#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217604.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217604_Fobs loop_ _publ_author_name 'Aghabozorg, Hossein' 'Khadivi, Ramona' 'Ghadermazi, Mohammad' 'Pasdar, Hoda' 'Hooshmand, Shabnam' _publ_section_title ; Poly[propane-1,3-diammonium [cuprate(II)-bis(\m~2~-pyridine-2,3-dicarboxylato)] trihydrate] ; _journal_coeditor_code OM2184 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m267 _journal_page_last m268 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.656 _cell_angle_beta 84.008 _cell_angle_gamma 71.952 _cell_length_a 6.6857 _cell_length_b 7.8251 _cell_length_c 9.9188 _exptl_crystal_F_000 271.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file om2184Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 84.18 100.71 1.50 o 2 0 0 491.67 672.56 7.55 o 3 0 0 9.60 15.13 1.83 o 4 0 0 290.08 232.64 5.43 o 5 0 0 76.60 188.16 8.80 o 6 0 0 362.57 366.21 7.28 o 7 0 0 82.07 85.13 4.09 o 8 0 0 33.48 39.18 3.43 o -8 1 0 160.69 158.94 7.38 o -7 1 0 389.71 372.29 8.04 o -6 1 0 767.82 735.66 11.24 o -5 1 0 94.19 98.12 2.72 o -4 1 0 46.87 69.48 4.43 o -3 1 0 505.33 646.43 8.83 o -2 1 0 2206.90 2175.75 17.27 o -1 1 0 2322.21 2249.75 17.98 o 0 1 0 2201.84 2104.14 14.92 o 1 1 0 102.27 94.13 2.35 o 2 1 0 97.11 103.71 4.13 o 3 1 0 77.26 72.32 2.98 o 4 1 0 599.53 580.66 6.61 o 5 1 0 106.62 111.71 3.65 o 6 1 0 3.16 16.54 2.61 o 7 1 0 32.28 35.45 2.89 o 8 1 0 356.86 355.62 8.92 o -7 2 0 305.70 309.85 11.63 o -6 2 0 506.22 462.05 8.53 o -5 2 0 4.34 5.39 1.69 o -4 2 0 299.35 280.43 3.77 o -3 2 0 96.79 67.58 1.77 o -2 2 0 1539.55 1464.68 12.26 o -1 2 0 679.09 858.70 7.46 o 0 2 0 31.49 220.72 4.69 o 1 2 0 2828.41 2584.66 20.13 o 2 2 0 870.11 795.29 7.61 o 3 2 0 71.90 112.55 6.45 o 4 2 0 106.89 129.58 3.36 o 5 2 0 496.08 475.59 5.41 o 6 2 0 103.63 179.29 5.81 o 7 2 0 198.21 182.83 5.44 o 8 2 0 109.67 115.89 4.86 o -7 3 0 26.40 39.55 4.13 o -6 3 0 20.47 16.10 2.99 o -5 3 0 141.25 127.71 4.24 o -4 3 0 23.76 31.32 1.78 o -3 3 0 390.01 355.73 4.56 o -2 3 0 147.92 256.58 5.78 o -1 3 0 593.11 726.98 6.82 o 0 3 0 1507.51 1581.94 12.91 o 2 3 0 170.03 249.85 6.66 o 3 3 0 34.11 37.34 1.55 o 4 3 0 603.86 681.54 6.96 o 5 3 0 441.85 413.85 5.56 o 6 3 0 1884.57 1886.09 21.56 o 7 3 0 136.94 179.56 5.27 o 8 3 0 182.48 158.38 5.49 o -6 4 0 246.98 249.71 8.17 o -5 4 0 198.23 157.67 5.93 o -4 4 0 7.07 14.24 1.65 o -3 4 0 247.80 271.70 4.15 o -2 4 0 901.61 903.30 8.81 o -1 4 0 592.63 676.29 10.39 o 0 4 0 256.51 235.82 3.61 o 1 4 0 12.51 209.20 5.70 o 2 4 0 546.34 511.25 5.83 o 3 4 0 1307.14 1294.78 11.30 o 4 4 0 835.91 770.13 11.23 o 5 4 0 411.02 393.62 5.16 o 6 4 0 596.90 606.43 8.02 o 7 4 0 8.40 5.79 2.01 o 8 4 0 192.63 188.81 6.28 o -6 5 0 31.27 42.28 6.70 o -5 5 0 22.52 36.39 3.66 o -4 5 0 119.73 120.63 4.32 o -3 5 0 347.64 389.35 5.44 o -2 5 0 400.47 428.79 5.49 o -1 5 0 348.81 329.33 4.43 o 0 5 0 1209.46 1150.34 10.48 o 1 5 0 13.43 83.73 5.55 o 2 5 0 2134.06 2081.58 23.55 o 3 5 0 222.88 201.43 3.52 o 4 5 0 657.68 607.78 7.60 o 5 5 0 1.30 9.09 1.32 o 6 5 0 181.29 186.41 4.14 o 7 5 0 123.39 119.31 5.27 o 8 5 0 7.04 4.98 2.77 o -5 6 0 221.78 222.80 7.69 o -4 6 0 327.23 315.18 7.89 o -3 6 0 563.11 551.65 8.10 o -2 6 0 43.80 46.98 2.08 o -1 6 0 467.01 459.27 6.16 o 0 6 0 153.22 214.63 4.25 o 1 6 0 68.09 50.83 2.09 o 2 6 0 199.97 179.32 4.43 o 3 6 0 287.06 269.07 6.59 o 4 6 0 114.90 97.63 2.77 o 5 6 0 13.43 104.89 5.78 o 6 6 0 34.27 34.22 2.20 o 7 6 0 6.77 19.64 3.05 o 8 6 0 135.45 140.46 8.18 o -4 7 0 49.19 42.49 3.97 o -3 7 0 178.87 183.61 5.44 o -2 7 0 111.86 101.83 4.06 o -1 7 0 172.64 179.50 4.17 o 0 7 0 354.11 366.98 7.78 o 1 7 0 104.75 91.74 3.58 o 2 7 0 32.02 23.62 2.46 o 3 7 0 462.02 413.40 7.59 o 4 7 0 85.07 74.31 3.39 o 5 7 0 24.12 73.98 3.87 o 6 7 0 46.01 37.68 3.51 o 7 7 0 169.68 168.82 6.34 o -3 8 0 97.39 102.45 6.50 o -2 8 0 21.43 21.48 2.63 o -1 8 0 60.80 102.61 5.11 o 0 8 0 274.78 292.96 6.51 o 1 8 0 156.20 141.31 4.68 o 2 8 0 265.94 254.30 7.36 o 3 8 0 73.09 63.78 3.41 o 4 8 0 104.16 105.03 4.28 o 5 8 0 117.39 112.55 4.50 o 6 8 0 196.74 186.05 7.29 o 7 8 0 6.36 23.92 5.48 o -1 9 0 263.56 282.65 8.81 o 0 9 0 28.26 28.76 3.61 o 1 9 0 291.71 304.40 7.06 o 2 9 0 204.27 178.96 5.52 o 3 9 0 133.11 124.40 4.76 o 4 9 0 18.81 9.56 2.37 o 5 9 0 211.27 174.66 5.82 o 6 9 0 2.59 1.94 2.28 o 1 10 0 160.38 152.01 6.88 o 2 10 0 150.01 150.84 6.80 o 3 10 0 172.86 149.77 5.50 o 4 10 0 13.79 24.72 3.57 o -3 -10 1 219.99 241.54 6.97 o -2 -10 1 7.27 6.92 2.92 o -6 -9 1 111.18 110.83 5.04 o -5 -9 1 583.47 597.96 11.30 o -4 -9 1 13.49 27.72 3.22 o -3 -9 1 82.88 86.84 4.19 o -2 -9 1 210.27 199.85 5.78 o -1 -9 1 79.97 64.84 4.62 o 0 -9 1 14.50 11.41 2.96 o 1 -9 1 151.60 160.77 6.72 o -7 -8 1 80.07 70.31 4.88 o -6 -8 1 34.09 29.14 2.93 o -5 -8 1 530.05 494.75 9.33 o -4 -8 1 46.83 157.34 5.13 o -3 -8 1 191.36 198.02 5.53 o -2 -8 1 136.78 109.44 4.13 o -1 -8 1 134.94 134.03 4.59 o 0 -8 1 1.09 2.90 2.27 o 1 -8 1 111.74 129.08 8.90 o 2 -8 1 5.68 21.17 2.62 o 3 -8 1 67.46 66.03 6.65 o -7 -7 1 124.07 117.88 5.58 o -6 -7 1 25.51 21.88 2.45 o -5 -7 1 33.08 62.00 3.32 o -4 -7 1 101.71 77.45 3.52 o -3 -7 1 53.87 62.98 3.29 o -2 -7 1 55.40 57.67 3.04 o -1 -7 1 489.27 481.92 8.13 o 0 -7 1 515.70 472.07 7.66 o 1 -7 1 1.33 2.72 1.62 o 2 -7 1 164.19 146.39 5.73 o 3 -7 1 201.83 210.29 5.84 o 4 -7 1 13.52 8.54 2.82 o -8 -6 1 76.14 72.57 6.56 o -7 -6 1 136.87 121.94 7.38 o -6 -6 1 13.19 12.95 2.53 o -5 -6 1 193.53 176.68 4.79 o -4 -6 1 81.27 88.70 4.52 o -3 -6 1 306.72 277.50 5.70 o -2 -6 1 686.72 638.27 9.32 o -1 -6 1 497.80 435.84 6.28 o 0 -6 1 197.58 202.43 3.44 o 1 -6 1 120.86 138.36 2.95 o 2 -6 1 19.11 25.86 1.89 o 3 -6 1 543.06 539.46 7.99 o 4 -6 1 287.58 313.19 7.19 o 5 -6 1 68.33 69.07 5.48 o -8 -5 1 247.44 231.81 7.72 o -7 -5 1 35.16 98.51 8.19 o -6 -5 1 98.76 101.82 3.97 o -5 -5 1 126.04 135.16 3.50 o -4 -5 1 652.20 655.32 7.92 o -3 -5 1 1036.70 1098.38 10.00 o -2 -5 1 680.96 940.96 9.94 o -1 -5 1 17.56 10.10 1.12 o 0 -5 1 70.30 102.02 3.58 o 1 -5 1 1533.57 1546.57 13.79 o 2 -5 1 1.55 45.84 4.20 o 3 -5 1 1039.64 994.02 11.57 o 4 -5 1 149.05 139.96 4.59 o 5 -5 1 43.25 48.09 4.02 o -8 -4 1 136.26 116.81 4.84 o -7 -4 1 75.54 88.51 4.00 o -6 -4 1 155.90 130.18 3.48 o -5 -4 1 605.03 654.42 8.06 o -4 -4 1 526.58 498.24 5.69 o -3 -4 1 977.65 941.41 8.71 o -2 -4 1 337.67 272.71 3.83 o -1 -4 1 695.95 696.23 7.86 o 0 -4 1 137.54 125.09 2.16 o 1 -4 1 382.46 373.60 4.44 o 2 -4 1 28.94 69.56 4.40 o 3 -4 1 160.57 180.56 4.38 o 4 -4 1 58.56 79.89 3.55 o 5 -4 1 448.28 438.70 8.98 o 6 -4 1 28.69 31.82 3.67 o -8 -3 1 202.12 182.05 6.92 o -7 -3 1 7.26 11.18 2.53 o -6 -3 1 648.38 640.54 9.14 o -5 -3 1 303.47 331.81 4.47 o -4 -3 1 6.77 168.16 5.46 o -3 -3 1 1696.84 1657.06 13.88 o -2 -3 1 119.39 95.11 2.10 o 0 -3 1 695.58 820.83 7.29 o 1 -3 1 54.31 106.95 4.84 o 2 -3 1 67.79 129.42 5.02 o 3 -3 1 1290.10 1300.22 12.59 o 4 -3 1 634.46 619.79 6.86 o 5 -3 1 151.84 126.11 4.47 o 6 -3 1 19.00 14.56 2.91 o 7 -3 1 63.47 55.49 4.63 o -8 -2 1 264.25 245.98 6.78 o -7 -2 1 51.49 49.76 3.24 o -6 -2 1 31.75 66.82 7.27 o -5 -2 1 130.00 97.18 2.68 o -4 -2 1 480.86 480.98 6.92 o -3 -2 1 43.86 48.84 2.74 o -2 -2 1 368.75 350.53 3.69 o -1 -2 1 388.71 446.97 3.81 o 0 -2 1 188.35 207.59 5.06 o 1 -2 1 3549.10 3678.42 28.46 o 2 -2 1 3438.44 3706.08 28.77 o 3 -2 1 1286.48 1147.48 10.26 o 4 -2 1 132.14 116.41 2.29 o 5 -2 1 5.71 45.42 4.05 o 6 -2 1 354.52 338.08 7.06 o 7 -2 1 294.62 302.39 9.22 o -8 -1 1 144.38 138.67 5.32 o -7 -1 1 19.06 13.36 2.30 o -6 -1 1 10.41 5.18 2.06 o -5 -1 1 1947.19 1886.89 20.82 o -4 -1 1 907.61 915.76 9.51 o -3 -1 1 270.72 254.29 3.54 o -2 -1 1 337.14 435.53 4.24 o -1 -1 1 212.31 258.53 5.56 o 0 -1 1 1653.81 1746.12 13.76 o 1 -1 1 3640.80 3759.19 28.13 o 2 -1 1 950.30 843.72 7.40 o 3 -1 1 567.95 600.82 6.42 o 4 -1 1 267.50 341.82 7.79 o 5 -1 1 619.70 649.19 9.12 o 6 -1 1 139.68 140.79 5.06 o 7 -1 1 128.17 102.25 4.35 o 8 -1 1 1.69 19.60 3.62 o -8 0 1 13.93 3.84 2.25 o -7 0 1 113.81 120.45 4.64 o -6 0 1 1472.61 1434.73 17.86 o -5 0 1 592.94 639.96 9.46 o -4 0 1 713.08 668.43 12.28 o -3 0 1 775.58 683.83 7.74 o -2 0 1 175.75 308.80 11.76 o -1 0 1 22.55 34.82 2.09 o 1 0 1 2.25 4.74 0.44 o 3 0 1 4680.59 4825.75 40.94 o 4 0 1 73.27 84.53 2.75 o 5 0 1 241.25 313.36 5.13 o 6 0 1 10.91 12.72 2.01 o 7 0 1 207.84 185.18 5.53 o 8 0 1 16.59 16.21 2.68 o -8 1 1 111.62 90.08 4.73 o -7 1 1 338.35 338.15 7.85 o -6 1 1 326.81 326.64 7.00 o -5 1 1 90.73 95.57 4.80 o -4 1 1 372.59 347.74 4.87 o -3 1 1 821.57 867.14 7.95 o -2 1 1 2219.44 2195.77 17.45 o -1 1 1 1.89 37.62 0.96 o 0 1 1 516.09 505.68 4.07 o 1 1 1 681.02 689.06 5.79 o 2 1 1 125.70 130.20 1.87 o 3 1 1 97.97 174.13 5.99 o 4 1 1 12.24 37.24 2.03 o 5 1 1 122.77 110.75 2.97 o 6 1 1 272.79 253.21 5.79 o 7 1 1 451.12 447.44 11.62 o 8 1 1 110.40 112.94 4.83 o -7 2 1 3.43 14.15 2.56 o -6 2 1 235.73 205.71 6.48 o -5 2 1 169.50 169.77 4.73 o -4 2 1 419.55 440.41 6.09 o -3 2 1 14.03 9.26 0.88 o -2 2 1 1577.00 1643.85 13.62 o -1 2 1 6.92 98.37 1.70 o 1 2 1 3151.03 3135.00 23.03 o 2 2 1 552.04 665.06 6.61 o 3 2 1 127.64 191.65 2.67 o 4 2 1 527.42 534.99 6.62 o 5 2 1 618.59 660.28 7.36 o 6 2 1 515.52 529.35 11.01 o 7 2 1 549.72 554.19 10.17 o 8 2 1 117.52 124.31 4.93 o -7 3 1 5.22 20.85 3.49 o -6 3 1 387.12 345.99 7.60 o -5 3 1 49.18 43.70 2.83 o -4 3 1 25.35 37.79 2.01 o -3 3 1 127.91 144.70 2.80 o -2 3 1 744.45 745.39 9.15 o -1 3 1 1006.36 1016.16 9.02 o 0 3 1 2236.98 2212.74 21.18 o 1 3 1 293.45 315.86 5.44 o 2 3 1 826.15 979.17 7.88 o 3 3 1 1419.57 1365.07 12.77 o 4 3 1 282.37 287.26 3.88 o 5 3 1 448.22 438.05 5.36 o 6 3 1 931.90 957.98 11.12 o 7 3 1 56.33 47.81 3.10 o 8 3 1 119.49 108.77 4.68 o -6 4 1 75.81 73.81 4.82 o -5 4 1 121.98 111.91 4.26 o -4 4 1 1.68 8.35 2.00 o -3 4 1 578.20 524.96 6.30 o -2 4 1 991.35 944.11 10.01 o -1 4 1 1370.03 1561.20 13.47 o 0 4 1 1001.11 1010.65 10.09 o 1 4 1 308.44 344.92 8.97 o 2 4 1 580.11 644.02 11.18 o 3 4 1 546.91 584.01 6.15 o 4 4 1 147.07 136.54 3.90 o 5 4 1 303.45 287.40 4.28 o 6 4 1 348.65 364.61 6.84 o 7 4 1 23.23 44.14 3.69 o 8 4 1 3.84 24.42 2.87 o -5 5 1 146.39 138.00 5.90 o -4 5 1 564.48 524.23 7.84 o -3 5 1 402.91 417.98 5.78 o -2 5 1 428.47 469.31 5.91 o -1 5 1 118.00 161.79 4.72 o 0 5 1 415.11 409.59 5.27 o 1 5 1 12.27 6.08 0.79 o 2 5 1 51.29 123.19 6.23 o 3 5 1 254.79 261.07 4.83 o 4 5 1 1094.01 1029.50 9.78 o 5 5 1 28.61 80.69 3.00 o 6 5 1 78.58 72.81 2.83 o 7 5 1 199.58 199.41 14.53 o 8 5 1 16.89 34.38 3.74 o -5 6 1 75.79 73.47 4.77 o -4 6 1 240.44 243.38 6.24 o -3 6 1 44.20 44.64 2.18 o -2 6 1 362.94 382.71 5.47 o -1 6 1 32.70 113.96 7.69 o 0 6 1 302.15 331.15 4.57 o 1 6 1 8.11 106.21 3.80 o 2 6 1 208.09 191.29 4.19 o 3 6 1 134.49 139.25 3.13 o 4 6 1 446.32 477.46 6.61 o 5 6 1 80.76 83.58 3.26 o 6 6 1 156.72 152.49 4.36 o 7 6 1 88.87 75.04 4.48 o 8 6 1 37.14 58.27 4.47 o -4 7 1 73.93 68.47 4.66 o -3 7 1 287.36 277.60 5.80 o -2 7 1 376.04 388.88 6.60 o -1 7 1 98.53 198.18 4.39 o 0 7 1 330.44 316.50 5.46 o 1 7 1 83.30 83.45 3.41 o 2 7 1 13.25 29.28 2.37 o 3 7 1 294.26 268.17 5.99 o 4 7 1 252.40 258.90 6.02 o 5 7 1 338.76 318.17 6.85 o 6 7 1 141.45 125.27 4.51 o 7 7 1 67.85 50.37 3.99 o 8 7 1 65.05 89.73 7.29 o -3 8 1 59.47 63.72 5.37 o -2 8 1 123.80 132.91 4.91 o -1 8 1 3.94 12.34 2.77 o 0 8 1 165.50 155.96 4.86 o 1 8 1 150.48 142.26 4.60 o 2 8 1 163.03 158.71 5.52 o 3 8 1 349.36 340.98 7.23 o 4 8 1 283.36 266.71 6.49 o 5 8 1 214.80 188.42 5.56 o 6 8 1 101.74 105.53 4.57 o 7 8 1 26.06 32.69 3.82 o -1 9 1 189.25 181.09 7.16 o 0 9 1 32.13 36.30 3.81 o 1 9 1 304.44 288.32 8.58 o 2 9 1 342.36 370.29 8.12 o 3 9 1 94.43 101.72 4.40 o 4 9 1 126.82 114.40 4.71 o 5 9 1 68.73 100.03 4.61 o 6 9 1 32.92 30.09 3.14 o 1 10 1 27.70 44.27 7.47 o 2 10 1 87.63 98.42 4.59 o 3 10 1 53.50 43.80 3.48 o 4 10 1 14.21 8.80 2.62 o -5 -9 2 262.33 303.13 7.62 o -4 -9 2 6.33 6.07 2.24 o -3 -9 2 11.09 5.47 2.12 o -2 -9 2 109.96 101.54 5.36 o -1 -9 2 26.77 27.44 3.46 o 0 -9 2 191.02 207.92 7.60 o 1 -9 2 132.54 139.43 6.53 o -6 -8 2 36.85 47.21 3.41 o -5 -8 2 366.65 372.79 8.03 o -4 -8 2 10.74 20.23 2.51 o -3 -8 2 1.55 32.30 3.93 o -2 -8 2 138.65 127.88 4.42 o -1 -8 2 70.91 77.68 5.27 o 0 -8 2 227.65 225.02 7.34 o 1 -8 2 226.20 200.73 6.99 o 2 -8 2 40.15 49.31 3.39 o -7 -7 2 277.62 260.27 10.95 o -6 -7 2 11.85 31.94 2.75 o -5 -7 2 29.11 30.77 2.66 o -4 -7 2 221.80 219.51 5.61 o -3 -7 2 3.00 26.18 2.57 o -2 -7 2 129.39 119.69 4.03 o -1 -7 2 391.28 412.73 7.42 o 0 -7 2 335.74 342.21 7.13 o 1 -7 2 6.01 11.22 2.31 o 2 -7 2 417.59 418.47 8.25 o 3 -7 2 255.88 261.48 8.67 o 4 -7 2 140.77 123.24 6.08 o -8 -6 2 43.18 52.81 5.98 o -7 -6 2 409.45 377.23 9.20 o -6 -6 2 2.25 5.09 2.24 o -5 -6 2 133.72 121.67 4.09 o -4 -6 2 219.52 200.08 5.09 o -3 -6 2 386.21 365.62 7.31 o -2 -6 2 409.86 366.61 5.40 o -1 -6 2 723.84 674.44 9.56 o 0 -6 2 264.01 248.27 4.45 o 1 -6 2 647.32 674.69 8.49 o 2 -6 2 85.11 75.09 2.91 o 3 -6 2 38.41 44.59 2.57 o 4 -6 2 64.94 80.65 5.20 o 5 -6 2 11.96 13.01 4.63 o -8 -5 2 204.78 212.29 7.65 o -7 -5 2 258.55 346.19 8.82 o -6 -5 2 131.61 125.05 4.10 o -5 -5 2 279.94 276.70 4.33 o -4 -5 2 266.63 294.18 6.10 o -3 -5 2 638.82 614.65 6.37 o -2 -5 2 790.04 922.63 9.98 o -1 -5 2 113.44 102.42 2.65 o 0 -5 2 697.85 727.97 10.53 o 1 -5 2 558.76 618.33 6.66 o 2 -5 2 503.39 487.62 6.89 o 3 -5 2 25.74 23.77 1.91 o 4 -5 2 310.90 299.56 6.76 o 5 -5 2 144.01 114.76 4.74 o -8 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