#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:47:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181096 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/76/2217615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217615_Fobs loop_ _publ_author_name 'Gowda, B. Thimme' 'Foro, Sabine' 'Sowmya, B. P.' 'Fuess, Hartmut' _publ_section_title ; 2-Methyl-N-(3-methylphenyl)benzamide ; _journal_coeditor_code OM2212 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o541 _journal_volume 64 _journal_year 2008 _space_group_IT_number 78 _symmetry_space_group_name_Hall 'P 4cw' _symmetry_space_group_name_H-M 'P 43' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9310 _cell_length_b 8.9310 _cell_length_c 15.8160 _exptl_crystal_F_000 480.00 _reflns_d_resolution_high 0.8390 _cod_data_source_file om2212Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' B75 P43' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' '-y, x, z+3/4' 'y, -x, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 2756.11 2624.58 60.80 o 1 1 0 1536.52 1382.48 11.05 o -1 2 0 232.07 220.46 1.61 o 0 2 0 2715.66 2536.64 75.83 o 1 2 0 345.64 307.57 1.97 o 2 2 0 176.71 169.16 1.57 o -2 3 0 80.92 73.08 1.17 o -1 3 0 1230.22 1076.15 5.19 o 0 3 0 604.75 576.92 2.34 o 1 3 0 5.63 5.87 0.24 o 2 3 0 117.87 117.14 1.47 o 3 3 0 95.30 105.69 1.56 o -3 4 0 4.84 5.89 0.36 o -2 4 0 600.52 688.96 4.49 o -1 4 0 844.44 793.00 4.71 o 0 4 0 347.63 409.23 9.64 o 1 4 0 104.97 105.69 1.52 o 2 4 0 16.30 16.25 0.50 o 3 4 0 7.54 10.79 0.42 o 4 4 0 165.15 184.62 2.53 o -4 5 0 22.87 20.88 0.65 o -3 5 0 61.02 58.20 1.48 o -2 5 0 22.79 21.66 0.67 o -1 5 0 152.39 158.34 2.16 o 0 5 0 130.67 108.79 1.25 o 1 5 0 119.52 109.90 1.81 o 2 5 0 24.72 22.39 0.67 o 3 5 0 10.85 10.74 0.50 o 4 5 0 2.12 2.08 0.38 o 5 5 0 3.04 3.54 0.43 o -5 6 0 1.63 1.20 0.48 o -4 6 0 8.16 5.99 0.54 o -3 6 0 22.56 24.31 0.73 o -2 6 0 0.09 0.86 0.34 o -1 6 0 44.07 37.23 1.09 o 0 6 0 18.75 19.45 0.62 o 1 6 0 20.53 19.82 0.63 o 2 6 0 32.67 30.96 0.89 o 3 6 0 5.03 5.81 0.48 o 4 6 0 5.41 4.91 0.58 o 5 6 0 2.24 1.87 0.48 o 6 6 0 6.23 7.28 0.58 o -6 7 0 49.89 52.40 1.47 o -5 7 0 14.64 13.32 0.67 o -4 7 0 14.74 14.56 0.73 o -3 7 0 6.97 6.12 0.52 o -2 7 0 0.08 0.40 0.77 o -1 7 0 136.61 129.49 2.49 o 0 7 0 35.03 32.90 1.24 o 1 7 0 90.78 87.21 2.14 o 2 7 0 165.75 175.27 2.98 o 3 7 0 0.04 0.94 0.47 o 4 7 0 7.92 9.17 0.63 o 5 7 0 7.91 8.17 0.58 o 6 7 0 1.41 1.90 0.47 o 7 7 0 5.22 5.66 0.48 o -7 8 0 7.37 5.80 0.39 o -6 8 0 40.00 35.32 1.12 o -5 8 0 7.37 9.13 0.56 o -4 8 0 53.77 52.48 1.51 o -3 8 0 30.48 31.81 0.96 o -2 8 0 10.42 8.69 0.58 o -1 8 0 0.01 1.41 0.39 o 0 8 0 66.65 66.05 1.39 o 1 8 0 22.46 21.54 0.82 o 2 8 0 0.21 -0.87 0.87 o 3 8 0 7.61 7.96 0.58 o 4 8 0 11.09 11.15 0.65 o 5 8 0 1.35 0.66 0.44 o 6 8 0 0.37 0.39 0.36 o 7 8 0 1.08 1.87 0.30 o -5 9 0 6.73 8.02 0.46 o -4 9 0 18.15 17.87 0.61 o -3 9 0 11.76 9.71 0.57 o -2 9 0 2.87 2.68 0.47 o -1 9 0 7.29 6.90 0.50 o 0 9 0 4.87 4.59 0.59 o 1 9 0 1.02 1.04 0.50 o 2 9 0 23.89 25.07 0.82 o 3 9 0 23.02 24.54 0.81 o 4 9 0 9.58 10.72 0.52 o 5 9 0 3.83 5.25 0.40 o -3 10 0 8.67 8.06 0.44 o -2 10 0 0.57 0.12 0.56 o -1 10 0 0.51 0.71 0.32 o 0 10 0 0.12 0.20 0.39 o 1 10 0 3.14 3.05 0.39 o 2 10 0 0.05 -0.39 0.56 o 3 10 0 2.64 3.40 0.36 o 0 1 1 1234.38 1264.22 7.88 o 1 1 1 1060.13 1053.96 4.72 o -1 2 1 46.03 43.06 0.50 o 0 2 1 3824.27 3766.27 25.82 o 1 2 1 29.94 26.99 1.77 o 2 2 1 791.79 592.91 83.71 o -2 3 1 542.30 432.23 51.97 o -1 3 1 234.56 205.30 1.97 o 0 3 1 93.51 91.48 4.50 o 1 3 1 163.93 150.59 1.11 o 2 3 1 7.94 8.31 1.54 o 3 3 1 81.03 76.52 0.96 o -3 4 1 344.92 354.71 2.47 o -2 4 1 55.39 32.13 1.75 o -1 4 1 485.08 458.04 2.76 o 0 4 1 485.98 427.87 19.46 o 1 4 1 353.51 363.18 5.84 o 2 4 1 455.96 455.08 3.55 o 3 4 1 274.75 267.38 2.00 o 4 4 1 51.54 48.38 0.96 o -4 5 1 7.11 6.49 0.62 o -3 5 1 2.76 3.61 0.25 o -2 5 1 98.93 86.47 5.03 o -1 5 1 40.44 38.80 1.24 o 0 5 1 94.36 102.89 3.74 o 1 5 1 6.56 5.31 0.25 o 2 5 1 24.02 22.03 0.48 o 3 5 1 92.17 88.72 1.47 o 4 5 1 47.09 50.58 1.00 o 5 5 1 58.57 59.31 1.24 o -5 6 1 35.74 29.61 0.64 o -4 6 1 58.79 55.17 1.06 o -3 6 1 29.61 30.51 0.66 o -2 6 1 19.79 20.17 2.03 o -1 6 1 157.55 164.13 1.80 o 0 6 1 42.24 42.95 1.20 o 1 6 1 2.85 3.51 0.43 o 2 6 1 96.34 103.11 3.68 o 3 6 1 154.31 148.74 2.77 o 4 6 1 78.15 76.43 1.41 o 5 6 1 82.10 83.53 1.56 o 6 6 1 14.50 14.42 0.49 o -6 7 1 0.11 0.02 0.53 o -5 7 1 12.04 12.88 0.47 o -4 7 1 27.00 30.22 0.63 o -3 7 1 27.78 25.54 0.58 o -2 7 1 2.23 2.33 0.48 o -1 7 1 2.72 2.69 0.30 o 0 7 1 29.29 27.81 0.89 o 1 7 1 51.77 57.45 1.15 o 2 7 1 123.59 121.09 1.78 o 3 7 1 95.13 96.60 2.57 o 4 7 1 25.90 26.85 0.62 o 5 7 1 16.55 16.81 0.52 o 6 7 1 18.11 17.70 0.50 o 7 7 1 9.51 10.55 0.39 o -7 8 1 2.60 2.52 0.46 o -6 8 1 0.00 -0.02 0.43 o -5 8 1 6.97 6.62 0.37 o -4 8 1 14.84 13.03 1.00 o -3 8 1 21.07 20.79 0.52 o -2 8 1 12.43 10.04 0.41 o -1 8 1 36.65 36.57 0.78 o 0 8 1 27.82 27.62 1.31 o 1 8 1 143.67 150.97 2.04 o 2 8 1 35.66 37.56 0.79 o 3 8 1 1.62 2.42 0.37 o 4 8 1 1.28 1.54 0.39 o 5 8 1 15.17 15.81 0.46 o 6 8 1 15.03 17.74 0.42 o 7 8 1 0.05 0.20 0.32 o -5 9 1 1.74 1.81 0.25 o -4 9 1 1.03 0.58 0.43 o -3 9 1 1.10 0.84 0.86 o -2 9 1 3.47 2.77 0.29 o -1 9 1 6.86 6.34 0.36 o 0 9 1 8.88 7.97 0.27 o 1 9 1 18.23 20.07 0.53 o 2 9 1 38.78 42.47 0.89 o 3 9 1 4.32 4.79 0.36 o 4 9 1 3.49 4.03 0.50 o 5 9 1 1.35 1.00 0.41 o -3 10 1 0.24 0.61 0.22 o -2 10 1 1.45 1.70 0.22 o -1 10 1 1.77 1.47 0.49 o 0 10 1 8.16 7.34 0.30 o 1 10 1 14.98 15.18 0.41 o 2 10 1 2.09 2.93 0.28 o 3 10 1 2.27 2.53 0.25 o 0 1 2 112.56 107.90 2.06 o 1 1 2 3599.93 3720.62 17.63 o -1 2 2 1712.72 1481.14 38.07 o 0 2 2 7689.85 8157.27 27.44 o 1 2 2 2259.30 2203.44 18.47 o 2 2 2 591.62 584.29 3.23 o -2 3 2 149.78 172.98 1.31 o -1 3 2 730.72 670.35 4.31 o 0 3 2 120.38 111.81 1.28 o 1 3 2 594.83 584.62 2.49 o 2 3 2 237.86 194.48 1.77 o 3 3 2 896.32 877.10 3.67 o -3 4 2 191.79 200.98 2.00 o -2 4 2 70.71 74.44 0.99 o -1 4 2 394.28 364.21 2.12 o 0 4 2 395.72 406.60 5.52 o 1 4 2 83.84 95.93 1.29 o 2 4 2 18.19 23.30 0.48 o 3 4 2 181.80 190.90 2.74 o 4 4 2 23.01 23.67 1.25 o -4 5 2 50.85 48.94 0.93 o -3 5 2 12.55 10.14 0.57 o -2 5 2 23.87 25.95 0.57 o -1 5 2 380.85 315.00 2.23 o 0 5 2 23.95 30.77 0.45 o 1 5 2 76.33 74.20 1.07 o 2 5 2 123.58 137.85 1.52 o 3 5 2 175.22 175.69 1.83 o 4 5 2 63.33 64.03 1.22 o 5 5 2 30.37 33.27 0.69 o -5 6 2 1.70 1.32 0.60 o -4 6 2 13.02 11.27 0.43 o -3 6 2 23.54 23.45 1.08 o -2 6 2 2.41 2.98 0.29 o -1 6 2 60.02 62.49 1.12 o 0 6 2 199.12 191.52 2.71 o 1 6 2 13.36 12.34 0.50 o 2 6 2 25.84 23.45 0.51 o 3 6 2 34.04 38.27 0.79 o 4 6 2 107.16 102.85 1.65 o 5 6 2 9.75 9.91 0.61 o 6 6 2 10.73 11.11 0.44 o -6 7 2 24.51 24.36 0.56 o -5 7 2 13.50 13.35 0.47 o -4 7 2 19.92 20.65 0.77 o -3 7 2 0.15 -0.39 0.85 o -2 7 2 7.53 7.04 0.39 o -1 7 2 12.66 12.37 0.41 o 0 7 2 70.60 68.59 1.40 o 1 7 2 41.13 43.13 0.94 o 2 7 2 67.20 62.40 1.22 o 3 7 2 4.81 4.44 0.38 o 4 7 2 31.12 33.48 0.74 o 5 7 2 17.94 16.62 0.50 o 6 7 2 6.90 6.78 0.42 o 7 7 2 14.11 11.79 0.41 o -6 8 2 4.77 5.58 0.53 o -5 8 2 10.29 10.37 0.44 o -4 8 2 0.61 0.10 0.53 o -3 8 2 6.54 5.86 0.38 o -2 8 2 7.53 8.31 0.41 o -1 8 2 95.49 91.15 1.58 o 0 8 2 66.73 64.84 1.12 o 1 8 2 11.32 9.88 0.45 o 2 8 2 30.92 31.32 1.37 o 3 8 2 30.55 31.37 0.84 o 4 8 2 0.42 0.08 0.34 o 5 8 2 8.81 7.77 0.37 o 6 8 2 12.44 12.83 0.41 o -5 9 2 0.64 0.32 0.26 o -4 9 2 11.25 11.02 0.39 o -3 9 2 3.70 3.88 0.33 o -2 9 2 3.17 3.11 0.61 o -1 9 2 5.66 5.16 0.45 o 0 9 2 35.18 35.65 0.56 o 1 9 2 33.43 33.59 0.72 o 2 9 2 2.74 3.04 0.46 o 3 9 2 0.07 0.23 0.35 o 4 9 2 1.17 1.29 0.28 o 5 9 2 1.53 2.15 0.24 o -3 10 2 0.84 1.52 0.23 o -2 10 2 2.29 2.62 0.26 o -1 10 2 2.02 2.39 0.24 o 0 10 2 0.77 0.72 0.26 o 1 10 2 3.69 4.36 0.41 o 2 10 2 7.31 8.02 0.32 o 3 10 2 1.21 1.09 0.22 o 0 1 3 2912.47 2949.33 10.08 o 1 1 3 7093.85 7706.07 28.60 o -1 2 3 56.35 52.20 0.94 o 0 2 3 3916.97 4022.39 39.59 o 1 2 3 1180.03 1052.97 29.86 o 2 2 3 1046.45 975.72 42.21 o -2 3 3 348.00 344.12 16.52 o -1 3 3 150.72 148.07 4.85 o 0 3 3 241.45 222.16 5.63 o 1 3 3 244.70 234.37 1.50 o 2 3 3 684.12 666.70 7.80 o 3 3 3 10.24 13.53 0.29 o -3 4 3 54.35 56.27 1.76 o -2 4 3 385.26 388.59 17.71 o -1 4 3 438.75 463.19 8.88 o 0 4 3 478.43 466.75 13.41 o 1 4 3 161.42 181.05 1.50 o 2 4 3 139.55 145.03 1.71 o 3 4 3 35.37 32.36 1.26 o 4 4 3 107.32 107.20 3.91 o -4 5 3 52.08 54.55 1.14 o -3 5 3 113.63 120.48 1.83 o -2 5 3 26.15 33.22 2.17 o -1 5 3 197.70 193.78 10.41 o 0 5 3 132.91 136.47 3.27 o 1 5 3 472.75 495.22 5.01 o 2 5 3 47.87 49.29 1.46 o 3 5 3 127.81 123.67 1.54 o 4 5 3 4.77 4.95 0.31 o 5 5 3 27.85 27.19 0.62 o -5 6 3 3.85 4.38 0.44 o -4 6 3 30.13 31.42 1.10 o -3 6 3 2.68 2.69 0.61 o -2 6 3 0.13 0.51 0.27 o -1 6 3 11.31 13.55 0.69 o 0 6 3 25.00 24.91 0.83 o 1 6 3 56.08 55.85 1.11 o 2 6 3 76.07 84.84 1.69 o 3 6 3 14.49 12.14 0.42 o 4 6 3 34.68 34.87 0.75 o 5 6 3 29.12 30.02 0.63 o 6 6 3 24.77 22.41 0.65 o -6 7 3 4.80 5.41 0.37 o -5 7 3 18.92 19.21 0.53 o -4 7 3 36.75 35.52 0.75 o -3 7 3 37.88 36.03 1.44 o -2 7 3 56.04 57.17 1.45 o -1 7 3 69.64 63.23 1.29 o 0 7 3 98.89 94.19 2.50 o 1 7 3 72.64 70.26 1.37 o 2 7 3 14.86 16.97 0.49 o 3 7 3 59.78 57.93 1.15 o 4 7 3 10.73 10.65 0.48 o 5 7 3 5.26 5.89 0.40 o 6 7 3 7.59 6.56 0.45 o 7 7 3 8.85 9.42 0.34 o -6 8 3 11.13 11.15 0.75 o -5 8 3 23.42 22.55 0.67 o -4 8 3 8.44 8.11 0.75 o -3 8 3 14.00 14.61 0.45 o -2 8 3 9.04 8.04 0.38 o -1 8 3 3.53 2.57 0.32 o 0 8 3 9.21 8.82 0.45 o 1 8 3 2.73 3.08 0.36 o 2 8 3 29.46 29.77 0.63 o 3 8 3 44.57 47.31 1.03 o 4 8 3 15.54 16.58 0.50 o 5 8 3 24.62 28.62 0.61 o 6 8 3 0.59 0.52 0.41 o -5 9 3 5.01 5.30 0.27 o -4 9 3 14.07 14.62 0.71 o -3 9 3 1.01 1.03 0.33 o -2 9 3 2.69 2.53 0.28 o -1 9 3 11.19 10.81 0.71 o 0 9 3 13.56 12.17 0.57 o 1 9 3 2.46 3.32 0.47 o 2 9 3 18.93 21.23 0.74 o 3 9 3 2.24 2.81 0.42 o 4 9 3 3.24 3.63 0.43 o 5 9 3 0.33 0.39 0.22 o -3 10 3 10.68 10.97 0.30 o -2 10 3 9.96 10.11 0.31 o -1 10 3 2.75 2.37 0.38 o 0 10 3 5.46 5.14 0.23 o 1 10 3 2.90 2.87 0.39 o 2 10 3 0.27 -0.34 0.55 o 3 10 3 1.81 1.61 0.34 o 0 0 4 1538.31 1744.99 6.90 o 0 1 4 298.30 308.73 1.48 o 1 1 4 3022.08 3282.74 24.48 o -1 2 4 1290.23 1020.87 5.00 o 0 2 4 1006.38 1064.97 8.56 o 1 2 4 487.38 464.28 2.97 o 2 2 4 223.95 215.60 2.04 o -2 3 4 173.57 177.40 2.04 o -1 3 4 86.00 70.09 1.19 o 0 3 4 170.42 164.14 1.27 o 1 3 4 2287.79 2276.93 9.74 o 2 3 4 372.62 386.80 3.10 o 3 3 4 71.35 75.25 1.43 o -3 4 4 34.45 32.06 0.96 o -2 4 4 41.53 41.11 1.16 o -1 4 4 193.79 164.37 2.06 o 0 4 4 777.58 807.59 16.77 o 1 4 4 1221.44 1272.05 6.85 o 2 4 4 12.18 15.70 0.48 o 3 4 4 67.15 72.18 1.58 o 4 4 4 15.02 16.68 0.57 o -4 5 4 23.00 23.09 0.74 o -3 5 4 37.53 31.07 0.96 o -2 5 4 71.30 61.22 1.58 o -1 5 4 182.90 167.87 2.36 o 0 5 4 115.55 126.35 3.27 o 1 5 4 9.45 9.47 0.46 o 2 5 4 60.42 51.98 1.44 o 3 5 4 24.60 23.83 0.73 o 4 5 4 58.58 62.34 1.78 o 5 5 4 81.55 77.88 2.11 o -5 6 4 14.11 12.57 0.67 o -4 6 4 56.24 61.65 1.86 o -3 6 4 49.00 51.28 1.44 o -2 6 4 162.06 149.86 2.64 o -1 6 4 4.75 3.90 0.39 o 0 6 4 8.49 9.92 0.34 o 1 6 4 74.67 61.29 1.62 o 2 6 4 33.60 34.49 1.05 o 3 6 4 92.21 89.97 2.09 o 4 6 4 6.55 5.92 0.56 o 5 6 4 0.16 0.67 0.48 o 6 6 4 5.47 5.49 0.56 o -6 7 4 9.26 9.65 0.55 o -5 7 4 3.28 3.52 0.50 o -4 7 4 6.03 8.47 0.58 o -3 7 4 49.01 52.26 1.59 o -2 7 4 78.90 75.58 2.07 o -1 7 4 111.85 101.23 2.25 o 0 7 4 135.74 133.66 9.50 o 1 7 4 63.12 70.62 1.93 o 2 7 4 15.27 13.79 0.70 o 3 7 4 10.97 9.61 0.67 o 4 7 4 70.10 71.24 2.07 o 5 7 4 8.62 8.89 0.65 o 6 7 4 2.70 2.91 0.44 o 7 7 4 1.74 1.52 0.36 o -6 8 4 0.06 -0.35 0.55 o -5 8 4 10.18 8.35 0.55 o -4 8 4 13.89 14.50 0.65 o -3 8 4 21.21 20.46 0.74 o -2 8 4 9.93 8.17 0.62 o -1 8 4 5.43 4.49 0.43 o 0 8 4 16.41 18.03 0.78 o 1 8 4 28.93 30.21 0.86 o 2 8 4 5.20 3.39 0.58 o 3 8 4 21.12 21.03 0.78 o 4 8 4 68.05 67.46 1.94 o 5 8 4 1.56 1.79 0.40 o 6 8 4 6.48 6.52 0.43 o -5 9 4 0.15 -0.05 0.30 o -4 9 4 0.29 0.28 0.31 o -3 9 4 0.66 0.62 0.36 o -2 9 4 11.85 10.75 0.57 o -1 9 4 14.09 12.89 0.59 o 0 9 4 13.22 11.19 0.84 o 1 9 4 20.94 21.72 0.71 o 2 9 4 14.75 16.10 0.63 o 3 9 4 16.24 14.65 0.58 o 4 9 4 3.00 3.31 0.40 o 5 9 4 0.62 0.51 0.31 o -2 10 4 0.01 -0.51 0.51 o -1 10 4 5.34 4.25 0.36 o 0 10 4 2.02 1.79 0.24 o 1 10 4 10.08 10.26 0.48 o 2 10 4 0.81 0.39 0.54 o 0 1 5 728.77 722.71 10.07 o 1 1 5 618.35 631.43 3.60 o -1 2 5 112.56 101.46 1.39 o 0 2 5 978.15 1010.27 13.08 o 1 2 5 60.09 50.16 0.98 o 2 2 5 169.75 187.35 2.01 o -2 3 5 284.65 290.80 2.76 o -1 3 5 597.87 604.98 4.03 o 0 3 5 695.93 678.72 3.17 o 1 3 5 2.34 4.65 0.34 o 2 3 5 493.36 564.29 4.04 o 3 3 5 68.61 77.13 1.54 o -3 4 5 20.68 22.08 0.67 o -2 4 5 20.44 18.45 0.50 o -1 4 5 153.08 152.67 2.08 o 0 4 5 345.05 353.80 3.50 o 1 4 5 196.07 189.79 2.36 o 2 4 5 44.05 42.16 1.24 o 3 4 5 25.32 29.98 0.89 o 4 4 5 2.53 2.37 0.40 o -4 5 5 17.51 18.36 0.73 o -3 5 5 56.72 50.56 1.35 o -2 5 5 125.61 125.49 2.20 o -1 5 5 50.59 41.67 1.14 o 0 5 5 65.97 59.06 1.26 o 1 5 5 105.52 100.07 1.93 o 2 5 5 27.43 27.81 0.81 o 3 5 5 79.51 75.70 1.80 o 4 5 5 8.96 9.00 0.55 o 5 5 5 50.61 52.14 1.55 o -5 6 5 49.22 50.51 1.49 o -4 6 5 7.50 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