#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217376.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217376_Fobs loop_ _publ_author_name 'Zhang, Bing-Yu' 'Yang, Qian' 'Nie, Jing-Jing' _publ_section_title ; Bis(pyrimidine-2-carboxylato-\k^2^N,O)copper(II) ; _journal_coeditor_code XU2383 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m7 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.025 _cell_angle_gamma 90.000 _cell_length_a 5.1408 _cell_length_b 13.2624 _cell_length_c 7.6735 _exptl_crystal_F_000 310.00 _reflns_d_resolution_high 0.7701 _[local]_cod_data_source_file xu2383Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' zby-3 in P21/C' _shelx_refln_list_code 4 _shelx_f_calc_maximum 169.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 635.83 596.92 6.85 o 2 0 0 2868.07 2740.30 50.15 o 3 0 0 4403.04 4538.97 47.13 o 4 0 0 371.79 361.01 7.16 o 5 0 0 2.78 3.25 1.02 o 6 0 0 587.76 574.80 11.03 o 1 1 0 1976.29 1961.13 14.29 o 2 1 0 13.94 9.24 0.60 o 3 1 0 670.71 723.10 6.95 o 4 1 0 0.17 0.51 0.45 o 5 1 0 0.63 0.84 0.61 o 6 1 0 65.67 61.53 2.38 o 0 2 0 1238.00 1324.16 19.87 o 1 2 0 305.83 297.69 3.36 o 2 2 0 43.14 20.11 0.81 o 3 2 0 2205.23 2185.02 17.23 o 4 2 0 639.98 626.54 6.89 o 5 2 0 132.08 127.80 3.01 o 6 2 0 234.62 234.38 4.22 o 1 3 0 470.76 537.49 5.44 o 2 3 0 601.81 664.99 6.39 o 3 3 0 27.29 29.13 1.14 o 4 3 0 71.31 71.72 2.00 o 5 3 0 2.86 3.27 0.70 o 6 3 0 3.44 3.29 0.86 o 0 4 0 4903.79 4576.93 69.70 o 1 4 0 530.92 474.95 5.14 o 2 4 0 2344.99 2303.23 17.97 o 3 4 0 1476.01 1514.76 13.07 o 4 4 0 1718.81 1734.01 13.61 o 5 4 0 440.85 440.76 5.53 o 6 4 0 272.99 270.68 5.16 o 1 5 0 3094.95 3406.64 28.88 o 2 5 0 7.83 11.72 2.34 o 3 5 0 3.19 4.81 0.65 o 4 5 0 1122.59 1111.25 10.92 o 5 5 0 293.25 294.03 4.96 o 6 5 0 1.54 2.35 0.97 o 0 6 0 3321.00 3254.96 33.81 o 1 6 0 2906.52 3024.12 26.10 o 2 6 0 120.74 82.37 6.67 o 3 6 0 1639.53 1662.83 16.35 o 4 6 0 44.25 46.83 1.78 o 5 6 0 29.62 28.50 1.74 o 6 6 0 150.11 154.58 4.67 o 1 7 0 40.91 39.43 2.32 o 2 7 0 149.96 177.75 3.26 o 3 7 0 31.31 27.67 1.49 o 4 7 0 0.90 0.44 0.62 o 5 7 0 5.63 4.05 1.47 o 6 7 0 3.57 3.92 2.32 o 0 8 0 762.09 724.17 9.72 o 1 8 0 1467.06 1450.80 14.09 o 2 8 0 1243.71 1269.03 18.09 o 3 8 0 297.75 307.41 5.11 o 4 8 0 487.97 510.11 9.02 o 5 8 0 306.50 318.70 12.01 o 1 9 0 26.54 25.32 1.33 o 2 9 0 18.46 19.54 1.32 o 3 9 0 51.39 48.41 2.02 o 4 9 0 103.86 102.92 4.08 o 5 9 0 0.16 1.51 1.24 o 0 10 0 4.31 5.59 1.41 o 1 10 0 1509.63 1475.22 14.86 o 2 10 0 386.16 391.73 5.93 o 3 10 0 355.40 373.31 7.83 o 4 10 0 345.72 355.12 11.95 o 5 10 0 305.46 341.38 12.79 o 1 11 0 194.47 197.52 3.89 o 2 11 0 41.66 34.13 1.78 o 3 11 0 37.66 34.76 3.55 o 4 11 0 15.06 17.12 2.29 o 5 11 0 4.75 6.94 2.72 o 0 12 0 530.27 520.70 8.78 o 1 12 0 278.96 285.73 4.33 o 2 12 0 317.65 297.88 6.85 o 3 12 0 246.96 253.70 6.72 o 4 12 0 117.74 122.77 7.46 o 1 13 0 1.62 2.56 0.80 o 2 13 0 16.72 14.49 1.91 o 3 13 0 0.62 0.73 1.06 o 4 13 0 0.66 3.85 2.37 o 0 14 0 165.78 167.18 4.82 o 1 14 0 425.63 406.62 6.68 o 2 14 0 231.85 235.56 6.42 o 3 14 0 127.12 126.22 7.51 o 1 15 0 7.11 6.11 1.13 o 2 15 0 0.41 -0.28 1.05 o 3 15 0 17.15 21.42 4.04 o 0 16 0 193.86 171.73 7.58 o 1 16 0 68.09 63.13 3.38 o 2 16 0 179.94 177.23 5.87 o 1 17 0 0.81 1.22 1.16 o -6 1 1 129.46 132.97 3.41 o -5 1 1 307.55 320.49 4.91 o -4 1 1 390.93 381.86 4.89 o -3 1 1 1617.79 1610.38 13.13 o -2 1 1 1399.70 1353.77 9.51 o -1 1 1 2382.59 2421.01 20.77 o 0 1 1 7959.19 7190.43 62.64 o 1 1 1 1582.84 1603.49 10.75 o 2 1 1 1801.73 1721.87 10.87 o 3 1 1 1152.76 1149.09 11.58 o 4 1 1 878.70 883.56 13.41 o 5 1 1 101.70 101.13 2.42 o 6 1 1 426.05 418.05 6.08 o -6 2 1 29.50 27.45 1.83 o -5 2 1 0.08 -0.42 0.54 o -4 2 1 3.60 3.78 0.65 o -3 2 1 8.76 10.64 0.77 o -2 2 1 7.51 5.83 0.58 o -1 2 1 329.63 367.01 3.34 o 0 2 1 819.89 872.75 8.81 o 1 2 1 199.47 204.65 2.16 o 2 2 1 48.74 49.71 1.09 o 3 2 1 63.12 78.92 2.75 o 4 2 1 29.69 30.58 1.59 o 5 2 1 41.10 34.17 1.55 o 6 2 1 1.17 1.86 0.80 o -6 3 1 69.63 74.16 4.13 o -5 3 1 278.34 281.10 4.59 o -4 3 1 633.97 631.75 7.28 o -3 3 1 1243.08 1196.47 12.05 o -2 3 1 717.14 681.26 8.79 o -1 3 1 1405.92 1389.84 12.29 o 0 3 1 3524.96 3363.56 47.28 o 1 3 1 998.91 970.20 8.61 o 2 3 1 1427.97 1376.20 10.08 o 3 3 1 1817.83 1830.30 13.54 o 4 3 1 796.74 800.06 7.53 o 5 3 1 155.06 158.31 3.08 o 6 3 1 238.39 237.51 4.86 o -6 4 1 4.02 3.19 1.20 o -5 4 1 12.41 12.42 1.39 o -4 4 1 4.54 5.16 0.88 o -3 4 1 0.78 0.92 0.46 o -2 4 1 7.68 7.41 0.69 o -1 4 1 211.98 241.69 2.76 o 0 4 1 638.09 667.67 6.56 o 1 4 1 96.09 96.23 1.72 o 2 4 1 29.43 34.24 1.05 o 3 4 1 91.50 95.66 1.88 o 4 4 1 0.23 0.17 0.45 o 5 4 1 1.81 1.91 0.67 o 6 4 1 4.71 3.50 1.03 o -6 5 1 186.97 195.07 6.85 o -5 5 1 424.03 424.89 6.15 o -4 5 1 1185.35 1177.36 11.41 o -3 5 1 1145.78 1129.72 11.36 o -2 5 1 1061.17 1072.46 9.44 o -1 5 1 2459.98 2456.98 21.30 o 0 5 1 2095.83 1989.76 21.49 o 1 5 1 673.44 622.14 6.56 o 2 5 1 2063.20 2053.90 18.64 o 3 5 1 1495.50 1500.33 14.85 o 4 5 1 795.26 805.80 8.51 o 5 5 1 500.01 492.94 6.94 o 6 5 1 359.88 353.58 8.67 o -6 6 1 0.67 0.82 1.08 o -5 6 1 25.16 22.61 1.93 o -4 6 1 227.97 232.22 5.23 o -3 6 1 0.07 -0.20 0.38 o -2 6 1 259.00 306.82 5.29 o -1 6 1 44.86 56.13 1.53 o 0 6 1 67.24 67.19 2.54 o 1 6 1 1358.57 1551.41 14.38 o 2 6 1 2.33 1.30 0.43 o 3 6 1 161.15 170.02 3.41 o 4 6 1 136.08 140.00 3.41 o 5 6 1 5.17 4.89 1.41 o 6 6 1 0.95 1.63 1.37 o -6 7 1 92.59 94.62 4.66 o -5 7 1 6.92 4.68 1.14 o -4 7 1 381.84 379.97 5.46 o -3 7 1 360.34 354.56 4.83 o -2 7 1 74.25 57.56 1.82 o -1 7 1 2821.61 2853.64 24.98 o 0 7 1 2034.18 2036.09 18.39 o 1 7 1 457.98 448.06 8.02 o 2 7 1 819.28 795.24 8.84 o 3 7 1 1141.00 1168.38 19.70 o 4 7 1 29.67 26.99 3.27 o 5 7 1 248.41 249.67 6.80 o 6 7 1 91.33 87.88 6.59 o -5 8 1 23.76 20.95 2.35 o -4 8 1 0.08 0.44 0.69 o -3 8 1 7.77 7.66 1.00 o -2 8 1 9.49 13.67 1.41 o -1 8 1 18.31 18.17 1.84 o 0 8 1 0.67 0.26 0.33 o 1 8 1 10.55 16.12 1.35 o 2 8 1 77.37 85.91 2.26 o 3 8 1 28.31 29.10 2.44 o 4 8 1 8.02 8.27 3.46 o 5 8 1 0.58 0.70 1.13 o -5 9 1 102.48 104.81 8.47 o -4 9 1 657.10 659.80 19.38 o -3 9 1 443.46 472.13 6.91 o -2 9 1 508.76 522.04 6.94 o -1 9 1 2099.00 2074.35 19.37 o 0 9 1 1679.42 1622.59 13.44 o 1 9 1 658.28 657.78 7.99 o 2 9 1 1211.25 1204.75 16.24 o 3 9 1 945.02 952.97 14.34 o 4 9 1 161.40 170.92 5.43 o 5 9 1 283.78 309.19 8.08 o -5 10 1 16.31 20.95 3.99 o -4 10 1 1.49 3.62 1.54 o -3 10 1 123.33 118.50 3.23 o -2 10 1 0.19 0.35 0.58 o -1 10 1 8.49 9.13 0.98 o 0 10 1 59.70 58.63 1.67 o 1 10 1 5.72 7.65 0.96 o 2 10 1 91.42 90.54 3.46 o 3 10 1 2.74 1.88 1.05 o 4 10 1 3.84 5.63 1.87 o 5 10 1 0.86 2.93 1.82 o -5 11 1 137.77 153.83 8.59 o -4 11 1 433.66 419.04 13.63 o -3 11 1 93.20 105.29 3.97 o -2 11 1 212.45 217.84 4.38 o -1 11 1 260.98 259.71 3.96 o 0 11 1 7.51 7.33 0.80 o 1 11 1 273.02 274.89 7.44 o 2 11 1 145.14 168.08 4.95 o 3 11 1 421.66 441.68 18.87 o 4 11 1 168.08 187.02 6.16 o 5 11 1 338.96 364.83 9.39 o -4 12 1 61.49 57.95 5.23 o -3 12 1 10.62 8.41 1.55 o -2 12 1 10.94 14.21 1.42 o -1 12 1 789.13 764.59 8.18 o 0 12 1 384.01 377.62 8.09 o 1 12 1 1.84 3.06 1.04 o 2 12 1 15.98 16.82 6.14 o 3 12 1 203.31 183.17 5.81 o 4 12 1 35.08 42.17 4.35 o -4 13 1 100.43 106.11 7.18 o -3 13 1 302.99 307.15 11.38 o -2 13 1 269.79 267.08 6.57 o -1 13 1 590.26 576.67 6.96 o 0 13 1 983.73 927.21 11.05 o 1 13 1 303.37 292.40 9.13 o 2 13 1 573.45 519.62 10.08 o 3 13 1 248.50 264.26 7.30 o 4 13 1 83.89 93.09 4.62 o -3 14 1 17.56 12.79 3.10 o -2 14 1 15.51 14.50 2.86 o -1 14 1 10.54 12.19 1.39 o 0 14 1 57.16 56.01 2.33 o 1 14 1 0.18 0.24 0.69 o 2 14 1 3.30 2.96 1.38 o 3 14 1 17.74 21.27 2.63 o -3 15 1 53.47 64.12 5.51 o -2 15 1 146.28 138.19 6.83 o -1 15 1 143.39 141.47 6.71 o 0 15 1 165.11 161.49 5.15 o 1 15 1 292.18 289.09 5.79 o 2 15 1 58.67 55.90 5.83 o 3 15 1 63.27 71.13 4.10 o -2 16 1 13.37 22.12 3.52 o -1 16 1 4.28 6.90 2.32 o 0 16 1 31.19 33.57 2.76 o 1 16 1 60.02 64.86 2.82 o 2 16 1 7.34 6.68 1.38 o 0 17 1 15.30 17.62 3.28 o -6 0 2 4.78 6.15 2.25 o -5 0 2 239.44 230.55 5.71 o -4 0 2 440.51 418.04 12.34 o -3 0 2 1260.57 1285.18 17.73 o -2 0 2 324.25 293.38 3.61 o -1 0 2 28657.03 22990.96 451.11 o 0 0 2 4625.42 4225.47 63.59 o 1 0 2 2862.92 2927.72 24.93 o 2 0 2 10127.26 9715.96 165.12 o 3 0 2 345.91 308.09 4.55 o 4 0 2 135.32 148.83 3.36 o 5 0 2 487.11 477.44 7.42 o 6 0 2 314.07 299.98 8.96 o -6 1 2 28.65 32.70 2.93 o -5 1 2 2.20 1.63 0.68 o -4 1 2 233.02 242.20 3.66 o -3 1 2 82.87 86.70 1.67 o -2 1 2 91.26 106.35 1.48 o -1 1 2 5435.33 5535.55 48.73 o 0 1 2 1456.97 1588.66 10.63 o 1 1 2 206.52 208.58 2.08 o 2 1 2 153.14 176.37 1.98 o 3 1 2 31.77 42.59 1.22 o 4 1 2 52.32 49.84 2.51 o 5 1 2 170.83 152.92 2.73 o 6 1 2 3.81 2.24 0.97 o -6 2 2 30.38 27.50 4.97 o -5 2 2 398.24 398.89 6.52 o -4 2 2 807.70 762.37 13.31 o -3 2 2 31.84 23.81 0.79 o -2 2 2 1423.76 1408.78 18.50 o -1 2 2 1637.66 1641.78 14.77 o 0 2 2 201.10 265.23 2.64 o 1 2 2 1262.66 1144.16 9.13 o 2 2 2 1901.60 1876.26 13.09 o 3 2 2 535.80 483.06 4.84 o 4 2 2 413.74 416.57 4.85 o 5 2 2 718.90 657.96 7.13 o 6 2 2 132.13 130.00 4.09 o -6 3 2 4.74 6.95 2.56 o -5 3 2 56.55 49.90 5.01 o -4 3 2 48.10 47.53 1.88 o -3 3 2 5.00 5.55 1.08 o -2 3 2 109.63 111.31 1.90 o -1 3 2 13.50 12.92 0.81 o 0 3 2 10.53 18.91 0.81 o 1 3 2 1351.99 1491.96 11.81 o 2 3 2 9.80 9.05 0.53 o 3 3 2 0.22 0.81 0.56 o 4 3 2 85.94 87.38 2.25 o 5 3 2 2.76 3.84 0.88 o 6 3 2 1.67 1.04 1.01 o -6 4 2 67.26 67.67 3.82 o -5 4 2 960.32 962.04 15.05 o -4 4 2 666.47 654.47 10.72 o -3 4 2 1076.33 1115.23 11.50 o -2 4 2 1202.05 1222.71 11.69 o -1 4 2 2789.63 2728.23 20.43 o 0 4 2 199.59 151.38 1.94 o 1 4 2 1566.16 1514.58 11.98 o 2 4 2 2430.13 2430.76 18.62 o 3 4 2 1081.04 1081.96 10.06 o 4 4 2 1305.46 1298.19 14.25 o 5 4 2 454.78 461.82 7.61 o 6 4 2 416.48 410.60 7.75 o -6 5 2 84.25 76.37 3.43 o -5 5 2 48.97 50.69 3.55 o -4 5 2 13.87 18.26 3.96 o -3 5 2 32.85 38.70 2.91 o -2 5 2 1767.85 1889.82 17.24 o -1 5 2 72.13 74.14 1.40 o 0 5 2 189.87 219.12 3.57 o 1 5 2 180.16 211.81 2.89 o 2 5 2 4.80 4.95 0.61 o 3 5 2 1920.05 2009.96 19.46 o 4 5 2 159.27 151.71 4.38 o 5 5 2 8.57 11.77 1.55 o 6 5 2 21.45 26.75 2.38 o -6 6 2 89.95 94.76 4.19 o -5 6 2 20.18 21.18 1.94 o -4 6 2 595.37 596.48 8.81 o -3 6 2 154.89 153.41 4.42 o -2 6 2 437.84 433.70 6.89 o -1 6 2 2414.00 2477.62 21.71 o 0 6 2 3987.52 4072.50 34.42 o 1 6 2 276.86 216.66 3.15 o 2 6 2 1778.07 1719.91 20.08 o 3 6 2 1094.66 1124.31 15.43 o 4 6 2 16.21 13.52 1.82 o 5 6 2 362.69 373.85 8.57 o 6 6 2 79.09 80.96 10.33 o -6 7 2 21.23 19.08 2.16 o -5 7 2 38.50 40.27 2.75 o -4 7 2 94.46 92.34 4.78 o -3 7 2 11.73 10.96 1.20 o -2 7 2 21.48 19.17 1.17 o -1 7 2 134.13 138.41 2.63 o 0 7 2 15.58 19.06 1.01 o 1 7 2 567.31 653.04 7.22 o 2 7 2 32.14 36.09 2.17 o 3 7 2 23.38 26.64 3.40 o 4 7 2 63.19 63.91 3.21 o 5 7 2 3.52 3.68 1.41 o -5 8 2 170.94 177.08 4.84 o -4 8 2 268.63 261.16 5.58 o -3 8 2 564.19 562.45 9.64 o -2 8 2 688.86 723.74 8.44 o -1 8 2 830.99 799.34 7.56 o 0 8 2 1593.57 1550.69 14.84 o 1 8 2 602.58 579.30 9.12 o 2 8 2 684.32 725.46 23.57 o 3 8 2 601.19 609.51 13.15 o 4 8 2 361.70 381.52 8.47 o 5 8 2 152.17 155.11 5.61 o -5 9 2 24.96 29.14 2.78 o -4 9 2 1.27 2.39 1.19 o -3 9 2 32.65 36.98 3.35 o -2 9 2 59.34 66.25 2.14 o -1 9 2 41.28 41.69 1.40 o 0 9 2 0.33 0.93 0.49 o 1 9 2 2.68 1.70 0.78 o 2 9 2 112.62 113.58 3.84 o 3 9 2 102.32 110.81 4.18 o 4 9 2 0.03 1.34 1.10 o 5 9 2 7.62 8.47 1.91 o -5 10 2 80.12 81.55 4.08 o -4 10 2 351.54 360.60 11.85 o -3 10 2 184.78 205.80 5.58 o -2 10 2 735.05 757.97 11.70 o -1 10 2 65.82 68.40 2.96 o 0 10 2 955.33 937.81 10.44 o 1 10 2 398.79 368.25 8.38 o 2 10 2 255.83 290.53 6.69 o 3 10 2 862.78 851.67 13.90 o 4 10 2 252.35 280.31 7.54 o 5 10 2 179.08 187.36 10.49 o -5 11 2 6.94 6.38 1.80 o -4 11 2 27.89 27.59 2.60 o -3 11 2 10.67 10.07 1.77 o -2 11 2 15.88 17.51 1.86 o -1 11 2 203.88 205.20 4.03 o 0 11 2 391.97 371.80 6.90 o 1 11 2 43.99 36.86 2.31 o 2 11 2 1.04 0.68 1.30 o 3 11 2 56.52 63.68 3.68 o 4 11 2 30.73 42.61 3.36 o -4 12 2 114.51 118.60 4.81 o -3 12 2 268.85 276.28 6.98 o -2 12 2 78.78 88.90 5.22 o -1 12 2 348.40 342.62 7.19 o 0 12 2 586.34 576.53 8.31 o 1 12 2 137.90 135.10 4.47 o 2 12 2 377.01 378.53 21.41 o 3 12 2 307.77 313.70 7.95 o 4 12 2 108.83 115.57 5.13 o -4 13 2 3.28 3.87 2.32 o -3 13 2 1.20 1.70 1.58 o -2 13 2 15.44 12.87 1.86 o -1 13 2 2.64 2.08 1.04 o 0 13 2 1.25 0.28 0.68 o 1 13 2 0.30 -0.10 0.89 o 2 13 2 0.44 0.50 1.08 o 3 13 2 0.11 0.31 1.14 o 4 13 2 5.63 3.86 2.44 o -3 14 2 99.51 113.18 6.40 o -2 14 2 312.78 299.08 10.37 o -1 14 2 188.83 180.99 5.41 o 0 14 2 243.28 235.19 6.30 o 1 14 2 341.96 324.09 6.07 o 2 14 2 118.48 120.30 6.11 o 3 14 2 115.76 114.45 6.11 o -2 15 2 0.82 0.43 1.21 o -1 15 2 38.73 29.31 2.58 o 0 15 2 45.93 42.89 3.94 o 1 15 2 5.65 4.67 1.31 o 2 15 2 4.21 4.42 1.60 o -2 16 2 71.66 71.49 5.37 o -1 16 2 103.78 98.91 4.33 o 0 16 2 72.68 67.85 3.63 o 1 16 2 226.57 233.67 6.96 o -6 1 3 42.54 40.26 3.26 o -5 1 3 182.89 181.18 5.48 o -4 1 3 594.38 557.15 9.56 o -3 1 3 312.97 320.61 3.43 o -2 1 3 796.87 739.07 6.97 o -1 1 3 6637.48 6552.94 66.44 o 0 1 3 194.06 175.07 1.73 o 1 1 3 1754.11 1693.42 11.92 o 2 1 3 2598.95 2625.22 16.48 o 3 1 3 618.87 584.92 5.53 o 4 1 3 74.56 78.87 1.88 o 5 1 3 891.76 814.08 17.02 o 6 1 3 151.99 147.99 5.66 o -6 2 3 0.04 -0.41 0.98 o -5 2 3 11.74 11.98 1.79 o -4 2 3 21.00 25.50 2.50 o -3 2 3 13.43 13.47 0.79 o -2 2 3 17.40 25.05 1.14 o -1 2 3 50.31 49.53 1.15 o 0 2 3 127.08 135.78 1.54 o 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