#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217514.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217514_Fobs loop_ _publ_author_name 'Almeida Paz, Filipe A.' 'Klinowski, Jacek' _publ_section_title ; Poly[[\m~2~-aqua-tetraaquahexakis(\m~4~-naphthalene-2,6-dicarboxylato)tetraholmium(III)] 1.75-hydrate] ; _journal_coeditor_code HB2668 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m336 _journal_page_last m337 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.126 _cell_angle_gamma 90.000 _cell_length_a 17.0505 _cell_length_b 15.1728 _cell_length_c 24.9142 _exptl_crystal_F_000 3982.00 _reflns_d_resolution_high 0.8402 _[local]_cod_data_source_file hb2668Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jk0220 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1112.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 150693.75 129275.21 5053.81 o 6 0 0 564772.69 640985.94 24395.75 o 8 0 0 23709.83 19452.77 930.81 o 10 0 0 76254.11 71854.80 3858.32 o 12 0 0 15227.16 19424.35 805.06 o 14 0 0 36861.34 32151.34 1692.24 o 16 0 0 30487.65 30276.66 2280.64 o 18 0 0 15998.20 17112.70 1611.59 o 3 1 0 0.22 604.82 117.43 o 4 1 0 224449.17 228074.50 6660.30 o 5 1 0 12441.25 12002.99 481.17 o 6 1 0 215.18 572.22 216.63 o 7 1 0 15244.70 17383.44 539.79 o 8 1 0 69534.65 70650.18 1855.38 o 9 1 0 18.06 -99.83 222.88 o 10 1 0 76834.66 86311.73 2781.50 o 11 1 0 3333.35 3277.43 429.67 o 12 1 0 238.66 41.06 251.16 o 13 1 0 11212.29 10963.03 518.14 o 14 1 0 60628.84 59944.51 2214.20 o 15 1 0 863.02 345.90 904.12 o 16 1 0 2944.65 3756.23 379.98 o 17 1 0 7438.09 7268.91 543.90 o 18 1 0 18.96 -594.59 620.45 o 19 1 0 22834.62 21649.11 1934.81 o 2 2 0 1347.70 670.00 331.13 o 3 2 0 1831.41 2921.72 243.73 o 4 2 0 19.25 821.68 135.52 o 5 2 0 6293.69 5893.01 322.13 o 6 2 0 13673.00 15758.07 669.31 o 7 2 0 1119.22 1186.15 207.35 o 8 2 0 11095.61 8860.12 390.44 o 9 2 0 46551.63 52371.11 1174.90 o 10 2 0 4001.25 3503.48 434.89 o 11 2 0 6790.28 5375.04 386.37 o 12 2 0 39032.01 42797.09 1025.85 o 13 2 0 4569.54 3980.73 329.06 o 14 2 0 1070.59 963.82 388.72 o 15 2 0 73858.79 82175.48 2150.28 o 16 2 0 24959.71 23256.68 974.82 o 17 2 0 13.04 -406.08 493.25 o 18 2 0 28677.14 26856.98 4300.21 o 19 2 0 12443.67 9653.72 1150.49 o 1 3 0 133145.69 136790.84 5775.06 o 2 3 0 14587.38 17279.96 895.08 o 3 3 0 55.67 96.24 253.02 o 4 3 0 52437.27 57446.40 1349.04 o 5 3 0 25231.82 25936.40 897.52 o 6 3 0 1073.19 343.11 144.45 o 7 3 0 154323.88 155061.84 4544.93 o 8 3 0 5456.30 4657.42 299.81 o 9 3 0 2.09 -71.47 259.24 o 10 3 0 13220.88 12968.74 475.01 o 11 3 0 79568.95 75077.32 2030.86 o 12 3 0 1433.61 1557.54 234.64 o 13 3 0 197.10 428.93 414.66 o 14 3 0 6488.80 6776.64 353.94 o 15 3 0 141.97 408.99 1023.45 o 16 3 0 24807.97 26930.24 965.57 o 17 3 0 34051.70 32010.49 2373.31 o 18 3 0 309.30 1071.38 802.41 o 19 3 0 1027.55 391.03 1073.64 o 0 4 0 1236929.38 1385315.13 83671.63 o 1 4 0 19649.00 18721.62 618.43 o 2 4 0 14422.39 16353.17 394.47 o 3 4 0 944979.63 1046805.31 31843.83 o 4 4 0 139.91 284.57 854.39 o 5 4 0 7346.03 8289.71 464.79 o 6 4 0 8.65 -331.51 331.51 o 7 4 0 125477.02 127168.78 6760.54 o 8 4 0 4891.85 5893.62 452.94 o 9 4 0 17675.74 21396.04 562.34 o 10 4 0 47.34 76.67 229.35 o 11 4 0 30166.31 27145.26 797.28 o 12 4 0 46382.29 51238.16 1737.21 o 13 4 0 18507.92 16987.48 687.66 o 14 4 0 211.59 108.31 298.26 o 15 4 0 31404.38 34104.38 949.05 o 16 4 0 562.95 163.81 1166.31 o 17 4 0 13614.89 7899.73 1175.35 o 18 4 0 162.81 -535.69 876.99 o 19 4 0 2884.07 1975.50 604.15 o 1 5 0 28629.59 25988.58 637.48 o 2 5 0 11486.28 13617.83 761.20 o 3 5 0 189.76 -136.09 203.78 o 4 5 0 4968.92 4732.47 231.89 o 5 5 0 6828.36 6408.27 1086.07 o 6 5 0 1918.52 1369.40 890.56 o 7 5 0 158408.97 178159.59 5437.32 o 8 5 0 765.59 -476.92 626.10 o 9 5 0 1428.21 1076.11 410.72 o 10 5 0 31194.79 31994.12 1923.51 o 11 5 0 58089.20 57128.78 2381.78 o 12 5 0 510.30 -630.62 630.62 o 13 5 0 4944.26 4021.07 1012.61 o 14 5 0 8242.99 7153.01 639.77 o 15 5 0 880.32 412.66 544.12 o 16 5 0 51051.57 54255.46 2538.63 o 17 5 0 11114.61 12173.95 1265.77 o 18 5 0 1.43 -705.21 1021.65 o 0 6 0 532.91 1174.78 279.34 o 1 6 0 158.43 -224.74 224.74 o 2 6 0 612.71 1157.96 207.37 o 3 6 0 224.39 124.17 295.58 o 4 6 0 1417.58 1293.22 151.11 o 5 6 0 10577.16 11172.07 421.01 o 6 6 0 14179.54 15407.55 1916.73 o 7 6 0 541.18 598.20 415.89 o 8 6 0 2224.97 1674.98 421.03 o 9 6 0 36999.27 39749.56 2018.44 o 10 6 0 104.49 -396.60 675.83 o 11 6 0 16053.28 14679.04 918.49 o 12 6 0 56329.84 65126.29 2468.71 o 13 6 0 10248.27 9043.37 753.76 o 14 6 0 312.49 -71.05 559.66 o 15 6 0 71078.92 73161.27 3496.68 o 16 6 0 5168.19 6749.24 1044.26 o 17 6 0 1960.37 2963.25 2624.20 o 18 6 0 10472.57 11310.52 1414.95 o 1 7 0 1563.12 1125.74 272.80 o 2 7 0 42246.21 42559.16 891.18 o 3 7 0 2182.51 2702.68 218.15 o 4 7 0 161077.28 176232.08 3954.45 o 5 7 0 20976.34 18189.36 444.55 o 6 7 0 220.71 -439.32 439.32 o 7 7 0 17141.38 20941.38 1269.16 o 8 7 0 45676.81 48763.28 1924.87 o 9 7 0 6114.76 7675.34 815.70 o 10 7 0 33912.13 40321.41 1726.96 o 11 7 0 904.83 421.90 526.32 o 12 7 0 1092.48 1413.63 610.68 o 13 7 0 43316.52 47562.59 1934.21 o 14 7 0 43088.31 46528.19 3189.28 o 15 7 0 2153.57 583.16 947.06 o 16 7 0 141.67 1164.05 922.20 o 17 7 0 110.69 -971.93 971.93 o 0 8 0 412288.09 484758.69 20552.05 o 1 8 0 37548.50 38975.94 7454.46 o 2 8 0 4768.35 3517.02 431.30 o 3 8 0 124672.34 155617.45 4197.82 o 4 8 0 76927.78 68357.02 1765.72 o 5 8 0 19843.33 20742.37 559.52 o 6 8 0 220980.36 249754.56 6411.17 o 7 8 0 1236.45 1494.06 657.75 o 8 8 0 15466.39 11026.25 852.13 o 9 8 0 383.51 272.57 475.24 o 10 8 0 45902.64 41366.00 1745.00 o 11 8 0 16550.25 15514.67 1423.99 o 12 8 0 15342.70 14409.61 895.97 o 13 8 0 2083.65 1166.31 849.87 o 14 8 0 18957.02 14061.30 2016.18 o 15 8 0 363.87 2741.74 1650.02 o 16 8 0 6668.36 8394.74 1238.64 o 17 8 0 390.72 -558.29 1066.86 o 1 9 0 2717.53 2325.72 334.12 o 2 9 0 13502.96 15349.87 673.70 o 3 9 0 2321.37 2494.55 316.27 o 4 9 0 115240.40 130000.34 3098.03 o 5 9 0 38.86 52.81 239.38 o 6 9 0 1859.77 1667.81 488.61 o 7 9 0 13066.35 10007.00 672.00 o 8 9 0 27671.74 25846.48 2013.92 o 9 9 0 4498.40 2922.26 643.05 o 10 9 0 48167.92 50252.90 2064.29 o 11 9 0 3024.77 1708.78 867.95 o 12 9 0 1871.27 754.94 779.80 o 13 9 0 19240.14 20202.52 1412.68 o 14 9 0 28298.91 26637.59 1995.84 o 15 9 0 1045.94 -24.86 1019.39 o 16 9 0 400.19 800.14 1455.63 o 0 10 0 2.15 322.90 372.65 o 1 10 0 1203.93 1021.67 372.36 o 2 10 0 2040.53 1982.80 322.83 o 3 10 0 3019.64 3220.75 278.40 o 4 10 0 721.58 647.93 337.95 o 5 10 0 12.28 -155.35 327.48 o 6 10 0 5359.85 6966.26 296.37 o 7 10 0 1222.82 1325.60 1038.61 o 8 10 0 8898.26 6685.24 834.05 o 9 10 0 13297.61 14305.47 877.38 o 10 10 0 3394.17 2384.61 897.34 o 12 10 0 26648.45 30285.71 1805.98 o 13 10 0 766.22 169.52 874.73 o 14 10 0 6755.05 7208.08 1093.98 o 16 10 0 9886.30 8747.35 1358.44 o 1 11 0 17803.46 19872.47 1020.48 o 2 11 0 6873.70 7030.65 416.88 o 3 11 0 356.76 515.01 291.20 o 4 11 0 7879.48 6865.94 569.11 o 5 11 0 16128.99 14384.81 828.66 o 6 11 0 7642.00 6802.50 377.39 o 7 11 0 48449.71 49263.09 3718.89 o 8 11 0 16613.51 13791.70 871.06 o 9 11 0 169.42 1053.30 806.93 o 10 11 0 13896.85 12119.71 1247.68 o 11 11 0 28741.00 30211.12 2077.21 o 12 11 0 5812.23 4405.32 1118.85 o 13 11 0 9521.70 10566.88 1338.10 o 15 11 0 317.06 2567.70 1161.79 o 0 12 0 23786.78 23712.47 975.11 o 1 12 0 5784.81 3946.40 517.75 o 2 12 0 26909.59 28574.11 980.77 o 3 12 0 84731.09 102065.26 2977.40 o 4 12 0 6691.04 5685.55 454.39 o 5 12 0 6280.92 6426.37 727.43 o 6 12 0 9809.86 10613.00 392.41 o 7 12 0 30495.89 24805.38 707.96 o 8 12 0 13343.90 12922.11 3336.20 o 9 12 0 32214.62 39277.16 2427.56 o 10 12 0 96.71 -610.28 904.12 o 11 12 0 19561.09 15351.93 1487.27 o 12 12 0 2294.07 1824.06 971.93 o 13 12 0 18735.45 19196.70 1774.33 o 14 12 0 25.11 -1186.66 1186.66 o 1 13 0 39752.71 40349.68 1281.23 o 2 13 0 3244.71 2373.76 347.82 o 3 13 0 249.68 849.67 468.55 o 4 13 0 6994.14 5806.50 385.56 o 5 13 0 333.46 696.93 301.14 o 6 13 0 3155.68 2416.29 302.02 o 7 13 0 57026.05 58958.92 1486.31 o 8 13 0 8.22 784.32 834.05 o 9 13 0 4128.01 3984.90 978.71 o 11 13 0 19291.97 19739.16 1948.38 o 12 13 0 1740.45 1555.08 1069.12 o 13 13 0 6411.42 4337.51 1283.85 o 0 14 0 1211.92 1262.38 557.80 o 1 14 0 30.49 722.58 434.44 o 2 14 0 130.12 353.90 347.31 o 3 14 0 1254.01 469.03 524.90 o 4 14 0 3134.93 2949.34 386.50 o 5 14 0 2056.29 2041.13 562.45 o 6 14 0 3064.50 3321.11 516.42 o 7 14 0 441.25 452.17 723.29 o 8 14 0 97.70 1735.91 881.52 o 10 14 0 429.32 1243.16 974.19 o 11 14 0 6390.01 11032.50 2090.77 o 1 15 0 5334.93 5258.62 408.75 o 2 15 0 881.78 364.55 413.05 o 3 15 0 1929.60 1644.60 515.21 o 4 15 0 18948.83 18809.85 1019.78 o 5 15 0 10460.54 10185.37 1178.74 o 6 15 0 111.89 1287.24 547.16 o 7 15 0 2082.48 806.93 1320.01 o 8 15 0 7562.56 9662.76 1317.75 o 9 15 0 7584.89 7088.29 1268.03 o 10 15 0 18297.77 21190.28 2359.75 o 0 16 0 30891.53 40742.64 2932.73 o 1 16 0 5775.37 5468.88 469.47 o 2 16 0 99.70 832.94 448.68 o 3 16 0 1617.58 497.61 525.14 o 4 16 0 7681.63 7235.33 726.69 o 5 16 0 11904.66 15385.83 3883.19 o 8 16 0 7980.92 6787.67 1679.40 o 9 16 0 4040.35 2404.95 1188.92 o 1 17 0 64.92 267.15 608.93 o 2 17 0 3164.40 3076.44 572.50 o 3 17 0 288.42 -74.44 548.41 o 4 17 0 13052.48 12962.80 1340.36 o 5 17 0 0.43 316.44 1216.04 o 0 18 0 80.34 967.41 990.01 o 1 18 0 582.67 281.76 991.14 o -17 0 1 438.86 -271.84 477.43 o -15 0 1 183292.19 221557.70 8021.62 o -13 0 1 19117.90 18835.16 926.33 o -11 0 1 10088.14 8395.83 551.56 o -9 0 1 111956.13 127788.09 6798.97 o -7 0 1 24.26 199.81 278.02 o -5 0 1 6445.39 4679.03 291.60 o -3 0 1 2368.84 307.40 178.56 o 3 0 1 5401.25 8042.84 448.67 o 5 0 1 10202.60 7450.25 357.63 o 7 0 1 156.69 -320.96 370.69 o 9 0 1 96207.77 110415.45 5058.54 o 11 0 1 11205.14 9599.96 1263.51 o 13 0 1 15797.20 14097.46 797.07 o 15 0 1 134485.38 154325.06 5655.35 o 17 0 1 106.64 -166.67 662.87 o -19 1 1 26119.46 27550.75 2940.65 o -18 1 1 57.71 -485.96 485.96 o -17 1 1 3669.53 3612.12 453.47 o -16 1 1 72715.81 76129.41 2015.79 o -15 1 1 776.29 1793.60 426.09 o -14 1 1 62127.70 65463.37 2105.20 o -13 1 1 23358.56 22619.88 952.84 o -12 1 1 363.10 137.81 262.12 o -11 1 1 39672.12 38473.05 1448.39 o -10 1 1 91107.57 100902.65 3220.87 o -9 1 1 413.37 -204.47 253.85 o -8 1 1 20228.89 20344.56 691.57 o -7 1 1 25221.04 31987.34 1033.99 o -6 1 1 119.28 372.65 150.34 o -5 1 1 17622.81 16281.90 516.37 o -4 1 1 144424.83 139846.84 3575.66 o -3 1 1 4.08 1081.78 412.67 o 3 1 1 198.65 902.25 128.21 o 4 1 1 171160.83 168346.38 4115.71 o 5 1 1 21260.61 21153.25 814.18 o 6 1 1 915.84 1563.93 205.07 o 7 1 1 66682.78 82603.03 2174.71 o 8 1 1 8152.13 8732.51 378.12 o 9 1 1 163.78 157.98 201.81 o 10 1 1 86355.16 97348.25 2667.20 o 11 1 1 35629.93 34575.82 1048.59 o 12 1 1 118.73 86.63 281.35 o 13 1 1 5946.99 6167.26 439.67 o 14 1 1 28347.48 26445.56 980.33 o 15 1 1 114.48 546.71 309.65 o 16 1 1 18565.96 19006.91 1079.87 o 17 1 1 1791.96 2035.67 589.56 o 18 1 1 87.32 1191.18 827.27 o 19 1 1 21140.61 20134.72 2099.81 o -19 2 1 97.25 -49.73 951.58 o -18 2 1 2856.02 2452.42 928.98 o -17 2 1 5309.51 4350.65 490.03 o -16 2 1 12357.41 10963.40 570.24 o -15 2 1 23847.56 21496.31 649.65 o -14 2 1 19320.65 17453.14 652.51 o -13 2 1 1447.07 1760.99 714.15 o -12 2 1 8027.95 10353.96 399.39 o -11 2 1 13375.13 10389.52 484.80 o -10 2 1 33708.57 32670.93 1171.62 o -9 2 1 65331.84 73605.70 1957.55 o -8 2 1 30773.76 30712.50 2229.78 o -7 2 1 51930.25 41243.67 1181.16 o -6 2 1 83385.54 90341.55 2738.64 o -5 2 1 2.34 555.71 400.71 o -4 2 1 98726.92 76070.45 10873.52 o -3 2 1 18324.70 23859.33 980.96 o -2 2 1 13652.31 2552.81 1368.96 o 2 2 1 2623.30 1737.16 1159.53 o 3 2 1 471018.94 571387.44 24560.39 o 4 2 1 76391.73 60030.53 4895.13 o 5 2 1 316.27 484.98 137.84 o 6 2 1 48442.96 51544.43 1277.22 o 7 2 1 90454.65 76872.79 2109.41 o 8 2 1 22961.35 23175.31 684.90 o 9 2 1 12795.13 13558.78 505.95 o 10 2 1 44138.38 43910.99 1606.50 o 11 2 1 7324.03 5693.23 349.54 o 12 2 1 6885.44 7550.99 501.32 o 13 2 1 3624.95 3308.49 341.86 o 14 2 1 16857.08 13668.42 573.65 o 15 2 1 45012.54 53478.21 1421.46 o 16 2 1 10115.13 8881.28 463.12 o 17 2 1 7368.93 5584.03 614.13 o 18 2 1 15521.99 15641.25 1464.67 o 19 2 1 1055.90 2775.64 1240.90 o -19 3 1 6894.13 5668.82 906.38 o -18 3 1 480.82 -434.52 1136.93 o -17 3 1 35416.26 29755.20 3312.46 o -16 3 1 45002.32 49250.56 1591.57 o -15 3 1 211.58 569.94 468.91 o -14 3 1 4656.42 4525.79 380.08 o -13 3 1 9212.42 9057.28 720.35 o -12 3 1 447.14 67.77 277.64 o -11 3 1 41587.15 38992.08 1702.00 o -10 3 1 585.94 1323.10 443.04 o -9 3 1 299.82 378.06 222.51 o -8 3 1 52315.71 50337.98 1295.95 o -7 3 1 120610.03 111995.95 9892.19 o -6 3 1 540.39 244.39 639.91 o -5 3 1 5680.04 6645.27 526.65 o -4 3 1 112551.51 104337.07 9948.28 o -3 3 1 129.16 1169.46 128.10 o -2 3 1 4618.82 6421.63 263.15 o -1 3 1 96289.59 95473.23 2298.69 o 0 3 1 33.73 269.81 136.19 o 1 3 1 85209.02 88478.02 2205.44 o 2 3 1 45.61 890.79 264.00 o 3 3 1 240.93 223.77 370.69 o 4 3 1 79758.57 85975.42 2811.09 o 5 3 1 9045.58 9561.80 1123.37 o 6 3 1 382.85 -176.43 176.43 o 7 3 1 183020.39 186249.92 7953.22 o 8 3 1 50545.01 46586.52 2352.55 o 9 3 1 222.13 262.08 168.67 o 10 3 1 7286.49 8193.02 326.89 o 11 3 1 28120.07 23877.12 708.38 o 12 3 1 1289.68 1079.83 235.25 o 13 3 1 16837.44 17468.70 1290.61 o 14 3 1 23331.18 22516.87 682.11 o 15 3 1 590.84 623.42 337.99 o 16 3 1 19983.73 22862.50 1044.11 o 17 3 1 29339.90 24634.96 2176.67 o 18 3 1 411.40 291.58 874.73 o 19 3 1 6295.03 4360.11 1193.44 o -19 4 1 2.02 72.33 928.98 o -18 4 1 37511.00 42480.00 2920.30 o -17 4 1 2842.39 782.51 966.28 o -16 4 1 35170.70 31671.58 1589.82 o -15 4 1 3419.25 4291.87 504.62 o -14 4 1 555.97 492.50 313.24 o -13 4 1 1105.12 743.69 294.01 o -12 4 1 99056.67 108526.73 3451.52 o -11 4 1 2096.37 1345.83 462.13 o -10 4 1 2944.30 3035.94 377.64 o -9 4 1 14.79 58.32 283.32 o -8 4 1 15861.13 14144.93 958.37 o -7 4 1 1301.66 1309.20 366.22 o -6 4 1 32314.67 37880.71 1314.65 o -5 4 1 1289.85 444.82 315.58 o -4 4 1 2153.40 2248.95 1067.99 o -3 4 1 2893.72 5175.78 777.76 o -2 4 1 33.32 -2.71 191.28 o -1 4 1 1128.54 1935.86 183.60 o 0 4 1 3386.91 4615.69 197.68 o 1 4 1 2159.37 3202.63 184.85 o 2 4 1 440.12 386.40 139.89 o 3 4 1 7252.25 10812.11 274.67 o 4 4 1 3029.80 2489.49 348.70 o 5 4 1 2740.62 2673.93 495.00 o 6 4 1 44695.36 52155.56 1668.59 o 7 4 1 691.81 1316.17 834.05 o 8 4 1 19603.65 14136.50 1090.94 o 9 4 1 109.65 433.81 346.25 o 10 4 1 3170.17 3009.31 246.64 o 11 4 1 1227.69 1014.76 298.84 o 12 4 1 84263.05 92837.08 2082.59 o 13 4 1 538.05 960.72 378.77 o 14 4 1 2008.41 2094.54 268.17 o 15 4 1 154.43 338.36 317.64 o 16 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