#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217533.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217533_Fobs loop_ _publ_author_name 'Mo, Juan' 'Hu, Gong-Zheng' 'Chen, Wen' 'Yuan, Li' 'Pan, Yu-Shan' _publ_section_title ; catena-Poly[[copper(I)-bis[\m-bis(diphenylphosphino)methane-\k^2^P:P']-copper(I)-\m-2,2'-bipyridine-\k^2^N:N'] bis(tetrafluoridoborate) dichloromethane 2.5-solvate] ; _journal_coeditor_code HG2367 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m391 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.821 _cell_angle_beta 89.030 _cell_angle_gamma 74.237 _cell_length_a 10.9860 _cell_length_b 16.1541 _cell_length_c 20.3362 _exptl_crystal_F_000 1462.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file hg2367Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50416B in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 299.90 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 66.86 514.62 16.84 o 2 0 0 5127.91 4153.50 67.82 o 3 0 0 109.71 79.07 39.92 o 4 0 0 12393.08 13111.52 198.74 o 5 0 0 8843.23 8216.78 190.05 o 6 0 0 187.77 148.93 38.32 o 7 0 0 478.08 504.85 55.16 o 8 0 0 381.01 461.59 63.58 o 9 0 0 1457.34 1397.83 88.93 o 10 0 0 771.74 945.82 78.38 o 11 0 0 7.87 17.13 49.64 o 12 0 0 2.85 -69.24 46.16 o -12 1 0 32.41 39.58 50.51 o -11 1 0 184.50 195.57 60.29 o -10 1 0 22.44 46.64 48.97 o -9 1 0 1502.59 1493.44 89.61 o -8 1 0 251.68 342.95 56.71 o -7 1 0 1367.62 1673.24 83.22 o -6 1 0 11.55 -19.45 30.68 o -5 1 0 5472.27 5655.88 142.35 o -4 1 0 1511.62 1526.34 58.45 o -3 1 0 3757.94 4203.76 102.67 o -2 1 0 1202.33 1866.97 54.19 o -1 1 0 2350.27 5280.22 108.67 o 0 1 0 20837.10 9827.70 198.67 o 1 1 0 22044.04 21629.10 418.04 o 2 1 0 492.34 1006.80 25.69 o 3 1 0 8824.23 8919.61 188.51 o 4 1 0 22.43 57.77 36.34 o 5 1 0 12515.36 13917.23 417.17 o 6 1 0 1205.52 1102.87 50.61 o 7 1 0 5.11 46.45 39.68 o 8 1 0 926.22 922.31 77.61 o 9 1 0 850.04 835.12 77.03 o 10 1 0 2956.17 3222.03 129.96 o 11 1 0 135.82 233.02 61.06 o 12 1 0 251.75 241.25 63.67 o -12 2 0 42.18 70.84 54.38 o -11 2 0 657.41 761.38 82.06 o -10 2 0 1561.21 1541.83 92.03 o -9 2 0 6.65 61.35 48.97 o -8 2 0 1124.16 1238.55 87.00 o -7 2 0 236.03 304.44 51.29 o -6 2 0 2846.27 2369.11 92.03 o -5 2 0 647.46 1123.39 58.64 o -4 2 0 2836.29 2951.27 86.42 o -3 2 0 15354.95 15349.36 308.79 o -2 2 0 35523.19 33921.03 646.23 o -1 2 0 1629.31 667.32 26.51 o 0 2 0 59.01 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60.24 o 10 3 0 295.57 370.05 58.93 o 11 3 0 1249.65 1545.60 100.35 o 12 3 0 580.18 584.39 75.48 o -11 4 0 179.81 256.73 59.90 o -10 4 0 230.81 197.70 57.09 o -9 4 0 1192.31 1263.42 84.58 o -8 4 0 682.17 515.39 64.35 o -7 4 0 15.21 33.68 44.03 o -6 4 0 2052.05 2068.06 87.48 o -5 4 0 39.37 -11.90 29.90 o -4 4 0 5669.31 4551.93 120.67 o -3 4 0 93.10 106.74 25.16 o -2 4 0 8313.63 9095.06 193.54 o -1 4 0 10152.35 8947.77 185.22 o 0 4 0 31206.34 31671.05 601.42 o 1 4 0 7191.49 9317.43 186.96 o 2 4 0 13.00 14.20 12.63 o 3 4 0 2234.42 2172.73 46.60 o 4 4 0 51.58 38.95 16.16 o 5 4 0 11813.26 11865.27 252.37 o 6 4 0 2091.81 1820.00 54.97 o 7 4 0 2882.96 2730.54 73.46 o 8 4 0 2288.36 2477.06 149.70 o 9 4 0 0.63 3.93 36.50 o 10 4 0 1744.28 1869.12 75.06 o 11 4 0 1.14 -65.03 45.19 o 12 4 0 237.35 258.18 67.54 o 13 4 0 297.09 312.27 69.38 o -11 5 0 7.69 -4.26 51.09 o -10 5 0 72.44 42.00 55.84 o -9 5 0 313.32 378.66 58.93 o -8 5 0 1217.32 1149.14 79.54 o -7 5 0 454.39 601.81 63.29 o -6 5 0 185.25 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75.66 o 4 6 0 89.16 34.25 11.42 o 5 6 0 979.84 1141.60 41.66 o 6 6 0 1486.02 1070.28 59.51 o 7 6 0 9227.91 8512.90 188.70 o 8 6 0 425.75 463.91 41.54 o 9 6 0 360.94 353.43 43.65 o 10 6 0 563.87 729.71 52.12 o 11 6 0 809.58 718.24 57.70 o 12 6 0 576.49 736.55 59.14 o 13 6 0 29.27 42.58 46.74 o -10 7 0 29.32 15.10 48.19 o -9 7 0 176.70 146.90 55.16 o -8 7 0 89.84 66.87 47.13 o -7 7 0 1929.02 1993.74 96.77 o -6 7 0 1072.10 1074.62 76.35 o -5 7 0 216.43 91.45 41.61 o -4 7 0 3167.71 2868.82 99.48 o -3 7 0 1048.03 1260.13 64.74 o -2 7 0 19056.78 17192.13 354.85 o -1 7 0 4870.50 5220.12 127.25 o 0 7 0 4230.51 4204.63 102.58 o 1 7 0 2956.63 2178.57 63.48 o 2 7 0 2856.82 2801.67 74.61 o 3 7 0 4508.95 4260.28 85.89 o 4 7 0 503.50 734.39 24.32 o 5 7 0 656.14 659.28 24.44 o 6 7 0 573.12 603.01 37.54 o 7 7 0 3162.24 3438.78 139.69 o 8 7 0 3160.37 2993.17 81.43 o 9 7 0 772.62 974.10 54.51 o 10 7 0 6.69 37.37 33.64 o 11 7 0 8.13 -46.66 46.93 o 12 7 0 542.76 576.11 56.52 o 13 7 0 439.24 459.70 55.89 o -9 8 0 197.05 221.80 61.64 o -8 8 0 413.14 450.65 67.74 o -7 8 0 64.30 75.87 45.97 o -6 8 0 1350.04 1562.24 86.61 o -5 8 0 98.04 77.13 45.68 o -4 8 0 130.80 143.12 45.38 o -3 8 0 3600.63 3632.62 116.22 o -2 8 0 1.80 29.13 30.97 o -1 8 0 4120.09 4594.99 118.25 o 0 8 0 840.90 509.78 37.74 o 1 8 0 448.75 625.23 36.77 o 2 8 0 3547.96 4193.69 103.54 o 3 8 0 8026.91 7899.47 105.58 o 4 8 0 3221.76 3379.86 55.78 o 5 8 0 282.30 356.09 20.96 o 6 8 0 2453.88 2377.89 64.30 o 7 8 0 72.98 75.85 27.66 o 8 8 0 10002.98 9820.38 175.67 o 9 8 0 21.27 33.60 31.68 o 10 8 0 41.26 52.56 30.34 o 11 8 0 218.26 236.11 45.63 o 12 8 0 154.69 111.44 51.82 o -9 9 0 25.39 6.39 48.24 o -8 9 0 625.20 617.19 68.80 o -7 9 0 462.89 473.30 65.80 o -6 9 0 77.94 99.58 47.71 o -5 9 0 2965.63 3184.97 117.38 o -4 9 0 54.89 95.70 46.55 o -3 9 0 435.00 353.11 48.19 o -2 9 0 1445.79 1675.46 77.42 o -1 9 0 26.03 44.51 26.22 o 0 9 0 1980.61 1818.88 65.61 o 1 9 0 27.23 111.19 23.81 o 2 9 0 6528.88 6009.18 140.32 o 3 9 0 1738.81 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