#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/73/2217361.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217361_Fobs loop_ _publ_author_name 'Li, Zhiying' 'Shang, Donglin' 'Guo, Jianping' _publ_section_title ; Bis[1,3-bis(diphenylphosphinoylimino)isoindolinato-\k^3^O,N,O']calcium(II) ; _journal_coeditor_code WW2103 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m160 _journal_volume 64 _journal_year 2008 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 126.172 _cell_angle_gamma 90.000 _cell_length_a 26.3506 _cell_length_b 12.4790 _cell_length_c 21.1997 _exptl_crystal_F_000 2344.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file ww2103Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s297p in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 437.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22638.54 27178.01 841.72 o 4 0 0 12131.84 13352.55 295.22 o 6 0 0 3855.49 4544.71 105.19 o 8 0 0 2596.79 4015.74 95.66 o 10 0 0 11167.33 15293.33 343.48 o 12 0 0 126.68 92.28 10.56 o 14 0 0 422.41 410.34 41.19 o 16 0 0 4679.77 4061.41 164.27 o 18 0 0 129.37 107.49 33.48 o 20 0 0 68.13 38.11 29.07 o 22 0 0 2.83 -26.43 21.36 o 24 0 0 417.64 477.30 59.02 o 1 1 0 30740.13 35232.66 545.28 o 3 1 0 34981.61 42242.37 753.76 o 5 1 0 4517.39 4742.88 90.21 o 7 1 0 57880.67 61559.61 1099.71 o 9 1 0 48.58 17.81 6.99 o 11 1 0 29.99 17.96 13.60 o 13 1 0 221.11 189.81 20.64 o 15 1 0 2110.74 1877.75 64.79 o 17 1 0 1260.69 1077.47 49.22 o 19 1 0 4.14 14.66 26.98 o 21 1 0 0.12 11.42 15.95 o 23 1 0 453.37 424.60 38.93 o 25 1 0 272.18 316.34 38.84 o 0 2 0 17907.62 20024.50 440.46 o 2 2 0 6195.76 6591.52 85.46 o 4 2 0 18425.10 21132.93 329.05 o 6 2 0 5973.96 6211.39 101.00 o 8 2 0 2824.55 2725.01 58.10 o 10 2 0 95.03 86.32 10.47 o 12 2 0 1723.43 1850.92 46.51 o 14 2 0 3488.93 3457.15 192.63 o 16 2 0 2089.70 2164.78 73.41 o 18 2 0 1169.73 1039.78 59.25 o 20 2 0 0.07 15.60 17.56 o 22 2 0 487.21 413.06 37.84 o 24 2 0 338.43 368.16 52.20 o 1 3 0 14958.64 16586.64 232.29 o 3 3 0 3653.97 3540.61 48.40 o 5 3 0 6827.48 7605.66 110.12 o 7 3 0 285.75 303.47 10.73 o 9 3 0 1877.62 2559.39 57.02 o 11 3 0 20.52 15.48 8.87 o 13 3 0 36.74 10.62 10.73 o 15 3 0 127.42 122.03 33.17 o 17 3 0 483.69 366.25 31.07 o 19 3 0 415.95 374.92 33.39 o 21 3 0 780.33 690.18 184.04 o 23 3 0 85.60 115.50 27.38 o 0 4 0 7346.26 7400.47 170.64 o 2 4 0 8611.35 9384.18 122.24 o 4 4 0 2608.60 2720.42 43.15 o 6 4 0 92.20 142.13 8.59 o 8 4 0 16091.48 16727.68 238.10 o 10 4 0 7156.01 7030.67 105.97 o 12 4 0 1800.24 1647.83 44.50 o 14 4 0 1381.76 1274.21 96.36 o 16 4 0 1027.84 1066.86 47.88 o 18 4 0 11.21 38.27 25.77 o 20 4 0 1946.61 1817.08 71.80 o 22 4 0 1163.86 1150.80 46.31 o 24 4 0 163.33 235.29 29.35 o 3 5 0 89.15 30.08 4.49 o 5 5 0 18283.83 19354.77 273.27 o 7 5 0 9021.67 9063.00 133.02 o 9 5 0 3741.14 3628.97 59.42 o 11 5 0 2016.30 2018.56 44.61 o 13 5 0 140.71 137.41 17.41 o 15 5 0 2195.72 2179.49 50.61 o 17 5 0 253.85 222.95 21.50 o 19 5 0 140.86 136.78 18.96 o 21 5 0 20.99 97.65 17.53 o 23 5 0 7.47 28.97 35.21 o 0 6 0 75492.66 79622.11 1744.08 o 2 6 0 3627.00 3640.19 57.83 o 4 6 0 10.94 27.86 7.53 o 6 6 0 299.75 303.10 12.13 o 8 6 0 5283.06 5215.31 81.60 o 10 6 0 558.48 582.71 21.31 o 12 6 0 756.76 671.30 37.12 o 14 6 0 4.80 13.01 10.57 o 16 6 0 82.96 113.17 17.23 o 18 6 0 16.83 44.90 14.57 o 20 6 0 77.32 102.05 21.04 o 22 6 0 103.89 73.78 19.97 o 1 7 0 39.90 32.66 8.28 o 3 7 0 6551.31 6656.39 100.98 o 5 7 0 7766.88 7963.31 108.06 o 7 7 0 5492.93 5903.88 91.34 o 9 7 0 334.68 322.45 16.42 o 11 7 0 3275.23 3426.58 68.17 o 13 7 0 13.12 12.26 10.97 o 15 7 0 147.00 164.62 16.53 o 17 7 0 2158.11 2239.99 55.31 o 19 7 0 96.97 190.51 23.19 o 21 7 0 91.71 177.39 46.58 o 0 8 0 421.51 448.76 26.48 o 2 8 0 1378.75 1211.10 37.13 o 4 8 0 4072.84 4215.03 113.15 o 6 8 0 3775.19 3776.56 84.17 o 8 8 0 901.97 906.44 34.71 o 10 8 0 626.18 609.91 35.98 o 12 8 0 3144.07 3000.48 142.63 o 14 8 0 717.09 592.52 50.66 o 16 8 0 2260.99 2252.62 80.19 o 18 8 0 8.49 32.91 21.12 o 20 8 0 134.97 161.23 48.46 o 1 9 0 314.46 325.95 17.56 o 3 9 0 224.06 232.45 15.73 o 5 9 0 252.97 292.32 25.38 o 7 9 0 463.00 418.32 23.83 o 9 9 0 955.52 759.88 55.28 o 11 9 0 1979.92 1739.39 92.84 o 13 9 0 3792.49 3522.08 109.04 o 15 9 0 26.14 33.33 19.44 o 17 9 0 137.32 205.24 30.39 o 19 9 0 1013.80 1105.92 87.89 o 0 10 0 539.70 545.81 32.90 o 2 10 0 3.19 -3.85 9.24 o 4 10 0 11.93 1.47 9.81 o 6 10 0 387.12 364.35 20.05 o 8 10 0 601.87 592.75 64.75 o 10 10 0 153.38 136.68 24.62 o 12 10 0 260.74 239.92 48.24 o 14 10 0 319.98 318.14 32.78 o 16 10 0 94.26 170.28 29.31 o 18 10 0 913.22 956.42 56.73 o 1 11 0 1384.97 1207.73 35.82 o 3 11 0 39.48 45.94 12.86 o 5 11 0 1682.06 1594.22 49.69 o 7 11 0 1313.85 1263.64 56.38 o 9 11 0 24.90 13.29 17.81 o 11 11 0 125.21 182.35 45.04 o 13 11 0 171.76 218.13 44.06 o 15 11 0 60.37 125.51 27.34 o 0 12 0 190.32 200.92 25.25 o 2 12 0 236.35 235.45 18.58 o 4 12 0 60.34 76.81 16.75 o 6 12 0 2182.35 1867.59 85.77 o 8 12 0 66.81 24.52 18.97 o 10 12 0 143.92 209.45 28.39 o 12 12 0 0.15 -13.05 19.02 o 14 12 0 26.21 43.67 25.15 o 1 13 0 44.77 55.32 14.61 o 3 13 0 2683.50 2616.21 62.40 o 5 13 0 203.30 260.95 25.73 o 7 13 0 5.88 14.44 28.74 o 9 13 0 121.38 153.42 27.08 o 11 13 0 22.64 13.86 20.43 o 0 14 0 1472.54 1486.57 64.79 o 2 14 0 1303.39 1266.38 42.25 o 4 14 0 453.66 436.57 39.98 o 6 14 0 18.01 11.34 19.10 o 8 14 0 16.05 14.61 19.94 o -25 1 1 28.25 63.27 23.57 o -23 1 1 42.29 27.34 21.14 o -21 1 1 1481.60 1378.86 60.58 o -19 1 1 829.74 666.81 40.90 o -17 1 1 3874.49 3575.20 105.75 o -15 1 1 478.53 467.73 32.38 o -13 1 1 954.31 972.33 49.73 o -11 1 1 12460.84 14372.76 266.78 o -9 1 1 9768.13 11031.89 205.20 o -7 1 1 6534.79 7518.07 140.74 o -5 1 1 14984.52 15394.16 278.53 o -3 1 1 1217.44 1298.95 26.45 o -1 1 1 22176.65 25777.12 582.65 o 1 1 1 9696.87 10473.49 146.41 o 3 1 1 191739.22 215927.97 3324.78 o 5 1 1 22295.26 23022.33 359.01 o 7 1 1 6813.54 5519.94 91.21 o 9 1 1 16646.78 17551.79 322.43 o 11 1 1 113.76 73.66 8.03 o 13 1 1 55.84 86.43 11.62 o 15 1 1 1296.09 1362.00 54.19 o 17 1 1 56.66 57.22 22.91 o 19 1 1 5079.48 4278.72 127.56 o 21 1 1 31.15 42.50 19.38 o 23 1 1 86.49 160.22 28.41 o -24 2 1 82.09 47.93 20.53 o -22 2 1 994.08 1019.58 52.33 o -20 2 1 1913.91 1666.85 66.82 o -18 2 1 419.89 383.03 31.60 o -16 2 1 61.23 89.84 19.52 o -14 2 1 3492.82 3563.42 78.43 o -12 2 1 14980.61 15380.86 286.48 o -10 2 1 2570.02 2400.25 53.68 o -8 2 1 247.37 171.95 10.79 o -6 2 1 1727.50 1432.12 28.51 o -4 2 1 18510.38 20692.82 321.99 o -2 2 1 32535.25 35529.43 491.98 o 0 2 1 3976.14 4950.58 70.99 o 2 2 1 36310.70 37882.18 585.91 o 4 2 1 431.94 352.83 9.92 o 6 2 1 7.95 8.13 4.37 o 8 2 1 129.56 119.89 11.39 o 10 2 1 26985.30 30235.00 549.38 o 12 2 1 3118.05 3080.14 69.19 o 14 2 1 152.95 183.61 30.40 o 16 2 1 917.79 802.74 42.28 o 18 2 1 1508.17 1377.52 131.16 o 20 2 1 1813.63 1740.11 70.56 o 22 2 1 80.42 148.14 28.73 o 24 2 1 0.82 16.07 22.17 o -25 3 1 58.79 61.41 23.63 o -23 3 1 83.98 95.72 23.20 o -21 3 1 1473.37 1460.67 153.53 o -19 3 1 1881.95 1776.79 67.66 o -17 3 1 2086.17 2027.23 147.24 o -15 3 1 9432.60 9652.08 188.98 o -13 3 1 21160.46 21070.25 389.32 o -11 3 1 6292.42 6544.51 186.03 o -9 3 1 617.57 675.78 22.08 o -7 3 1 156.93 119.27 7.39 o -5 3 1 5494.31 5137.26 84.30 o -3 3 1 11677.86 12183.99 156.76 o -1 3 1 65274.73 73025.51 1127.28 o 1 3 1 6793.88 7553.37 98.35 o 3 3 1 10693.66 11601.82 164.38 o 5 3 1 5412.75 4892.55 73.33 o 7 3 1 2414.98 2647.33 49.25 o 9 3 1 443.78 418.42 18.26 o 11 3 1 5317.92 5216.05 107.34 o 13 3 1 996.26 837.83 29.88 o 15 3 1 416.31 398.57 33.92 o 17 3 1 5.73 -2.87 15.78 o 19 3 1 1799.34 1796.42 181.49 o 21 3 1 1049.21 1081.96 56.16 o 23 3 1 74.76 148.87 27.75 o -24 4 1 54.41 97.30 32.38 o -22 4 1 1.73 11.50 44.82 o -20 4 1 414.33 435.65 35.58 o -18 4 1 708.69 729.89 42.19 o -16 4 1 4423.22 4337.25 96.24 o -14 4 1 180.62 170.84 27.45 o -12 4 1 16.18 5.31 9.78 o -10 4 1 15621.37 17945.23 284.99 o -8 4 1 6518.68 6831.67 112.83 o -6 4 1 16577.94 17176.37 242.64 o -4 4 1 141.90 149.18 6.27 o -2 4 1 12117.55 12267.64 174.26 o 0 4 1 64950.77 73900.05 1142.13 o 2 4 1 5958.29 4815.94 65.21 o 4 4 1 2738.52 1947.51 33.00 o 6 4 1 355.94 316.96 11.00 o 8 4 1 9.83 12.26 5.74 o 10 4 1 8527.98 8176.23 138.88 o 12 4 1 6702.61 6595.16 156.48 o 14 4 1 2672.31 2566.25 55.51 o 16 4 1 1310.18 1260.23 43.18 o 18 4 1 233.46 198.34 31.79 o 20 4 1 42.23 55.24 16.84 o 22 4 1 351.35 415.85 49.82 o -23 5 1 196.42 249.91 25.36 o -21 5 1 65.27 67.36 27.42 o -19 5 1 161.27 165.79 21.33 o -17 5 1 5814.33 5852.69 243.60 o -15 5 1 736.56 749.29 45.69 o -13 5 1 961.30 896.96 27.18 o -11 5 1 3321.73 3337.15 64.50 o -9 5 1 2387.69 2034.53 36.82 o -7 5 1 3.53 44.13 6.35 o -5 5 1 395.94 397.23 14.53 o -3 5 1 17651.92 20126.34 258.20 o -1 5 1 2803.54 3112.59 56.57 o 1 5 1 871.18 706.16 15.95 o 3 5 1 7616.71 7671.49 102.36 o 5 5 1 16251.52 18186.32 257.83 o 7 5 1 1130.35 1087.77 23.55 o 9 5 1 81.82 129.10 9.59 o 11 5 1 932.24 888.69 27.09 o 13 5 1 50.31 50.70 12.06 o 15 5 1 2306.30 2168.16 133.49 o 17 5 1 2.98 30.61 13.62 o 19 5 1 20.38 27.40 15.79 o 21 5 1 242.51 294.95 27.34 o 23 5 1 196.01 255.71 45.02 o -22 6 1 90.38 118.98 21.53 o -20 6 1 567.28 567.21 32.86 o -18 6 1 87.65 113.46 30.14 o -16 6 1 886.61 826.86 29.31 o -14 6 1 662.29 633.19 26.77 o -12 6 1 134.28 143.84 13.40 o -10 6 1 641.85 629.54 21.55 o -8 6 1 7.10 -4.07 6.04 o -6 6 1 452.47 523.53 14.72 o -4 6 1 344.80 418.95 13.33 o -2 6 1 21741.56 23445.16 330.22 o 0 6 1 17244.16 17440.68 278.55 o 2 6 1 410.97 192.17 8.96 o 4 6 1 195.04 118.63 7.30 o 6 6 1 357.79 245.19 11.20 o 8 6 1 5604.71 5710.43 88.96 o 10 6 1 2128.94 2017.27 44.99 o 12 6 1 116.60 122.89 13.45 o 14 6 1 11415.70 11353.04 193.67 o 16 6 1 50.42 65.46 27.26 o 18 6 1 0.06 38.61 21.69 o 20 6 1 190.38 201.87 44.54 o 22 6 1 13.11 41.85 21.81 o -23 7 1 68.60 95.07 31.16 o -21 7 1 277.77 350.07 29.65 o -19 7 1 0.74 21.32 15.08 o -17 7 1 6.33 -3.78 11.88 o -15 7 1 704.11 755.60 28.75 o -13 7 1 232.23 248.22 22.29 o -11 7 1 1685.76 1634.46 39.31 o -9 7 1 1289.82 1269.61 30.16 o -7 7 1 38.60 52.29 9.90 o -5 7 1 820.26 607.34 15.01 o -3 7 1 14646.23 15655.82 224.52 o -1 7 1 5953.87 6277.48 108.81 o 1 7 1 6361.62 6429.19 111.13 o 3 7 1 5274.21 5001.75 78.36 o 5 7 1 1739.38 1546.79 31.85 o 7 7 1 2987.91 2671.69 47.03 o 9 7 1 644.16 567.41 47.02 o 11 7 1 472.49 511.72 42.87 o 13 7 1 566.20 474.95 23.25 o 15 7 1 308.35 353.02 21.37 o 17 7 1 306.60 457.49 25.33 o 19 7 1 56.50 121.14 39.54 o 21 7 1 8.36 56.80 27.94 o -22 8 1 633.42 608.57 71.58 o -20 8 1 985.55 1101.07 86.55 o -18 8 1 205.19 264.17 34.36 o -16 8 1 1394.84 1317.03 57.25 o -14 8 1 5714.04 5557.90 151.75 o -12 8 1 710.69 696.73 39.39 o -10 8 1 1266.66 1214.07 69.39 o -8 8 1 1735.47 1848.24 87.02 o -6 8 1 2657.53 2837.65 82.00 o -4 8 1 0.59 1.82 8.51 o -2 8 1 981.19 923.06 26.83 o 0 8 1 107.49 102.91 11.76 o 2 8 1 4409.63 4254.89 79.36 o 4 8 1 483.25 471.38 25.34 o 6 8 1 10.45 22.52 10.67 o 8 8 1 959.76 885.06 49.34 o 10 8 1 291.75 297.57 27.64 o 12 8 1 286.65 259.53 49.66 o 14 8 1 1405.30 1346.91 70.70 o 16 8 1 357.42 490.69 77.64 o 18 8 1 338.26 423.11 53.09 o 20 8 1 753.50 814.53 78.41 o -19 9 1 477.82 494.31 41.64 o -17 9 1 45.84 62.51 23.75 o -15 9 1 1536.12 1509.37 63.31 o -13 9 1 1838.26 1767.54 68.06 o -11 9 1 117.14 111.92 33.92 o -9 9 1 308.44 364.25 30.03 o -7 9 1 96.37 111.50 15.07 o -5 9 1 142.73 117.28 13.12 o -3 9 1 744.95 650.26 23.75 o -1 9 1 709.20 640.44 23.47 o 1 9 1 150.25 171.54 13.82 o 3 9 1 1796.37 1652.17 47.25 o 5 9 1 389.28 378.74 19.01 o 7 9 1 4066.18 4081.40 92.54 o 9 9 1 166.11 171.87 24.27 o 11 9 1 85.95 80.20 22.49 o 13 9 1 63.57 87.93 41.41 o 15 9 1 39.30 24.57 26.76 o 17 9 1 150.64 165.45 27.56 o 19 9 1 948.99 1042.05 89.65 o -18 10 1 503.46 515.52 42.52 o -16 10 1 392.24 463.94 39.13 o -14 10 1 6.22 -15.69 18.13 o -12 10 1 881.41 815.92 47.13 o -10 10 1 174.78 117.65 23.15 o -8 10 1 2123.34 1844.65 107.53 o -6 10 1 86.80 125.77 14.41 o -4 10 1 2092.55 1929.59 72.83 o -2 10 1 0.65 -10.48 8.90 o 0 10 1 1100.14 1103.36 32.37 o 2 10 1 5632.13 5531.99 102.76 o 4 10 1 825.89 739.95 26.77 o 6 10 1 450.34 360.08 23.54 o 8 10 1 519.81 397.21 33.42 o 10 10 1 4.01 33.55 19.09 o 12 10 1 1615.38 1617.11 66.57 o 14 10 1 938.12 964.83 52.44 o 16 10 1 241.23 220.50 31.72 o -17 11 1 718.49 743.85 51.42 o -15 11 1 486.02 504.76 42.11 o -13 11 1 785.51 699.11 46.32 o -11 11 1 113.37 168.75 25.83 o -9 11 1 497.76 523.64 38.69 o -7 11 1 370.08 414.28 27.04 o -5 11 1 128.04 104.62 14.08 o -3 11 1 441.13 425.20 21.91 o -1 11 1 5118.25 4740.59 92.57 o 1 11 1 135.82 128.96 14.67 o 3 11 1 69.26 97.31 13.53 o 5 11 1 47.17 36.70 12.37 o 7 11 1 425.27 453.53 35.90 o 9 11 1 415.43 437.79 54.30 o 11 11 1 3.68 -1.79 20.16 o 13 11 1 189.71 175.53 28.98 o 15 11 1 225.88 361.34 38.66 o -14 12 1 8.25 31.62 22.69 o -12 12 1 973.89 1010.62 56.25 o -10 12 1 579.77 562.85 41.74 o -8 12 1 1684.61 1583.34 65.64 o -6 12 1 98.48 117.70 14.69 o -4 12 1 598.92 558.54 41.77 o -2 12 1 254.62 296.37 19.99 o 0 12 1 2330.56 2550.68 59.52 o 2 12 1 417.06 378.99 22.31 o 4 12 1 0.93 14.91 23.48 o 6 12 1 1549.66 1588.40 64.95 o 8 12 1 1985.28 2021.92 77.40 o 10 12 1 14.33 14.93 19.73 o 12 12 1 655.66 688.42 48.09 o 14 12 1 370.75 420.89 41.59 o -11 13 1 0.32 22.07 20.37 o -9 13 1 873.76 859.07 99.12 o -7 13 1 1099.09 1044.80 53.11 o -5 13 1 372.55 399.21 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43.06 o -16 6 23 159.10 240.24 33.48 o -24 0 24 1198.87 1301.97 86.79 o -22 0 24 364.39 370.69 50.88 o -20 0 24 224.74 249.55 44.28 o -18 0 24 52.70 56.17 27.09 o -16 0 24 1819.11 1847.54 106.16 o -14 0 24 722.94 962.99 78.85 o -12 0 24 113.27 142.29 40.75 o -10 0 24 122.68 132.38 40.97 o -25 1 24 54.55 0.08 19.97 o -23 1 24 569.96 652.77 46.02 o -21 1 24 90.15 131.67 25.85 o -19 1 24 117.04 134.31 24.36 o -17 1 24 446.87 437.16 38.34 o -15 1 24 409.12 448.80 39.90 o -13 1 24 7.97 24.60 21.55 o -11 1 24 87.87 31.13 24.84 o -24 2 24 1.22 -16.46 18.93 o -22 2 24 168.30 196.04 30.21 o -20 2 24 609.60 553.86 69.28 o -18 2 24 1.55 7.11 28.96 o -16 2 24 11.99 48.69 21.82 o -14 2 24 59.99 88.92 25.75 o -12 2 24 61.44 89.77 28.63 o -23 3 24 192.65 192.86 30.07 o -21 3 24 44.68 44.72 19.40 o -19 3 24 33.86 15.11 18.81 o -17 3 24 47.17 64.18 20.61 o -15 3 24 0.22 33.22 19.63 o -13 3 24 0.63 12.22 20.47 o -20 4 24 6.09 40.19 20.38 o -18 4 24 29.63 27.61 19.80 o -16 4 24 298.06 379.68 38.15 o -14 4 24 55.48 113.85 26.72 o -21 1 25 217.17 219.08 34.23 o -19 1 25 33.67 38.57 22.81 o -17 1 25 420.52 487.53 42.21 o