#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/76/2217676.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2217676_Fobs
loop_
_publ_author_name
'Kai, Zhao'
'Yin, Xian-Hong'
'Yu, Feng'
'Zhu, Jie'
'Lin, Cui-Wu'
_publ_section_title
;
 Bis[6-(3,5-dimethyl-1<i>H</i>-pyrazol-1-yl)picolinato-\k^2^<i>N</i>^1^,<i>O</i>^2^]cadmium(II)
 1.75-hydrate
;
_journal_coeditor_code           TK2242
_journal_issue                   2
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m434
_journal_volume                  64
_journal_year                    2008
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                63.905
_cell_angle_beta                 72.253
_cell_angle_gamma                82.688
_cell_length_a                   9.7503
_cell_length_b                   11.4398
_cell_length_c                   12.8429
_exptl_crystal_F_000             583.00
_reflns_d_resolution_high        0.8406
_[local]_cod_data_source_file    tk2242Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 071230a in P-1'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            228.93
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 1.46 -3.35 2.24 o
2 0 0 15813.02 17901.75 502.32 o
3 0 0 402.56 490.28 20.45 o
4 0 0 3444.02 3791.95 114.50 o
5 0 0 1065.81 1250.41 46.15 o
7 0 0 563.19 586.58 30.71 o
8 0 0 1161.13 1110.50 29.98 o
9 0 0 786.44 705.54 23.78 o
10 0 0 164.05 141.97 17.78 o
-9 1 0 19.43 28.01 9.80 o
-8 1 0 303.13 277.94 21.72 o
-7 1 0 249.30 254.29 12.51 o
-6 1 0 1150.31 1233.77 28.94 o
-4 1 0 1113.91 1137.24 39.66 o
-3 1 0 5517.79 6174.38 176.99 o
-2 1 0 2695.73 3253.80 94.48 o
-1 1 0 10083.00 12594.16 362.92 o
0 1 0 1549.55 1175.94 36.09 o
1 1 0 2034.51 2103.18 65.55 o
2 1 0 4517.36 5217.00 150.85 o
3 1 0 4177.79 4518.95 133.23 o
4 1 0 104.92 144.72 13.47 o
5 1 0 476.71 360.15 21.67 o
7 1 0 1580.73 1575.00 37.24 o
8 1 0 143.98 149.46 14.03 o
9 1 0 58.08 48.52 15.76 o
10 1 0 42.86 58.91 12.01 o
11 1 0 67.37 48.35 19.38 o
-10 2 0 26.38 38.60 20.66 o
-9 2 0 641.53 599.63 36.78 o
-8 2 0 225.01 161.76 22.68 o
-7 2 0 343.00 309.04 11.90 o
-6 2 0 267.04 271.82 9.96 o
-5 2 0 786.23 781.27 16.74 o
-4 2 0 3914.16 4649.10 141.80 o
-3 2 0 3699.96 3992.36 120.83 o
-2 2 0 3486.03 4061.93 121.15 o
-1 2 0 1358.83 1379.60 43.81 o
0 2 0 1772.30 1667.22 35.71 o
1 2 0 296.03 227.36 12.27 o
2 2 0 6111.23 6180.44 127.37 o
3 2 0 78.60 93.57 7.30 o
4 2 0 7303.82 8361.10 243.20 o
5 2 0 250.13 202.07 18.10 o
7 2 0 0.17 2.16 10.09 o
8 2 0 1587.11 1476.46 37.36 o
9 2 0 22.48 20.99 9.60 o
10 2 0 201.65 186.62 15.79 o
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-9 3 0 10.81 -1.86 16.03 o
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-7 3 0 39.33 62.94 15.87 o
-6 3 0 658.88 702.81 16.21 o
-5 3 0 87.21 84.65 6.39 o
-4 3 0 3150.89 3200.30 49.80 o
-3 3 0 453.80 397.80 22.79 o
-2 3 0 1485.01 1424.04 47.53 o
-1 3 0 4319.58 4476.32 133.34 o
0 3 0 2146.06 2137.37 67.12 o
1 3 0 1250.99 1133.30 21.70 o
2 3 0 580.12 589.85 17.44 o
3 3 0 7496.43 8184.08 169.45 o
4 3 0 313.33 338.22 15.57 o
5 3 0 2773.46 3223.41 104.76 o
7 3 0 453.86 485.79 18.90 o
8 3 0 1.91 -6.02 8.10 o
9 3 0 637.85 563.75 22.38 o
10 3 0 1.83 7.88 10.38 o
-10 4 0 6.08 -27.80 19.01 o
-9 4 0 230.87 247.59 27.53 o
-8 4 0 523.69 490.92 33.60 o
-7 4 0 1856.50 1986.41 74.04 o
-6 4 0 89.58 116.66 16.24 o
-5 4 0 428.09 469.41 25.98 o
-4 4 0 1999.52 2115.12 71.49 o
-3 4 0 3162.64 3304.00 103.64 o
-2 4 0 310.36 306.16 17.73 o
-1 4 0 4387.36 4385.91 91.40 o
0 4 0 537.73 500.80 10.32 o
1 4 0 3771.67 3888.68 67.69 o
2 4 0 5865.19 5859.79 157.26 o
3 4 0 1224.43 1210.52 32.49 o
4 4 0 2811.77 3180.81 73.32 o
5 4 0 123.58 75.29 16.72 o
6 4 0 1383.29 1462.26 35.52 o
7 4 0 19.06 8.33 12.70 o
8 4 0 687.51 645.97 23.67 o
9 4 0 9.18 -4.76 9.71 o
10 4 0 161.00 151.14 16.32 o
-10 5 0 147.29 148.29 25.56 o
-9 5 0 3.22 -4.15 18.48 o
-8 5 0 936.34 915.65 45.56 o
-7 5 0 94.21 99.52 19.91 o
-6 5 0 421.58 476.12 29.77 o
-5 5 0 9.20 -0.96 10.81 o
-4 5 0 1146.94 1209.69 46.79 o
-3 5 0 1525.87 1575.48 56.53 o
-2 5 0 2401.73 2452.65 80.75 o
-1 5 0 325.44 312.49 32.77 o
0 5 0 3738.33 3274.01 86.29 o
1 5 0 2621.88 2803.71 40.01 o
2 5 0 13.98 -0.51 3.85 o
3 5 0 978.18 910.38 40.56 o
4 5 0 1185.78 1144.00 49.56 o
5 5 0 1474.11 1580.25 32.23 o
6 5 0 9.05 7.59 7.83 o
7 5 0 500.96 478.00 20.23 o
8 5 0 10.94 11.58 10.21 o
9 5 0 308.10 254.77 17.19 o
10 5 0 2.53 -13.23 15.68 o
-9 6 0 134.06 133.17 24.49 o
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-7 6 0 449.34 406.05 30.19 o
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-5 6 0 1277.60 1351.81 54.56 o
-4 6 0 1.34 4.47 10.65 o
-3 6 0 2480.45 2467.12 83.62 o
-2 6 0 3.33 -3.73 9.58 o
-1 6 0 4067.97 4261.55 90.81 o
0 6 0 27.86 21.05 7.30 o
1 6 0 2611.90 2405.88 35.81 o
2 6 0 1068.54 1051.26 23.25 o
3 6 0 2249.17 2248.41 40.29 o
4 6 0 918.45 1020.26 23.76 o
5 6 0 1357.14 1397.55 32.20 o
6 6 0 24.11 19.09 8.90 o
7 6 0 828.12 711.63 40.08 o
8 6 0 463.87 423.98 31.20 o
9 6 0 14.36 0.59 11.65 o
-9 7 0 99.45 63.63 23.64 o
-8 7 0 32.36 50.74 20.02 o
-7 7 0 5.26 -15.65 15.55 o
-6 7 0 95.61 79.50 20.02 o
-5 7 0 20.27 20.71 16.24 o
-4 7 0 1730.49 1689.13 64.41 o
-3 7 0 74.15 74.60 16.03 o
-2 7 0 1470.94 1558.39 60.15 o
-1 7 0 6.24 -5.64 12.89 o
0 7 0 2307.28 2356.41 45.67 o
1 7 0 0.72 2.50 4.42 o
2 7 0 1486.46 1539.07 29.67 o
3 7 0 253.00 261.13 11.56 o
4 7 0 1610.37 1610.18 33.10 o
5 7 0 683.16 713.11 34.92 o
6 7 0 853.21 893.82 24.90 o
7 7 0 165.29 192.30 17.25 o
8 7 0 69.15 75.16 17.68 o
9 7 0 117.37 120.53 18.34 o
-8 8 0 70.45 65.55 22.10 o
-7 8 0 413.40 442.31 34.45 o
-6 8 0 461.29 457.54 34.18 o
-5 8 0 520.12 550.23 36.30 o
-4 8 0 531.84 560.88 35.61 o
-3 8 0 958.38 926.08 44.29 o
-2 8 0 239.97 252.97 25.29 o
-1 8 0 1286.06 1231.36 37.10 o
0 8 0 29.01 10.54 10.00 o
1 8 0 1330.38 1417.14 39.41 o
2 8 0 21.69 32.99 7.06 o
3 8 0 2037.04 2045.52 47.31 o
4 8 0 26.40 16.15 8.29 o
5 8 0 847.63 843.77 24.55 o
6 8 0 56.27 59.89 11.19 o
7 8 0 480.62 459.47 19.26 o
8 8 0 34.03 35.48 13.13 o
-7 9 0 253.46 243.49 28.59 o
-6 9 0 225.69 252.43 28.38 o
-5 9 0 201.84 186.20 25.98 o
-4 9 0 35.59 55.59 20.34 o
-3 9 0 233.34 206.17 25.56 o
-2 9 0 11.20 -1.67 17.28 o
-1 9 0 54.10 12.40 11.31 o
0 9 0 449.56 529.79 36.47 o
1 9 0 6.68 27.26 19.27 o
2 9 0 737.49 789.23 46.47 o
3 9 0 206.22 192.21 12.05 o
4 9 0 461.85 462.34 17.63 o
5 9 0 2.88 -13.36 9.26 o
6 9 0 224.05 220.56 29.30 o
7 9 0 8.52 -15.59 10.40 o
-6 10 0 121.80 129.70 27.37 o
-5 10 0 32.05 15.49 20.34 o
-4 10 0 190.14 149.99 27.69 o
-3 10 0 79.09 26.81 15.57 o
-2 10 0 8.73 -26.76 17.84 o
-1 10 0 242.87 219.85 28.22 o
0 10 0 404.29 484.80 38.12 o
1 10 0 884.04 868.33 50.09 o
2 10 0 202.78 186.52 32.27 o
3 10 0 579.23 594.41 44.71 o
4 10 0 20.56 -8.57 24.01 o
5 10 0 207.99 213.03 21.93 o
6 10 0 0.44 -11.02 18.32 o
-4 11 0 53.84 63.20 18.20 o
-3 11 0 238.83 310.85 33.39 o
-2 11 0 161.77 209.63 31.36 o
-1 11 0 413.85 462.97 39.24 o
0 11 0 167.76 162.40 30.09 o
1 11 0 33.86 6.39 25.34 o
2 11 0 305.83 324.48 37.32 o
3 11 0 72.47 48.72 27.63 o
4 11 0 88.78 110.64 31.68 o
-2 12 0 137.90 145.15 31.20 o
-1 12 0 28.80 -11.93 28.65 o
0 12 0 157.68 140.94 33.28 o
1 12 0 58.29 31.68 28.33 o
2 12 0 42.91 15.60 28.11 o
-3 -11 1 200.26 237.10 36.69 o
-2 -11 1 38.79 -23.05 25.24 o
-1 -11 1 175.08 155.32 31.95 o
0 -11 1 40.23 21.24 25.93 o
1 -11 1 72.67 79.55 29.02 o
2 -11 1 368.70 404.03 37.91 o
3 -11 1 141.23 118.47 29.71 o
4 -11 1 181.09 246.69 34.50 o
-5 -10 1 0.01 -0.46 10.29 o
-4 -10 1 370.73 425.64 41.26 o
-3 -10 1 12.78 3.78 24.07 o
-2 -10 1 392.28 391.35 38.50 o
-1 -10 1 5.94 -27.10 21.30 o
0 -10 1 893.55 946.58 53.02 o
1 -10 1 184.18 205.64 30.99 o
2 -10 1 42.80 11.18 21.46 o
3 -10 1 19.51 16.40 22.42 o
4 -10 1 50.42 49.20 22.95 o
5 -10 1 53.02 50.10 23.43 o
6 -10 1 96.22 102.82 27.16 o
-6 -9 1 29.79 25.92 11.40 o
-5 -9 1 312.70 330.57 27.07 o
-4 -9 1 25.33 5.12 9.03 o
-3 -9 1 563.58 569.43 18.93 o
-2 -9 1 10.79 -5.48 21.99 o
-1 -9 1 1001.18 1126.70 56.69 o
0 -9 1 22.11 23.53 20.18 o
1 -9 1 40.39 31.15 19.70 o
2 -9 1 54.63 -6.60 17.62 o
3 -9 1 270.90 215.16 26.94 o
4 -9 1 326.15 312.34 29.87 o
5 -9 1 98.95 102.71 24.38 o
6 -9 1 154.94 157.13 28.54 o
7 -9 1 82.07 65.55 25.45 o
-7 -8 1 60.71 58.85 12.83 o
-6 -8 1 224.74 255.39 15.45 o
-5 -8 1 175.96 173.01 14.26 o
-4 -8 1 757.83 727.69 21.82 o
-3 -8 1 201.45 180.74 12.81 o
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-1 -8 1 315.72 267.77 27.21 o
0 -8 1 46.27 35.67 17.57 o
1 -8 1 33.44 -22.15 14.91 o
2 -8 1 845.55 815.85 42.48 o
3 -8 1 75.41 47.97 18.53 o
4 -8 1 665.45 609.10 36.99 o
5 -8 1 279.44 266.33 27.85 o
6 -8 1 369.92 341.30 30.40 o
7 -8 1 142.73 144.72 25.13 o
8 -8 1 118.50 92.43 25.50 o
-8 -7 1 162.56 196.29 18.52 o
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-6 -7 1 400.19 415.70 18.00 o
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-4 -7 1 950.05 1050.05 52.64 o
-3 -7 1 186.23 202.49 24.81 o
-2 -7 1 22.71 -13.05 13.90 o
-1 -7 1 968.85 927.15 44.87 o
0 -7 1 95.95 98.10 7.59 o
1 -7 1 1848.78 1899.11 71.22 o
2 -7 1 35.34 45.74 15.23 o
3 -7 1 1280.76 1254.83 52.70 o
4 -7 1 38.30 57.72 17.15 o
5 -7 1 936.16 888.24 43.75 o
6 -7 1 33.84 12.94 17.94 o
7 -7 1 148.04 163.25 25.24 o
8 -7 1 151.42 163.99 27.64 o
9 -7 1 99.83 107.18 25.02 o
-9 -6 1 162.95 163.17 17.99 o
-8 -6 1 23.26 14.09 11.73 o
-7 -6 1 821.86 813.83 28.41 o
-6 -6 1 1336.57 1353.51 63.34 o
-5 -6 1 678.15 755.76 61.03 o
-4 -6 1 737.87 800.77 29.22 o
-3 -6 1 494.21 525.12 21.98 o
-2 -6 1 411.79 346.06 16.74 o
-1 -6 1 359.48 346.73 19.26 o
0 -6 1 1831.64 1839.29 67.44 o
1 -6 1 246.65 198.23 13.67 o
2 -6 1 3164.00 3147.45 103.80 o
3 -6 1 115.35 87.32 15.81 o
4 -6 1 609.68 605.48 32.20 o
5 -6 1 0.05 -7.51 13.74 o
6 -6 1 160.47 146.96 21.40 o
7 -6 1 9.45 -24.12 16.08 o
8 -6 1 283.76 278.47 28.12 o
9 -6 1 67.54 50.00 23.27 o
-9 -5 1 25.40 26.05 11.50 o
-8 -5 1 919.13 848.77 29.01 o
-6 -5 1 222.44 250.41 18.81 o
-5 -5 1 24.49 3.96 10.18 o
-4 -5 1 3508.98 3826.08 100.90 o
-3 -5 1 2045.03 2102.83 66.00 o
-2 -5 1 3388.68 3710.93 82.89 o
-1 -5 1 1051.45 1079.35 23.23 o
0 -5 1 2140.87 2247.41 51.41 o
1 -5 1 3757.85 3556.54 97.36 o
2 -5 1 1445.52 1359.00 51.26 o
3 -5 1 212.89 164.79 17.25 o
4 -5 1 514.60 514.99 28.38 o
5 -5 1 909.51 988.15 42.80 o
6 -5 1 148.50 144.61 19.75 o
7 -5 1 1339.10 1369.11 57.97 o
8 -5 1 4.44 21.14 18.64 o
9 -5 1 269.17 226.72 26.78 o
10 -5 1 28.68 23.75 21.09 o
-10 -4 1 1.26 0.19 11.16 o
-9 -4 1 366.17 340.43 18.76 o
-8 -4 1 1.72 1.42 9.44 o
-6 -4 1 46.61 36.95 15.55 o
-5 -4 1 2633.44 2834.71 69.14 o
-4 -4 1 53.74 57.78 9.77 o
-3 -4 1 1251.33 1264.02 34.52 o
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-1 -4 1 3990.38 4059.66 88.66 o
0 -4 1 1997.09 1946.52 54.11 o
1 -4 1 3347.48 3112.16 66.28 o
2 -4 1 412.96 356.69 19.86 o
3 -4 1 3143.35 3375.43 106.83 o
4 -4 1 1486.75 1599.33 57.81 o
5 -4 1 205.85 231.99 19.75 o
6 -4 1 254.38 283.90 22.31 o
7 -4 1 67.15 89.88 19.65 o
8 -4 1 1948.76 2002.91 78.03 o
9 -4 1 74.20 86.68 23.27 o
10 -4 1 409.47 388.42 34.45 o
-10 -3 1 175.35 156.62 15.86 o
-9 -3 1 90.89 86.08 13.20 o
-8 -3 1 866.05 821.43 33.16 o
-7 -3 1 32.90 -0.96 15.07 o
-6 -3 1 1220.13 1241.63 53.66 o
-5 -3 1 80.77 79.92 15.18 o
-4 -3 1 5136.03 5602.00 120.91 o
-3 -3 1 789.44 865.84 25.37 o
-2 -3 1 6088.44 6368.71 132.94 o
-1 -3 1 997.02 839.52 52.96 o
0 -3 1 5719.56 5956.29 122.45 o
1 -3 1 1725.93 1842.96 40.41 o
2 -3 1 3829.57 4131.50 125.41 o
3 -3 1 771.71 743.19 30.34 o
4 -3 1 2210.30 2509.61 62.89 o
5 -3 1 1890.49 1961.03 45.91 o
6 -3 1 339.22 314.95 23.11 o
7 -3 1 468.38 501.15 30.62 o
8 -3 1 43.30 17.68 17.68 o
9 -3 1 459.08 406.47 32.37 o
10 -3 1 41.08 27.53 20.29 o
-10 -2 1 48.04 29.06 10.93 o
-9 -2 1 181.33 172.42 13.87 o
-7 -2 1 1043.13 1145.33 52.59 o
-6 -2 1 855.52 940.08 44.23 o
-5 -2 1 2180.17 2326.23 80.11 o
-4 -2 1 2.15 -8.14 7.88 o
-3 -2 1 2446.03 2454.12 61.85 o
-2 -2 1 130.38 103.04 7.09 o
-1 -2 1 8384.21 9632.49 195.35 o
0 -2 1 1.79 -0.67 2.40 o
1 -2 1 349.00 308.68 8.67 o
2 -2 1 2.88 8.37 4.85 o
3 -2 1 698.04 753.55 18.99 o
4 -2 1 926.55 991.02 25.40 o
5 -2 1 837.23 983.85 27.05 o
6 -2 1 1337.88 1457.52 38.13 o
7 -2 1 474.68 509.40 20.64 o
8 -2 1 424.32 420.91 32.00 o
9 -2 1 60.92 38.34 20.23 o
10 -2 1 294.40 278.85 28.59 o
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-1 0 1 6604.42 8059.41 135.08 o
0 0 1 1701.58 1294.06 38.91 o
1 0 1 20170.80 20944.72 595.42 o
2 0 1 869.84 1052.29 33.32 o
3 0 1 8.25 9.31 2.40 o
4 0 1 7295.81 8879.98 152.48 o
5 0 1 767.56 805.14 21.34 o
6 0 1 195.45 188.76 10.10 o
7 0 1 1215.33 1317.79 31.92 o
8 0 1 136.22 153.45 20.71 o
9 0 1 600.77 536.44 35.02 o
10 0 1 319.11 277.36 27.85 o
-9 1 1 546.89 450.89 18.45 o
-8 1 1 340.44 290.66 14.75 o
-7 1 1 662.28 652.17 34.01 o
-6 1 1 1471.53 1575.75 58.23 o
-5 1 1 1596.04 1604.92 56.74 o
-4 1 1 7007.85 8241.86 237.83 o
-3 1 1 3568.51 4153.32 122.53 o
-2 1 1 42171.25 51302.18 1430.16 o
-1 1 1 9398.51 10110.85 286.37 o
0 1 1 24186.82 21000.20 431.31 o
1 1 1 212.89 130.24 6.44 o
2 1 1 2896.60 3245.64 56.80 o
3 1 1 676.51 813.91 30.61 o
4 1 1 1421.06 1560.13 31.78 o
5 1 1 258.94 218.92 9.69 o
6 1 1 2366.43 2657.06 53.31 o
7 1 1 528.91 573.12 19.75 o
8 1 1 1832.92 1730.68 40.98 o
9 1 1 456.93 356.00 29.50 o
10 1 1 128.66 139.61 23.59 o
11 1 1 77.77 67.78 22.57 o
-10 2 1 365.32 348.33 30.09 o
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-8 2 1 451.07 431.09 16.87 o
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