#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:47:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181096 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/76/2217673.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217673_Fobs loop_ _publ_author_name 'Butcher, Ray J.' 'Gultneh, Yilma' 'Yisgedu, Teshome B.' 'Tesema, Yohannes T.' _publ_section_title ; Di-\m-bromido-bis({bis[2-(2-pyridyl)ethyl]amine}copper(II)) bis(perchlorate) ; _journal_coeditor_code TK2238 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m323 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.212 _cell_angle_beta 77.019 _cell_angle_gamma 87.033 _cell_length_a 6.8002 _cell_length_b 11.4130 _cell_length_c 12.6679 _exptl_crystal_F_000 470.00 _reflns_d_resolution_high 0.7698 _cod_data_source_file tk2238Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Ty46 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 126.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6645.99 6668.63 58.79 o 2 0 0 11898.46 12604.96 115.42 o 3 0 0 7.43 6.34 4.61 o 4 0 0 87.48 87.61 8.50 o 5 0 0 2010.37 1880.74 85.30 o 6 0 0 307.19 338.63 18.16 o 7 0 0 385.22 349.72 22.19 o 8 0 0 128.37 134.73 24.64 o -8 1 0 193.70 175.08 22.77 o -7 1 0 140.06 113.98 17.44 o -6 1 0 263.49 240.21 17.44 o -5 1 0 814.32 729.56 31.85 o -4 1 0 179.91 199.14 10.81 o -3 1 0 0.39 9.65 4.61 o -2 1 0 30.11 24.93 4.03 o -1 1 0 659.59 692.24 22.05 o 1 1 0 5271.78 5714.13 64.99 o 2 1 0 4450.87 4379.08 85.16 o 3 1 0 54.87 72.48 7.20 o 4 1 0 295.86 311.10 13.83 o 5 1 0 854.82 930.28 36.02 o 6 1 0 1464.95 1570.36 61.10 o 7 1 0 36.48 42.08 15.56 o 8 1 0 186.22 208.94 24.78 o -8 2 0 211.37 212.25 25.51 o -7 2 0 195.57 163.41 19.16 o -6 2 0 697.44 694.11 30.69 o -5 2 0 604.57 487.05 25.36 o -4 2 0 20.92 31.12 7.93 o -3 2 0 225.96 204.33 10.37 o -2 2 0 23.95 31.12 4.32 o -1 2 0 3134.09 3111.76 52.31 o 0 2 0 1473.82 1466.97 22.98 o 1 2 0 1579.32 1441.25 38.33 o 2 2 0 15.92 31.41 4.90 o 3 2 0 59.79 59.66 7.20 o 4 2 0 159.04 192.80 12.10 o 5 2 0 98.49 124.64 13.40 o 6 2 0 846.09 910.26 32.57 o 7 2 0 8.01 14.12 16.28 o 8 2 0 240.23 315.43 27.67 o -8 3 0 135.29 105.33 21.47 o -7 3 0 474.06 449.44 24.50 o -6 3 0 556.56 542.95 27.09 o -5 3 0 2093.02 2041.27 90.78 o -4 3 0 392.81 378.11 18.59 o -3 3 0 9.79 13.40 6.05 o -2 3 0 660.74 603.76 23.20 o -1 3 0 1912.16 1708.12 45.97 o 0 3 0 12987.95 12958.35 81.82 o 1 3 0 398.16 399.29 15.27 o 2 3 0 101.87 113.12 7.06 o 3 3 0 302.29 351.02 13.11 o 4 3 0 105.86 113.12 11.82 o 5 3 0 513.87 566.73 22.19 o 6 3 0 358.84 422.49 24.06 o 7 3 0 0.21 25.65 18.16 o 8 3 0 76.54 94.96 24.50 o -8 4 0 62.61 68.16 19.89 o -7 4 0 400.73 345.69 22.91 o -6 4 0 212.87 204.62 17.72 o -5 4 0 2305.15 2227.29 98.85 o -4 4 0 34.97 26.23 8.50 o -3 4 0 906.14 900.89 34.29 o -2 4 0 2634.75 2534.22 69.17 o -1 4 0 21.02 21.18 4.61 o 0 4 0 10028.52 9810.03 209.80 o 1 4 0 10798.22 10471.90 129.40 o 2 4 0 324.94 289.06 12.54 o 3 4 0 668.83 716.59 27.95 o 4 4 0 262.39 264.70 13.55 o 5 4 0 219.37 268.16 17.44 o 6 4 0 878.98 976.54 37.75 o 7 4 0 0.52 32.42 19.74 o 8 4 0 159.19 183.29 29.11 o -8 5 0 59.55 50.00 22.05 o -7 5 0 131.36 125.65 19.60 o -6 5 0 27.50 47.84 13.55 o -5 5 0 315.99 301.88 17.72 o -4 5 0 117.95 91.93 11.10 o -3 5 0 135.92 131.85 10.81 o -2 5 0 524.72 566.15 22.62 o -1 5 0 251.81 239.20 9.80 o 0 5 0 4737.85 5023.09 95.18 o 1 5 0 7621.45 7300.63 122.05 o 2 5 0 12.97 11.38 6.20 o 3 5 0 1102.89 962.56 37.61 o 4 5 0 293.97 296.26 15.42 o 5 5 0 12.93 2.59 13.40 o 6 5 0 1022.40 1127.98 51.87 o 7 5 0 1.30 -15.85 22.48 o -7 6 0 179.17 141.79 21.33 o -6 6 0 24.38 25.94 13.55 o -5 6 0 404.06 364.85 20.17 o -4 6 0 92.70 92.80 12.10 o -3 6 0 401.42 337.33 16.72 o -2 6 0 247.85 214.27 11.67 o -1 6 0 4.04 2.02 6.05 o 0 6 0 1386.78 1412.03 69.60 o 1 6 0 1093.08 1050.46 38.91 o 2 6 0 139.83 138.62 10.37 o 3 6 0 86.93 69.45 10.37 o 4 6 0 7.66 18.16 9.94 o 5 6 0 0.17 -12.97 12.97 o 6 6 0 382.64 444.97 25.22 o 7 6 0 87.22 70.75 24.78 o -7 7 0 329.37 348.42 25.65 o -6 7 0 0.41 10.81 14.99 o -5 7 0 575.19 518.03 29.54 o -4 7 0 0.29 -11.53 11.67 o -3 7 0 87.98 68.73 10.95 o -2 7 0 1571.25 1547.59 76.80 o -1 7 0 84.61 77.24 9.08 o 0 7 0 3242.44 3175.97 85.81 o 1 7 0 2216.57 2098.47 87.61 o 2 7 0 203.95 160.52 12.82 o 3 7 0 125.23 135.02 13.55 o 4 7 0 27.13 14.99 11.96 o 5 7 0 31.13 28.39 14.84 o 6 7 0 191.85 196.11 21.18 o 7 7 0 40.85 72.34 22.77 o -6 8 0 66.91 48.99 17.87 o -5 8 0 445.92 473.21 24.50 o -4 8 0 454.08 382.86 20.46 o -3 8 0 597.25 580.42 27.38 o -2 8 0 3.43 20.17 9.37 o -1 8 0 1003.48 1061.84 41.79 o 0 8 0 1134.07 1106.81 30.50 o 1 8 0 2528.01 2423.84 99.43 o 2 8 0 94.89 83.43 11.96 o 3 8 0 111.27 139.20 14.12 o 4 8 0 171.58 149.86 15.99 o 5 8 0 2.36 15.56 15.13 o 6 8 0 230.42 251.16 23.78 o -6 9 0 2.33 30.55 16.57 o -5 9 0 185.14 179.98 20.17 o -4 9 0 123.15 124.07 16.57 o -3 9 0 1.29 1.01 11.96 o -2 9 0 1.20 -9.37 11.67 o -1 9 0 584.88 549.01 23.78 o 0 9 0 61.61 78.39 12.18 o 1 9 0 1811.76 1729.01 63.26 o 2 9 0 21.93 8.65 11.82 o 3 9 0 290.14 240.78 18.59 o 4 9 0 53.89 77.52 15.56 o 5 9 0 25.57 10.23 22.77 o 6 9 0 176.14 157.35 23.78 o -5 10 0 66.70 66.57 18.59 o -4 10 0 3.51 38.19 13.40 o -3 10 0 19.71 48.85 15.71 o -2 10 0 243.87 255.34 18.16 o -1 10 0 3.81 4.47 11.67 o 0 10 0 207.78 238.09 16.21 o 1 10 0 532.51 506.35 23.06 o 2 10 0 257.71 210.38 18.01 o 3 10 0 5.51 -15.27 15.85 o 4 10 0 0.30 -13.55 13.55 o 5 10 0 1.33 19.60 19.02 o -4 11 0 63.36 32.13 16.14 o -3 11 0 2.38 9.65 15.13 o -2 11 0 140.83 116.29 16.43 o -1 11 0 171.26 209.23 18.73 o 0 11 0 193.37 198.12 13.09 o 1 11 0 534.71 598.14 25.36 o 2 11 0 53.45 42.08 14.27 o 3 11 0 0.96 -1.87 15.27 o 4 11 0 10.48 -3.03 18.88 o -3 12 0 16.83 26.51 18.59 o -2 12 0 0.23 11.82 14.55 o -1 12 0 167.80 185.31 19.60 o 0 12 0 0.33 -1.28 20.39 o 1 12 0 294.32 285.74 23.63 o 2 12 0 65.50 77.81 19.45 o 3 12 0 0.33 33.00 18.88 o -2 13 0 0.10 13.11 16.72 o -1 13 0 42.93 23.20 18.88 o 0 13 0 16.78 29.43 13.18 o 1 13 0 104.27 102.88 20.32 o 2 13 0 83.13 84.58 20.17 o -1 -13 1 56.35 84.73 21.33 o 0 -13 1 9.27 36.17 18.44 o 1 -13 1 193.23 234.59 24.50 o 2 -13 1 15.59 -18.59 19.60 o -3 -12 1 2.97 -0.29 20.61 o -2 -12 1 3.30 -17.00 17.00 o -1 -12 1 29.48 31.70 17.58 o 0 -12 1 6.84 -15.42 15.42 o 1 -12 1 244.03 268.88 23.63 o 2 -12 1 199.38 167.15 22.48 o 3 -12 1 10.30 -6.48 18.01 o -4 -11 1 33.27 4.76 21.61 o -3 -11 1 6.36 13.98 17.72 o -2 -11 1 90.15 79.11 19.60 o -1 -11 1 123.58 132.28 19.16 o 0 -11 1 70.68 53.89 21.18 o 1 -11 1 438.02 440.65 24.06 o 2 -11 1 161.21 143.95 18.16 o 3 -11 1 1.52 7.20 17.00 o 4 -11 1 10.60 -5.62 17.72 o -5 -10 1 1.49 5.91 24.35 o -4 -10 1 125.51 133.72 19.45 o -3 -10 1 14.15 1.59 15.56 o -2 -10 1 27.26 35.02 13.83 o -1 -10 1 360.67 382.00 21.47 o 0 -10 1 0.60 -6.05 11.96 o 1 -10 1 1027.98 1167.61 51.01 o 2 -10 1 219.50 218.16 18.73 o 3 -10 1 5.13 20.03 14.70 o 4 -10 1 3.16 15.99 15.99 o 5 -10 1 3.38 14.41 17.29 o -5 -9 1 8.10 39.91 21.33 o -4 -9 1 478.72 490.07 26.23 o -3 -9 1 96.78 94.24 15.85 o -2 -9 1 0.46 -9.94 10.81 o -1 -9 1 379.40 417.01 19.16 o 0 -9 1 110.75 104.47 13.26 o 1 -9 1 1284.36 1394.27 55.04 o 2 -9 1 508.67 501.02 23.06 o 3 -9 1 245.37 240.06 18.01 o 4 -9 1 2.18 -2.74 13.26 o 5 -9 1 137.81 133.00 20.75 o 6 -9 1 26.70 37.32 18.01 o -6 -8 1 131.93 85.30 21.61 o -5 -8 1 16.43 21.18 18.44 o -4 -8 1 152.79 133.00 17.29 o -3 -8 1 4.44 -13.11 13.11 o -2 -8 1 24.10 28.96 10.81 o -1 -8 1 121.89 114.70 12.97 o 0 -8 1 187.23 205.77 13.98 o 1 -8 1 170.36 155.34 13.11 o 2 -8 1 1187.80 1256.09 48.99 o 3 -8 1 96.85 92.51 14.55 o 4 -8 1 18.92 18.16 13.55 o 5 -8 1 147.90 162.68 18.16 o 6 -8 1 1.67 40.35 16.57 o -6 -7 1 269.12 238.19 24.93 o -5 -7 1 11.91 33.14 15.71 o -4 -7 1 250.42 281.13 18.88 o -3 -7 1 0.12 0.14 10.23 o -2 -7 1 37.98 61.53 10.37 o -1 -7 1 470.57 433.30 17.15 o 0 -7 1 181.92 189.05 11.96 o 1 -7 1 411.05 418.31 17.72 o 2 -7 1 1134.63 1118.04 44.38 o 3 -7 1 119.92 96.11 12.25 o 4 -7 1 154.65 126.37 14.55 o 5 -7 1 43.74 48.13 14.27 o 6 -7 1 1.19 40.06 15.13 o 7 -7 1 237.54 239.49 24.21 o -7 -6 1 13.73 37.03 25.65 o -6 -6 1 453.18 495.98 28.10 o -5 -6 1 5.24 16.14 17.00 o -4 -6 1 1061.03 1005.79 39.34 o -3 -6 1 90.67 112.83 12.39 o -2 -6 1 23.24 33.43 8.65 o -1 -6 1 2621.58 2595.89 89.77 o 0 -6 1 405.81 414.85 18.01 o 1 -6 1 1994.11 1921.81 74.93 o 2 -6 1 2235.99 2243.00 83.86 o 3 -6 1 2.26 2.45 10.66 o 4 -6 1 9.81 10.09 9.94 o 5 -6 1 32.61 21.33 12.54 o 6 -6 1 5.22 23.63 13.69 o 7 -6 1 315.55 395.98 28.10 o -7 -5 1 1.90 -11.38 22.33 o -6 -5 1 678.13 663.85 30.98 o -5 -5 1 345.37 353.90 20.61 o -4 -5 1 725.00 642.52 26.80 o -3 -5 1 356.03 339.35 16.14 o -2 -5 1 517.77 543.10 23.34 o -1 -5 1 2305.99 2356.40 78.24 o 0 -5 1 3181.17 2908.00 80.98 o 1 -5 1 2274.09 2253.95 72.48 o 2 -5 1 7202.25 7163.74 130.12 o 3 -5 1 163.67 158.07 12.39 o 4 -5 1 113.31 123.06 11.67 o 5 -5 1 299.19 300.01 18.30 o 6 -5 1 2.52 2.59 13.26 o 7 -5 1 443.61 422.35 26.80 o 8 -5 1 55.35 82.42 21.61 o -7 -4 1 52.90 87.47 24.35 o -6 -4 1 639.36 735.32 32.28 o -5 -4 1 367.66 364.13 22.05 o -4 -4 1 33.97 44.67 11.10 o -3 -4 1 555.65 491.08 18.59 o -2 -4 1 247.65 263.70 11.67 o -1 -4 1 983.22 1101.33 50.00 o 0 -4 1 7215.21 7369.22 112.25 o 1 -4 1 437.26 502.90 20.46 o 2 -4 1 6014.63 5747.13 107.78 o 3 -4 1 912.21 843.97 32.42 o 4 -4 1 441.47 364.28 16.57 o 5 -4 1 260.34 257.36 15.99 o 6 -4 1 72.72 81.99 14.84 o 7 -4 1 548.32 508.66 26.23 o 8 -4 1 168.11 160.09 23.49 o -8 -3 1 24.75 69.60 24.35 o -7 -3 1 21.67 23.63 19.60 o -6 -3 1 1128.80 1144.12 51.15 o -5 -3 1 338.67 354.48 20.17 o -4 -3 1 727.36 721.06 31.27 o -3 -3 1 613.76 630.71 26.80 o -2 -3 1 20.44 44.53 6.48 o -1 -3 1 782.74 738.49 26.66 o 0 -3 1 2205.47 2275.71 55.62 o 1 -3 1 540.82 546.84 20.61 o 2 -3 1 3161.98 3225.02 74.07 o 3 -3 1 186.75 150.87 10.09 o 4 -3 1 83.70 76.95 9.51 o 5 -3 1 34.83 5.62 10.37 o 6 -3 1 78.74 63.69 13.98 o 7 -3 1 226.56 232.14 21.33 o 8 -3 1 267.39 307.07 25.51 o -8 -2 1 14.10 16.43 23.78 o -7 -2 1 7.76 35.59 17.00 o -6 -2 1 1099.73 1086.49 39.05 o -5 -2 1 712.85 753.48 29.97 o -4 -2 1 1356.57 1278.42 49.86 o -3 -2 1 1938.47 1943.71 77.81 o -2 -2 1 43.68 41.07 6.48 o -1 -2 1 4773.73 4926.22 80.69 o 0 -2 1 8862.79 9193.05 93.81 o 1 -2 1 6274.73 6502.20 81.99 o 2 -2 1 11395.26 10852.17 123.06 o 3 -2 1 144.89 155.77 9.08 o 4 -2 1 372.55 421.05 17.87 o 5 -2 1 242.15 208.22 14.41 o 6 -2 1 40.08 34.58 11.53 o 7 -2 1 194.41 210.38 18.73 o 8 -2 1 182.50 174.50 21.61 o -8 -1 1 3.80 12.25 21.33 o -7 -1 1 13.68 14.84 15.99 o -6 -1 1 683.71 770.34 29.40 o -5 -1 1 1248.30 1291.39 50.00 o -4 -1 1 619.60 689.36 27.95 o -3 -1 1 2481.09 2435.80 81.13 o -2 -1 1 81.74 94.24 6.77 o -1 -1 1 2927.00 3227.90 61.24 o 1 -1 1 416.70 357.36 13.26 o 2 -1 1 11565.92 11723.52 119.46 o 3 -1 1 1646.36 1620.36 57.35 o 4 -1 1 687.77 648.29 27.95 o 5 -1 1 609.24 641.23 28.82 o 6 -1 1 397.93 360.10 18.59 o 7 -1 1 358.82 367.59 21.61 o 8 -1 1 262.98 231.42 24.21 o -8 0 1 37.34 16.72 25.65 o -7 0 1 14.15 32.57 15.85 o -6 0 1 1461.81 1504.51 58.07 o -5 0 1 1874.34 1936.51 90.49 o -4 0 1 375.39 390.79 17.72 o -3 0 1 627.77 650.74 25.65 o -2 0 1 748.55 851.03 35.88 o -1 0 1 1107.98 1155.51 31.85 o 1 0 1 361.40 456.21 19.74 o 2 0 1 8236.17 8684.82 101.88 o 3 0 1 3059.40 3022.27 74.35 o 4 0 1 116.30 104.33 9.08 o 5 0 1 0.68 -0.58 8.65 o 6 0 1 208.14 213.26 15.27 o 7 0 1 240.08 241.79 19.45 o 8 0 1 393.98 442.52 26.37 o -8 1 1 65.52 108.65 20.17 o -7 1 1 50.54 76.23 15.42 o -6 1 1 1240.65 1308.68 49.71 o -5 1 1 1329.95 1191.10 46.40 o -4 1 1 312.53 298.86 12.54 o -3 1 1 859.26 834.32 29.97 o -2 1 1 833.15 895.56 34.87 o -1 1 1 12048.65 12735.22 92.37 o 0 1 1 3120.24 3473.58 34.87 o 1 1 1 49.97 54.61 2.88 o 2 1 1 1480.56 1284.47 46.25 o 3 1 1 2715.96 2875.15 73.78 o 4 1 1 18.32 8.36 6.48 o 5 1 1 43.56 57.35 10.52 o 6 1 1 99.51 100.15 12.97 o 7 1 1 29.97 26.51 15.13 o 8 1 1 296.52 314.13 24.50 o -8 2 1 1.22 -17.87 18.73 o -7 2 1 116.91 100.58 17.87 o -6 2 1 469.90 471.91 25.79 o -5 2 1 2242.99 1987.95 89.48 o -4 2 1 330.41 330.99 16.57 o -3 2 1 1174.99 1183.03 50.72 o -2 2 1 747.93 733.02 34.01 o 0 2 1 7974.82 8874.45 72.48 o 1 2 1 173.49 207.21 7.78 o 2 2 1 4994.44 4900.42 77.52 o 3 2 1 2531.40 2376.87 67.87 o 4 2 1 230.68 233.87 12.97 o 5 2 1 98.12 126.23 11.67 o 6 2 1 743.88 760.25 32.28 o 7 2 1 5.50 11.24 15.99 o 8 2 1 286.07 284.01 23.92 o -8 3 1 5.06 24.06 17.15 o -7 3 1 70.23 68.16 16.72 o -6 3 1 101.48 116.72 15.71 o -5 3 1 1850.97 2085.79 91.50 o -4 3 1 78.69 60.23 9.51 o -3 3 1 1577.46 1473.10 58.65 o -2 3 1 1399.74 1486.06 48.56 o -1 3 1 720.36 769.62 31.12 o 0 3 1 6424.07 6511.13 77.24 o 1 3 1 4870.79 4787.88 71.47 o 2 3 1 2127.94 1930.02 54.61 o 3 3 1 1412.02 1402.06 56.34 o 4 3 1 166.56 154.18 10.09 o 5 3 1 12.37 9.37 11.24 o 6 3 1 677.36 691.23 27.95 o 7 3 1 17.85 26.08 17.72 o 8 3 1 361.09 415.72 29.11 o -8 4 1 7.44 44.67 21.18 o -7 4 1 26.94 16.14 15.99 o -6 4 1 475.93 438.05 24.50 o -5 4 1 1234.03 1270.78 51.30 o -4 4 1 172.81 141.50 11.67 o -3 4 1 2113.25 2315.77 76.08 o -2 4 1 962.66 883.02 43.52 o -1 4 1 493.29 487.91 20.03 o 0 4 1 453.51 437.19 17.00 o 1 4 1 3281.12 3049.65 67.44 o 2 4 1 608.16 603.19 23.63 o 3 4 1 2919.62 2758.00 82.86 o 4 4 1 46.31 71.33 8.93 o 5 4 1 112.80 134.59 14.27 o 6 4 1 444.92 547.57 25.36 o 7 4 1 0.31 16.86 18.44 o 8 4 1 378.78 526.53 37.32 o -8 5 1 0.77 -8.07 18.01 o -7 5 1 96.21 103.89 17.87 o -6 5 1 229.83 217.44 18.01 o -5 5 1 1577.86 1633.91 61.10 o -4 5 1 9.61 22.19 8.79 o -3 5 1 183.61 169.89 11.10 o -2 5 1 67.25 65.56 7.35 o -1 5 1 351.61 295.83 12.68 o 0 5 1 9373.75 9600.98 126.80 o 1 5 1 1243.18 1248.59 51.15 o 2 5 1 2027.27 1822.96 66.28 o 3 5 1 1909.36 1886.07 76.37 o 4 5 1 92.20 93.95 11.24 o 5 5 1 1.49 6.48 10.66 o 6 5 1 25.60 27.23 14.41 o 7 5 1 7.62 3.03 18.59 o 8 5 1 107.02 174.21 26.51 o -7 6 1 134.48 116.57 20.61 o -6 6 1 0.21 -1.87 12.82 o -5 6 1 1534.94 1559.84 60.09 o -4 6 1 368.30 328.11 16.57 o -3 6 1 1234.94 1179.86 44.53 o -2 6 1 1.38 -3.03 6.34 o -1 6 1 96.39 75.94 7.93 o 0 6 1 3562.02 3651.69 89.92 o 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