#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/75/2217570.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217570_Fobs loop_ _publ_author_name 'Xu, Hai-Yun' 'Ma, Huai-Ling' 'Xu, Mao-Tian' 'Zhao, Wen-Xian' 'Guo, Bao-Guo' _publ_section_title ; catena-Poly[[[diaquairon(II)]-\m-pyridine-2,5-dicarboxylato-[tetraaquairon(II)]-\m-pyridine-2,5-dicarboxylato] tetrahydrate] ; _journal_coeditor_code IS2270 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m413 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 90.942 _cell_angle_beta 101.375 _cell_angle_gamma 108.112 _cell_length_a 7.0980 _cell_length_b 8.9222 _cell_length_c 9.7204 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file is2270Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 123 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1.73 1.02 0.41 o 2 0 0 1378.20 1457.40 13.20 o 3 0 0 84.16 76.68 3.25 o 4 0 0 1896.63 1856.94 19.70 o 5 0 0 158.68 155.68 14.83 o 6 0 0 239.66 220.70 30.62 o 7 0 0 3.47 4.37 1.83 o -8 1 0 46.47 41.34 4.47 o -7 1 0 9.82 8.33 2.13 o -6 1 0 700.75 683.19 58.40 o -5 1 0 3.67 2.74 1.93 o -4 1 0 3261.82 3270.87 27.52 o -3 1 0 241.72 229.22 5.18 o -2 1 0 2843.47 3067.24 22.14 o -1 1 0 15.01 13.10 0.81 o 0 1 0 2889.04 2699.19 59.72 o 1 1 0 463.02 513.46 54.79 o 2 1 0 5.58 7.81 0.95 o 3 1 0 112.10 96.69 11.07 o 4 1 0 25.54 26.69 2.03 o 5 1 0 82.41 88.09 7.72 o 6 1 0 143.15 133.99 12.59 o 7 1 0 0.80 1.73 1.73 o -8 2 0 123.36 136.09 7.82 o -7 2 0 0.96 0.20 1.32 o -6 2 0 578.34 584.68 24.02 o -5 2 0 141.10 153.66 5.59 o -4 2 0 2096.74 2216.26 21.02 o -3 2 0 5.11 7.92 1.42 o -2 2 0 1816.22 1927.52 16.05 o -1 2 0 250.97 228.36 14.88 o 0 2 0 2241.40 2291.79 36.71 o 1 2 0 145.93 149.47 11.37 o 2 2 0 32.22 40.62 4.72 o 3 2 0 170.32 172.04 21.02 o 4 2 0 177.00 190.46 19.80 o 5 2 0 121.89 118.19 9.19 o 6 2 0 416.99 451.14 44.53 o 7 2 0 17.34 20.01 3.25 o -8 3 0 130.04 145.13 8.23 o -7 3 0 3.23 2.95 1.73 o -6 3 0 428.43 439.86 10.26 o -5 3 0 23.23 35.75 2.84 o -4 3 0 1137.13 1193.54 14.62 o -3 3 0 239.30 231.25 5.48 o -2 3 0 163.15 249.54 5.28 o -1 3 0 94.48 89.74 6.65 o 0 3 0 136.51 139.84 1.75 o 1 3 0 497.19 619.41 19.86 o 2 3 0 2222.91 2466.93 217.85 o 3 3 0 131.38 165.84 14.57 o 4 3 0 500.22 517.98 41.79 o 5 3 0 22.21 25.12 2.12 o 6 3 0 242.66 250.15 17.52 o -8 4 0 86.39 92.01 6.60 o -7 4 0 35.05 39.51 4.06 o -6 4 0 97.45 91.30 4.77 o -5 4 0 9.39 8.43 2.03 o -4 4 0 157.39 199.87 5.89 o -3 4 0 52.73 46.62 2.74 o -2 4 0 397.77 422.54 21.53 o -1 4 0 1553.13 1618.33 120.55 o 0 4 0 1223.35 1240.11 24.17 o 1 4 0 133.43 135.29 12.64 o 2 4 0 1449.40 1468.47 151.38 o 3 4 0 29.05 24.13 2.69 o 4 4 0 610.25 597.90 32.50 o 5 4 0 3.15 3.96 1.83 o 6 4 0 291.22 287.62 10.97 o -8 5 0 89.66 87.04 6.50 o -7 5 0 21.28 24.98 3.35 o -6 5 0 86.06 88.56 4.77 o -4 5 0 940.67 985.24 14.52 o -3 5 0 49.38 60.49 2.64 o -2 5 0 3362.19 3223.79 271.22 o -1 5 0 20.04 15.77 1.83 o 0 5 0 2152.23 1955.18 170.62 o 1 5 0 25.85 23.56 2.84 o 2 5 0 991.26 1040.69 16.96 o 3 5 0 508.70 519.79 12.59 o 4 5 0 394.98 367.96 11.27 o 5 5 0 0.21 0.00 1.62 o -7 6 0 5.68 7.92 2.23 o -6 6 0 207.75 205.05 7.62 o -5 6 0 27.08 22.85 2.54 o -4 6 0 729.11 742.05 11.17 o -3 6 0 303.22 304.32 18.84 o -2 6 0 880.56 812.05 39.15 o -1 6 0 59.25 52.44 2.46 o 0 6 0 1433.31 1325.05 124.92 o 1 6 0 414.32 427.06 10.97 o 2 6 0 4.72 6.80 2.13 o 3 6 0 1.85 2.13 1.73 o 4 6 0 224.43 219.68 9.45 o -7 7 0 8.96 9.45 2.23 o -5 7 0 9.02 10.39 1.43 o -4 7 0 268.45 261.75 5.77 o -3 7 0 0.50 2.10 1.05 o -2 7 0 423.53 399.34 20.26 o -1 7 0 42.89 29.73 2.12 o 0 7 0 520.01 524.44 19.25 o 1 7 0 671.38 606.52 14.12 o 2 7 0 112.07 120.35 6.70 o 3 7 0 3.14 0.41 1.83 o 4 7 0 107.57 121.16 7.82 o -5 8 0 35.33 34.94 3.45 o -4 8 0 280.21 280.21 15.08 o -3 8 0 6.38 6.15 1.29 o -2 8 0 103.91 101.51 3.83 o -1 8 0 21.17 22.33 2.01 o 0 8 0 874.97 897.44 14.78 o 1 8 0 12.66 10.16 2.54 o 2 8 0 181.42 198.35 9.14 o 3 8 0 29.56 27.93 4.27 o -5 9 0 0.01 0.51 1.32 o -4 9 0 19.87 21.12 2.95 o -3 9 0 15.35 14.42 2.54 o -2 9 0 194.42 180.58 8.12 o -1 9 0 7.81 7.19 1.61 o 0 9 0 359.80 358.00 12.09 o 1 9 0 33.33 33.72 3.96 o -5 10 0 0.02 1.22 1.52 o -3 10 0 22.98 23.66 3.25 o -2 10 0 216.56 204.34 9.24 o -1 10 0 1.61 1.22 1.42 o 0 10 0 54.79 42.86 4.57 o 0 -10 1 15.76 16.66 3.05 o 1 -10 1 25.06 24.56 2.55 o 2 -10 1 25.25 24.48 3.35 o 3 -10 1 132.30 125.73 7.01 o 4 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366.02 6.75 o 3 -6 1 670.10 641.78 52.30 o 4 -6 1 60.98 71.29 3.16 o 5 -6 1 369.62 395.68 9.19 o 6 -6 1 12.94 16.76 2.64 o 7 -6 1 212.97 218.86 9.14 o -5 -5 1 336.65 353.43 11.98 o -4 -5 1 156.63 162.80 7.62 o -3 -5 1 6.74 9.55 2.34 o -2 -5 1 109.78 89.78 5.08 o -1 -5 1 867.95 863.34 10.02 o 0 -5 1 596.16 560.06 14.02 o 1 -5 1 2.24 3.92 1.02 o 2 -5 1 630.92 614.98 34.99 o 3 -5 1 1105.50 1120.40 36.16 o 4 -5 1 116.58 141.73 3.69 o 5 -5 1 194.99 206.45 4.84 o 6 -5 1 1.13 2.54 1.62 o 7 -5 1 12.27 15.13 2.74 o -6 -4 1 0.67 2.23 2.13 o -5 -4 1 118.37 120.76 6.60 o -4 -4 1 26.21 28.44 3.25 o -3 -4 1 484.66 497.16 33.01 o -2 -4 1 324.73 306.94 19.20 o -1 -4 1 1687.99 1841.76 66.42 o 0 -4 1 422.08 453.32 18.38 o 1 -4 1 1992.08 2124.50 135.14 o 2 -4 1 153.28 150.09 7.35 o 3 -4 1 538.54 618.30 9.45 o 4 -4 1 1.98 0.78 0.90 o 5 -4 1 384.67 395.79 14.37 o 6 -4 1 40.95 46.51 4.06 o 7 -4 1 90.55 92.93 5.99 o 8 -4 1 8.09 8.43 2.84 o -6 -3 1 3.44 2.79 1.29 o -5 -3 1 453.82 500.74 57.53 o -4 -3 1 1.84 2.06 1.14 o -3 -3 1 1060.07 1158.14 117.40 o -2 -3 1 235.89 221.87 34.58 o -1 -3 1 2475.07 2561.67 70.84 o 0 -3 1 1216.14 1102.47 37.07 o 1 -3 1 369.43 504.89 30.12 o 2 -3 1 305.44 365.48 8.38 o 3 -3 1 889.50 1012.40 8.62 o 4 -3 1 64.82 75.22 5.48 o 5 -3 1 2365.53 2396.63 128.32 o 6 -3 1 7.40 5.38 1.83 o 7 -3 1 79.17 78.81 5.59 o 8 -3 1 7.08 3.45 2.64 o -7 -2 1 157.67 160.80 14.73 o -6 -2 1 0.04 0.00 0.88 o -5 -2 1 290.15 327.14 34.43 o -4 -2 1 485.89 501.61 52.10 o -3 -2 1 567.22 485.87 9.65 o -2 -2 1 347.14 290.16 6.50 o -1 -2 1 2041.02 2281.60 186.77 o 0 -2 1 242.59 226.31 3.05 o 1 -2 1 1936.15 2061.78 54.59 o 2 -2 1 506.67 543.31 5.89 o 3 -2 1 810.03 910.86 16.55 o 4 -2 1 372.71 391.12 5.69 o 5 -2 1 1360.68 1397.48 96.69 o 6 -2 1 2.55 3.15 1.83 o 7 -2 1 63.28 65.20 5.18 o 8 -2 1 3.69 4.57 1.83 o -7 -1 1 248.77 254.15 36.66 o -6 -1 1 13.18 10.35 1.58 o -5 -1 1 288.34 223.64 7.52 o -4 -1 1 96.07 85.72 4.37 o -3 -1 1 1768.46 1352.18 15.84 o -2 -1 1 3.12 7.82 1.42 o -1 -1 1 3671.47 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24.78 3.45 o 0 0 10 174.77 160.87 8.02 o 1 0 10 32.02 31.28 3.96 o 2 0 10 163.71 158.33 8.73 o -5 1 10 1.07 3.29 1.54 o -4 1 10 59.32 64.58 3.69 o -3 1 10 0.68 0.00 1.83 o -2 1 10 166.70 152.65 7.82 o -1 1 10 4.26 3.76 2.03 o 0 1 10 190.26 175.40 8.53 o 1 1 10 3.94 1.62 2.23 o 2 1 10 82.98 78.20 6.50 o -5 2 10 5.36 5.56 1.73 o -4 2 10 59.01 47.77 5.08 o -3 2 10 0.90 1.52 2.03 o -2 2 10 43.49 43.37 4.57 o -1 2 10 68.50 59.21 5.08 o 0 2 10 275.69 274.93 10.87 o 1 2 10 1.90 3.55 2.13 o -5 3 10 3.38 3.18 1.56 o -4 3 10 73.90 79.66 11.37 o -3 3 10 7.51 7.62 2.34 o -2 3 10 286.81 247.61 10.16 o -1 3 10 2.05 2.95 1.83 o 0 3 10 338.03 336.57 12.19 o -4 4 10 203.07 212.67 6.75 o -3 4 10 129.18 124.72 7.41 o -2 4 10 6.49 5.38 2.34 o -1 4 10 4.71 7.52 2.54 o -3 5 10 6.44 10.16 2.64 o -2 5 10 34.20 39.00 4.47 o 0 -3 11 6.24 7.72 2.84 o -3 -2 11 56.67 64.80 5.59 o -2 -2 11 2.41 3.96 2.64 o -1 -2 11 210.74 272.08 10.66 o 0 -2 11 20.27 21.73 3.76 o -3 -1 11 39.56 44.38 4.87 o -2 -1 11 2.60 4.16 2.64 o -1 -1 11 363.55 355.87 12.29 o 0 -1 11 27.25 25.90 3.86 o -4 0 11 2.77 5.59 2.74 o -3 0 11 63.38 73.43 5.99 o -2 0 11 43.68 48.85 4.98 o -1 0 11 107.81 119.23 7.41 o 0 0 11 0.00 0.00 2.13 o -4 1 11 0.88 0.00 2.74 o -3 1 11 16.55 13.00 3.35 o -2 1 11 1.75 0.91 2.34 o -1 1 11 46.38 41.03 4.77 o 0 1 11 19.87 20.92 3.86 o -3 2 11 60.85 61.34 5.79 o -2 2 11 1.45 1.42 2.74 o -1 2 11 100.55 105.52 7.21 o -2 3 11 47.98 47.63 4.98 o