#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/76/2217690.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217690_Fobs loop_ _publ_author_name 'Sun, Shi-Zhu' 'Kang, Wen-Jun' 'Li, Da-Cheng' 'Wang, Da-Qi' 'Dou, Jian-Min' _publ_section_title ; [3-Hydroxy-N'-(2-oxidobenzylidene)-2-naphthohydrazidato-\k^3^O,N,O']tris(pyridine-\kN)nickel(II) pyridine trisolvate ; _journal_coeditor_code XU2364 _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m438 _journal_volume 64 _journal_year 2008 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.378 _cell_angle_gamma 90.000 _cell_length_a 18.3698 _cell_length_b 27.7200 _cell_length_c 16.8623 _exptl_crystal_F_000 3504.00 _reflns_d_resolution_high 0.8406 _[local]_cod_data_source_file xu2364Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 080118d in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 718.29 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 165770.89 187049.70 2252.27 o 3 0 0 57.84 56.96 46.39 o 4 0 0 515944.47 585435.38 5176.94 o 5 0 0 843.06 591.34 62.25 o 6 0 0 111275.59 114930.69 1070.02 o 7 0 0 24.19 -67.54 51.68 o 8 0 0 276.53 134.20 78.69 o 9 0 0 111.29 57.32 66.22 o 10 0 0 412.46 121.28 77.85 o 11 0 0 49.24 66.71 72.37 o 12 0 0 1901.71 1100.03 130.38 o 13 0 0 13.87 -68.71 140.36 o 14 0 0 8806.89 8098.76 364.71 o 15 0 0 1.15 52.26 173.23 o 16 0 0 2931.57 2778.77 270.15 o 17 0 0 0.28 -27.02 159.73 o 18 0 0 2752.98 2685.39 372.28 o 19 0 0 0.39 -206.73 210.25 o 20 0 0 517.63 559.64 242.53 o 21 0 0 0.08 -58.14 246.05 o 1 1 0 2.89 -18.66 12.44 o 2 1 0 23437.49 27174.12 486.96 o 3 1 0 597.05 415.21 117.80 o 4 1 0 1042.34 250.05 52.13 o 5 1 0 6.70 23.70 29.12 o 6 1 0 14600.89 11003.92 132.00 o 7 1 0 51.17 -10.64 33.79 o 8 1 0 35993.22 34519.22 308.81 o 9 1 0 72.24 70.11 46.48 o 10 1 0 4156.87 2781.31 83.98 o 11 1 0 58.13 18.48 48.02 o 12 1 0 5409.20 5452.38 120.42 o 13 1 0 5.96 -71.55 97.91 o 14 1 0 269.42 394.47 135.35 o 15 1 0 0.01 -10.12 106.81 o 16 1 0 0.31 -15.20 130.00 o 17 1 0 1.77 -143.57 102.07 o 18 1 0 361.13 522.44 177.67 o 19 1 0 1.15 -27.41 151.75 o 20 1 0 1818.18 1305.92 232.58 o 21 1 0 0.06 -188.16 142.12 o 0 2 0 149500.97 157895.33 2292.79 o 1 2 0 342.30 427.41 40.30 o 2 2 0 95957.98 109791.00 875.40 o 3 2 0 311.67 486.98 43.06 o 4 2 0 20057.62 23973.95 198.16 o 5 2 0 2.37 -9.04 25.45 o 6 2 0 2778.82 2499.74 71.37 o 7 2 0 118.69 59.08 36.11 o 8 2 0 3237.42 3029.36 78.03 o 9 2 0 11.42 -58.42 44.25 o 10 2 0 1649.37 1428.65 69.97 o 11 2 0 9.22 -66.37 44.86 o 12 2 0 163.34 216.80 58.97 o 13 2 0 1.49 -97.50 84.99 o 14 2 0 5991.16 5047.09 216.72 o 15 2 0 0.22 -92.52 101.22 o 16 2 0 3348.62 2810.70 190.56 o 17 2 0 1.64 -26.44 112.26 o 18 2 0 2558.17 2593.87 196.98 o 19 2 0 1.01 -92.12 155.93 o 20 2 0 857.19 904.75 232.54 o 21 2 0 3.62 -226.86 159.41 o 1 3 0 47.06 59.39 16.83 o 2 3 0 10824.55 10082.42 96.25 o 3 3 0 754.92 459.08 26.82 o 4 3 0 79175.02 109543.94 809.02 o 5 3 0 1253.09 1535.54 60.83 o 6 3 0 53504.95 39940.71 323.14 o 7 3 0 106.44 309.25 49.08 o 8 3 0 6883.89 7936.16 123.59 o 9 3 0 717.09 429.99 69.03 o 10 3 0 11908.87 13336.43 198.30 o 11 3 0 21.12 65.59 53.28 o 12 3 0 25.68 163.79 60.64 o 13 3 0 6.89 -36.27 100.28 o 14 3 0 205.55 402.38 124.30 o 15 3 0 2.79 -86.40 117.13 o 16 3 0 994.69 863.27 165.68 o 17 3 0 0.56 -72.21 119.61 o 18 3 0 519.07 680.06 169.81 o 19 3 0 0.36 -186.91 128.51 o 20 3 0 2140.82 3017.88 293.28 o 21 3 0 0.88 16.80 173.31 o 0 4 0 51572.27 55567.85 771.70 o 1 4 0 1228.51 1333.04 39.10 o 2 4 0 22345.74 21919.02 204.57 o 3 4 0 251.97 357.81 31.34 o 4 4 0 485.76 553.09 58.23 o 5 4 0 7.65 36.18 27.85 o 6 4 0 602.63 637.39 78.68 o 7 4 0 4.79 -47.41 31.61 o 8 4 0 41.80 -7.09 40.27 o 9 4 0 90.37 70.13 52.65 o 10 4 0 2878.26 2668.44 97.21 o 11 4 0 2.98 -72.57 48.38 o 12 4 0 1240.59 1370.33 98.15 o 13 4 0 3.77 -101.23 126.26 o 14 4 0 4020.43 3985.27 192.44 o 15 4 0 0.13 -151.20 109.36 o 16 4 0 3441.99 2680.58 190.35 o 17 4 0 8.27 -159.21 106.14 o 18 4 0 2172.76 2544.52 273.94 o 19 4 0 14.03 44.94 154.54 o 20 4 0 630.91 485.72 191.44 o 21 4 0 1.42 -75.64 150.83 o 1 5 0 4.34 22.94 23.16 o 2 5 0 6649.19 7723.52 107.78 o 3 5 0 33.01 37.65 25.09 o 4 5 0 1623.98 735.96 64.08 o 5 5 0 491.07 559.48 61.16 o 6 5 0 261.00 759.94 76.04 o 7 5 0 49.96 21.30 33.26 o 8 5 0 14602.98 12994.61 200.65 o 9 5 0 274.56 588.04 98.56 o 10 5 0 707.37 977.58 78.22 o 11 5 0 55.10 -52.35 47.31 o 12 5 0 581.84 808.21 78.27 o 13 5 0 41.28 -86.29 90.12 o 14 5 0 49.22 36.14 118.14 o 15 5 0 19.23 -42.43 121.48 o 16 5 0 60.69 89.50 139.43 o 17 5 0 6.05 -38.50 141.14 o 18 5 0 294.97 318.19 151.08 o 19 5 0 21.25 -74.76 182.05 o 20 5 0 527.23 547.28 237.25 o 21 5 0 14.97 -171.86 171.66 o 0 6 0 163164.98 148866.89 1923.38 o 1 6 0 701.44 581.64 47.76 o 2 6 0 15466.11 13576.84 162.34 o 3 6 0 817.64 662.97 46.86 o 4 6 0 19720.43 18742.65 181.76 o 5 6 0 0.47 -13.65 26.46 o 6 6 0 1313.71 1587.93 53.58 o 7 6 0 207.23 207.80 42.59 o 8 6 0 1946.62 2364.03 77.09 o 9 6 0 511.69 650.77 63.71 o 10 6 0 1108.78 1007.86 128.75 o 11 6 0 360.11 472.96 81.29 o 12 6 0 2247.53 2272.90 93.83 o 13 6 0 167.17 -76.65 104.39 o 14 6 0 967.37 1118.35 161.83 o 15 6 0 96.81 -35.82 126.67 o 16 6 0 1712.35 2232.44 232.38 o 17 6 0 60.37 9.27 144.19 o 18 6 0 621.95 470.87 157.48 o 19 6 0 9.97 16.12 163.87 o 20 6 0 88.81 15.54 171.59 o 21 6 0 0.64 -84.44 178.15 o 1 7 0 7.74 -2.46 38.65 o 2 7 0 854.89 779.29 47.64 o 3 7 0 2216.57 2433.77 92.54 o 4 7 0 4381.36 4328.42 81.29 o 5 7 0 778.62 760.68 44.20 o 6 7 0 42.20 99.69 37.89 o 7 7 0 385.29 580.76 54.79 o 8 7 0 2907.42 2409.30 74.01 o 9 7 0 1.88 -18.11 43.73 o 10 7 0 1943.90 1668.74 71.16 o 11 7 0 1.44 -28.58 49.80 o 12 7 0 838.20 1215.32 99.42 o 13 7 0 10.41 -146.78 97.85 o 14 7 0 114.08 -164.53 111.84 o 15 7 0 14.53 -37.54 170.89 o 16 7 0 3.67 20.06 146.23 o 17 7 0 23.66 -128.62 140.65 o 18 7 0 55.04 -38.93 134.08 o 19 7 0 4.79 -215.59 150.91 o 20 7 0 240.00 381.41 195.76 o 21 7 0 31.44 -226.54 151.03 o 0 8 0 3769.96 2348.35 129.20 o 1 8 0 125.99 127.91 42.93 o 2 8 0 18920.27 14860.59 189.20 o 3 8 0 2355.36 2336.06 74.15 o 4 8 0 4215.21 3594.23 78.96 o 5 8 0 304.66 242.50 43.38 o 6 8 0 13.75 4.92 35.71 o 7 8 0 10.91 -53.14 36.66 o 8 8 0 37.30 -32.37 42.23 o 9 8 0 295.12 329.11 58.65 o 10 8 0 217.16 157.36 55.83 o 11 8 0 64.05 2.89 54.10 o 12 8 0 355.78 280.79 71.96 o 13 8 0 4.31 -85.43 76.62 o 14 8 0 196.64 -20.45 157.39 o 15 8 0 26.78 -151.35 105.83 o 16 8 0 317.41 475.95 235.19 o 17 8 0 95.34 31.67 151.59 o 18 8 0 140.55 166.14 144.78 o 19 8 0 2.25 -32.41 152.81 o 20 8 0 65.55 -74.50 158.37 o 21 8 0 0.14 15.43 166.99 o 1 9 0 1037.82 782.56 67.62 o 2 9 0 1109.75 1072.19 59.22 o 3 9 0 546.83 689.06 64.81 o 4 9 0 513.90 654.83 61.04 o 5 9 0 558.80 910.83 62.38 o 6 9 0 90.15 -24.96 37.35 o 7 9 0 1134.06 790.20 66.38 o 8 9 0 401.46 730.03 68.99 o 9 9 0 195.00 196.03 58.19 o 10 9 0 1810.07 1585.49 77.52 o 11 9 0 377.71 487.23 70.45 o 12 9 0 413.10 196.61 69.39 o 13 9 0 33.40 -117.74 78.50 o 14 9 0 295.43 87.68 131.06 o 15 9 0 11.59 -176.46 117.64 o 16 9 0 0.10 -172.12 131.64 o 17 9 0 27.58 -77.52 145.05 o 18 9 0 405.52 295.58 158.41 o 19 9 0 2.71 -14.50 160.63 o 20 9 0 301.02 319.58 171.18 o 21 9 0 17.55 -167.80 166.48 o 0 10 0 24386.36 23021.27 470.42 o 1 10 0 1763.80 1654.72 68.00 o 2 10 0 2909.65 3738.35 166.08 o 3 10 0 2182.97 1997.21 78.09 o 4 10 0 2367.11 2928.92 91.38 o 5 10 0 2.93 -40.12 35.49 o 6 10 0 2256.41 2898.43 83.11 o 7 10 0 550.65 592.31 65.29 o 8 10 0 1779.06 1954.86 77.56 o 9 10 0 69.13 93.26 57.73 o 10 10 0 1120.57 1216.09 93.48 o 11 10 0 36.06 -32.86 58.06 o 12 10 0 6.31 -87.37 58.25 o 13 10 0 11.42 -87.24 86.46 o 14 10 0 97.77 14.11 109.03 o 15 10 0 145.88 -9.47 126.06 o 16 10 0 374.43 323.31 214.34 o 17 10 0 221.98 169.03 159.78 o 18 10 0 104.07 57.14 143.87 o 19 10 0 71.05 11.15 163.82 o 20 10 0 31.40 39.21 164.24 o 1 11 0 0.42 24.77 59.41 o 2 11 0 302.02 291.52 54.49 o 3 11 0 572.60 717.23 74.14 o 4 11 0 2214.60 2023.94 83.52 o 5 11 0 473.98 477.51 59.61 o 6 11 0 391.06 167.46 52.19 o 7 11 0 1308.87 1328.12 65.90 o 8 11 0 9.98 -27.05 51.97 o 9 11 0 2964.08 2978.89 99.03 o 10 11 0 353.37 372.26 75.37 o 11 11 0 1428.46 1664.27 127.60 o 12 11 0 1.29 -141.05 94.04 o 13 11 0 168.37 -49.55 84.16 o 14 11 0 178.71 -21.69 211.12 o 15 11 0 41.34 13.28 139.53 o 16 11 0 65.49 43.81 134.19 o 17 11 0 38.98 122.63 150.24 o 18 11 0 64.28 -89.84 170.31 o 19 11 0 42.84 -112.83 162.38 o 20 11 0 41.01 58.04 165.88 o 0 12 0 13.97 -61.08 92.20 o 1 12 0 15713.39 16021.84 351.49 o 2 12 0 367.32 512.94 75.37 o 3 12 0 6889.87 7419.04 222.64 o 4 12 0 5869.65 5428.21 133.86 o 5 12 0 777.63 720.46 80.89 o 6 12 0 24.90 -9.40 47.71 o 7 12 0 18.21 -40.49 52.35 o 8 12 0 1253.37 1668.47 82.49 o 9 12 0 141.61 225.43 70.04 o 10 12 0 1144.78 1292.41 103.57 o 11 12 0 312.38 398.69 85.88 o 12 12 0 10.45 -107.86 87.46 o 13 12 0 123.59 132.42 94.60 o 14 12 0 43.77 -121.92 107.27 o 15 12 0 73.33 216.72 150.71 o 16 12 0 172.41 38.57 152.93 o 17 12 0 309.02 329.65 152.74 o 18 12 0 231.55 84.81 197.32 o 19 12 0 82.18 -219.70 146.47 o 20 12 0 62.93 -64.73 236.67 o 1 13 0 8.31 72.78 85.33 o 2 13 0 1472.00 1659.64 86.32 o 3 13 0 3344.35 2956.96 157.85 o 4 13 0 1017.19 1248.59 161.01 o 5 13 0 3864.29 4191.55 125.43 o 6 13 0 45.49 49.16 55.61 o 7 13 0 3494.40 3185.60 102.88 o 8 13 0 41.03 41.35 64.09 o 9 13 0 5079.72 4619.97 126.47 o 10 13 0 157.25 372.30 83.57 o 11 13 0 2380.83 2326.23 148.42 o 12 13 0 184.53 119.92 99.42 o 13 13 0 264.85 203.36 104.51 o 14 13 0 56.17 -117.74 131.61 o 15 13 0 77.40 90.50 144.25 o 16 13 0 308.57 484.52 181.87 o 17 13 0 40.71 96.53 164.02 o 18 13 0 0.05 -54.60 164.47 o 19 13 0 79.15 -59.08 177.41 o 20 13 0 5.95 -152.22 158.61 o 0 14 0 1277.32 1919.68 173.25 o 1 14 0 2417.50 2026.25 124.58 o 2 14 0 58.73 322.37 74.31 o 3 14 0 855.22 900.91 163.21 o 4 14 0 1828.57 1843.59 94.95 o 5 14 0 371.25 554.58 86.39 o 6 14 0 2350.91 2460.38 93.40 o 7 14 0 983.34 1007.13 93.52 o 8 14 0 2767.02 2523.62 100.48 o 9 14 0 77.61 114.53 72.43 o 10 14 0 1691.53 1817.68 141.64 o 11 14 0 92.79 174.98 80.80 o 12 14 0 388.57 475.86 113.66 o 13 14 0 4.98 -42.15 89.14 o 14 14 0 520.53 523.48 167.29 o 15 14 0 298.35 404.06 168.42 o 16 14 0 17.87 92.59 156.64 o 17 14 0 268.48 159.79 169.97 o 18 14 0 534.43 406.47 196.65 o 19 14 0 44.50 -90.59 171.00 o 1 15 0 667.70 847.34 123.75 o 2 15 0 2216.86 2025.40 126.04 o 3 15 0 2080.09 2013.32 101.02 o 4 15 0 447.00 535.61 85.80 o 5 15 0 1580.51 1426.89 117.91 o 6 15 0 2105.71 1833.87 86.41 o 7 15 0 3050.10 2866.82 105.68 o 8 15 0 792.44 764.42 93.07 o 9 15 0 1211.00 1461.77 114.77 o 10 15 0 1378.40 1911.25 125.10 o 11 15 0 798.41 755.79 105.86 o 12 15 0 2235.87 2195.96 143.09 o 13 15 0 2.84 6.31 105.84 o 14 15 0 174.82 -31.78 141.89 o 15 15 0 6.97 -56.42 141.38 o 16 15 0 16.47 133.37 152.76 o 17 15 0 75.22 58.30 168.21 o 18 15 0 2.82 74.89 165.03 o 19 15 0 155.07 64.55 175.83 o 0 16 0 6405.46 5723.75 264.28 o 1 16 0 5227.07 5535.63 190.61 o 2 16 0 6701.39 6712.64 208.85 o 3 16 0 2800.99 2098.37 102.61 o 4 16 0 3007.67 2864.67 116.82 o 5 16 0 193.72 237.08 79.76 o 6 16 0 185.04 175.93 70.37 o 7 16 0 99.29 13.73 64.35 o 8 16 0 311.01 218.08 80.30 o 9 16 0 798.50 974.95 104.62 o 10 16 0 928.96 984.87 111.61 o 11 16 0 1857.72 1937.94 175.62 o 12 16 0 361.38 540.29 116.41 o 13 16 0 1173.62 1317.80 238.49 o 14 16 0 727.23 950.39 470.68 o 15 16 0 1101.84 1347.65 499.73 o 16 16 0 428.77 607.60 367.89 o 17 16 0 316.82 257.02 178.00 o 18 16 0 554.47 752.74 270.71 o 19 16 0 45.65 -40.21 262.51 o 1 17 0 103.08 175.11 98.79 o 2 17 0 1443.92 1407.54 150.47 o 3 17 0 187.86 142.81 102.95 o 4 17 0 617.23 915.16 105.30 o 5 17 0 1218.11 1589.97 128.97 o 6 17 0 1987.06 1612.91 103.07 o 7 17 0 615.26 515.41 85.52 o 8 17 0 1035.19 1184.51 108.66 o 9 17 0 685.51 817.13 104.43 o 10 17 0 1498.67 1907.52 124.55 o 11 17 0 669.99 823.50 110.06 o 12 17 0 1097.83 905.63 142.36 o 13 17 0 40.00 27.88 108.09 o 14 17 0 119.36 26.12 134.12 o 15 17 0 166.94 264.74 166.89 o 16 17 0 0.41 149.97 168.50 o 17 17 0 25.56 150.48 172.05 o 18 17 0 6.48 -69.72 165.22 o 0 18 0 3085.41 2883.90 217.30 o 1 18 0 33.87 19.13 86.77 o 2 18 0 4678.01 4335.96 182.09 o 3 18 0 14.48 9.81 86.70 o 4 18 0 299.30 198.98 85.45 o 5 18 0 3.04 -105.29 70.20 o 6 18 0 1.35 -106.18 70.78 o 7 18 0 77.37 -3.22 71.91 o 8 18 0 446.89 325.97 93.59 o 9 18 0 584.51 877.39 108.69 o 10 18 0 980.00 1475.78 128.30 o 11 18 0 906.20 1049.97 121.63 o 12 18 0 402.56 572.39 170.48 o 13 18 0 1376.11 1703.64 176.15 o 14 18 0 776.43 865.24 357.34 o 15 18 0 601.66 492.41 188.70 o 16 18 0 443.65 515.51 192.38 o 17 18 0 455.36 431.73 392.29 o 18 18 0 326.50 556.93 203.34 o 1 19 0 35.41 -14.33 95.23 o 2 19 0 67.49 137.03 100.97 o 3 19 0 314.58 281.85 112.95 o 4 19 0 84.38 45.50 78.33 o 5 19 0 416.13 444.24 101.44 o 6 19 0 593.10 580.38 112.81 o 7 19 0 392.28 424.62 90.10 o 8 19 0 1113.03 1594.62 130.95 o 9 19 0 757.91 833.69 110.57 o 10 19 0 1096.60 1383.51 131.69 o 11 19 0 13.00 -112.10 74.73 o 12 19 0 359.10 320.60 124.01 o 13 19 0 1.46 -48.32 110.86 o 14 19 0 73.29 99.85 156.33 o 15 19 0 2.64 -99.53 170.31 o 16 19 0 0.26 68.74 163.49 o 17 19 0 41.65 199.62 179.28 o 0 20 0 1978.40 2458.76 223.17 o 1 20 0 1.85 -43.45 100.07 o 2 20 0 1834.02 1766.08 179.99 o 3 20 0 2.35 -63.57 94.46 o 4 20 0 519.49 655.66 110.05 o 5 20 0 0.42 -58.67 81.50 o 6 20 0 97.31 99.20 95.23 o 7 20 0 93.82 -23.79 77.97 o 8 20 0 28.98 -34.75 75.91 o 9 20 0 1.61 -53.66 78.98 o 10 20 0 357.55 269.87 97.61 o 11 20 0 76.40 -39.02 88.83 o 12 20 0 299.25 278.34 119.90 o 13 20 0 2.45 -157.62 105.08 o 14 20 0 229.75 338.59 173.95 o 15 20 0 67.95 -49.93 153.01 o 16 20 0 53.52 69.12 163.67 o 17 20 0 33.45 -36.52 169.40 o 1 21 0 149.73 -50.16 103.15 o 2 21 0 211.45 46.61 109.98 o 3 21 0 116.79 172.44 121.26 o 4 21 0 84.24 1.27 104.48 o 5 21 0 44.75 -145.64 97.10 o 6 21 0 813.09 1200.30 142.40 o 7 21 0 145.64 34.48 81.40 o 8 21 0 1485.18 1952.26 142.89 o 9 21 0 24.60 -115.94 77.29 o 10 21 0 684.67 983.22 122.45 o 11 21 0 62.20 -23.09 95.55 o 12 21 0 115.18 124.13 119.89 o 13 21 0 139.66 -5.50 118.82 o 14 21 0 14.25 62.35 149.29 o 15 21 0 150.25 133.79 171.20 o 16 21 0 25.49 -159.65 156.98 o 0 22 0 9.41 -64.60 119.22 o 1 22 0 135.28 22.53 114.22 o 2 22 0 28.15 -19.65 145.06 o 3 22 0 132.53 156.48 123.69 o 4 22 0 7.17 -93.26 109.19 o 5 22 0 481.34 496.90 122.61 o 6 22 0 19.64 -64.46 91.38 o 7 22 0 429.29 248.58 93.44 o 8 22 0 0.23 -100.93 83.94 o 9 22 0 125.83 72.14 88.84 o 10 22 0 345.18 314.91 103.17 o 11 22 0 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