 2 8.49 3.99 21.24 o 2 8 2 28.56 17.57 20.84 o 2 0 3 158.54 171.25 16.43 o 4 0 3 1125.04 1116.52 16.07 o 6 0 3 272.66 310.91 28.60 o 0 1 3 2113.19 2045.62 57.17 o 1 1 3 23669.42 23610.43 827.82 o 2 1 3 1035.16 1004.18 11.49 o 3 1 3 1331.27 1295.21 34.43 o 4 1 3 57.48 62.77 8.85 o 5 1 3 25.22 42.59 9.29 o 6 1 3 20.23 8.03 13.60 o 7 1 3 57.51 66.13 21.25 o 1 2 3 1271.48 1236.17 22.21 o 2 2 3 97.37 87.25 11.51 o 3 2 3 580.38 625.68 18.01 o 4 2 3 382.48 376.48 9.80 o 5 2 3 176.21 189.32 12.63 o 6 2 3 92.71 72.95 13.30 o 7 2 3 35.87 23.84 18.66 o 0 3 3 4197.91 3869.54 205.22 o 1 3 3 1996.39 2010.79 62.64 o 2 3 3 2387.35 2414.48 64.30 o 3 3 3 234.51 233.25 10.14 o 4 3 3 171.55 251.46 20.10 o 5 3 3 25.98 20.64 10.23 o 6 3 3 44.06 52.74 19.10 o 7 3 3 3.69 8.43 14.10 o 1 4 3 292.66 306.24 13.45 o 2 4 3 164.30 165.72 12.82 o 3 4 3 414.98 479.32 19.26 o 4 4 3 11.66 12.87 12.75 o 5 4 3 118.00 137.93 12.75 o 6 4 3 1.97 13.44 19.68 o 0 5 3 559.96 550.51 54.60 o 1 5 3 90.15 91.72 14.89 o 2 5 3 573.55 650.86 24.80 o 3 5 3 4.49 4.59 12.63 o 4 5 3 37.36 40.59 12.27 o 5 5 3 14.48 30.61 13.06 o 6 5 3 3.01 7.16 17.62 o 1 6 3 0.84 6.37 15.79 o 2 6 3 90.17 99.23 15.53 o 3 6 3 73.72 65.64 15.39 o 4 6 3 28.17 40.26 14.31 o 5 6 3 12.64 17.02 15.99 o 0 7 3 10.55 6.26 25.72 o 1 7 3 80.06 80.19 21.12 o 2 7 3 38.48 27.46 21.09 o 3 7 3 7.96 11.84 15.90 o 4 7 3 2.49 2.82 21.27 o 1 8 3 8.89 9.37 23.87 o 2 8 3 18.25 -0.05 20.28 o 0 0 4 7127.00 6708.79 1188.82 o 2 0 4 3113.53 2975.51 97.83 o 4 0 4 188.97 175.72 20.75 o 6 0 4 50.23 67.39 30.81 o 1 1 4 2811.22 2989.06 105.38 o 2 1 4 821.27 757.77 37.20 o 3 1 4 2471.57 2498.59 63.68 o 4 1 4 446.77 444.06 9.44 o 5 1 4 710.77 741.45 27.04 o 6 1 4 55.05 49.50 15.93 o 7 1 4 57.35 49.88 15.02 o 0 2 4 2006.53 2134.78 149.13 o 1 2 4 690.02 684.82 17.68 o 2 2 4 941.65 906.96 21.56 o 3 2 4 407.64 392.31 10.00 o 4 2 4 46.30 59.79 8.74 o 5 2 4 36.09 40.62 10.53 o 6 2 4 12.74 20.92 12.30 o 7 2 4 4.62 7.69 14.97 o 1 3 4 259.07 270.17 14.22 o 2 3 4 1736.81 1945.51 87.39 o 3 3 4 196.90 208.02 9.58 o 4 3 4 1056.54 1179.81 36.38 o 5 3 4 26.18 17.37 10.55 o 6 3 4 149.41 145.86 19.58 o 7 3 4 3.65 3.28 15.15 o 0 4 4 37.59 31.08 20.96 o 1 4 4 506.65 548.77 15.92 o 2 4 4 75.65 81.72 12.30 o 3 4 4 225.53 263.82 11.15 o 4 4 4 10.65 13.02 13.19 o 5 4 4 26.27 34.71 15.16 o 6 4 4 1.17 4.85 15.87 o 1 5 4 10.59 18.12 14.37 o 2 5 4 289.78 360.03 28.14 o 3 5 4 8.59 23.34 11.98 o 4 5 4 205.88 251.48 19.57 o 5 5 4 55.83 67.73 11.29 o 6 5 4 26.97 7.96 17.12 o 0 6 4 136.76 161.68 24.93 o 1 6 4 34.02 46.09 15.83 o 2 6 4 70.24 83.65 14.35 o 3 6 4 8.31 3.51 15.86 o 4 6 4 27.28 39.81 14.70 o 5 6 4 3.97 6.59 18.42 o 1 7 4 3.61 8.90 21.61 o 2 7 4 3.44 5.53 17.26 o 3 7 4 1.80 3.06 18.35 o 4 7 4 2.26 22.60 24.72 o 0 8 4 13.16 20.13 56.58 o 1 8 4 0.91 -2.16 27.79 o 2 8 4 9.40 13.89 25.70 o 2 0 5 2916.21 2684.53 136.75 o 4 0 5 2548.08 2446.77 80.73 o 6 0 5 275.00 263.02 22.65 o 0 1 5 2139.48 1923.48 81.22 o 1 1 5 10196.59 10702.94 192.49 o 2 1 5 1139.88 1035.24 25.97 o 3 1 5 2136.25 2109.95 48.67 o 4 1 5 30.15 33.68 9.55 o 5 1 5 33.06 54.67 17.21 o 6 1 5 0.13 16.38 15.50 o 7 1 5 28.04 24.64 15.65 o 1 2 5 113.14 107.66 12.11 o 2 2 5 942.54 942.52 27.25 o 3 2 5 991.73 1021.97 24.03 o 4 2 5 858.17 819.41 20.61 o 5 2 5 281.05 272.53 21.43 o 6 2 5 114.49 105.30 16.53 o 7 2 5 20.78 38.34 13.59 o 0 3 5 4286.46 3947.08 156.55 o 1 3 5 641.15 660.57 28.90 o 2 3 5 2518.16 2585.47 59.93 o 3 3 5 198.76 205.16 10.00 o 4 3 5 100.48 133.26 10.79 o 5 3 5 10.54 19.58 10.90 o 6 3 5 0.05 16.80 13.92 o 7 3 5 1.12 13.09 18.41 o 1 4 5 33.97 40.61 14.63 o 2 4 5 73.73 74.05 11.77 o 3 4 5 537.82 585.77 24.05 o 4 4 5 5.80 6.62 13.36 o 5 4 5 173.99 197.47 15.42 o 6 4 5 4.17 12.12 17.72 o 0 5 5 870.94 871.73 86.73 o 1 5 5 44.51 65.29 14.68 o 2 5 5 574.38 655.90 36.52 o 3 5 5 85.65 86.06 14.27 o 4 5 5 44.68 56.80 14.54 o 5 5 5 0.69 14.56 14.97 o 6 5 5 1.03 6.12 18.43 o 1 6 5 12.61 10.44 16.52 o 2 6 5 104.22 112.69 17.07 o 3 6 5 28.90 23.23 13.17 o 4 6 5 17.03 21.25 13.16 o 5 6 5 13.62 2.39 17.24 o 0 7 5 38.23 22.64 28.70 o 1 7 5 37.81 53.91 24.95 o 2 7 5 15.03 11.84 16.31 o 3 7 5 63.88 61.62 17.47 o 4 7 5 6.74 -9.94 23.36 o 1 8 5 10.13 15.47 25.88 o 2 8 5 22.82 12.91 29.32 o 0 0 6 9281.49 8326.27 96.42 o 2 0 6 4876.58 4628.06 71.59 o 4 0 6 188.70 231.41 49.92 o 6 0 6 24.88 70.98 19.46 o 1 1 6 880.97 919.72 20.78 o 2 1 6 361.64 330.25 10.42 o 3 1 6 1747.31 1726.08 44.94 o 4 1 6 157.40 148.45 9.62 o 5 1 6 600.54 616.15 17.05 o 6 1 6 32.29 42.75 16.59 o 7 1 6 80.22 58.66 14.90 o 0 2 6 3385.94 3409.45 91.05 o 1 2 6 4020.32 4089.62 112.05 o 2 2 6 1890.36 1830.53 45.28 o 3 2 6 303.02 303.15 9.67 o 4 2 6 101.08 113.02 11.29 o 5 2 6 21.52 44.81 16.24 o 6 2 6 4.88 7.28 15.15 o 7 2 6 24.76 9.78 16.09 o 1 3 6 37.98 34.68 14.46 o 2 3 6 681.77 733.65 19.90 o 3 3 6 53.95 56.73 10.81 o 4 3 6 381.08 417.64 19.88 o 5 3 6 47.05 31.12 12.27 o 6 3 6 96.59 68.34 18.74 o 7 3 6 10.92 15.07 16.70 o 0 4 6 229.79 216.35 22.54 o 1 4 6 2053.14 2052.70 75.62 o 2 4 6 128.33 125.48 11.48 o 3 4 6 196.79 225.01 11.47 o 4 4 6 25.52 26.42 13.63 o 5 4 6 13.66 33.29 13.19 o 6 4 6 1.07 21.93 16.85 o 1 5 6 92.59 92.62 16.61 o 2 5 6 98.76 120.58 13.37 o 3 5 6 137.38 134.76 14.41 o 4 5 6 84.67 95.91 14.01 o 5 5 6 22.11 23.13 16.28 o 6 5 6 29.13 36.32 19.02 o 0 6 6 239.75 228.25 53.14 o 1 6 6 111.17 109.18 21.67 o 2 6 6 39.39 61.23 16.44 o 3 6 6 16.82 13.72 18.39 o 4 6 6 7.93 2.68 13.10 o 5 6 6 0.68 1.04 18.73 o 1 7 6 35.68 33.04 19.08 o 2 7 6 4.19 0.29 23.07 o 3 7 6 67.72 66.51 17.59 o 4 7 6 7.78 21.78 19.84 o 0 8 6 28.53 32.04 31.89 o 1 8 6 1.39 9.33 29.05 o 2 8 6 2.55 -3.61 20.25 o 2 0 7 1297.62 1344.64 129.02 o 4 0 7 1925.10 1873.04 77.65 o 6 0 7 209.02 185.55 28.25 o 0 1 7 1858.59 1704.54 73.33 o 1 1 7 7815.35 7614.41 163.23 o 2 1 7 622.97 559.21 13.21 o 3 1 7 1384.09 1254.35 25.80 o 4 1 7 84.10 81.07 9.06 o 5 1 7 218.37 229.79 14.65 o 6 1 7 13.48 25.30 19.26 o 7 1 7 23.62 16.51 12.87 o 1 2 7 569.67 584.20 19.58 o 2 2 7 426.09 447.10 17.15 o 3 2 7 634.13 654.97 19.12 o 4 2 7 679.83 676.21 15.92 o 5 2 7 276.26 250.40 19.35 o 6 2 7 61.55 50.93 22.16 o 7 2 7 3.24 18.35 15.54 o 0 3 7 3090.09 2923.40 67.68 o 1 3 7 341.99 301.40 13.85 o 2 3 7 1420.31 1412.01 34.83 o 3 3 7 161.59 171.15 12.17 o 4 3 7 271.28 307.87 13.69 o 5 3 7 45.39 27.21 16.98 o 6 3 7 35.94 36.84 14.07 o 7 3 7 0.11 14.47 14.86 o 1 4 7 221.77 210.82 18.63 o 2 4 7 20.61 11.14 11.80 o 3 4 7 362.11 374.26 14.69 o 4 4 7 17.55 12.54 14.86 o 5 4 7 161.26 174.55 17.51 o 6 4 7 3.76 -1.67 16.78 o 0 5 7 466.63 476.30 29.36 o 1 5 7 181.90 190.89 20.66 o 2 5 7 326.99 335.25 21.87 o 3 5 7 29.40 30.88 12.58 o 4 5 7 70.71 68.14 14.15 o 5 5 7 5.29 3.45 17.82 o 6 5 7 7.90 7.25 14.19 o 1 6 7 1.06 15.62 19.01 o 2 6 7 22.38 9.44 16.30 o 3 6 7 29.52 7.11 15.77 o 4 6 7 21.23 41.42 15.45 o 5 6 7 7.61 16.65 16.32 o 0 7 7 3.60 -8.10 28.28 o 1 7 7 87.54 69.71 19.76 o 2 7 7 16.16 14.99 18.76 o 3 7 7 18.69 5.53 25.48 o 4 7 7 1.19 -3.76 21.56 o 1 8 7 11.32 5.62 23.57 o 2 8 7 8.05 4.42 19.41 o 0 0 8 7314.81 6951.70 918.52 o 2 0 8 4684.45 4756.12 114.64 o 4 0 8 185.25 177.81 13.03 o 1 1 8 411.95 423.15 22.56 o 2 1 8 514.53 484.78 10.50 o 3 1 8 3028.84 2826.85 73.79 o 4 1 8 410.08 411.64 11.97 o 5 1 8 773.17 812.31 91.30 o 6 1 8 50.09 51.32 14.40 o 7 1 8 51.21 32.13 12.93 o 0 2 8 2357.23 2362.69 101.74 o 1 2 8 963.40 918.06 27.60 o 2 2 8 1588.06 1609.24 30.84 o 3 2 8 594.23 559.40 24.90 o 4 2 8 61.23 80.41 12.34 o 5 2 8 3.62 11.04 12.22 o 6 2 8 11.98 -0.79 18.49 o 7 2 8 10.86 18.55 16.80 o 1 3 8 16.09 10.72 12.59 o 2 3 8 888.68 853.05 24.73 o 3 3 8 331.66 319.84 15.61 o 4 3 8 1134.47 1227.55 60.40 o 5 3 8 74.08 64.42 17.33 o 6 3 8 141.11 156.30 19.35 o 7 3 8 4.65 -24.26 18.31 o 0 4 8 54.47 51.45 27.38 o 1 4 8 652.17 649.02 40.59 o 2 4 8 7.09 5.88 13.66 o 3 4 8 395.21 436.09 25.90 o 4 4 8 12.21 23.96 19.73 o 5 4 8 6.18 -2.04 16.15 o 6 4 8 1.82 -6.25 12.54 o 1 5 8 10.57 6.76 14.80 o 2 5 8 134.97 140.15 25.53 o 3 5 8 66.07 85.16 14.00 o 4 5 8 270.51 278.42 34.03 o 5 5 8 9.82 19.93 17.43 o 6 5 8 33.45 21.86 16.96 o 0 6 8 26.20 22.97 24.30 o 1 6 8 48.93 67.82 17.08 o 2 6 8 75.35 96.48 17.94 o 3 6 8 63.47 67.39 19.45 o 4 6 8 23.43 18.75 16.74 o 5 6 8 1.18 -5.79 13.87 o 1 7 8 2.82 6.12 19.40 o 2 7 8 4.42 7.28 18.83 o 3 7 8 21.57 26.39 17.72 o 4 7 8 6.42 25.63 18.06 o 0 8 8 1.48 -5.09 33.77 o 1 8 8 8.72 9.51 21.11 o 2 8 8 14.91 24.31 20.17 o 2 0 9 2680.68 2537.51 96.57 o 4 0 9 1000.34 988.93 36.25 o 6 0 9 102.90 96.67 20.30 o 0 1 9 2935.69 2590.43 39.93 o 1 1 9 11243.52 11281.99 238.70 o 2 1 9 733.67 694.63 13.39 o 3 1 9 1631.25 1472.54 41.54 o 4 1 9 11.96 11.06 9.75 o 5 1 9 96.78 149.38 20.86 o 6 1 9 17.59 14.58 13.79 o 7 1 9 39.96 19.05 14.22 o 1 2 9 196.00 224.44 16.46 o 2 2 9 652.53 624.82 12.72 o 3 2 9 717.31 673.40 20.65 o 4 2 9 345.84 358.83 11.76 o 5 2 9 162.87 197.28 16.81 o 6 2 9 39.78 28.61 14.23 o 7 2 9 11.70 6.03 14.45 o 0 3 9 5863.24 5168.14 184.43 o 1 3 9 850.86 848.51 30.87 o 2 3 9 1722.12 1689.27 41.91 o 3 3 9 201.64 180.64 11.87 o 4 3 9 34.70 32.91 13.00 o 5 3 9 6.15 2.05 15.13 o 6 3 9 51.73 25.34 15.66 o 1 4 9 100.22 85.75 14.59 o 2 4 9 22.29 15.82 12.74 o 3 4 9 439.36 418.61 23.23 o 4 4 9 3.34 7.60 12.37 o 5 4 9 119.28 120.64 16.55 o 6 4 9 2.39 3.05 12.67 o 0 5 9 1074.77 877.80 66.80 o 1 5 9 64.36 56.41 14.64 o 2 5 9 284.98 290.88 25.08 o 3 5 9 52.48 50.77 15.08 o 4 5 9 12.30 18.44 12.57 o 5 5 9 4.38 7.10 12.52 o 1 6 9 3.63 16.56 17.01 o 2 6 9 102.97 125.20 16.89 o 3 6 9 34.40 19.36 15.78 o 4 6 9 33.81 37.81 15.13 o 5 6 9 18.51 5.93 14.08 o 0 7 9 18.26 0.61 29.81 o 1 7 9 38.10 35.55 19.16 o 2 7 9 6.00 9.42 15.98 o 3 7 9 34.92 17.99 15.82 o 4 7 9 1.83 14.20 16.61 o 1 8 9 6.20 -4.30 23.05 o 2 8 9 28.02 15.75 19.51 o 0 0 10 8201.45 7915.68 171.89 o 2 0 10 1788.22 1670.20 36.31 o 4 0 10 585.72 562.30 34.00 o 6 0 10 6.25 -9.04 17.31 o 1 1 10 802.83 791.62 61.76 o 2 1 10 262.59 271.80 12.06 o 3 1 10 1530.99 1532.31 40.21 o 4 1 10 121.15 121.85 12.07 o 5 1 10 842.97 943.73 89.23 o 6 1 10 11.91 3.47 17.15 o 7 1 10 6.77 7.35 15.23 o 0 2 10 1227.34 1076.36 77.84 o 1 2 10 2600.06 2432.28 63.39 o 2 2 10 557.96 513.81 13.94 o 3 2 10 703.75 657.21 22.17 o 4 2 10 326.83 320.03 12.15 o 5 2 10 8.38 17.68 15.44 o 6 2 10 7.63 3.68 10.29 o 7 2 10 11.50 7.48 13.19 o 1 3 10 168.80 178.57 12.14 o 2 3 10 617.24 586.33 16.38 o 3 3 10 92.49 102.44 10.96 o 4 3 10 283.78 288.35 28.32 o 5 3 10 84.61 79.49 25.86 o 6 3 10 31.17 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41.01 13.23 o 5 2 22 1.69 0.94 13.26 o 1 3 22 51.23 42.77 12.26 o 2 3 22 181.36 162.89 13.84 o 3 3 22 56.60 65.15 13.05 o 4 3 22 150.03 146.04 18.83 o 5 3 22 29.54 10.94 17.00 o 0 4 22 3.13 17.33 19.65 o 1 4 22 645.92 613.44 25.36 o 2 4 22 8.50 14.12 13.09 o 3 4 22 35.31 36.18 13.66 o 4 4 22 4.23 10.08 16.22 o 5 4 22 0.84 -0.10 17.63 o 1 5 22 30.39 26.97 15.76 o 2 5 22 40.19 22.26 14.82 o 3 5 22 21.68 14.96 15.74 o 4 5 22 29.88 26.93 14.91 o 0 6 22 38.73 7.14 27.58 o 1 6 22 67.19 54.41 17.12 o 2 6 22 31.48 24.54 16.68 o 3 6 22 4.63 14.73 16.60 o 2 0 23 466.58 487.34 23.18 o 4 0 23 258.51 303.59 24.48 o 6 0 23 59.04 66.26 37.60 o 0 1 23 131.66 143.74 17.25 o 1 1 23 767.17 837.65 23.02 o 2 1 23 62.10 55.36 13.88 o 3 1 23 77.89 95.41 12.41 o 4 1 23 3.35 10.35 12.66 o 5 1 23 5.16 -4.28 15.34 o 1 2 23 171.91 173.41 12.46 o 2 2 23 147.91 159.68 12.93 o 3 2 23 230.78 247.46 16.00 o 4 2 23 67.52 61.70 12.86 o 5 2 23 54.30 50.70 14.19 o 0 3 23 375.15 367.70 23.35 o 1 3 23 62.42 64.45 12.14 o 2 3 23 131.97 125.10 16.41 o 3 3 23 3.04 22.34 13.03 o 4 3 23 10.69 14.63 12.63 o 5 3 23 3.37 -10.41 17.09 o 1 4 23 134.27 126.63 13.49 o 2 4 23 1.50 8.50 13.72 o 3 4 23 124.38 100.75 14.13 o 4 4 23 4.93 2.85 15.85 o 0 5 23 94.63 91.28 20.27 o 1 5 23 28.91 21.91 14.94 o 2 5 23 11.32 3.24 14.84 o 3 5 23 4.60 16.75 16.04 o 4 5 23 5.08 8.62 18.71 o 1 6 23 25.93 3.61 17.05 o 2 6 23 6.04 2.89 16.90 o 0 0 24 6883.06 8086.87 1275.53 o 2 0 24 663.18 655.01 24.15 o 4 0 24 33.63 44.53 21.90 o 1 1 24 324.95 350.35 21.19 o 2 1 24 85.56 90.45 16.51 o 3 1 24 81.17 91.91 13.10 o 4 1 24 18.83 27.27 14.33 o 5 1 24 76.45 51.59 14.61 o 0 2 24 2874.91 3272.05 156.87 o 1 2 24 657.03 689.78 27.30 o 2 2 24 213.66 243.90 16.64 o 3 2 24 70.87 77.41 15.31 o 4 2 24 17.71 23.54 11.15 o 5 2 24 5.48 7.04 17.19 o 1 3 24 110.79 109.23 12.85 o 2 3 24 290.79 285.73 18.01 o 3 3 24 5.73 7.27 13.21 o 4 3 24 48.55 15.86 13.40 o 5 3 24 9.59 10.50 18.39 o 0 4 24 122.38 119.94 18.86 o 1 4 24 446.39 393.52 22.22 o 2 4 24 6.70 18.77 13.52 o 3 4 24 38.58 35.22 14.51 o 4 4 24 3.96 18.76 16.18 o 1 5 24 20.39 13.29 14.66 o 2 5 24 117.28 66.25 16.38 o 3 5 24 3.72 19.34 17.47 o 0 6 24 31.24 23.76 44.09 o 1 6 24 52.38 34.90 18.20 o 2 6 24 16.44 8.14 16.32 o 2 0 25 524.30 461.83 40.48 o 4 0 25 392.69 428.32 32.09 o 0 1 25 142.85 169.89 18.26 o 1 1 25 179.44 176.06 17.94 o 2 1 25 50.60 32.16 15.75 o 3 1 25 252.59 255.79 17.71 o 4 1 25 3.25 29.69 14.04 o 5 1 25 14.50 24.57 15.76 o 1 2 25 100.22 124.16 19.38 o 2 2 25 165.00 160.61 13.68 o 3 2 25 100.74 82.81 17.05 o 4 2 25 157.98 141.79 18.48 o 5 2 25 65.36 59.83 14.98 o 0 3 25 361.80 356.13 43.17 o 1 3 25 10.15 15.51 12.55 o 2 3 25 176.45 212.56 16.38 o 3 3 25 43.30 37.14 14.37 o 4 3 25 9.75 17.55 15.07 o 5 3 25 3.07 3.90 27.04 o 1 4 25 108.71 80.41 13.41 o 2 4 25 3.06 15.02 13.36 o 3 4 25 53.69 46.95 14.61 o 4 4 25 13.54 16.20 15.91 o 0 5 25 73.25 56.25 21.25 o 1 5 25 8.84 16.40 14.63 o 2 5 25 84.17 39.96 15.27 o 3 5 25 1.58 8.94 15.53 o 1 6 25 34.39 22.40 18.32 o 2 6 25 14.80 2.01 26.03 o 0 0 26 113.96 105.29 26.01 o 2 0 26 785.37 765.94 37.35 o 4 0 26 60.85 62.47 20.31 o 1 1 26 137.32 176.60 20.24 o 2 1 26 13.50 19.55 17.31 o 3 1 26 301.54 305.58 15.42 o 4 1 26 28.02 41.47 14.26 o 5 1 26 76.21 54.72 15.20 o 0 2 26 25.08 34.20 16.81 o 1 2 26 237.84 244.41 16.57 o 2 2 26 321.66 322.32 14.50 o 3 2 26 109.49 83.07 15.01 o 4 2 26 24.15 30.61 15.67 o 5 2 26 0.55 -2.53 15.84 o 1 3 26 66.31 73.36 13.23 o 2 3 26 28.35 33.98 16.68 o 3 3 26 34.21 25.39 15.45 o 4 3 26 77.36 54.68 15.09 o 0 4 26 34.40 31.34 20.41 o 1 4 26 156.37 139.05 15.59 o 2 4 26 10.05 2.59 13.72 o 3 4 26 98.37 79.78 14.57 o 4 4 26 0.72 2.31 16.00 o 1 5 26 12.70 2.85 15.33 o 2 5 26 5.95 -3.69 12.68 o 3 5 26 1.59 13.53 15.66 o 0 6 26 11.77 -11.68 26.27 o 1 6 26 17.66 18.17 17.68 o 2 0 27 127.53 164.27 61.22 o 4 0 27 149.62 166.47 23.38 o 0 1 27 106.00 113.03 18.34 o 1 1 27 1039.51 1234.11 50.17 o 2 1 27 79.79 75.66 14.02 o 3 1 27 171.14 162.97 16.37 o 4 1 27 3.50 -2.05 15.31 o 5 1 27 18.48 31.83 16.59 o 1 2 27 34.41 46.14 12.33 o 2 2 27 58.52 57.78 14.45 o 3 2 27 94.36 79.71 16.50 o 4 2 27 56.19 39.97 15.67 o 5 2 27 18.54 -32.31 35.40 o 0 3 27 282.72 325.14 41.78 o 1 3 27 125.13 119.90 13.01 o 2 3 27 235.92 227.09 17.73 o 3 3 27 32.58 18.37 15.72 o 4 3 27 10.90 2.74 16.40 o 1 4 27 26.61 6.21 14.33 o 2 4 27 8.10 3.40 13.91 o 3 4 27 77.12 48.75 14.74 o 0 5 27 72.03 70.54 21.81 o 1 5 27 5.44 4.88 14.72 o 2 5 27 73.13 36.76 15.05 o 0 0 28 349.54 338.32 25.05 o 2 0 28 156.23 166.10 26.32 o 4 0 28 11.04 -0.18 25.64 o 1 1 28 165.17 160.00 13.56 o 2 1 28 29.78 25.84 14.90 o 3 1 28 154.02 161.91 18.14 o 4 1 28 24.29 14.49 17.32 o 0 2 28 102.18 111.66 16.84 o 1 2 28 95.45 117.46 12.55 o 2 2 28 60.64 69.89 13.37 o 3 2 28 12.97 7.38 17.30 o 4 2 28 1.86 3.26 13.74 o 1 3 28 16.46 11.18 13.10 o 2 3 28 73.91 63.83 15.18 o 3 3 28 14.11 9.02 13.86 o 4 3 28 64.41 56.29 15.86 o 0 4 28 3.48 -14.18 18.77 o 1 4 28 53.24 33.34 15.50 o 2 4 28 7.65 11.89 13.71 o 3 4 28 6.68 4.71 15.68 o 1 5 28 2.27 14.61 15.40 o 2 5 28 12.71 6.20 15.41 o 2 0 29 129.60 148.54 21.37 o 4 0 29 163.18 169.44 48.64 o 0 1 29 112.11 105.02 17.43 o 1 1 29 421.31 504.38 29.65 o 2 1 29 49.10 49.79 14.78 o 3 1 29 112.66 101.87 15.80 o 4 1 29 3.03 39.29 19.54 o 1 2 29 7.14 14.49 12.16 o 2 2 29 44.35 45.97 14.05 o 3 2 29 42.25 41.52 17.88 o 4 2 29 62.72 38.18 15.69 o 0 3 29 315.07 336.31 24.34 o 1 3 29 40.70 23.72 13.19 o 2 3 29 143.21 148.29 13.07 o 3 3 29 9.34 10.09 14.14 o 1 4 29 6.30 16.62 14.81 o 2 4 29 2.78 16.88 14.16 o 3 4 29 23.80 13.02 15.51 o 0 5 29 83.86 76.86 22.05 o 1 5 29 4.01 -0.67 13.10 o 0 0 30 404.16 453.30 25.92 o 2 0 30 208.43 234.95 18.89 o 4 0 30 16.48 20.00 24.44 o 1 1 30 13.38 25.42 13.45 o 2 1 30 18.92 35.69 14.56 o 3 1 30 82.61 82.85 15.90 o 4 1 30 10.82 8.13 21.27 o 0 2 30 130.84 149.48 17.58 o 1 2 30 119.95 144.82 13.55 o 2 2 30 77.15 89.04 14.47 o 3 2 30 20.61 18.04 16.79 o 4 2 30 8.71 8.14 14.99 o 1 3 30 0.25 2.64 12.91 o 2 3 30 48.89 42.85 14.00 o 3 3 30 1.61 2.83 15.95 o 0 4 30 1.82 21.52 19.29 o 1 4 30 71.04 52.91 15.06 o 2 4 30 2.28 18.91 13.85 o 1 5 30 2.21 4.50 36.63 o 2 0 31 86.65 64.51 19.82 o 4 0 31 78.49 73.15 25.71 o 0 1 31 46.46 61.41 19.17 o 1 1 31 245.06 321.76 15.81 o 2 1 31 17.70 24.86 14.52 o 3 1 31 47.36 54.96 16.05 o 4 1 31 3.19 42.48 24.04 o 1 2 31 25.68 26.95 13.30 o 2 2 31 29.57 6.34 13.81 o 3 2 31 45.57 21.48 17.04 o 0 3 31 117.24 154.81 20.77 o 1 3 31 13.95 -8.54 13.25 o 2 3 31 48.62 42.13 13.99 o 3 3 31 9.31 11.90 14.71 o 1 4 31 14.07 11.03 14.69 o 2 4 31 0.98 16.27 15.02 o 0 0 32 254.66 327.18 25.07 o 2 0 32 147.50 175.60 18.58 o 1 1 32 25.08 51.78 13.06 o 2 1 32 6.81 5.53 13.08 o 3 1 32 83.46 84.74 15.34 o 0 2 32 90.11 74.89 18.18 o 1 2 32 70.74 60.02 12.90 o 2 2 32 53.56 54.99 14.28 o 3 2 32 14.83 3.19 18.24 o 1 3 32 3.44 23.25 13.74 o 2 3 32 17.24 5.68 14.52 o 0 4 32 2.79 5.20 19.97 o 1 4 32 45.30 33.91 15.65 o 2 0 33 93.35 84.34 19.75 o 0 1 33 42.65 65.46 18.51 o 1 1 33 200.76 251.72 18.95 o 2 1 33 18.69 13.81 13.61 o 3 1 33 35.67 19.45 15.79 o 1 2 33 8.04 19.25 13.38 o 2 2 33 31.57 20.39 14.35 o 3 2 33 31.05 25.62 16.89 o 0 3 33 123.88 148.37 37.96 o 1 3 33 21.10 30.95 14.00 o 2 3 33 50.20 62.98 15.32 o 0 0 34 176.69 205.25 56.98 o 2 0 34 49.58 28.83 21.51 o 1 1 34 9.73 14.43 13.69 o 2 1 34 10.01 11.81 13.73 o 3 1 34 40.05 4.22 28.26 o 0 2 34 49.02 79.06 19.91 o 1 2 34 55.92 51.02 14.18 o 2 2 34 14.89 18.30 14.23 o 1 3 34 0.51 -0.18 13.70 o 2 0 35 57.55 24.15 18.85 o 0 1 35 17.84 28.39 20.09 o 1 1 35 98.89 91.27 14.33 o 2 1 35 6.68 7.80 13.91 o 1 2 35 6.16 20.10 13.52 o 0 0 36 146.02 201.38 29.80 o 1 1 36 3.36 -6.88 14.53 o 0 2 36 53.02 56.37 20.87 o