#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/75/2217552.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217552_Fobs loop_ _publ_author_name 'Miklovi\trans-Tetraaquabis[3-(3-pyridyl)acrylato-\kN]cobalt(II) ; _journal_coeditor_code HK2421 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m426 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.810 _cell_angle_gamma 90.000 _cell_length_a 11.2350 _cell_length_b 7.0200 _cell_length_c 12.0120 _exptl_crystal_F_000 442.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file hk2421Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\XSCANS\CO2 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 1553.78 1811.05 24.34 o 6 0 0 2168.75 2230.59 33.96 o 8 0 0 2246.87 2407.53 40.65 o 10 0 0 26.23 53.90 2.96 o 12 0 0 48.00 50.80 3.19 o 14 0 0 501.58 521.78 9.98 o 1 1 0 3919.64 3751.70 60.47 o 2 1 0 771.91 817.95 26.04 o 3 1 0 4463.98 4724.31 28.17 o 4 1 0 1192.05 1333.57 15.43 o 5 1 0 9009.87 9873.59 46.15 o 6 1 0 14.91 23.63 3.85 o 7 1 0 575.23 605.48 14.67 o 8 1 0 168.38 174.59 6.66 o 9 1 0 283.57 267.72 14.26 o 10 1 0 26.37 30.79 1.68 o 11 1 0 478.21 461.47 10.37 o 12 1 0 97.20 97.65 4.40 o 13 1 0 140.69 136.86 9.87 o 14 1 0 20.12 18.17 2.50 o 0 2 0 7893.63 8004.36 43.49 o 1 2 0 3115.56 3164.57 20.10 o 2 2 0 4084.61 4219.27 34.65 o 3 2 0 70.18 68.20 3.38 o 4 2 0 3056.48 3158.78 36.34 o 5 2 0 57.76 68.57 2.44 o 6 2 0 517.44 520.52 18.02 o 7 2 0 65.12 72.13 4.14 o 8 2 0 153.08 159.52 8.49 o 9 2 0 0.07 0.92 1.98 o 10 2 0 172.35 190.00 11.02 o 11 2 0 81.54 74.99 3.81 o 12 2 0 189.11 192.59 8.69 o 13 2 0 6.87 4.40 3.05 o 14 2 0 232.13 224.82 6.97 o 1 3 0 765.13 705.40 12.00 o 2 3 0 1317.54 1428.94 24.48 o 3 3 0 2816.39 2675.96 34.85 o 4 3 0 103.93 123.01 6.31 o 5 3 0 539.68 585.84 19.38 o 6 3 0 4.61 4.91 1.52 o 7 3 0 150.24 157.78 6.77 o 8 3 0 78.04 74.20 4.22 o 9 3 0 268.95 268.74 12.75 o 10 3 0 2.23 4.96 2.26 o 11 3 0 201.71 211.93 9.56 o 12 3 0 5.92 4.51 2.75 o 13 3 0 53.28 42.60 3.74 o 0 4 0 9.21 16.90 1.37 o 1 4 0 211.20 225.49 8.02 o 2 4 0 853.44 822.81 22.22 o 3 4 0 0.37 0.00 1.30 o 4 4 0 375.90 370.60 16.88 o 5 4 0 25.74 27.03 1.78 o 6 4 0 208.42 194.81 9.39 o 7 4 0 13.32 14.01 2.12 o 8 4 0 350.78 336.47 14.50 o 9 4 0 8.50 10.31 2.33 o 10 4 0 448.43 429.95 13.34 o 11 4 0 0.41 0.00 2.52 o 12 4 0 45.85 40.64 3.36 o 13 4 0 56.12 57.58 3.87 o 1 5 0 362.69 344.60 11.65 o 2 5 0 273.16 266.35 13.24 o 3 5 0 529.14 511.05 20.12 o 4 5 0 27.37 26.26 1.92 o 5 5 0 51.03 47.33 2.30 o 6 5 0 246.74 253.53 12.46 o 7 5 0 80.75 78.35 4.48 o 8 5 0 25.16 20.90 2.62 o 9 5 0 11.97 12.28 2.38 o 10 5 0 94.06 91.62 4.85 o 11 5 0 261.00 262.14 8.49 o 12 5 0 1.54 4.51 2.96 o 0 6 0 1.79 4.37 1.64 o 1 6 0 68.96 72.17 2.89 o 2 6 0 62.99 61.17 3.30 o 3 6 0 1.58 2.29 1.83 o 4 6 0 56.76 55.79 2.53 o 5 6 0 80.48 73.54 4.30 o 6 6 0 752.45 751.63 19.26 o 7 6 0 47.79 51.73 2.82 o 8 6 0 390.20 399.34 12.51 o 9 6 0 91.74 94.28 3.74 o 10 6 0 56.45 56.20 3.42 o 11 6 0 21.69 22.65 3.36 o 1 7 0 113.46 121.87 4.64 o 2 7 0 203.81 215.92 10.54 o 3 7 0 294.01 305.13 12.65 o 4 7 0 0.54 0.00 2.01 o 5 7 0 89.44 87.77 5.20 o 6 7 0 71.77 76.77 3.35 o 7 7 0 62.79 67.27 3.58 o 8 7 0 46.60 54.19 3.27 o 9 7 0 42.55 40.82 3.42 o 10 7 0 0.85 0.00 2.98 o 0 8 0 165.96 183.76 8.33 o 1 8 0 14.83 11.36 1.65 o 2 8 0 75.53 84.12 3.85 o 3 8 0 8.20 10.76 2.29 o 4 8 0 11.46 15.95 2.46 o 5 8 0 7.81 9.21 2.29 o 6 8 0 116.68 126.21 5.95 o 7 8 0 28.99 36.86 3.27 o 8 8 0 497.99 519.23 9.38 o 1 9 0 28.55 40.20 2.05 o 2 9 0 2.24 8.70 2.18 o 3 9 0 127.70 149.79 6.31 o 4 9 0 1.73 3.07 2.55 o 5 9 0 76.61 85.82 3.84 o 6 9 0 3.40 1.63 2.78 o -13 0 1 236.58 242.91 8.96 o -11 0 1 898.26 880.29 20.30 o -9 0 1 758.06 884.83 24.46 o -7 0 1 209.19 177.24 10.56 o -5 0 1 78.88 57.18 2.89 o -3 0 1 1645.91 1864.26 21.42 o -1 0 1 3129.52 2877.54 43.92 o 3 0 1 151.96 146.10 7.09 o 5 0 1 3949.85 4256.66 43.60 o 7 0 1 486.65 563.05 20.06 o 9 0 1 17.27 14.66 2.09 o 11 0 1 222.01 231.79 10.54 o 13 0 1 12.89 11.94 3.02 o -14 1 1 277.89 273.34 5.84 o -13 1 1 0.17 1.72 1.94 o -12 1 1 523.01 503.32 9.91 o -11 1 1 112.64 108.55 3.85 o -10 1 1 95.88 106.66 3.62 o -9 1 1 13.70 9.73 1.38 o -8 1 1 532.83 577.90 14.83 o -7 1 1 334.45 383.07 25.18 o -6 1 1 1710.94 1636.24 21.11 o -5 1 1 1004.10 1111.58 38.07 o -4 1 1 1592.56 1624.28 139.96 o -3 1 1 8.77 9.37 0.62 o -2 1 1 148.87 194.15 4.86 o -1 1 1 166.61 182.03 4.27 o 1 1 1 83.15 98.75 4.01 o 2 1 1 4233.29 4482.94 97.22 o 3 1 1 2411.52 2545.62 43.79 o 4 1 1 387.55 355.61 9.65 o 5 1 1 63.23 79.39 2.96 o 6 1 1 688.62 774.87 15.07 o 7 1 1 549.06 595.13 14.75 o 8 1 1 94.88 101.47 3.81 o 9 1 1 233.90 202.58 7.83 o 10 1 1 263.08 262.09 8.50 o 11 1 1 110.18 100.02 3.33 o 12 1 1 74.67 70.37 2.48 o 13 1 1 70.91 68.93 5.19 o 14 1 1 30.74 25.18 2.63 o -14 2 1 121.73 132.81 5.88 o -13 2 1 237.72 236.44 8.75 o -12 2 1 95.03 84.95 3.93 o -11 2 1 509.69 515.11 15.73 o -10 2 1 160.98 121.79 6.06 o -9 2 1 448.86 500.01 18.14 o -8 2 1 172.19 185.07 9.68 o -7 2 1 202.16 215.20 9.71 o -6 2 1 7.09 6.60 1.35 o -5 2 1 1682.82 1746.89 29.14 o -4 2 1 311.83 326.74 12.54 o -3 2 1 2924.95 2965.45 31.57 o -2 2 1 3438.13 3556.37 32.06 o -1 2 1 262.87 268.33 6.44 o 1 2 1 2739.46 2833.32 85.58 o 2 2 1 0.39 0.57 0.86 o 3 2 1 2189.52 2228.31 28.70 o 4 2 1 11.69 7.52 1.20 o 5 2 1 1894.33 2007.37 32.78 o 6 2 1 122.28 126.67 5.51 o 7 2 1 584.61 591.06 21.03 o 8 2 1 3.72 4.48 1.84 o 9 2 1 65.47 71.46 3.61 o 10 2 1 1.54 0.00 2.32 o 11 2 1 75.83 76.72 3.90 o 12 2 1 10.41 15.84 2.82 o 13 2 1 143.92 131.31 6.26 o -14 3 1 152.70 151.41 6.12 o -13 3 1 19.09 20.49 3.18 o -12 3 1 266.88 265.06 9.50 o -11 3 1 3.46 1.35 2.47 o -10 3 1 741.83 739.43 18.83 o -9 3 1 4.74 8.78 2.01 o -8 3 1 120.51 114.23 5.95 o -7 3 1 0.07 14.30 1.78 o -6 3 1 492.08 502.92 19.61 o -5 3 1 1137.05 1285.53 27.64 o -4 3 1 3450.40 3576.22 43.11 o -3 3 1 550.96 618.27 17.30 o -2 3 1 1060.51 990.71 20.72 o -1 3 1 606.35 648.56 11.72 o 0 3 1 345.51 324.73 13.63 o 1 3 1 380.19 368.80 9.24 o 2 3 1 4152.90 4020.97 41.44 o 3 3 1 17.36 14.67 1.29 o 4 3 1 2310.95 2357.91 36.11 o 5 3 1 1044.53 1097.56 27.19 o 6 3 1 268.99 302.81 13.17 o 7 3 1 17.32 26.29 2.00 o 8 3 1 413.99 432.20 16.08 o 9 3 1 8.97 8.20 2.19 o 10 3 1 287.71 301.37 11.63 o 11 3 1 25.60 30.08 2.90 o 12 3 1 157.09 156.02 7.43 o 13 3 1 10.18 7.21 3.35 o -13 4 1 1.99 6.20 2.92 o -12 4 1 18.51 17.76 2.96 o -11 4 1 222.65 223.96 9.61 o -10 4 1 111.82 97.47 4.63 o -9 4 1 1409.26 1457.52 26.32 o -8 4 1 282.68 271.41 13.52 o -7 4 1 443.58 444.79 18.03 o -6 4 1 90.99 101.57 5.40 o -5 4 1 2.70 4.01 1.49 o -4 4 1 88.59 98.54 5.79 o -3 4 1 749.43 725.97 21.35 o -2 4 1 100.05 108.15 4.99 o -1 4 1 6109.88 6135.49 40.95 o 0 4 1 3047.35 3269.69 30.85 o 1 4 1 1359.02 1327.88 19.61 o 2 4 1 219.22 254.58 12.20 o 3 4 1 219.28 222.33 11.60 o 4 4 1 48.32 43.52 1.87 o 5 4 1 469.78 466.35 18.60 o 6 4 1 189.12 191.24 9.36 o 7 4 1 1744.52 1783.89 32.14 o 8 4 1 31.86 33.66 2.50 o 9 4 1 305.59 310.30 12.57 o 10 4 1 7.15 8.41 2.49 o 11 4 1 14.94 16.39 2.84 o 12 4 1 0.08 0.00 2.98 o -12 5 1 117.19 122.15 5.66 o -11 5 1 9.01 16.36 2.66 o -10 5 1 66.22 64.78 3.33 o -9 5 1 17.21 17.51 2.44 o -8 5 1 197.15 196.38 10.71 o -7 5 1 45.39 47.93 2.99 o -6 5 1 1254.33 1296.56 28.13 o -5 5 1 100.13 124.03 6.20 o -4 5 1 235.11 235.51 12.28 o -3 5 1 45.68 44.31 2.67 o -2 5 1 466.38 526.02 20.15 o -1 5 1 65.17 68.14 2.33 o 0 5 1 861.77 843.72 18.03 o 1 5 1 73.38 74.76 2.59 o 2 5 1 1115.75 1076.01 28.61 o 3 5 1 14.41 19.83 1.87 o 4 5 1 787.37 751.88 23.01 o 5 5 1 3.22 9.27 1.93 o 6 5 1 215.13 214.69 11.62 o 7 5 1 5.00 1.69 2.23 o 8 5 1 642.38 631.45 16.50 o 9 5 1 36.63 31.66 2.93 o 10 5 1 311.93 308.81 9.75 o 11 5 1 2.06 8.44 2.84 o 12 5 1 154.54 160.02 5.86 o -11 6 1 73.41 76.34 4.59 o -10 6 1 8.51 8.82 2.78 o -9 6 1 146.39 147.76 7.57 o -8 6 1 39.25 45.04 2.85 o -7 6 1 215.00 218.71 10.02 o -6 6 1 0.86 2.99 2.07 o -5 6 1 131.03 133.78 6.75 o -4 6 1 2.18 4.11 1.78 o -3 6 1 534.84 550.14 18.52 o -2 6 1 23.97 29.33 2.07 o -1 6 1 1132.17 1185.02 34.92 o 0 6 1 3.52 3.90 1.20 o 1 6 1 2.12 5.87 3.18 o 2 6 1 0.01 0.00 1.72 o 3 6 1 425.56 422.52 16.59 o 4 6 1 1.34 0.74 1.95 o 5 6 1 957.69 1031.20 22.67 o 6 6 1 18.95 18.75 2.44 o 7 6 1 308.15 302.84 11.92 o 8 6 1 115.28 111.88 5.92 o 9 6 1 18.65 19.31 2.95 o 10 6 1 0.11 0.00 2.89 o 11 6 1 197.44 188.42 6.26 o -10 7 1 1.20 5.83 2.76 o -9 7 1 42.91 48.71 3.39 o -8 7 1 89.56 102.64 4.91 o -7 7 1 47.34 53.45 3.07 o -6 7 1 446.93 466.66 13.24 o -5 7 1 59.92 59.41 3.79 o -4 7 1 104.53 121.50 4.94 o -3 7 1 115.50 126.72 5.76 o -2 7 1 97.01 103.39 4.65 o -1 7 1 13.80 12.28 1.46 o 0 7 1 123.45 123.26 6.20 o 1 7 1 55.29 67.91 2.35 o 2 7 1 322.36 299.79 12.69 o 3 7 1 0.39 0.00 2.10 o 4 7 1 257.11 272.39 11.39 o 5 7 1 9.91 6.23 2.33 o 6 7 1 43.34 45.40 2.90 o 7 7 1 56.83 60.67 3.28 o 8 7 1 221.77 242.30 7.73 o 9 7 1 52.68 50.88 3.68 o -8 8 1 31.37 37.02 3.41 o -7 8 1 68.67 79.51 3.62 o -6 8 1 2.77 3.84 2.47 o -5 8 1 44.51 51.20 3.01 o -4 8 1 20.89 29.08 2.52 o -3 8 1 162.51 166.59 8.21 o -2 8 1 14.27 20.67 2.39 o -1 8 1 87.99 100.78 4.51 o 0 8 1 136.86 134.25 6.21 o 1 8 1 69.68 79.72 2.90 o 2 8 1 41.17 40.73 2.79 o 3 8 1 101.81 110.48 5.63 o 4 8 1 1.30 3.38 2.30 o 5 8 1 31.86 31.83 2.89 o 6 8 1 26.65 25.15 2.99 o 7 8 1 70.57 75.14 3.84 o 8 8 1 1.23 6.29 3.01 o -6 9 1 17.69 20.95 3.10 o -5 9 1 8.35 7.69 2.82 o -4 9 1 104.76 130.51 5.85 o -3 9 1 0.00 4.21 2.49 o -2 9 1 54.04 65.45 3.35 o -1 9 1 2.22 3.83 1.64 o 0 9 1 13.12 11.41 2.22 o 1 9 1 17.53 20.71 4.87 o 2 9 1 74.30 88.15 3.91 o 3 9 1 5.67 2.62 2.78 o 4 9 1 46.94 53.15 3.41 o 5 9 1 58.92 58.56 3.55 o -14 0 2 54.99 50.35 3.48 o -12 0 2 554.46 514.65 14.81 o -10 0 2 2031.86 1814.81 32.97 o -8 0 2 1622.54 1636.47 34.85 o -6 0 2 108.80 71.55 2.93 o -4 0 2 75.57 86.11 4.77 o -2 0 2 1663.73 1414.41 17.54 o 0 0 2 2742.05 3193.40 91.94 o 2 0 2 10.83 18.08 0.81 o 4 0 2 3135.58 3256.28 36.69 o 6 0 2 4538.66 4642.04 52.89 o 8 0 2 351.62 327.47 15.90 o 10 0 2 303.38 278.52 12.15 o 12 0 2 223.95 220.83 8.70 o -15 1 2 960.47 921.59 8.40 o -14 1 2 0.03 0.00 2.17 o -13 1 2 411.95 398.46 8.21 o -12 1 2 124.36 133.85 6.15 o -11 1 2 387.16 382.79 20.44 o -10 1 2 13.19 7.25 1.51 o -9 1 2 694.61 741.01 26.24 o -8 1 2 303.70 336.10 11.38 o -7 1 2 788.40 755.25 19.94 o -6 1 2 244.36 266.34 12.59 o -5 1 2 354.85 505.47 25.52 o -4 1 2 471.40 506.52 34.85 o -3 1 2 445.11 438.47 11.68 o -2 1 2 366.72 371.80 6.95 o -1 1 2 4259.25 4309.00 109.17 o 0 1 2 221.33 242.31 18.19 o 1 1 2 4801.16 4861.97 190.37 o 2 1 2 136.01 134.89 10.96 o 3 1 2 278.57 264.20 7.47 o 4 1 2 249.58 264.50 8.44 o 5 1 2 506.71 482.14 11.73 o 6 1 2 471.23 482.25 12.88 o 7 1 2 1206.51 1211.45 20.31 o 8 1 2 68.71 58.75 1.78 o 9 1 2 129.04 146.21 6.06 o 10 1 2 25.09 27.39 1.78 o 11 1 2 348.66 376.76 8.29 o 12 1 2 70.28 79.81 2.64 o 13 1 2 201.44 192.34 4.99 o -14 2 2 129.40 125.92 6.25 o -13 2 2 2.39 2.85 2.79 o -12 2 2 529.72 533.02 14.40 o -11 2 2 66.67 58.87 2.89 o -10 2 2 1082.09 1068.17 24.09 o -9 2 2 76.95 69.57 3.35 o -8 2 2 196.36 196.81 12.69 o -7 2 2 707.76 729.53 23.08 o -6 2 2 648.40 658.20 20.41 o -5 2 2 117.73 126.09 6.81 o -4 2 2 4678.77 4929.02 45.46 o -3 2 2 1065.62 1138.52 20.38 o -2 2 2 13.02 13.57 0.92 o -1 2 2 5013.18 5314.81 46.62 o 0 2 2 1688.41 1892.61 34.88 o 1 2 2 571.38 575.02 10.06 o 2 2 2 2800.35 2680.75 30.66 o 3 2 2 385.73 440.66 14.09 o 4 2 2 3879.30 3966.03 44.02 o 5 2 2 16.70 23.16 1.47 o 6 2 2 1776.00 1836.50 35.67 o 7 2 2 1407.42 1465.67 31.42 o 8 2 2 230.26 251.87 12.22 o 9 2 2 13.09 15.52 2.29 o 10 2 2 139.51 139.01 6.91 o 11 2 2 12.20 17.66 2.72 o 12 2 2 378.55 354.70 9.85 o 13 2 2 181.25 185.47 6.54 o -14 3 2 21.77 27.81 3.36 o -13 3 2 282.78 273.62 9.16 o -12 3 2 66.39 57.44 3.33 o -11 3 2 254.87 278.16 11.86 o -10 3 2 2.02 0.00 2.26 o -9 3 2 296.60 324.67 14.79 o -8 3 2 134.53 140.52 7.07 o -7 3 2 673.30 700.11 23.80 o -6 3 2 306.99 327.29 15.47 o -5 3 2 2474.82 2480.37 38.28 o -4 3 2 132.98 141.08 6.72 o -3 3 2 38.91 20.15 1.26 o -2 3 2 19.40 14.81 1.14 o -1 3 2 7.41 5.60 0.71 o 0 3 2 29.80 38.67 4.38 o 1 3 2 6315.13 6547.86 82.58 o 2 3 2 498.13 545.74 16.68 o 3 3 2 1604.07 1635.07 29.50 o 4 3 2 76.59 79.68 3.70 o 5 3 2 3.89 4.76 1.57 o 6 3 2 10.24 12.17 1.78 o 7 3 2 985.81 955.64 24.63 o 8 3 2 481.17 469.62 16.36 o 9 3 2 1067.73 1036.32 21.30 o 10 3 2 112.58 112.52 5.54 o 11 3 2 49.17 43.42 3.30 o 12 3 2 39.14 44.08 3.56 o 13 3 2 59.04 49.60 3.91 o -13 4 2 6.70 6.71 2.99 o -12 4 2 215.40 204.93 8.90 o -11 4 2 15.31 13.87 2.53 o -10 4 2 419.21 464.83 14.49 o -9 4 2 47.74 48.73 2.69 o -8 4 2 174.47 178.01 9.12 o -7 4 2 2.37 1.58 1.81 o -6 4 2 149.83 176.94 8.79 o -5 4 2 2.79 4.37 1.60 o -4 4 2 1208.16 1271.44 29.37 o -3 4 2 204.22 218.30 10.16 o -2 4 2 1233.30 1189.59 26.49 o -1 4 2 187.55 163.73 6.68 o 0 4 2 2720.44 2751.33 30.97 o 1 4 2 377.99 399.85 11.52 o 2 4 2 801.13 796.46 22.54 o 3 4 2 614.25 660.17 21.38 o 4 4 2 486.32 520.66 19.95 o 5 4 2 11.54 9.41 1.78 o 6 4 2 254.40 268.77 13.64 o 7 4 2 0.56 4.56 2.16 o 8 4 2 690.60 679.29 18.17 o 9 4 2 186.39 187.40 8.46 o 10 4 2 163.72 154.11 7.86 o 11 4 2 45.02 47.65 3.33 o 12 4 2 68.18 65.95 4.02 o -13 5 2 53.58 54.56 3.70 o -12 5 2 29.20 22.04 3.24 o -11 5 2 29.73 27.81 2.85 o -10 5 2 13.54 14.38 2.46 o -9 5 2 633.26 645.16 16.54 o -8 5 2 43.96 44.38 2.66 o -7 5 2 955.09 968.73 23.13 o -6 5 2 231.05 212.95 11.60 o -5 5 2 682.74 672.38 22.08 o 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