#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:47:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181096 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/76/2217688.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217688_Fobs loop_ _publ_author_name 'Liu, Changying' 'Shi, Xiufang' 'Du, Bin' 'Wu, Chunli' 'Zhang, Mingjie' _publ_section_title ; Hexaaquamanganese(II) dipicrate dihydrate ; _journal_coeditor_code WW2104 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m270 _journal_page_last m271 _journal_volume 64 _journal_year 2008 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 25.3443 _cell_length_b 7.1625 _cell_length_c 13.2166 _exptl_crystal_F_000 1340.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file ww2104Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 60525B in Pccn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 528.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' '-x, y+1/2, -z+1/2' 'x+1/2, -y, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' 'x, -y-1/2, z-1/2' '-x-1/2, y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 24.48 324.90 9.51 o 6 0 0 97547.80 100963.23 2275.91 o 8 0 0 954.72 693.77 17.43 o 10 0 0 2512.43 3350.66 52.34 o 12 0 0 20986.03 21441.19 222.24 o 14 0 0 12193.48 17186.48 182.43 o 16 0 0 6155.02 5951.64 96.38 o 18 0 0 12180.46 12756.24 280.53 o 20 0 0 9458.71 9318.74 145.13 o 22 0 0 499.45 393.56 28.43 o 24 0 0 132.21 54.79 23.77 o 26 0 0 12081.33 12523.47 196.68 o 28 0 0 456.32 556.89 37.43 o 30 0 0 134.06 85.58 41.21 o 1 1 0 140.51 143.54 7.84 o 3 1 0 629.80 661.77 23.74 o 5 1 0 238.09 241.31 6.33 o 7 1 0 2886.98 3191.90 30.67 o 9 1 0 2881.55 3235.49 31.88 o 11 1 0 1630.46 1745.55 24.95 o 13 1 0 620.77 656.76 15.32 o 15 1 0 99.99 101.93 11.21 o 17 1 0 107.51 100.10 13.09 o 19 1 0 1013.15 1064.58 25.93 o 21 1 0 934.95 918.00 25.34 o 23 1 0 286.13 319.72 20.00 o 25 1 0 3.25 -19.84 13.23 o 27 1 0 67.69 61.38 16.61 o 29 1 0 106.52 108.88 21.92 o 0 2 0 279086.19 158489.30 2687.98 o 2 2 0 3766.06 5695.53 89.55 o 4 2 0 350.43 817.73 18.50 o 6 2 0 23196.79 22172.61 177.46 o 8 2 0 57461.18 58842.92 1148.04 o 10 2 0 1675.94 1437.67 20.26 o 12 2 0 23044.42 23847.68 368.82 o 14 2 0 95.40 282.63 9.88 o 16 2 0 676.65 664.79 19.47 o 18 2 0 8875.34 8908.38 111.93 o 20 2 0 3889.10 3757.34 61.90 o 22 2 0 16.60 3.92 13.66 o 24 2 0 214.92 245.08 22.21 o 26 2 0 5440.99 5426.00 76.46 o 28 2 0 365.32 439.68 34.96 o 1 3 0 539.28 582.89 22.95 o 3 3 0 630.19 667.84 25.20 o 5 3 0 30.35 39.46 10.60 o 7 3 0 18.04 8.32 6.34 o 9 3 0 32.20 33.05 6.45 o 11 3 0 922.96 1071.69 19.73 o 13 3 0 235.52 258.17 13.96 o 15 3 0 231.05 221.91 16.23 o 17 3 0 443.99 466.47 17.62 o 19 3 0 206.27 225.95 19.17 o 21 3 0 83.60 95.72 15.50 o 23 3 0 96.27 94.86 23.10 o 25 3 0 433.46 455.07 41.04 o 27 3 0 4.76 -36.11 24.08 o 2 4 0 6300.30 5759.75 139.47 o 4 4 0 6427.08 6438.71 128.38 o 6 4 0 1185.65 1034.65 35.29 o 8 4 0 8534.92 8474.02 137.38 o 10 4 0 1352.51 1304.50 42.99 o 12 4 0 631.55 648.35 17.70 o 14 4 0 696.22 781.69 22.29 o 16 4 0 2017.42 1948.63 36.24 o 18 4 0 2114.96 2155.51 39.57 o 20 4 0 791.04 757.63 28.91 o 22 4 0 1913.72 1915.01 45.73 o 24 4 0 304.31 309.05 44.38 o 26 4 0 1673.48 1610.25 80.83 o 1 5 0 40.05 50.72 16.81 o 3 5 0 88.83 98.57 19.59 o 5 5 0 1117.36 1276.51 43.66 o 7 5 0 1917.10 2090.70 66.17 o 9 5 0 190.37 182.99 20.72 o 11 5 0 0.94 -15.94 11.60 o 13 5 0 1.73 -5.72 12.18 o 15 5 0 110.13 107.55 22.33 o 17 5 0 25.19 16.81 14.58 o 19 5 0 0.29 -21.66 14.44 o 21 5 0 170.54 170.62 38.04 o 23 5 0 0.01 -20.60 26.94 o 0 6 0 7771.91 8136.84 202.87 o 2 6 0 419.76 486.36 34.52 o 4 6 0 2292.87 2414.51 66.67 o 6 6 0 380.13 326.88 70.53 o 8 6 0 277.16 304.20 25.00 o 10 6 0 4395.74 4680.44 80.19 o 12 6 0 499.19 526.84 27.75 o 14 6 0 4.68 -2.24 18.66 o 16 6 0 5271.65 5160.59 108.69 o 18 6 0 513.84 531.78 38.05 o 20 6 0 27.50 -11.09 28.53 o 1 7 0 11.77 29.99 21.66 o 3 7 0 260.69 280.47 33.05 o 5 7 0 45.37 0.00 32.49 o 7 7 0 0.41 -23.25 15.50 o 9 7 0 28.30 22.98 17.23 o 11 7 0 65.08 47.68 19.42 o 13 7 0 121.70 142.24 30.68 o 15 7 0 0.83 -15.73 22.79 o 17 7 0 210.07 192.58 55.47 o 0 8 0 328.79 370.86 57.06 o 2 8 0 654.42 657.67 43.14 o 4 8 0 583.53 637.33 44.00 o 6 8 0 181.70 178.95 25.78 o 8 8 0 841.48 914.55 39.62 o 10 8 0 596.89 700.54 38.75 o 1 1 1 3310.52 2322.26 30.35 o 2 1 1 23.07 23.41 2.57 o 3 1 1 17395.07 16404.35 118.38 o 4 1 1 10.32 6.85 2.26 o 5 1 1 11077.92 10557.37 68.27 o 6 1 1 487.76 459.12 6.12 o 7 1 1 3752.46 3364.78 30.32 o 8 1 1 2982.28 3486.71 23.63 o 9 1 1 2933.10 4427.98 31.01 o 10 1 1 18.67 22.45 3.39 o 11 1 1 485.89 1195.31 18.53 o 12 1 1 1862.29 2318.25 23.24 o 13 1 1 10008.58 10006.90 64.67 o 14 1 1 309.87 419.91 9.21 o 15 1 1 2407.42 2165.04 22.31 o 16 1 1 55.39 29.67 6.17 o 17 1 1 76.80 39.53 7.41 o 18 1 1 512.73 518.17 13.98 o 19 1 1 1790.84 1583.55 23.75 o 20 1 1 497.47 541.79 15.02 o 21 1 1 709.84 783.52 17.93 o 22 1 1 1560.98 1633.18 24.93 o 23 1 1 3061.42 3073.71 35.56 o 24 1 1 38.83 58.15 10.04 o 25 1 1 313.33 399.70 18.92 o 26 1 1 83.84 55.13 12.11 o 27 1 1 581.58 597.53 19.86 o 28 1 1 0.00 10.75 13.33 o 29 1 1 175.01 200.73 21.18 o 1 2 1 8008.92 9045.41 115.86 o 2 2 1 1206.06 1208.42 27.68 o 3 2 1 20006.99 22260.32 235.01 o 4 2 1 5.56 12.96 4.29 o 5 2 1 2445.92 2698.27 29.58 o 6 2 1 2110.18 2267.82 18.90 o 7 2 1 794.33 919.96 10.60 o 8 2 1 1.96 -2.53 2.90 o 9 2 1 2602.33 2696.21 21.23 o 10 2 1 1037.56 1116.43 12.18 o 11 2 1 2124.51 2443.88 20.19 o 12 2 1 21.85 13.07 3.58 o 13 2 1 2384.06 2643.61 21.72 o 14 2 1 390.19 418.26 9.63 o 15 2 1 440.15 481.35 9.97 o 16 2 1 29.20 21.51 5.88 o 17 2 1 1587.97 1655.66 28.59 o 18 2 1 667.08 648.11 20.67 o 19 2 1 139.91 113.61 11.50 o 20 2 1 39.51 46.18 9.87 o 21 2 1 10.45 2.66 8.87 o 22 2 1 25.25 8.75 8.86 o 23 2 1 240.79 248.47 14.31 o 24 2 1 6.56 6.56 11.40 o 25 2 1 14.93 -6.30 10.98 o 26 2 1 9.47 -0.93 11.75 o 27 2 1 25.57 10.90 12.05 o 28 2 1 53.82 37.53 13.30 o 29 2 1 89.63 73.44 15.40 o 1 3 1 6.51 131.19 10.09 o 2 3 1 1151.05 1182.05 25.54 o 3 3 1 6580.84 6166.96 88.72 o 4 3 1 250.98 365.67 13.62 o 5 3 1 10614.71 10129.70 153.51 o 6 3 1 373.74 409.69 11.44 o 7 3 1 4032.60 3765.89 35.48 o 8 3 1 1008.88 1069.70 13.37 o 9 3 1 624.48 507.25 14.48 o 10 3 1 58.47 39.03 4.85 o 11 3 1 1088.56 786.26 11.78 o 12 3 1 998.61 1017.86 13.64 o 13 3 1 3720.56 3359.94 34.55 o 14 3 1 544.15 588.28 11.80 o 15 3 1 459.61 435.49 11.62 o 16 3 1 564.08 566.79 13.22 o 17 3 1 85.52 91.40 8.25 o 18 3 1 69.15 54.20 8.43 o 19 3 1 74.21 59.06 9.88 o 20 3 1 47.52 38.25 9.78 o 21 3 1 135.68 132.75 12.26 o 22 3 1 553.99 539.61 19.38 o 23 3 1 3251.00 3211.62 50.02 o 24 3 1 9.33 24.00 13.95 o 25 3 1 595.68 632.95 25.51 o 26 3 1 21.52 1.84 13.45 o 27 3 1 333.17 339.77 21.75 o 28 3 1 0.68 3.87 16.50 o 1 4 1 3.92 0.73 8.50 o 2 4 1 1013.69 1133.76 43.69 o 3 4 1 324.64 341.30 16.23 o 4 4 1 238.31 276.71 18.76 o 5 4 1 1565.22 1624.35 27.61 o 6 4 1 493.98 500.91 17.60 o 7 4 1 146.35 144.81 11.04 o 8 4 1 9.48 5.16 6.73 o 9 4 1 254.12 262.30 14.00 o 10 4 1 248.79 297.15 11.66 o 11 4 1 444.04 456.04 13.02 o 12 4 1 27.71 29.29 6.81 o 13 4 1 0.71 5.30 5.82 o 14 4 1 358.71 353.96 11.43 o 15 4 1 1689.50 1769.77 25.67 o 16 4 1 14.94 2.27 7.50 o 17 4 1 97.75 91.13 9.48 o 18 4 1 2.67 -8.74 7.70 o 19 4 1 106.65 100.83 13.02 o 20 4 1 3.78 -2.54 10.39 o 21 4 1 290.66 301.15 17.65 o 22 4 1 245.85 262.30 20.20 o 23 4 1 16.57 -4.62 13.37 o 24 4 1 73.83 63.71 16.61 o 25 4 1 487.54 436.51 25.29 o 26 4 1 256.64 266.03 32.07 o 1 5 1 1186.68 1073.11 28.51 o 2 5 1 225.88 238.71 17.41 o 3 5 1 4832.86 4950.42 98.81 o 4 5 1 203.37 245.66 17.23 o 5 5 1 3179.28 3001.28 49.10 o 6 5 1 6.81 18.24 9.59 o 7 5 1 4.24 2.53 9.36 o 8 5 1 2.83 -1.01 9.03 o 9 5 1 7.98 -0.10 8.62 o 10 5 1 4.95 3.92 8.32 o 11 5 1 173.28 178.82 12.86 o 12 5 1 44.52 58.70 10.01 o 13 5 1 771.37 744.75 22.15 o 14 5 1 34.31 25.44 10.93 o 15 5 1 442.87 463.81 18.56 o 16 5 1 171.20 189.28 14.97 o 17 5 1 2271.58 2274.23 39.19 o 18 5 1 14.50 1.23 10.37 o 19 5 1 207.84 182.86 15.14 o 20 5 1 77.32 31.96 14.90 o 21 5 1 177.53 146.18 20.89 o 22 5 1 274.55 281.87 25.53 o 23 5 1 1741.92 1783.79 47.86 o 24 5 1 67.86 39.14 19.72 o 1 6 1 84.83 94.02 15.58 o 2 6 1 9.37 3.85 12.00 o 3 6 1 341.20 436.31 24.16 o 4 6 1 0.95 -5.62 11.69 o 5 6 1 1.30 -3.43 11.43 o 6 6 1 34.86 24.59 11.73 o 7 6 1 312.96 372.57 23.13 o 8 6 1 3.92 3.06 10.27 o 9 6 1 2.13 -11.55 9.87 o 10 6 1 5.31 10.44 10.92 o 11 6 1 0.30 -2.11 11.46 o 12 6 1 44.87 29.87 12.69 o 13 6 1 362.05 384.82 23.91 o 14 6 1 19.74 11.97 14.00 o 15 6 1 77.95 55.12 15.47 o 16 6 1 17.31 -1.37 14.58 o 17 6 1 428.64 431.35 25.85 o 18 6 1 78.69 63.87 22.42 o 19 6 1 197.68 168.30 20.94 o 20 6 1 16.09 5.15 18.85 o 21 6 1 45.31 53.09 24.66 o 1 7 1 111.35 117.62 17.77 o 2 7 1 9.74 -9.65 14.05 o 3 7 1 470.69 505.55 27.46 o 4 7 1 43.62 55.58 16.50 o 5 7 1 1579.98 1723.65 38.07 o 6 7 1 13.52 1.14 13.40 o 7 7 1 32.57 15.95 14.07 o 8 7 1 31.19 33.57 13.25 o 9 7 1 447.82 487.05 21.88 o 10 7 1 67.19 46.33 13.46 o 11 7 1 718.39 777.69 31.82 o 12 7 1 1.01 -22.82 15.21 o 13 7 1 325.27 334.22 34.09 o 14 7 1 80.14 56.86 18.37 o 15 7 1 18.12 8.63 17.29 o 16 7 1 99.82 109.29 25.16 o 17 7 1 1055.70 1113.74 37.32 o 1 8 1 2.97 -4.03 17.96 o 2 8 1 0.12 -1.74 18.34 o 3 8 1 92.61 81.68 21.12 o 4 8 1 1.49 -12.00 15.75 o 5 8 1 21.94 13.76 21.29 o 6 8 1 18.04 16.81 16.52 o 7 8 1 247.62 242.63 20.59 o 8 8 1 1.73 -6.92 14.68 o 9 8 1 11.66 9.68 14.98 o 10 8 1 2.59 -0.64 17.01 o 0 0 2 29866.75 25840.09 448.52 o 1 0 2 925.91 915.36 17.93 o 2 0 2 6554.19 5120.51 80.04 o 3 0 2 2186.63 2224.12 24.55 o 4 0 2 14096.82 12664.09 119.41 o 5 0 2 414.92 465.19 9.48 o 6 0 2 85.97 283.92 8.46 o 7 0 2 366.34 448.56 9.33 o 8 0 2 2058.33 1651.40 18.78 o 9 0 2 6534.39 7400.81 83.30 o 10 0 2 3773.09 5619.33 50.90 o 11 0 2 1042.93 1225.22 17.25 o 12 0 2 6282.36 6035.28 55.14 o 13 0 2 2937.51 3418.38 35.06 o 14 0 2 4315.31 3586.37 43.70 o 15 0 2 4512.14 4769.93 54.99 o 16 0 2 14.23 49.48 8.15 o 17 0 2 1278.03 1297.43 26.67 o 18 0 2 1031.28 1011.13 30.41 o 19 0 2 889.88 813.17 22.08 o 20 0 2 4005.33 3881.95 54.34 o 21 0 2 86.29 139.60 14.13 o 22 0 2 1801.44 1811.45 36.34 o 23 0 2 758.15 770.65 24.34 o 24 0 2 2.82 14.26 29.89 o 25 0 2 34.97 15.76 16.42 o 26 0 2 93.65 101.33 29.16 o 27 0 2 1.12 -13.20 17.98 o 28 0 2 776.32 728.63 34.36 o 29 0 2 430.93 473.22 39.38 o 0 1 2 4413.63 5004.07 56.41 o 1 1 2 4875.20 5409.90 49.04 o 2 1 2 3070.16 3319.64 27.68 o 3 1 2 4.87 5.83 2.69 o 4 1 2 157.41 169.93 5.33 o 5 1 2 1155.06 1221.16 13.12 o 6 1 2 2784.48 3006.82 22.90 o 7 1 2 976.59 1067.55 11.53 o 8 1 2 310.95 331.29 5.60 o 9 1 2 2894.76 3151.19 31.59 o 10 1 2 474.60 443.15 8.08 o 11 1 2 2.97 0.70 3.27 o 12 1 2 50.27 66.69 4.48 o 13 1 2 942.55 1086.19 14.88 o 14 1 2 1065.72 1133.54 13.14 o 15 1 2 18.45 20.31 4.46 o 16 1 2 1265.46 1265.98 17.59 o 17 1 2 562.37 586.65 12.74 o 18 1 2 214.61 210.62 12.21 o 19 1 2 480.94 457.00 13.63 o 20 1 2 4.72 2.54 8.07 o 21 1 2 40.74 41.76 9.22 o 22 1 2 32.28 34.67 9.28 o 23 1 2 287.61 299.14 22.44 o 24 1 2 77.53 62.98 11.55 o 25 1 2 183.02 180.04 14.18 o 26 1 2 404.84 370.36 25.16 o 27 1 2 132.83 110.50 14.97 o 28 1 2 5.38 -11.39 14.77 o 29 1 2 111.89 108.29 16.77 o 0 2 2 11900.94 11918.70 156.88 o 1 2 2 22251.62 25249.31 204.19 o 2 2 2 12691.73 16843.18 135.42 o 3 2 2 1204.32 1201.99 16.84 o 4 2 2 1933.80 1360.13 15.85 o 5 2 2 7897.81 8417.45 62.23 o 6 2 2 10148.14 9275.93 64.20 o 7 2 2 19183.24 21072.05 119.72 o 8 2 2 1108.55 711.48 9.50 o 9 2 2 768.15 870.89 10.52 o 10 2 2 6133.37 5591.92 37.57 o 11 2 2 778.62 891.44 10.92 o 12 2 2 15350.40 16035.94 94.24 o 13 2 2 1546.77 1776.00 22.02 o 14 2 2 678.97 487.27 9.94 o 15 2 2 259.17 281.52 12.94 o 16 2 2 1720.81 1652.47 20.70 o 17 2 2 467.85 439.38 12.54 o 18 2 2 95.91 81.37 9.44 o 19 2 2 986.53 918.10 19.77 o 20 2 2 1521.60 1418.12 23.21 o 21 2 2 4.52 15.83 9.52 o 22 2 2 2308.49 2300.07 44.60 o 23 2 2 1984.07 1939.89 32.18 o 24 2 2 273.60 232.33 16.25 o 25 2 2 175.84 192.11 25.08 o 26 2 2 299.92 395.67 22.45 o 27 2 2 4.18 6.70 17.16 o 28 2 2 514.67 548.72 25.17 o 29 2 2 321.69 278.03 22.48 o 0 3 2 6533.76 7498.13 158.49 o 1 3 2 10512.88 11433.42 179.58 o 2 3 2 8246.69 8878.20 94.94 o 3 3 2 336.09 396.53 12.14 o 4 3 2 3365.63 3638.26 37.25 o 5 3 2 5038.95 5440.85 55.29 o 6 3 2 427.89 443.76 14.65 o 7 3 2 20.71 15.66 5.23 o 8 3 2 32.62 23.75 5.46 o 9 3 2 56.53 56.43 6.82 o 10 3 2 1805.74 1900.57 20.04 o 11 3 2 3124.08 3388.28 27.62 o 12 3 2 2352.90 2641.28 23.56 o 13 3 2 280.63 321.09 8.71 o 14 3 2 14.16 1.89 5.51 o 15 3 2 0.57 -7.68 5.49 o 16 3 2 56.29 40.59 7.42 o 17 3 2 1.50 -9.87 6.58 o 18 3 2 166.23 169.77 10.80 o 19 3 2 36.65 28.94 9.13 o 20 3 2 207.27 236.49 23.56 o 21 3 2 867.98 819.68 33.86 o 22 3 2 748.65 714.63 26.72 o 23 3 2 0.75 -3.45 12.53 o 24 3 2 190.68 208.97 17.50 o 25 3 2 273.88 218.89 18.40 o 26 3 2 62.36 59.41 14.96 o 27 3 2 125.09 92.61 17.21 o 0 4 2 18957.06 18880.92 259.13 o 1 4 2 3865.42 4086.74 83.10 o 2 4 2 20.06 14.12 8.66 o 3 4 2 291.95 391.78 16.20 o 4 4 2 2210.60 1979.43 30.68 o 5 4 2 0.24 -1.21 6.85 o 6 4 2 3724.53 3386.10 73.14 o 7 4 2 1607.39 1635.22 31.18 o 8 4 2 61.57 18.93 6.97 o 9 4 2 25.07 16.68 6.42 o 10 4 2 786.37 708.84 15.45 o 11 4 2 633.85 637.20 21.99 o 12 4 2 3230.87 3119.01 32.43 o 13 4 2 1554.08 1550.95 21.69 o 14 4 2 60.60 80.80 9.45 o 15 4 2 41.31 34.56 8.33 o 16 4 2 426.50 412.53 13.98 o 17 4 2 42.17 39.53 9.16 o 18 4 2 623.80 641.30 23.17 o 19 4 2 0.37 -5.14 10.03 o 20 4 2 769.17 732.72 29.28 o 21 4 2 8.99 -13.33 12.64 o 22 4 2 1117.49 1075.83 30.93 o 23 4 2 604.41 609.78 25.51 o 24 4 2 17.44 33.66 14.99 o 25 4 2 14.67 21.25 16.13 o 26 4 2 491.51 557.97 26.91 o 0 5 2 5755.74 6042.52 147.40 o 1 5 2 2288.08 2484.64 43.75 o 2 5 2 1563.22 1684.50 43.85 o 3 5 2 14.57 11.33 11.05 o 4 5 2 350.64 375.37 17.32 o 5 5 2 33.86 44.03 10.51 o 6 5 2 114.64 90.06 11.56 o 7 5 2 120.78 126.89 12.76 o 8 5 2 40.85 39.31 10.22 o 9 5 2 378.87 382.21 17.08 o 10 5 2 1040.75 1099.79 23.24 o 11 5 2 270.63 285.51 14.74 o 12 5 2 311.03 332.19 16.77 o 13 5 2 51.45 45.82 10.39 o 14 5 2 402.83 410.87 18.27 o 15 5 2 225.10 270.05 18.64 o 16 5 2 9.77 -14.53 10.84 o 17 5 2 0.13 5.34 11.25 o 18 5 2 3.18 -13.73 10.72 o 19 5 2 133.01 121.74 15.10 o 20 5 2 62.15 49.59 15.29 o 21 5 2 11.68 -7.09 14.35 o 22 5 2 98.97 97.96 17.92 o 23 5 2 13.29 3.41 15.90 o 24 5 2 116.75 79.93 19.22 o 0 6 2 1799.22 1763.07 55.47 o 1 6 2 115.09 101.43 15.58 o 2 6 2 200.69 209.99 18.81 o 3 6 2 0.51 -1.64 12.26 o 4 6 2 269.48 271.93 17.69 o 5 6 2 68.92 39.38 12.14 o 6 6 2 300.36 286.74 24.10 o 7 6 2 108.07 104.90 13.66 o 8 6 2 934.87 937.44 25.73 o 9 6 2 514.36 508.44 20.82 o 10 6 2 192.82 241.41 16.27 o 11 6 2 149.32 129.59 13.55 o 12 6 2 2055.29 2006.86 38.27 o 13 6 2 472.56 456.15 24.19 o 14 6 2 492.98 501.84 33.17 o 15 6 2 200.99 230.96 21.42 o 16 6 2 145.28 134.90 18.80 o 17 6 2 636.08 645.64 27.33 o 18 6 2 1498.63 1511.53 39.35 o 19 6 2 0.29 -9.57 16.04 o 20 6 2 269.63 310.97 28.54 o 21 6 2 23.82 19.60 19.51 o 0 7 2 166.99 108.88 25.20 o 1 7 2 86.39 76.92 17.16 o 2 7 2 1171.38 1186.92 47.35 o 3 7 2 637.46 639.54 27.25 o 4 7 2 50.78 42.59 13.97 o 5 7 2 0.02 8.21 12.98 o 6 7 2 3.53 10.07 12.89 o 7 7 2 150.56 159.11 17.12 o 8 7 2 59.48 61.32 15.17 o 9 7 2 38.71 31.83 13.12 o 10 7 2 11.36 11.61 12.70 o 11 7 2 0.45 7.12 14.69 o 12 7 2 105.52 82.70 21.11 o 13 7 2 123.81 130.23 20.10 o 14 7 2 121.99 117.92 20.11 o 15 7 2 156.72 163.38 22.53 o 16 7 2 44.88 -3.56 17.44 o 0 8 2 1249.76 1382.10 57.71 o 1 8 2 214.48 195.31 23.91 o 2 8 2 18.29 21.99 16.13 o 3 8 2 1.48 -17.47 15.53 o 4 8 2 186.25 236.55 25.56 o 5 8 2 0.28 -3.40 15.83 o 6 8 2 645.62 696.41 28.30 o 7 8 2 108.22 107.37 18.89 o 8 8 2 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116.35 119.13 5.99 o 3 1 7 5279.54 5251.47 38.89 o 4 1 7 775.41 885.93 14.24 o 5 1 7 116.47 19.30 5.35 o 6 1 7 95.02 210.08 8.86 o 7 1 7 8335.94 9044.95 66.96 o 8 1 7 1360.54 1600.29 20.31 o 9 1 7 11.45 9.64 5.73 o 10 1 7 66.95 70.08 7.31 o 11 1 7 115.53 73.25 7.37 o 12 1 7 124.39 131.68 10.93 o 13 1 7 3616.02 3523.86 34.58 o 14 1 7 770.38 771.65 17.00 o 15 1 7 686.63 686.67 16.18 o 16 1 7 1181.43 1240.65 24.42 o 17 1 7 3879.63 3773.06 45.83 o 18 1 7 1903.96 1862.87 34.48 o 19 1 7 7913.46 7865.97 111.82 o 20 1 7 490.88 540.13 23.94 o 21 1 7 1123.66 1123.90 41.86 o 22 1 7 174.63 173.45 21.50 o 23 1 7 79.71 129.29 18.23 o 24 1 7 246.58 260.41 25.62 o 25 1 7 439.43 543.84 29.26 o 26 1 7 18.46 16.23 17.99 o 1 2 7 72.40 46.89 5.13 o 2 2 7 97.73 72.66 6.49 o 3 2 7 277.79 282.33 8.60 o 4 2 7 2.27 4.93 5.49 o 5 2 7 1094.05 1120.59 17.51 o 6 2 7 1810.43 1925.87 22.76 o 7 2 7 1736.47 1867.36 22.52 o 8 2 7 144.69 168.34 8.94 o 9 2 7 12.24 8.10 6.19 o 10 2 7 95.92 90.63 7.75 o 11 2 7 304.65 301.28 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1427.68 1479.84 40.79 o 2 1 15 399.81 503.85 43.01 o 3 1 15 183.69 238.29 23.17 o 4 1 15 431.74 496.70 35.46 o 5 1 15 1184.12 1273.86 38.03 o 6 1 15 587.98 649.50 30.46 o 7 1 15 252.09 301.10 25.41 o 8 1 15 3.18 5.55 17.20 o 1 2 15 60.04 50.23 22.65 o 2 2 15 217.38 218.81 23.33 o 3 2 15 310.92 343.38 27.75 o 4 2 15 115.75 101.13 19.84 o 5 2 15 2.51 -26.15 17.43 o