#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217682.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217682_Fobs loop_ _publ_author_name 'Zang, Yan' 'Wu, Xiu-Mei' 'Zheng, Zhan-Ying' 'Song, Hai-Bin' 'Liu, Qing-Xiang' _publ_section_title ; 1-Benzylimidazolium hexafluorophosphate--1-benzylimidazole (1/1) ; _journal_coeditor_code WN2226 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o478 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.109 _cell_angle_gamma 90.000 _cell_length_a 6.6459 _cell_length_b 6.9825 _cell_length_c 22.3558 _exptl_crystal_F_000 476.00 _reflns_d_resolution_high 0.8407 _[local]_cod_data_source_file wn2226Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 70729D in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2451.58 2220.04 25.98 o 4 0 0 2593.85 2503.41 30.59 o 6 0 0 6.86 10.17 1.70 o 1 1 0 4137.16 4158.97 35.87 o 2 1 0 204.40 200.39 2.53 o 3 1 0 900.76 830.32 8.06 o 4 1 0 90.53 110.65 2.33 o 5 1 0 111.31 108.40 2.61 o 6 1 0 1.00 -0.31 0.80 o 7 1 0 1.60 0.39 0.98 o 0 2 0 92.15 202.82 2.37 o 1 2 0 1196.50 1139.90 5.58 o 2 2 0 1437.39 1519.64 10.70 o 3 2 0 35.21 40.01 1.30 o 4 2 0 427.93 429.95 5.40 o 5 2 0 48.34 48.54 1.85 o 6 2 0 56.43 59.17 1.77 o 7 2 0 1.04 2.14 0.80 o 1 3 0 668.40 621.04 3.44 o 2 3 0 183.87 178.77 1.65 o 3 3 0 28.72 17.96 0.77 o 4 3 0 694.72 697.81 6.28 o 5 3 0 108.09 117.80 2.28 o 6 3 0 63.67 56.16 1.74 o 7 3 0 15.08 18.16 1.59 o 0 4 0 72.75 54.59 1.06 o 1 4 0 227.62 232.67 1.78 o 2 4 0 0.55 1.05 0.35 o 3 4 0 0.01 1.19 0.42 o 4 4 0 176.13 168.49 2.23 o 5 4 0 82.80 77.65 1.95 o 6 4 0 0.23 -0.12 0.80 o 1 5 0 26.17 23.38 0.87 o 2 5 0 11.60 9.35 0.67 o 3 5 0 9.96 11.28 1.15 o 4 5 0 283.15 268.72 7.99 o 5 5 0 2.54 1.55 0.90 o 6 5 0 4.87 8.77 1.18 o 0 6 0 252.35 237.53 4.61 o 1 6 0 0.00 0.06 0.52 o 2 6 0 337.55 339.52 7.45 o 3 6 0 121.43 113.60 2.46 o 4 6 0 126.29 107.17 3.21 o 5 6 0 0.53 1.18 1.52 o 1 7 0 87.67 91.80 2.19 o 2 7 0 0.26 0.19 0.66 o 3 7 0 28.27 25.24 1.42 o 4 7 0 0.22 0.51 0.95 o 0 8 0 116.45 115.71 4.79 o 1 8 0 6.46 3.76 1.27 o 2 8 0 0.49 -0.80 0.92 o -7 0 1 158.30 152.84 5.24 o -5 0 1 234.60 211.25 5.20 o -3 0 1 2764.32 2563.58 30.38 o -1 0 1 114.36 119.11 2.03 o 1 0 1 379.43 375.30 5.00 o 3 0 1 1224.76 1128.77 14.73 o 5 0 1 127.57 121.93 3.87 o 7 0 1 78.55 80.35 3.88 o -7 1 1 7.38 9.31 1.42 o -6 1 1 48.52 44.27 1.92 o -5 1 1 71.27 74.42 2.17 o -4 1 1 1883.18 1898.43 21.79 o -3 1 1 1147.55 1263.03 11.42 o -2 1 1 146.90 96.21 1.57 o -1 1 1 5201.18 5513.00 51.74 o 0 1 1 606.97 608.96 5.39 o 1 1 1 6095.55 6060.91 36.15 o 2 1 1 896.76 765.09 7.16 o 3 1 1 139.13 145.12 2.79 o 4 1 1 262.07 235.10 3.60 o 5 1 1 236.88 237.49 3.99 o 6 1 1 34.40 33.03 1.79 o 7 1 1 4.56 8.14 1.31 o -7 2 1 98.22 113.39 2.63 o -6 2 1 42.87 42.67 1.52 o -5 2 1 23.67 26.27 3.46 o -4 2 1 79.32 80.73 1.64 o -3 2 1 579.28 602.28 5.16 o -2 2 1 2.01 4.80 0.39 o -1 2 1 1020.26 929.04 5.10 o 0 2 1 4970.59 5133.58 28.77 o 1 2 1 720.91 823.95 4.62 o 2 2 1 272.06 258.07 3.25 o 3 2 1 35.35 27.14 1.12 o 4 2 1 1.44 -0.22 0.70 o 5 2 1 225.51 225.01 3.95 o 6 2 1 81.73 81.74 4.42 o 7 2 1 48.20 52.10 1.88 o -7 3 1 8.77 8.98 1.28 o -6 3 1 20.34 18.40 2.98 o -5 3 1 6.60 6.49 0.79 o -4 3 1 291.32 290.31 3.46 o -3 3 1 7.64 5.49 0.54 o -2 3 1 8.68 6.05 0.38 o -1 3 1 15.93 15.32 0.47 o 0 3 1 653.69 615.95 3.90 o 1 3 1 721.16 740.04 4.68 o 2 3 1 386.81 425.09 2.97 o 3 3 1 92.19 86.91 1.35 o 4 3 1 466.60 439.72 4.56 o 5 3 1 63.85 61.31 1.45 o 6 3 1 45.56 46.44 1.63 o 7 3 1 36.74 37.82 2.08 o -6 4 1 2.23 4.07 1.04 o -5 4 1 487.14 471.91 6.59 o -4 4 1 104.98 100.58 2.02 o -3 4 1 421.62 425.33 3.67 o -2 4 1 109.24 105.08 1.32 o -1 4 1 299.87 301.37 2.38 o 0 4 1 207.74 250.58 2.56 o 1 4 1 2226.80 2300.25 13.73 o 2 4 1 60.68 47.38 0.90 o 3 4 1 47.02 44.10 1.05 o 4 4 1 6.68 8.23 1.08 o 5 4 1 24.48 28.20 1.30 o 6 4 1 1.39 1.96 0.70 o -6 5 1 15.27 19.41 1.59 o -5 5 1 18.07 17.58 1.49 o -4 5 1 187.13 194.37 8.15 o -3 5 1 4.86 6.13 1.11 o -2 5 1 104.54 107.56 1.78 o -1 5 1 6.08 5.32 0.62 o 0 5 1 803.45 794.30 5.84 o 1 5 1 39.90 39.58 1.08 o 2 5 1 66.57 64.05 1.37 o 3 5 1 164.53 158.27 2.27 o 4 5 1 317.45 339.82 6.04 o 5 5 1 11.10 9.21 1.21 o 6 5 1 0.72 1.73 0.91 o -5 6 1 5.07 6.37 1.34 o -4 6 1 5.43 7.93 1.18 o -3 6 1 33.44 35.08 1.49 o -2 6 1 55.54 53.76 1.70 o -1 6 1 5.32 5.51 0.77 o 0 6 1 8.31 8.71 0.73 o 1 6 1 141.94 138.81 2.10 o 2 6 1 37.21 34.38 1.43 o 3 6 1 0.01 -1.00 0.67 o 4 6 1 27.48 18.42 1.51 o 5 6 1 60.33 56.70 2.44 o -4 7 1 72.58 82.48 2.91 o -3 7 1 41.97 35.30 1.61 o -2 7 1 45.03 34.96 1.48 o -1 7 1 1.02 1.40 0.69 o 0 7 1 0.30 -0.94 0.63 o 1 7 1 19.24 18.39 1.44 o 2 7 1 25.92 30.14 1.45 o 3 7 1 86.04 90.44 2.69 o 4 7 1 15.91 19.76 2.52 o -2 8 1 5.86 5.03 1.19 o -1 8 1 3.13 4.68 1.12 o 0 8 1 1.18 0.12 0.94 o 1 8 1 9.59 13.10 1.43 o 2 8 1 17.96 21.14 2.78 o -6 0 2 67.18 74.77 3.35 o -4 0 2 4790.36 4990.32 57.70 o -2 0 2 5645.64 5363.79 63.89 o 0 0 2 4865.20 5121.16 62.99 o 2 0 2 168.62 115.95 2.58 o 4 0 2 924.98 914.22 13.16 o 6 0 2 456.58 433.37 8.88 o -7 1 2 23.00 22.32 1.45 o -6 1 2 9.92 11.12 1.52 o -5 1 2 490.97 484.28 6.14 o -4 1 2 17.82 20.94 1.21 o -3 1 2 105.58 70.07 4.78 o -2 1 2 406.03 410.59 3.43 o -1 1 2 12881.16 13159.29 285.26 o 0 1 2 545.29 527.79 3.78 o 1 1 2 4402.16 4239.17 25.68 o 2 1 2 3.23 3.61 0.49 o 3 1 2 385.27 386.27 6.52 o 4 1 2 10.30 11.55 0.91 o 5 1 2 210.21 228.77 3.98 o 6 1 2 21.34 19.47 1.46 o 7 1 2 0.92 2.34 0.98 o -7 2 2 1.53 1.33 0.95 o -6 2 2 2.98 2.53 0.84 o -5 2 2 283.22 268.85 3.48 o -4 2 2 30.73 22.89 1.02 o -3 2 2 2.76 1.34 0.39 o -2 2 2 1622.25 1827.57 12.63 o -1 2 2 268.39 280.24 1.92 o 0 2 2 6965.27 6872.93 39.53 o 1 2 2 977.11 1021.58 5.60 o 2 2 2 55.21 68.63 1.17 o 3 2 2 113.65 104.01 2.14 o 4 2 2 1009.24 992.25 12.61 o 5 2 2 17.92 17.79 1.36 o 6 2 2 9.32 7.23 1.13 o 7 2 2 41.88 42.47 2.18 o -7 3 2 26.63 33.12 1.98 o -6 3 2 56.16 56.41 2.29 o -5 3 2 0.52 1.62 0.62 o -4 3 2 0.53 1.30 0.58 o -3 3 2 7.99 18.11 0.77 o -2 3 2 167.18 185.96 1.69 o -1 3 2 1011.29 1080.55 6.06 o 0 3 2 1366.37 1423.68 7.69 o 1 3 2 134.23 163.23 1.51 o 2 3 2 1286.73 1260.56 6.48 o 3 3 2 147.91 147.91 1.81 o 4 3 2 24.81 26.78 1.12 o 5 3 2 0.60 0.29 0.66 o 6 3 2 0.31 1.23 0.71 o 7 3 2 11.51 13.85 1.48 o -6 4 2 3.57 3.15 1.01 o -5 4 2 15.01 15.59 1.38 o -4 4 2 123.16 113.29 2.17 o -3 4 2 75.33 81.28 1.39 o -2 4 2 141.43 152.24 1.62 o -1 4 2 62.61 65.65 1.00 o 0 4 2 364.32 331.56 2.53 o 1 4 2 549.86 594.10 3.96 o 2 4 2 411.85 427.05 3.13 o 3 4 2 77.73 71.67 1.31 o 4 4 2 687.16 712.83 5.64 o 5 4 2 142.55 151.19 2.30 o 6 4 2 12.77 13.92 1.38 o -6 5 2 7.73 9.84 1.54 o -5 5 2 1.43 2.65 0.91 o -4 5 2 5.94 3.36 2.11 o -3 5 2 164.92 159.87 3.36 o -2 5 2 1.11 0.24 0.57 o -1 5 2 15.70 13.93 0.87 o 0 5 2 29.93 30.03 0.97 o 1 5 2 931.64 927.00 6.67 o 2 5 2 403.52 388.96 3.68 o 3 5 2 647.89 645.26 9.92 o 4 5 2 19.50 17.96 1.41 o 5 5 2 95.06 85.82 2.74 o 6 5 2 1.24 0.87 1.05 o -5 6 2 32.80 26.19 1.82 o -4 6 2 31.20 30.45 1.81 o -3 6 2 36.45 43.10 1.94 o -2 6 2 3.74 3.41 0.74 o -1 6 2 116.02 123.74 2.37 o 0 6 2 230.81 217.90 2.67 o 1 6 2 42.91 42.15 1.23 o 2 6 2 11.51 15.02 1.69 o 3 6 2 212.00 226.94 3.51 o 4 6 2 3.70 3.95 1.08 o 5 6 2 0.00 0.49 0.88 o -4 7 2 12.67 10.67 1.36 o -3 7 2 13.85 16.14 1.47 o -2 7 2 3.97 3.93 0.79 o -1 7 2 23.75 27.89 1.36 o 0 7 2 20.45 20.18 1.18 o 1 7 2 65.81 64.74 2.35 o 2 7 2 5.59 2.64 0.80 o 3 7 2 4.01 4.78 1.41 o 4 7 2 0.23 0.35 0.96 o -2 8 2 40.95 44.65 1.82 o -1 8 2 31.22 32.40 1.99 o 0 8 2 43.95 49.03 2.29 o 1 8 2 1.21 0.79 0.95 o -7 0 3 100.28 102.21 3.03 o -5 0 3 323.69 308.99 6.42 o -3 0 3 5081.31 4867.89 57.12 o -1 0 3 944.75 869.88 11.06 o 1 0 3 10613.46 10472.10 626.06 o 3 0 3 7.92 6.10 0.92 o 5 0 3 82.18 93.90 3.52 o 7 0 3 3.68 6.41 1.68 o -7 1 3 19.12 19.64 1.31 o -6 1 3 0.92 0.26 0.97 o -5 1 3 46.01 45.51 1.72 o -4 1 3 1782.25 1849.42 16.70 o -3 1 3 495.98 510.37 4.44 o -2 1 3 758.05 674.31 5.39 o -1 1 3 447.76 413.71 3.25 o 0 1 3 1477.19 1403.73 8.18 o 1 1 3 1253.81 1306.17 7.69 o 2 1 3 173.00 232.84 2.98 o 3 1 3 312.92 319.21 4.10 o 4 1 3 160.23 143.85 2.77 o 5 1 3 201.83 206.13 3.78 o 6 1 3 3.63 5.01 1.08 o 7 1 3 23.81 18.20 1.59 o -7 2 3 22.47 24.01 1.74 o -6 2 3 69.84 64.80 1.81 o -5 2 3 65.33 66.78 1.70 o -4 2 3 246.16 262.09 3.20 o -3 2 3 366.19 338.73 3.33 o -2 2 3 347.70 358.99 3.17 o -1 2 3 411.83 476.04 3.89 o 0 2 3 76.28 64.58 0.77 o 1 2 3 1226.55 1053.29 5.77 o 2 2 3 391.54 379.02 2.98 o 3 2 3 187.47 205.93 3.19 o 4 2 3 4.88 4.62 0.90 o 5 2 3 1.62 2.08 0.88 o 6 2 3 2.36 1.08 0.88 o 7 2 3 38.95 44.89 2.29 o -7 3 3 0.82 -0.03 0.80 o -6 3 3 3.47 1.61 0.86 o -5 3 3 0.04 1.24 0.68 o -4 3 3 566.05 582.86 5.43 o -3 3 3 58.27 60.43 1.26 o -2 3 3 5.39 7.98 0.82 o -1 3 3 0.01 -0.35 0.23 o 0 3 3 1909.13 1963.21 10.32 o 1 3 3 294.04 282.35 2.18 o 2 3 3 23.73 32.09 0.63 o 3 3 3 104.40 112.72 1.87 o 4 3 3 297.60 280.58 3.43 o 5 3 3 127.47 132.34 3.19 o 6 3 3 45.92 58.41 2.33 o 7 3 3 6.25 2.75 0.90 o -6 4 3 7.31 8.78 1.22 o -5 4 3 82.25 81.04 3.56 o -4 4 3 50.41 51.47 1.90 o -3 4 3 537.94 532.54 5.14 o -2 4 3 0.44 -0.26 0.27 o -1 4 3 2029.13 2070.73 12.49 o 0 4 3 5.40 3.91 0.41 o 1 4 3 381.91 414.41 3.07 o 2 4 3 464.78 493.28 3.61 o 3 4 3 24.93 23.83 0.83 o 4 4 3 92.58 87.66 1.63 o 5 4 3 202.85 196.23 3.00 o 6 4 3 34.06 34.63 1.83 o -6 5 3 15.32 9.88 1.63 o -5 5 3 13.11 9.45 1.18 o -4 5 3 312.82 309.15 6.83 o -3 5 3 72.89 63.89 3.25 o -2 5 3 56.60 61.73 1.65 o -1 5 3 8.52 9.81 0.56 o 0 5 3 699.54 669.98 4.53 o 1 5 3 0.41 -0.03 0.76 o 2 5 3 15.28 15.98 0.72 o 3 5 3 113.85 131.33 2.34 o 4 5 3 24.63 24.41 1.55 o 5 5 3 48.28 47.78 2.12 o 6 5 3 0.22 -0.37 0.85 o -5 6 3 22.40 19.08 1.60 o -4 6 3 9.76 8.53 1.14 o -3 6 3 3.89 4.83 0.99 o -2 6 3 45.47 41.11 1.48 o -1 6 3 64.45 68.18 2.94 o 0 6 3 31.22 34.01 1.34 o 1 6 3 126.40 130.09 2.05 o 2 6 3 49.81 50.48 1.35 o 3 6 3 95.82 84.13 2.17 o 4 6 3 37.09 33.89 2.94 o 5 6 3 10.93 13.81 1.98 o -4 7 3 1.90 4.13 1.08 o -3 7 3 23.59 23.43 1.67 o -2 7 3 4.61 4.41 0.91 o -1 7 3 50.76 52.08 1.86 o 0 7 3 12.61 13.14 1.01 o 1 7 3 0.46 2.63 0.91 o 2 7 3 2.04 0.43 0.87 o 3 7 3 113.03 105.07 2.53 o 4 7 3 51.24 48.35 2.32 o -2 8 3 10.54 8.14 1.38 o -1 8 3 16.62 20.78 2.16 o 0 8 3 4.97 4.10 1.49 o 1 8 3 4.03 4.97 1.14 o -6 0 4 451.59 434.89 6.20 o -4 0 4 785.20 726.97 7.68 o -2 0 4 0.92 1.83 0.40 o 0 0 4 5307.94 5439.95 46.39 o 2 0 4 3564.92 3956.27 48.19 o 4 0 4 653.01 630.81 10.17 o 6 0 4 28.09 25.11 2.33 o -7 1 4 172.68 176.63 2.84 o -6 1 4 0.33 -0.78 1.08 o -5 1 4 539.90 512.16 5.22 o -4 1 4 70.00 72.28 2.31 o -3 1 4 690.69 625.29 5.19 o -2 1 4 211.97 207.62 1.81 o -1 1 4 1094.77 908.76 6.47 o 0 1 4 113.13 140.42 1.19 o 1 1 4 261.18 341.88 2.17 o 2 1 4 185.26 199.75 2.25 o 3 1 4 311.60 310.53 4.07 o 4 1 4 374.28 407.25 4.33 o 5 1 4 0.01 0.77 1.34 o 6 1 4 210.20 205.80 4.14 o 7 1 4 13.06 17.55 1.60 o -7 2 4 2.78 2.23 0.97 o -6 2 4 4.48 8.30 1.09 o -5 2 4 0.01 0.43 0.57 o -4 2 4 225.85 205.64 2.67 o -3 2 4 176.51 175.87 2.15 o -2 2 4 160.82 182.18 2.67 o -1 2 4 18.56 16.98 0.51 o 0 2 4 0.09 4.99 0.43 o 1 2 4 450.05 497.88 3.09 o 2 2 4 1.47 0.07 0.22 o 3 2 4 14.54 15.51 0.96 o 4 2 4 694.76 731.75 8.17 o 5 2 4 58.94 51.80 1.63 o 6 2 4 3.45 4.20 1.01 o 7 2 4 1.40 1.05 1.02 o -7 3 4 5.89 5.62 1.19 o -6 3 4 14.28 13.21 1.68 o -5 3 4 0.26 0.00 0.72 o -4 3 4 0.78 2.08 0.58 o -3 3 4 270.85 337.94 3.40 o -2 3 4 1042.41 1052.52 9.99 o -1 3 4 243.16 304.45 2.23 o 0 3 4 204.42 223.18 1.83 o 1 3 4 650.50 636.01 4.00 o 2 3 4 0.52 1.53 0.42 o 3 3 4 510.28 519.32 4.88 o 4 3 4 372.23 376.76 4.14 o 5 3 4 409.18 410.17 4.97 o 6 3 4 6.94 8.63 1.17 o 7 3 4 44.11 38.86 1.76 o -6 4 4 0.07 0.20 1.14 o -5 4 4 0.93 -0.16 0.82 o -4 4 4 321.10 313.26 4.81 o -3 4 4 77.50 75.07 1.65 o -2 4 4 2.39 4.79 0.52 o -1 4 4 103.41 98.69 1.24 o 0 4 4 1863.66 1907.96 10.36 o 1 4 4 339.27 319.02 2.59 o 2 4 4 747.27 766.21 5.01 o 3 4 4 14.52 13.88 0.86 o 4 4 4 275.81 288.23 3.90 o 5 4 4 10.02 10.00 1.85 o 6 4 4 16.18 16.98 2.29 o -6 5 4 6.28 4.27 1.06 o -5 5 4 45.68 52.72 2.21 o -4 5 4 12.83 10.75 1.50 o -3 5 4 244.58 244.55 3.31 o -2 5 4 190.11 190.08 2.38 o -1 5 4 172.96 185.10 2.26 o 0 5 4 107.49 111.75 1.93 o 1 5 4 569.53 567.87 4.10 o 2 5 4 99.22 94.87 1.47 o 3 5 4 31.74 35.19 1.17 o 4 5 4 17.42 16.97 1.10 o 5 5 4 51.31 67.78 2.43 o 6 5 4 10.58 14.74 2.26 o -5 6 4 1.47 1.21 0.94 o -4 6 4 67.46 72.62 2.54 o -3 6 4 28.59 28.73 1.63 o -2 6 4 73.08 73.72 1.95 o -1 6 4 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