#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/75/2217548.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217548_Fobs loop_ _publ_author_name 'Mahon, Andrew B.' 'Jensen, Paul' 'Try, Andrew C.' _publ_section_title ; 5,11-Dimethyldibenzo[b,f][1,5]diazocine-6,12(5H,11H)-dione ; _journal_coeditor_code HK2415 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o469 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.611 _cell_angle_gamma 90.000 _cell_length_a 11.2715 _cell_length_b 7.9113 _cell_length_c 15.4100 _exptl_crystal_F_000 560.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file hk2415Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' act07pj3 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 119.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 68.03 59.51 2.18 o 2 0 0 10813.21 9309.96 134.68 o 3 0 0 3176.20 3166.72 37.20 o 4 0 0 2480.16 2378.23 28.16 o 5 0 0 1887.36 2041.55 24.41 o 6 0 0 0.88 0.19 0.33 o 7 0 0 1.19 3.92 0.55 o 8 0 0 8.89 4.83 0.87 o 9 0 0 30.63 31.53 1.77 o 10 0 0 613.59 588.08 10.71 o 11 0 0 492.38 488.54 15.12 o 12 0 0 21.27 29.93 3.72 o 13 0 0 30.34 28.68 2.31 o 14 0 0 269.74 335.75 8.07 o 1 1 0 14331.14 11041.21 265.51 o 2 1 0 3.16 4.95 0.23 o 3 1 0 122.34 94.67 1.10 o 4 1 0 592.51 573.51 7.66 o 5 1 0 6.17 8.62 0.38 o 6 1 0 1314.41 1465.39 13.64 o 7 1 0 4.41 3.46 0.36 o 8 1 0 278.96 279.54 4.02 o 9 1 0 69.35 58.70 1.64 o 10 1 0 0.80 -0.05 0.60 o 11 1 0 242.38 240.70 4.43 o 12 1 0 20.07 18.06 1.32 o 13 1 0 64.17 72.62 2.88 o 14 1 0 3.26 2.82 1.12 o 0 2 0 267.14 293.38 3.94 o 1 2 0 3390.03 3294.72 23.88 o 2 2 0 6607.70 6250.04 53.29 o 3 2 0 529.61 545.00 4.53 o 4 2 0 73.42 74.25 1.06 o 5 2 0 0.15 2.38 0.30 o 6 2 0 25.34 25.24 0.68 o 7 2 0 116.58 113.55 1.62 o 8 2 0 195.52 181.46 2.59 o 9 2 0 153.38 140.31 2.67 o 10 2 0 328.61 304.13 4.65 o 11 2 0 4.69 3.00 0.81 o 12 2 0 0.14 0.03 0.82 o 13 2 0 86.35 82.11 3.00 o 14 2 0 99.70 120.36 4.58 o 1 3 0 1691.20 1731.79 14.67 o 2 3 0 247.01 274.04 2.62 o 3 3 0 275.40 285.19 2.26 o 4 3 0 12.44 14.32 0.57 o 5 3 0 93.60 103.08 1.46 o 6 3 0 138.02 150.32 1.94 o 7 3 0 0.83 1.25 0.36 o 8 3 0 452.64 447.68 5.16 o 9 3 0 9.49 11.55 0.91 o 10 3 0 163.34 164.30 3.22 o 11 3 0 88.95 81.47 4.21 o 12 3 0 3.17 3.11 1.43 o 13 3 0 0.07 -0.21 1.33 o 0 4 0 2122.05 2249.45 26.94 o 1 4 0 9.61 6.20 0.38 o 2 4 0 76.18 67.45 1.08 o 3 4 0 302.35 333.56 2.84 o 4 4 0 0.01 -0.21 0.22 o 5 4 0 0.45 0.09 0.28 o 6 4 0 0.76 0.21 0.35 o 7 4 0 0.06 0.19 0.39 o 8 4 0 0.57 0.62 0.61 o 9 4 0 8.32 7.17 2.13 o 10 4 0 138.22 135.49 12.16 o 11 4 0 0.80 -0.45 1.13 o 12 4 0 16.51 21.25 2.15 o 1 5 0 0.05 1.26 0.33 o 2 5 0 147.30 162.85 2.06 o 3 5 0 31.17 39.17 0.86 o 4 5 0 87.16 85.29 1.12 o 5 5 0 81.43 84.99 1.33 o 6 5 0 233.19 240.47 2.83 o 7 5 0 142.67 136.28 2.21 o 8 5 0 5.66 2.57 0.66 o 9 5 0 30.56 28.26 1.50 o 10 5 0 0.41 -0.45 0.78 o 11 5 0 0.01 -0.01 0.96 o 12 5 0 19.19 29.22 2.51 o 0 6 0 339.09 339.09 5.21 o 1 6 0 714.88 726.20 6.92 o 2 6 0 28.35 26.84 0.86 o 3 6 0 905.28 906.88 8.53 o 4 6 0 161.77 162.02 2.58 o 5 6 0 223.48 220.55 3.21 o 6 6 0 198.44 196.52 3.11 o 7 6 0 18.99 18.55 1.15 o 8 6 0 139.34 136.68 2.96 o 9 6 0 96.41 93.84 2.61 o 10 6 0 8.04 9.69 1.39 o 11 6 0 20.24 22.44 1.69 o 1 7 0 14.71 15.51 1.03 o 2 7 0 949.18 972.55 11.33 o 3 7 0 0.19 -0.37 0.54 o 4 7 0 149.85 157.82 3.63 o 5 7 0 11.66 10.27 0.88 o 6 7 0 33.45 36.98 1.57 o 7 7 0 155.09 156.13 3.20 o 8 7 0 10.17 12.91 1.07 o 9 7 0 6.00 5.67 1.14 o 10 7 0 35.77 30.56 1.83 o 0 8 0 89.99 88.13 4.68 o 1 8 0 7.73 5.78 2.87 o 2 8 0 53.91 47.87 2.05 o 3 8 0 0.91 1.68 0.84 o 4 8 0 6.11 3.19 0.76 o 5 8 0 91.24 90.37 2.14 o 6 8 0 8.29 7.02 1.03 o 7 8 0 0.01 -0.90 0.90 o 8 8 0 0.41 -0.24 1.21 o 9 8 0 28.02 28.39 3.33 o 1 9 0 7.87 9.30 1.34 o 2 9 0 0.63 -0.86 1.01 o 3 9 0 44.62 40.04 2.16 o 4 9 0 2.09 0.98 1.15 o 5 9 0 15.05 14.58 2.52 o 6 9 0 18.74 21.81 2.97 o 7 9 0 38.34 44.25 2.50 o 0 10 0 0.11 0.42 1.53 o 1 10 0 78.45 89.38 5.38 o 2 10 0 8.82 9.01 1.59 o 3 10 0 34.53 41.00 3.37 o 4 10 0 19.45 19.86 3.41 o -14 1 1 27.62 34.66 1.89 o -13 1 1 3.51 3.18 1.01 o -12 1 1 14.55 16.52 1.22 o -11 1 1 117.47 120.27 2.81 o -10 1 1 194.68 196.20 3.38 o -9 1 1 17.99 17.65 0.99 o -8 1 1 499.41 500.07 4.96 o -7 1 1 299.48 279.31 3.16 o -6 1 1 127.48 137.38 2.08 o -5 1 1 2928.46 2976.76 24.91 o -4 1 1 3.74 2.46 0.24 o -3 1 1 4004.34 3842.15 31.84 o -2 1 1 500.77 483.43 4.24 o -1 1 1 65.06 62.03 1.08 o 0 1 1 395.99 350.94 3.09 o 1 1 1 249.42 256.20 2.32 o 2 1 1 8981.26 8209.98 72.30 o 3 1 1 910.74 960.51 8.26 o 4 1 1 85.82 90.37 1.52 o 5 1 1 281.96 294.57 3.19 o 6 1 1 368.97 391.47 3.84 o 7 1 1 129.02 147.71 1.85 o 8 1 1 185.02 182.40 3.02 o 9 1 1 415.01 409.72 5.62 o 10 1 1 9.95 9.45 0.88 o 11 1 1 0.40 -0.68 0.71 o 12 1 1 65.90 66.52 2.43 o 13 1 1 44.72 49.07 2.03 o 14 1 1 20.64 19.29 1.99 o -14 2 1 0.39 -0.75 1.48 o -13 2 1 56.70 57.06 4.97 o -12 2 1 29.72 25.82 1.45 o -11 2 1 120.09 116.67 2.62 o -10 2 1 2.10 1.27 0.67 o -9 2 1 44.18 47.43 1.47 o -8 2 1 665.82 658.94 6.33 o -7 2 1 2.36 1.03 0.34 o -6 2 1 8.35 7.78 0.48 o -5 2 1 76.45 85.06 1.40 o -4 2 1 1150.52 1298.14 11.17 o -3 2 1 240.85 227.81 2.48 o -2 2 1 698.59 668.16 4.57 o -1 2 1 2636.35 2670.68 20.55 o 0 2 1 1676.81 1654.65 13.90 o 1 2 1 0.77 1.73 0.31 o 2 2 1 1574.44 1542.01 13.33 o 3 2 1 10.91 12.28 0.35 o 4 2 1 113.17 127.14 1.54 o 5 2 1 15.66 7.37 0.39 o 6 2 1 397.50 454.92 4.44 o 7 2 1 0.31 1.05 0.34 o 8 2 1 62.98 63.90 1.66 o 9 2 1 79.71 78.78 3.00 o 10 2 1 12.10 8.15 0.88 o 11 2 1 5.42 5.50 1.30 o 12 2 1 37.14 33.90 1.65 o 13 2 1 9.45 8.55 1.23 o -13 3 1 0.10 -0.51 2.55 o -12 3 1 10.67 14.46 2.15 o -11 3 1 16.10 11.94 2.02 o -10 3 1 33.69 34.11 1.63 o -9 3 1 324.66 327.69 5.08 o -8 3 1 37.31 31.66 0.93 o -7 3 1 2.60 3.14 0.42 o -6 3 1 57.04 57.07 1.28 o -5 3 1 40.75 50.72 1.05 o -4 3 1 126.20 147.01 1.57 o -3 3 1 100.82 134.60 1.26 o -2 3 1 440.31 437.61 3.78 o -1 3 1 2060.70 2064.95 18.96 o 0 3 1 1970.90 1948.89 16.45 o 1 3 1 898.16 928.94 7.08 o 2 3 1 0.70 0.58 0.18 o 3 3 1 13.64 11.06 0.44 o 4 3 1 31.65 34.43 0.65 o 5 3 1 445.35 488.63 5.28 o 6 3 1 132.54 146.01 2.17 o 7 3 1 6.58 5.17 0.47 o 8 3 1 11.95 10.03 0.82 o 9 3 1 4.11 5.10 0.77 o 10 3 1 354.94 331.37 5.03 o 11 3 1 66.69 60.12 1.95 o 12 3 1 2.31 2.10 1.21 o 13 3 1 18.77 22.31 2.25 o -13 4 1 78.85 88.06 3.85 o -12 4 1 4.45 3.96 1.31 o -11 4 1 8.99 8.71 1.48 o -10 4 1 52.97 55.49 3.56 o -9 4 1 79.53 70.57 2.81 o -8 4 1 0.04 -0.52 0.52 o -7 4 1 384.85 376.83 3.89 o -6 4 1 37.10 39.78 0.85 o -5 4 1 0.75 1.42 0.31 o -4 4 1 15.48 16.29 0.47 o -3 4 1 118.69 121.86 1.61 o -2 4 1 1138.96 1184.36 9.59 o -1 4 1 1429.16 1512.02 13.02 o 0 4 1 198.36 212.96 2.33 o 1 4 1 28.38 42.45 0.92 o 2 4 1 2.79 3.04 0.28 o 3 4 1 124.16 110.77 1.35 o 4 4 1 134.79 127.35 1.36 o 5 4 1 271.86 279.89 2.86 o 6 4 1 172.35 167.29 2.21 o 7 4 1 251.72 235.09 3.13 o 8 4 1 132.05 130.46 2.58 o 9 4 1 21.32 20.74 1.77 o 10 4 1 19.76 23.57 1.92 o 11 4 1 1.50 -0.22 1.10 o 12 4 1 0.94 -0.53 1.25 o -12 5 1 1.65 2.79 1.15 o -11 5 1 10.79 6.92 1.27 o -10 5 1 1.78 1.41 0.82 o -9 5 1 5.45 3.49 0.77 o -8 5 1 11.50 8.21 0.72 o -7 5 1 264.19 269.02 3.44 o -6 5 1 60.40 64.08 1.40 o -5 5 1 49.06 49.18 1.18 o -4 5 1 243.42 229.54 2.50 o -3 5 1 223.66 228.27 3.09 o -2 5 1 420.46 454.34 4.19 o -1 5 1 80.26 69.92 1.18 o 0 5 1 2255.59 2394.54 20.40 o 1 5 1 704.88 718.66 6.70 o 2 5 1 248.56 247.51 2.81 o 3 5 1 22.57 21.57 0.64 o 4 5 1 218.00 226.05 2.12 o 5 5 1 212.78 220.22 2.13 o 6 5 1 101.50 99.50 1.63 o 7 5 1 2.51 2.46 0.51 o 8 5 1 106.35 121.75 3.79 o 9 5 1 3.76 3.51 1.21 o 10 5 1 28.25 31.84 2.25 o 11 5 1 21.22 15.55 1.91 o 12 5 1 178.47 221.66 6.66 o -11 6 1 0.00 -0.10 1.06 o -10 6 1 2.85 2.69 1.02 o -9 6 1 57.79 63.49 1.90 o -8 6 1 97.08 94.72 2.00 o -7 6 1 70.49 65.24 1.58 o -6 6 1 59.12 56.65 1.71 o -5 6 1 1.19 0.87 0.62 o -4 6 1 124.90 121.74 2.19 o -3 6 1 354.72 339.86 4.27 o -2 6 1 556.97 530.86 5.40 o -1 6 1 39.15 44.37 1.05 o 0 6 1 12.70 11.04 0.60 o 1 6 1 266.24 267.40 3.09 o 2 6 1 41.43 37.59 0.99 o 3 6 1 258.48 263.45 3.13 o 4 6 1 153.00 146.97 2.18 o 5 6 1 76.09 70.24 1.39 o 6 6 1 127.42 136.18 3.49 o 7 6 1 79.34 73.71 1.67 o 8 6 1 87.86 87.88 2.41 o 9 6 1 10.93 9.81 1.50 o 10 6 1 0.04 -0.84 0.90 o 11 6 1 9.12 9.01 1.34 o -10 7 1 9.28 10.06 1.31 o -9 7 1 101.91 88.11 3.75 o -8 7 1 0.02 0.21 0.87 o -7 7 1 39.21 40.48 1.69 o -6 7 1 8.26 6.47 1.24 o -5 7 1 258.70 257.33 3.77 o -4 7 1 199.01 201.27 3.16 o -3 7 1 447.24 435.66 6.76 o -2 7 1 2001.48 2019.04 20.39 o -1 7 1 672.79 657.31 8.11 o 0 7 1 195.88 185.75 4.10 o 1 7 1 106.96 103.90 2.28 o 2 7 1 1019.13 1012.75 11.71 o 3 7 1 42.33 38.64 1.60 o 4 7 1 1.39 0.81 0.60 o 5 7 1 0.97 0.07 0.64 o 6 7 1 0.02 0.47 0.66 o 7 7 1 65.03 69.05 1.72 o 8 7 1 22.43 26.04 1.57 o 9 7 1 110.26 118.40 3.12 o 10 7 1 0.44 -0.88 1.10 o -9 8 1 20.78 29.41 2.60 o -8 8 1 21.69 20.13 1.80 o -7 8 1 38.66 43.94 1.92 o -6 8 1 3.78 5.22 1.33 o -5 8 1 25.66 25.88 1.82 o -4 8 1 0.28 -0.69 0.69 o -3 8 1 338.83 330.52 4.56 o -2 8 1 3.04 3.50 0.84 o -1 8 1 29.86 28.64 1.44 o 0 8 1 27.55 24.91 1.97 o 1 8 1 66.39 62.29 3.78 o 2 8 1 3.13 2.31 1.43 o 3 8 1 17.99 15.44 1.41 o 4 8 1 93.89 87.48 2.38 o 5 8 1 11.84 10.66 0.97 o 6 8 1 1.52 0.41 0.89 o 7 8 1 58.12 57.75 2.45 o 8 8 1 11.49 13.73 2.04 o 9 8 1 66.89 66.96 6.58 o -7 9 1 46.60 50.03 2.20 o -6 9 1 0.06 -1.21 1.21 o -5 9 1 5.59 5.94 1.37 o -4 9 1 25.34 25.96 1.90 o -3 9 1 73.95 82.66 2.98 o -2 9 1 23.24 19.32 1.69 o -1 9 1 1.01 1.70 1.03 o 0 9 1 20.89 24.32 2.45 o 1 9 1 0.00 1.10 1.23 o 2 9 1 14.30 15.22 1.57 o 3 9 1 40.27 48.52 2.28 o 4 9 1 26.59 30.45 1.94 o 5 9 1 75.71 90.88 3.08 o 6 9 1 0.00 0.23 1.55 o 7 9 1 30.40 39.62 3.98 o -3 10 1 0.07 -0.26 2.32 o -2 10 1 2.78 2.64 1.40 o -1 10 1 32.02 34.35 2.50 o 0 10 1 0.02 -1.10 1.10 o 1 10 1 0.44 -0.80 1.12 o 2 10 1 3.40 1.58 1.29 o 3 10 1 14.35 11.31 4.04 o 4 10 1 1.70 3.72 2.60 o -14 0 2 133.72 170.09 5.29 o -13 0 2 37.14 40.16 2.59 o -12 0 2 25.92 27.15 3.81 o -11 0 2 665.92 680.97 12.23 o -10 0 2 65.23 66.68 2.55 o -9 0 2 231.41 227.15 5.01 o -8 0 2 0.01 -0.10 0.46 o -7 0 2 1101.80 1138.75 16.03 o -6 0 2 449.65 416.29 5.73 o -5 0 2 550.99 545.84 7.09 o -4 0 2 386.57 397.97 5.23 o -3 0 2 9507.15 8988.27 192.76 o -2 0 2 290.27 304.05 3.97 o -1 0 2 3421.03 3156.04 37.38 o 0 0 2 4413.01 3922.62 46.51 o 1 0 2 203.15 149.48 1.82 o 2 0 2 8708.98 7939.40 115.21 o 3 0 2 195.80 215.58 5.55 o 4 0 2 16.15 13.33 1.05 o 5 0 2 2701.97 3028.49 78.52 o 6 0 2 686.30 761.67 9.70 o 7 0 2 545.79 533.96 9.37 o 8 0 2 29.50 30.94 3.62 o 9 0 2 3.51 3.55 1.00 o 10 0 2 13.23 8.80 1.42 o 11 0 2 320.71 313.73 10.27 o 12 0 2 90.89 76.78 3.22 o 13 0 2 47.71 56.66 6.58 o 14 0 2 18.26 21.89 2.26 o -14 1 2 3.71 4.04 1.75 o -13 1 2 22.18 22.32 1.47 o -12 1 2 76.31 78.67 2.22 o -11 1 2 17.64 19.24 1.18 o -10 1 2 2.31 1.90 0.67 o -9 1 2 7.97 6.64 0.54 o -8 1 2 45.92 42.82 1.37 o -7 1 2 0.42 0.47 0.30 o -6 1 2 99.37 96.39 1.36 o -5 1 2 1077.34 1110.17 9.67 o -4 1 2 88.45 90.92 1.15 o -3 1 2 2317.02 2308.55 19.28 o -2 1 2 381.06 378.23 2.98 o -1 1 2 4948.86 4639.82 57.19 o 0 1 2 2296.77 2355.41 19.61 o 1 1 2 1146.39 1256.56 9.77 o 2 1 2 2132.56 2090.93 16.20 o 3 1 2 60.52 70.26 0.81 o 4 1 2 30.87 38.78 0.88 o 5 1 2 689.26 675.28 6.10 o 6 1 2 42.61 26.12 0.61 o 7 1 2 70.40 86.23 1.85 o 8 1 2 61.40 68.45 3.12 o 9 1 2 576.19 510.60 6.73 o 10 1 2 145.64 126.74 2.71 o 11 1 2 43.15 44.05 1.70 o 12 1 2 2.08 2.25 0.92 o 13 1 2 2.80 1.46 1.00 o 14 1 2 0.02 -0.63 1.63 o -14 2 2 13.63 12.81 2.54 o -13 2 2 16.72 17.98 2.04 o -12 2 2 0.89 1.33 1.22 o -11 2 2 3.87 2.64 0.78 o -10 2 2 13.02 13.01 0.96 o -9 2 2 398.54 381.78 5.83 o -8 2 2 282.58 283.31 3.20 o -7 2 2 200.48 196.65 2.69 o -6 2 2 6.79 4.10 0.37 o -5 2 2 895.97 927.42 8.21 o -4 2 2 0.79 2.12 0.22 o -3 2 2 1124.35 1098.63 8.28 o -2 2 2 2306.89 2272.16 19.08 o -1 2 2 464.96 437.64 3.95 o 0 2 2 1064.35 1092.83 7.64 o 1 2 2 4096.08 3940.12 43.59 o 2 2 2 262.90 251.49 2.70 o 3 2 2 2697.42 2752.78 21.35 o 4 2 2 276.81 309.73 3.02 o 5 2 2 5.21 5.37 0.40 o 6 2 2 155.92 156.44 1.92 o 7 2 2 559.96 562.30 6.96 o 8 2 2 15.78 16.93 0.98 o 9 2 2 24.14 18.87 1.10 o 10 2 2 471.55 420.84 6.00 o 11 2 2 53.50 53.55 1.96 o 12 2 2 180.22 183.74 3.71 o 13 2 2 17.94 21.53 1.58 o 14 2 2 0.52 -2.45 2.45 o -13 3 2 4.60 4.93 1.52 o -12 3 2 55.13 55.86 2.90 o -11 3 2 42.22 39.89 2.33 o -10 3 2 29.32 28.10 4.42 o -9 3 2 12.41 14.73 0.84 o -8 3 2 6.55 8.13 0.58 o -7 3 2 14.75 11.18 0.57 o -6 3 2 4.10 5.15 0.38 o -5 3 2 416.29 464.47 3.97 o -4 3 2 996.15 1007.50 7.82 o -3 3 2 801.37 851.13 8.20 o -2 3 2 35.39 35.51 0.60 o -1 3 2 597.11 636.86 5.28 o 0 3 2 109.78 120.01 1.42 o 1 3 2 28.97 26.87 0.51 o 2 3 2 463.51 534.95 4.94 o 3 3 2 1514.10 1616.38 13.85 o 4 3 2 0.07 0.31 0.22 o 5 3 2 157.90 180.70 1.99 o 6 3 2 40.76 32.79 0.84 o 7 3 2 879.61 878.78 9.03 o 8 3 2 3.40 3.64 0.67 o 9 3 2 9.01 12.67 1.63 o 10 3 2 62.72 66.64 1.96 o 11 3 2 56.48 59.36 1.97 o 12 3 2 0.00 -0.33 0.87 o 13 3 2 3.33 0.30 1.59 o -13 4 2 53.44 61.49 2.42 o -12 4 2 1.00 -0.95 0.95 o -11 4 2 78.14 74.65 2.34 o -10 4 2 0.54 0.81 0.76 o -9 4 2 4.37 3.85 0.79 o -8 4 2 4.26 1.48 0.50 o -7 4 2 52.64 50.06 1.23 o -6 4 2 173.48 163.82 2.07 o -5 4 2 19.48 15.85 0.99 o -4 4 2 29.86 38.84 0.90 o -3 4 2 397.96 441.75 5.13 o -2 4 2 361.47 360.10 3.31 o -1 4 2 20.97 19.45 0.53 o 0 4 2 59.25 65.51 1.20 o 1 4 2 481.16 542.80 5.11 o 2 4 2 182.55 208.82 2.06 o 3 4 2 143.96 143.38 1.83 o 4 4 2 24.81 39.27 0.90 o 5 4 2 278.26 260.85 2.55 o 6 4 2 1.64 0.72 0.41 o 7 4 2 0.03 -0.45 0.45 o 8 4 2 291.59 286.43 5.39 o 9 4 2 35.84 34.55 1.47 o 10 4 2 2.94 1.98 0.95 o 11 4 2 12.20 13.90 1.79 o 12 4 2 43.80 39.03 5.67 o -12 5 2 8.94 7.52 1.26 o -11 5 2 11.10 11.64 1.29 o -10 5 2 5.00 4.22 1.06 o -9 5 2 17.40 16.76 1.05 o -8 5 2 103.67 95.62 1.88 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