#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217724.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217724_Fobs loop_ _publ_author_name 'Song, Xing-Min' 'Huang, Xian-Qiang' 'Dou, Jian-Min' 'Li, Da-Cheng' _publ_section_title ; Tetrakis[(benzene-18-crown-6)potassium]bis[tris(thiocyanato)copper(I)] ; _journal_coeditor_code BI2279 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m489 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.015 _cell_angle_beta 97.167 _cell_angle_gamma 105.558 _cell_length_a 9.7021 _cell_length_b 13.1192 _cell_length_c 17.9678 _exptl_crystal_F_000 980.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file bi2279Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 040618c in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 251.36 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1035.93 1056.33 59.69 o 2 0 0 184.91 146.10 39.93 o 3 0 0 211.14 136.92 51.89 o 4 0 0 65.12 3.76 46.22 o 5 0 0 58.21 152.20 74.75 o 6 0 0 549.91 582.20 137.54 o 7 0 0 109.94 55.21 98.22 o 8 0 0 14.15 -98.56 98.56 o 9 0 0 71.31 170.01 134.39 o 10 0 0 0.41 -140.39 140.39 o 11 0 0 14.16 31.58 186.11 o -11 1 0 108.13 -45.43 159.75 o -10 1 0 69.52 159.72 156.03 o -9 1 0 5.27 -11.96 116.83 o -8 1 0 213.80 181.04 120.10 o -7 1 0 1257.30 1184.71 197.31 o -6 1 0 769.47 374.79 109.81 o -5 1 0 581.23 826.62 133.86 o -4 1 0 3029.28 2809.30 176.49 o -3 1 0 1362.75 1285.92 95.11 o -2 1 0 4945.16 5618.48 245.54 o 1 1 0 1524.04 1505.12 62.53 o 2 1 0 5407.65 5714.08 191.87 o 3 1 0 5057.40 4864.80 182.68 o 4 1 0 155.68 134.70 68.65 o 5 1 0 1500.52 1704.68 206.61 o 6 1 0 198.44 48.19 86.09 o 7 1 0 584.49 507.21 157.26 o 8 1 0 941.84 643.54 186.22 o 9 1 0 309.03 104.45 134.76 o 10 1 0 11.55 -167.49 167.49 o -11 2 0 60.42 86.69 189.30 o -10 2 0 78.31 -44.67 133.90 o -9 2 0 552.61 456.12 177.10 o -8 2 0 3.44 -48.44 97.30 o -7 2 0 303.56 226.70 108.45 o -6 2 0 30.53 -49.98 65.20 o -5 2 0 322.26 334.05 89.29 o -4 2 0 24.87 -0.12 39.25 o -3 2 0 1.48 1.79 32.72 o -2 2 0 11.49 -14.24 14.24 o -1 2 0 792.49 726.40 53.04 o 0 2 0 375.04 407.61 16.77 o 1 2 0 3276.94 3508.74 124.67 o 2 2 0 35408.73 36437.29 1021.07 o 3 2 0 4974.11 4935.80 192.01 o 4 2 0 7736.96 7794.09 286.64 o 5 2 0 221.38 195.49 90.34 o 6 2 0 10.75 -25.02 71.48 o 7 2 0 171.61 389.08 143.15 o 8 2 0 0.51 -55.95 112.27 o 9 2 0 60.94 49.67 153.00 o 10 2 0 26.98 77.68 137.41 o -11 3 0 4.49 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64.45 o 2 4 0 70.97 64.29 28.07 o 3 4 0 7580.66 8233.69 298.51 o 4 4 0 3742.58 3598.93 332.61 o 5 4 0 2703.06 2646.96 158.82 o 6 4 0 1763.19 2056.15 191.56 o 7 4 0 194.21 56.63 112.58 o 8 4 0 85.20 153.99 160.16 o 9 4 0 71.55 25.50 122.63 o -10 5 0 149.00 -53.36 128.48 o -9 5 0 7.23 -94.13 108.05 o -8 5 0 668.45 715.93 313.04 o -7 5 0 689.42 729.98 109.44 o -6 5 0 643.93 892.39 102.14 o -5 5 0 1550.18 1378.15 84.23 o -4 5 0 1511.87 1405.96 74.69 o -3 5 0 705.32 1186.99 133.55 o -2 5 0 4491.41 4725.77 256.81 o -1 5 0 507.31 449.85 33.45 o 0 5 0 579.71 557.02 28.80 o 1 5 0 4822.20 4947.64 115.43 o 2 5 0 21.50 -21.44 21.44 o 3 5 0 233.90 339.76 69.36 o 4 5 0 369.29 364.29 174.33 o 5 5 0 1581.69 1994.33 370.53 o 6 5 0 279.30 236.14 96.32 o 7 5 0 55.96 -28.91 71.41 o 8 5 0 10.90 -108.62 108.62 o 9 5 0 0.43 -56.99 148.55 o -9 6 0 7.15 -87.78 147.23 o -8 6 0 39.45 -60.50 71.97 o -7 6 0 23.78 14.58 139.15 o -6 6 0 1615.10 1506.82 96.11 o -5 6 0 1363.52 1267.31 77.80 o -4 6 0 8.55 -27.37 27.37 o -3 6 0 2.61 10.04 47.51 o -2 6 0 96.96 62.60 53.80 o -1 6 0 1262.11 1298.04 145.56 o 0 6 0 71.06 45.35 23.82 o 1 6 0 1141.23 1140.98 48.41 o 2 6 0 1464.11 1459.00 56.56 o 3 6 0 193.55 156.42 49.14 o 4 6 0 556.98 786.69 117.51 o 5 6 0 14.47 1.27 51.45 o 6 6 0 628.01 757.32 111.07 o 7 6 0 102.07 93.35 90.59 o 8 6 0 133.50 151.13 164.07 o -11 7 0 5.22 -16.39 121.46 o -9 7 0 32.97 133.59 132.12 o -8 7 0 1091.29 1340.62 222.01 o -7 7 0 641.21 919.88 166.81 o -6 7 0 912.90 1383.00 192.69 o -5 7 0 628.23 626.66 131.89 o -4 7 0 506.52 478.51 83.40 o -3 7 0 709.33 834.69 136.08 o -2 7 0 1146.37 1173.98 259.65 o -1 7 0 477.59 584.41 98.43 o 0 7 0 140.76 111.13 33.27 o 1 7 0 1288.13 1212.88 143.23 o 2 7 0 1900.27 1981.50 72.04 o 3 7 0 2307.53 2677.02 115.60 o 4 7 0 66.90 93.70 57.76 o 5 7 0 317.23 318.09 130.25 o 6 7 0 14.78 -39.39 74.60 o 7 7 0 31.89 76.48 107.03 o 8 7 0 49.25 74.89 118.77 o -11 8 0 5.38 -35.19 120.04 o -9 8 0 0.09 43.75 126.88 o -8 8 0 0.57 48.62 108.64 o -7 8 0 347.93 115.05 114.61 o -6 8 0 57.59 -19.90 84.86 o -5 8 0 177.72 174.88 96.62 o -4 8 0 111.31 173.84 82.64 o -3 8 0 3.04 -22.92 58.79 o -2 8 0 872.24 849.71 183.05 o -1 8 0 106.15 104.08 33.38 o 0 8 0 127.46 118.18 37.73 o 1 8 0 1020.85 1052.04 138.06 o 2 8 0 2659.84 2592.58 106.89 o 3 8 0 352.05 246.78 66.79 o 4 8 0 86.68 -14.54 61.21 o 5 8 0 409.20 404.92 96.25 o 6 8 0 1.49 -71.96 86.48 o 7 8 0 24.16 3.92 105.56 o -8 9 0 2.86 -74.84 116.98 o -7 9 0 1.16 -43.19 94.16 o -6 9 0 1580.71 2265.12 266.92 o -5 9 0 1228.03 1603.22 208.77 o -4 9 0 517.00 556.44 127.19 o -3 9 0 856.68 1033.23 161.83 o -2 9 0 473.71 449.43 123.86 o -1 9 0 38.27 53.95 52.12 o 0 9 0 153.45 66.54 52.67 o 1 9 0 610.61 590.07 98.66 o 2 9 0 138.69 52.01 59.26 o 3 9 0 778.17 842.35 101.05 o 4 9 0 1.58 -34.74 67.83 o 5 9 0 80.49 10.42 81.79 o 6 9 0 42.99 19.64 116.82 o 7 9 0 5.71 -16.76 120.87 o -10 10 0 135.58 41.96 153.44 o -8 10 0 69.52 100.13 122.20 o -7 10 0 1.44 -16.27 104.33 o -6 10 0 219.01 378.05 145.86 o -5 10 0 1671.92 1648.74 226.81 o -4 10 0 814.50 1022.51 193.55 o -3 10 0 280.95 281.97 79.39 o -2 10 0 6.91 -29.35 52.41 o -1 10 0 89.99 88.58 64.56 o 0 10 0 5.11 -77.60 83.01 o 1 10 0 94.08 44.73 110.55 o 2 10 0 31.97 90.12 77.64 o 3 10 0 39.40 32.04 56.51 o 4 10 0 16.46 -25.78 78.42 o 5 10 0 12.81 5.59 107.96 o 6 10 0 215.67 138.69 138.35 o -10 11 0 0.60 -124.93 124.93 o -9 11 0 10.76 -21.26 126.39 o -8 11 0 0.07 -91.60 122.59 o -7 11 0 0.26 72.22 131.19 o -6 11 0 582.41 516.99 113.91 o -5 11 0 1566.54 1871.08 182.42 o -4 11 0 119.52 61.28 70.37 o -3 11 0 1695.92 1969.27 176.66 o -2 11 0 418.09 474.10 101.34 o -1 11 0 409.53 299.32 84.74 o 0 11 0 73.91 130.82 109.99 o 1 11 0 168.16 18.18 105.62 o 2 11 0 36.80 15.78 121.95 o 3 11 0 26.80 -41.96 123.43 o 4 11 0 198.31 102.50 122.72 o 5 11 0 5.19 -111.84 137.91 o -9 12 0 31.62 -54.47 157.57 o -8 12 0 6.63 117.88 142.47 o -7 12 0 87.31 -56.75 84.47 o -6 12 0 393.23 293.44 102.49 o -5 12 0 59.50 52.27 78.55 o -4 12 0 1049.21 1135.02 148.12 o -3 12 0 1207.79 1472.20 170.78 o -2 12 0 101.71 18.24 78.53 o -1 12 0 69.72 117.88 86.10 o 0 12 0 21.19 109.93 131.99 o 1 12 0 0.69 46.96 127.43 o 2 12 0 1.63 -22.00 128.54 o 3 12 0 0.67 -20.64 146.91 o 4 12 0 20.06 -28.66 161.26 o -8 13 0 84.71 26.93 158.68 o -7 13 0 34.55 -52.33 98.71 o -6 13 0 8.83 -75.89 101.99 o -5 13 0 0.14 -50.57 80.38 o -4 13 0 5.17 -36.73 87.93 o -3 13 0 81.90 91.06 83.48 o -2 13 0 34.52 51.72 87.94 o -1 13 0 184.65 328.94 159.72 o 0 13 0 443.04 859.45 221.33 o 1 13 0 188.51 94.10 152.26 o 2 13 0 263.18 120.78 171.00 o 3 13 0 141.41 372.13 198.11 o -7 14 0 1.51 -113.22 149.20 o -6 14 0 2.17 153.34 112.31 o -5 14 0 49.67 -24.53 99.24 o -4 14 0 504.11 283.11 107.42 o -3 14 0 43.75 89.09 96.89 o -2 14 0 32.92 38.88 142.41 o -1 14 0 47.03 105.44 141.98 o 0 14 0 0.26 -77.31 157.94 o 1 14 0 30.43 50.59 154.24 o 2 14 0 37.34 169.58 191.09 o -6 15 0 103.74 14.51 117.47 o -5 15 0 80.26 67.40 147.97 o -4 15 0 0.32 -93.59 102.84 o -3 15 0 27.15 40.42 167.49 o -2 15 0 14.89 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74.75 o 5 -8 1 1248.02 1477.06 198.11 o 6 -8 1 2071.63 2390.85 278.37 o 7 -8 1 0.93 -22.92 95.57 o 8 -8 1 53.93 110.24 120.41 o 9 -8 1 2.88 112.03 140.38 o -8 -7 1 15.85 33.75 138.49 o -7 -7 1 6.46 -45.61 105.26 o -6 -7 1 397.77 498.36 114.96 o -5 -7 1 160.15 123.20 86.88 o -4 -7 1 350.86 435.44 130.51 o -3 -7 1 15.94 -47.20 47.20 o -2 -7 1 55.98 90.66 38.67 o -1 -7 1 18.01 6.41 25.40 o 0 -7 1 2264.67 2178.03 65.52 o 1 -7 1 12861.51 13121.14 393.49 o 2 -7 1 14.38 37.84 60.14 o 3 -7 1 110.21 51.45 59.47 o 4 -7 1 575.40 743.95 130.72 o 5 -7 1 236.46 342.49 115.54 o 6 -7 1 4.77 -36.23 66.62 o 7 -7 1 703.19 791.45 170.63 o 8 -7 1 2.17 -95.42 100.35 o 9 -7 1 13.41 75.92 144.32 o 10 -7 1 0.35 147.95 205.69 o -9 -6 1 72.52 121.82 232.58 o -8 -6 1 0.65 2.33 104.25 o -7 -6 1 27.28 -68.30 94.18 o -6 -6 1 395.13 373.16 102.47 o -5 -6 1 1.13 -61.74 61.74 o -4 -6 1 0.52 -46.02 48.23 o -3 -6 1 50.68 55.18 53.15 o -2 -6 1 628.67 612.66 82.67 o -1 -6 1 277.84 322.73 43.18 o 0 -6 1 57.58 66.05 24.07 o 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