#------------------------------------------------------------------------------ #$Date: 2016-04-03 01:47:52 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181097 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/21/77/2217727.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217727_Fobs loop_ _publ_author_name 'Tahir, M. Nawaz' 'Shafiq, Muhammad' 'Khan, Islam Ullah' 'Siddiqui, Waseeq Ahmad' 'Arshad, Muhammad Nadeem' _publ_section_title ; 1-Methyl-1H-2,1-benzothiazin-4(3H)-one 2,2-dioxide ; _journal_coeditor_code BQ2063 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o557 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 67.691 _cell_angle_beta 70.467 _cell_angle_gamma 66.327 _cell_length_a 7.4553 _cell_length_b 8.5437 _cell_length_c 8.7097 _exptl_crystal_F_000 220.00 _reflns_d_resolution_high 0.8124 _cod_data_source_file bq2063Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' HS2_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 61.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 145.01 157.85 3.40 o 3 0 0 5.03 9.04 0.14 o 4 0 0 897.83 957.86 10.10 o 5 0 0 81.74 83.52 1.47 o 6 0 0 8.14 6.26 0.31 o 7 0 0 2.83 2.14 0.21 o 8 0 0 5.72 6.69 0.68 o -7 1 0 0.06 0.14 0.28 o -6 1 0 63.94 60.78 3.10 o -5 1 0 38.08 37.47 0.83 o -4 1 0 3.58 5.85 0.25 o -3 1 0 82.03 103.78 1.25 o -2 1 0 434.26 510.72 6.39 o -1 1 0 231.78 234.60 2.30 o 0 1 0 82.89 79.94 2.31 o 1 1 0 2841.58 2371.53 27.32 o 2 1 0 157.22 192.41 1.64 o 3 1 0 237.36 239.60 2.21 o 4 1 0 0.78 0.61 0.05 o 5 1 0 93.69 103.91 0.98 o 6 1 0 26.30 25.16 0.47 o 7 1 0 1.64 1.33 0.16 o 8 1 0 2.35 2.65 0.47 o -7 2 0 5.52 6.27 0.58 o -6 2 0 3.90 3.63 0.42 o -5 2 0 130.19 131.23 2.15 o -4 2 0 163.54 169.05 2.05 o -3 2 0 1.26 1.39 0.09 o -2 2 0 383.65 353.38 3.47 o -1 2 0 43.85 49.16 0.51 o 0 2 0 2857.99 2484.00 27.01 o 1 2 0 553.20 525.34 3.83 o 2 2 0 108.59 115.62 1.01 o 3 2 0 0.62 -0.03 0.03 o 4 2 0 26.66 23.53 0.27 o 5 2 0 2.27 2.83 0.09 o 6 2 0 126.43 130.45 1.31 o 7 2 0 14.08 12.27 0.77 o 8 2 0 29.14 30.43 1.37 o -6 3 0 6.78 5.54 0.51 o -5 3 0 93.95 91.39 2.81 o -4 3 0 88.59 85.13 1.08 o -3 3 0 17.14 15.78 0.20 o -2 3 0 47.57 42.78 0.44 o -1 3 0 180.86 186.47 2.07 o 0 3 0 183.72 178.60 1.41 o 1 3 0 38.12 35.13 0.44 o 2 3 0 165.53 174.75 1.59 o 3 3 0 11.78 9.31 0.19 o 4 3 0 32.19 28.25 0.31 o 5 3 0 5.99 6.55 0.17 o 6 3 0 0.11 0.27 0.09 o 7 3 0 4.33 4.18 0.19 o 8 3 0 9.86 6.55 0.62 o -6 4 0 1.77 1.55 0.39 o -5 4 0 8.29 9.63 0.62 o -4 4 0 71.36 70.76 1.55 o -3 4 0 76.23 77.65 1.25 o -2 4 0 13.59 12.42 0.20 o -1 4 0 158.92 163.46 2.20 o 0 4 0 28.63 23.07 0.25 o 1 4 0 236.68 227.59 2.02 o 2 4 0 307.98 350.23 2.83 o 3 4 0 0.21 0.22 0.06 o 4 4 0 522.74 528.26 6.25 o 5 4 0 15.16 13.84 0.23 o 6 4 0 207.03 213.64 2.53 o 7 4 0 3.03 2.73 0.18 o 8 4 0 26.53 29.14 0.63 o -5 5 0 0.34 0.71 0.30 o -4 5 0 35.17 37.94 1.41 o -3 5 0 80.48 81.86 1.76 o -2 5 0 5.45 5.96 0.15 o -1 5 0 156.07 164.04 1.56 o 0 5 0 18.29 20.45 0.24 o 1 5 0 127.55 119.29 1.14 o 2 5 0 287.04 297.84 2.56 o 3 5 0 0.61 2.05 0.10 o 4 5 0 317.14 306.91 2.86 o 5 5 0 56.79 62.22 0.72 o 6 5 0 43.04 44.82 0.67 o 7 5 0 23.81 23.41 0.53 o 8 5 0 2.57 3.71 0.44 o -4 6 0 0.09 -0.14 0.27 o -3 6 0 0.30 0.21 0.23 o -2 6 0 64.52 65.24 1.40 o -1 6 0 11.46 11.31 0.26 o 0 6 0 263.68 271.56 3.69 o 1 6 0 2.21 1.75 0.08 o 2 6 0 271.19 276.13 2.81 o 3 6 0 36.49 41.11 0.44 o 4 6 0 163.15 159.81 1.66 o 5 6 0 126.21 129.72 1.78 o 6 6 0 7.39 7.50 0.47 o 7 6 0 28.68 29.26 0.64 o 8 6 0 0.23 0.34 0.15 o -3 7 0 55.84 57.26 2.03 o -2 7 0 105.70 100.19 3.13 o -1 7 0 67.11 68.55 1.50 o 0 7 0 4.48 5.11 0.19 o 1 7 0 0.53 0.33 0.10 o 2 7 0 30.85 27.95 0.46 o 3 7 0 15.25 15.33 0.32 o 4 7 0 84.68 77.11 1.03 o 5 7 0 51.61 55.11 0.89 o 6 7 0 2.01 1.17 0.17 o 7 7 0 5.48 6.62 0.30 o -2 8 0 19.80 20.80 1.07 o -1 8 0 65.14 64.12 2.24 o 0 8 0 49.75 52.55 2.38 o 1 8 0 0.66 0.82 0.31 o 2 8 0 7.52 8.11 0.40 o 3 8 0 13.93 13.86 0.40 o 4 8 0 0.32 -0.11 0.11 o 5 8 0 41.27 37.10 0.75 o 6 8 0 13.80 15.70 0.56 o 0 9 0 14.25 13.92 0.87 o 1 9 0 15.85 17.91 0.99 o 2 9 0 2.86 2.20 0.42 o 3 9 0 46.40 53.48 1.28 o 4 9 0 2.98 2.97 0.29 o 5 9 0 48.33 52.81 0.99 o -4 -9 1 39.46 46.99 1.20 o -3 -9 1 0.11 -0.20 0.20 o -2 -9 1 27.69 30.94 1.46 o -1 -9 1 4.42 3.62 0.53 o -6 -8 1 28.99 30.41 0.68 o -5 -8 1 2.55 1.64 0.24 o -4 -8 1 9.35 10.19 0.35 o -3 -8 1 3.39 3.40 0.28 o -2 -8 1 2.51 2.60 0.24 o -1 -8 1 14.80 16.14 0.93 o 0 -8 1 84.29 85.12 2.85 o 1 -8 1 2.07 0.45 0.32 o 2 -8 1 27.14 27.98 1.32 o -7 -7 1 4.96 4.85 0.29 o -6 -7 1 13.40 14.52 0.39 o -5 -7 1 4.93 3.99 0.32 o -4 -7 1 0.14 0.39 0.14 o -3 -7 1 6.17 5.49 0.20 o -2 -7 1 5.82 5.18 0.22 o -1 -7 1 21.16 21.32 0.44 o 0 -7 1 122.54 121.33 2.06 o 1 -7 1 21.93 21.87 0.65 o 2 -7 1 48.01 47.11 1.77 o 3 -7 1 16.76 16.11 0.93 o -7 -6 1 6.29 7.09 0.45 o -6 -6 1 74.26 73.91 1.13 o -5 -6 1 49.95 49.24 0.81 o -4 -6 1 0.21 -0.07 0.10 o -3 -6 1 0.32 0.37 0.08 o -2 -6 1 50.77 49.61 0.55 o -1 -6 1 0.07 -0.07 0.07 o 0 -6 1 323.26 322.38 3.18 o 1 -6 1 95.25 90.65 1.88 o 2 -6 1 16.74 15.54 0.49 o 3 -6 1 39.29 35.12 1.40 o 4 -6 1 4.65 3.89 0.50 o -8 -5 1 0.43 0.04 0.12 o -7 -5 1 21.72 21.81 0.51 o -6 -5 1 8.39 7.45 0.23 o -5 -5 1 158.04 152.22 1.86 o -4 -5 1 41.51 40.70 0.48 o -3 -5 1 42.38 45.62 0.55 o -2 -5 1 66.11 66.98 0.65 o -1 -5 1 13.00 17.70 0.24 o 0 -5 1 330.12 333.98 2.99 o 1 -5 1 132.22 128.24 1.69 o 2 -5 1 26.64 26.03 0.44 o 3 -5 1 29.22 27.03 1.21 o 4 -5 1 1.71 1.71 0.34 o 5 -5 1 3.86 4.00 0.49 o -8 -4 1 1.29 1.22 0.43 o -7 -4 1 41.00 42.38 0.78 o -6 -4 1 13.94 12.63 0.35 o -5 -4 1 378.34 376.95 3.50 o -4 -4 1 7.80 6.49 0.15 o -3 -4 1 209.04 237.96 2.22 o -2 -4 1 0.48 2.21 0.08 o -1 -4 1 164.95 217.50 1.78 o 0 -4 1 95.89 88.92 0.83 o 1 -4 1 45.75 36.41 0.44 o 2 -4 1 4.22 5.53 0.12 o 3 -4 1 4.64 3.70 0.14 o 4 -4 1 17.06 17.23 0.50 o 5 -4 1 0.00 0.17 0.24 o 6 -4 1 13.09 13.04 0.84 o -8 -3 1 0.81 1.04 0.40 o -7 -3 1 6.49 5.98 0.59 o -6 -3 1 50.70 53.31 0.99 o -5 -3 1 93.01 88.39 0.95 o -4 -3 1 1000.61 1012.73 8.52 o -3 -3 1 5.03 4.02 0.10 o -2 -3 1 1636.99 1618.73 14.67 o -1 -3 1 48.08 63.03 0.71 o 0 -3 1 1162.11 1186.52 10.08 o 1 -3 1 55.55 50.77 0.45 o 2 -3 1 0.69 0.64 0.07 o 3 -3 1 22.12 20.92 0.32 o 4 -3 1 61.31 60.30 0.92 o 5 -3 1 0.00 0.05 0.12 o 6 -3 1 23.36 23.85 1.12 o 7 -3 1 1.69 1.44 0.39 o -8 -2 1 2.98 1.83 0.43 o -7 -2 1 10.21 9.20 0.68 o -6 -2 1 21.45 20.39 0.41 o -5 -2 1 44.17 43.22 0.48 o -4 -2 1 0.07 0.04 0.04 o -3 -2 1 122.01 124.72 1.04 o -2 -2 1 75.95 90.53 1.17 o -1 -2 1 493.36 464.61 3.68 o 0 -2 1 19.22 20.48 0.22 o 1 -2 1 225.16 215.03 1.88 o 2 -2 1 32.63 30.94 0.41 o 3 -2 1 2.74 2.18 0.08 o 4 -2 1 72.92 75.07 0.88 o 5 -2 1 28.29 25.53 0.66 o 6 -2 1 9.78 11.27 0.79 o 7 -2 1 2.33 2.56 0.44 o -8 -1 1 2.39 3.22 0.48 o -7 -1 1 10.69 10.12 0.40 o -6 -1 1 16.21 18.04 0.58 o -5 -1 1 0.12 -0.06 0.06 o -4 -1 1 254.79 265.64 2.67 o -3 -1 1 429.15 446.16 3.58 o -2 -1 1 137.87 135.86 1.13 o -1 -1 1 1384.16 1217.62 11.47 o 0 -1 1 16.45 21.71 0.21 o 1 -1 1 65.01 47.74 0.49 o 2 -1 1 771.61 775.60 6.97 o 3 -1 1 159.19 180.71 1.55 o 4 -1 1 826.39 868.15 8.47 o 5 -1 1 393.61 389.63 4.94 o 6 -1 1 118.59 122.11 2.52 o 7 -1 1 97.32 94.55 3.50 o -7 0 1 4.86 3.73 0.44 o -6 0 1 5.40 4.73 0.26 o -5 0 1 6.62 4.91 0.15 o -4 0 1 0.03 0.06 0.05 o -3 0 1 178.99 193.23 2.09 o -2 0 1 102.53 114.01 1.52 o -1 0 1 2323.84 2227.04 56.69 o 0 0 1 22.17 19.26 0.24 o 1 0 1 1940.58 1691.08 16.40 o 2 0 1 1623.80 1601.67 15.39 o 3 0 1 332.51 362.30 3.51 o 4 0 1 400.09 419.80 3.75 o 5 0 1 39.36 33.45 0.43 o 6 0 1 303.71 295.28 4.44 o 7 0 1 3.25 4.07 0.32 o 8 0 1 48.18 40.10 1.67 o -7 1 1 2.24 2.58 0.42 o -6 1 1 26.49 23.63 1.01 o -5 1 1 100.99 101.06 1.68 o -4 1 1 46.35 41.90 0.51 o -3 1 1 831.27 819.04 8.67 o -2 1 1 13.21 15.13 0.22 o -1 1 1 3098.07 2775.15 49.69 o 1 1 1 558.11 542.03 4.17 o 2 1 1 3841.88 3178.20 36.42 o 3 1 1 123.75 142.65 1.40 o 4 1 1 1924.23 1970.47 18.50 o 5 1 1 55.47 51.63 0.56 o 6 1 1 73.77 77.13 1.08 o 7 1 1 0.14 -0.11 0.11 o 8 1 1 4.08 2.62 0.48 o -7 2 1 0.97 1.35 0.36 o -6 2 1 2.82 2.88 0.37 o -5 2 1 81.14 80.62 1.72 o -4 2 1 10.41 12.43 0.36 o -3 2 1 371.58 364.53 5.65 o -2 2 1 96.30 94.10 1.50 o -1 2 1 2005.16 1935.74 37.39 o 0 2 1 622.89 643.28 6.60 o 1 2 1 69.62 76.50 0.56 o 2 2 1 6.76 11.65 0.24 o 3 2 1 14.74 16.81 0.21 o 4 2 1 19.27 23.70 0.28 o 5 2 1 178.85 184.94 1.88 o 6 2 1 49.39 48.02 0.57 o 7 2 1 3.53 3.59 0.29 o 8 2 1 1.87 2.37 0.44 o -6 3 1 0.28 0.23 0.26 o -5 3 1 10.73 10.82 0.62 o -4 3 1 46.86 49.56 1.87 o -3 3 1 34.71 30.13 0.57 o -2 3 1 47.95 53.86 0.90 o -1 3 1 243.47 263.37 3.15 o 0 3 1 285.93 278.85 2.32 o 1 3 1 542.32 554.49 4.56 o 2 3 1 96.14 117.45 0.93 o 3 3 1 300.42 289.29 3.84 o 4 3 1 12.72 15.34 0.27 o 5 3 1 257.42 263.78 2.62 o 6 3 1 75.48 74.94 0.83 o 7 3 1 0.07 0.01 0.09 o 8 3 1 17.33 18.67 0.42 o -6 4 1 31.72 30.22 1.28 o -5 4 1 50.57 48.36 1.69 o -4 4 1 0.16 0.06 0.11 o -3 4 1 23.96 24.95 0.48 o -2 4 1 13.73 12.50 0.24 o -1 4 1 117.36 131.32 1.54 o 0 4 1 460.58 465.42 4.05 o 1 4 1 72.68 67.91 0.63 o 2 4 1 58.03 66.99 0.56 o 3 4 1 3.44 2.91 0.11 o 4 4 1 14.24 12.63 0.17 o 5 4 1 64.15 66.89 0.75 o 6 4 1 79.45 77.17 0.93 o 7 4 1 1.42 0.61 0.12 o 8 4 1 0.03 0.11 0.12 o -5 5 1 23.45 24.82 1.10 o -4 5 1 45.93 45.03 1.57 o -3 5 1 0.29 0.91 0.14 o -2 5 1 10.79 13.42 0.31 o -1 5 1 0.01 0.14 0.07 o 0 5 1 31.63 37.20 0.37 o 1 5 1 409.59 421.01 3.92 o 2 5 1 259.58 269.48 2.19 o 3 5 1 107.86 112.07 1.13 o 4 5 1 81.61 87.33 0.87 o 5 5 1 42.32 44.02 0.47 o 6 5 1 88.08 91.14 1.30 o 7 5 1 13.85 11.70 0.42 o 8 5 1 6.35 7.77 0.30 o -4 6 1 27.94 30.17 1.22 o -3 6 1 29.45 28.67 1.13 o -2 6 1 22.65 26.02 1.58 o -1 6 1 196.04 196.52 3.70 o 0 6 1 99.07 104.53 1.09 o 1 6 1 1131.42 1120.38 11.02 o 2 6 1 9.60 12.06 0.18 o 3 6 1 561.11 561.06 4.52 o 4 6 1 7.43 9.38 0.19 o 5 6 1 190.62 185.66 1.91 o 6 6 1 17.80 17.59 0.41 o 7 6 1 3.07 2.84 0.19 o 8 6 1 0.02 0.04 0.14 o -3 7 1 0.52 0.04 0.27 o -2 7 1 26.77 24.06 1.03 o -1 7 1 3.48 3.51 0.39 o 0 7 1 224.84 219.03 4.01 o 1 7 1 42.45 41.54 0.77 o 2 7 1 953.82 945.32 10.07 o 3 7 1 19.02 18.72 0.33 o 4 7 1 506.90 519.93 5.46 o 5 7 1 3.77 3.40 0.18 o 6 7 1 101.23 97.04 1.65 o 7 7 1 6.00 5.76 0.29 o 8 7 1 0.96 0.76 0.17 o -2 8 1 52.83 52.60 1.90 o -1 8 1 20.82 21.82 1.04 o 0 8 1 54.81 52.84 1.87 o 1 8 1 49.22 49.15 1.56 o 2 8 1 1.66 1.92 0.14 o 3 8 1 1.62 1.33 0.16 o 4 8 1 12.12 12.79 0.31 o 5 8 1 5.25 5.28 0.26 o 6 8 1 4.65 4.11 0.25 o 7 8 1 9.39 10.47 0.37 o -1 9 1 8.12 7.57 0.65 o 0 9 1 12.76 12.44 0.78 o 1 9 1 7.40 5.11 0.53 o 2 9 1 66.59 68.74 2.39 o 3 9 1 0.36 0.71 0.34 o 4 9 1 29.57 32.54 0.89 o 5 9 1 3.42 3.54 0.23 o 6 9 1 0.29 0.27 0.15 o 3 10 1 9.23 11.08 0.83 o -5 -8 2 21.02 20.75 0.78 o -4 -8 2 1.91 1.86 0.19 o -3 -8 2 0.08 0.05 0.17 o -2 -8 2 1.76 2.24 0.27 o -1 -8 2 21.90 23.07 0.72 o 0 -8 2 0.00 0.19 0.32 o 1 -8 2 19.44 18.66 1.07 o -6 -7 2 8.55 9.09 0.35 o -5 -7 2 0.00 0.30 0.13 o -4 -7 2 18.22 18.59 0.43 o -3 -7 2 54.01 46.34 0.78 o -2 -7 2 1.37 1.58 0.27 o -1 -7 2 138.96 130.50 2.14 o 0 -7 2 19.18 18.87 0.60 o 1 -7 2 47.85 48.13 1.84 o 2 -7 2 28.73 30.58 1.38 o 3 -7 2 3.97 3.84 0.54 o -7 -6 2 16.45 15.89 0.45 o -6 -6 2 0.03 0.06 0.18 o -5 -6 2 16.26 15.60 0.39 o -4 -6 2 10.49 6.60 0.25 o -3 -6 2 3.45 4.27 0.20 o -2 -6 2 91.46 73.95 0.98 o -1 -6 2 97.02 98.65 1.44 o 0 -6 2 236.24 218.44 2.66 o 1 -6 2 30.40 30.11 0.45 o 2 -6 2 80.37 74.24 2.49 o 3 -6 2 2.20 1.48 0.37 o 4 -6 2 37.86 34.64 1.50 o -7 -5 2 1.55 1.22 0.15 o -6 -5 2 68.39 66.90 1.14 o -5 -5 2 11.67 12.68 0.30 o -4 -5 2 42.60 41.63 0.62 o -3 -5 2 87.70 90.96 0.94 o -2 -5 2 0.44 0.65 0.06 o -1 -5 2 187.29 188.86 1.83 o 0 -5 2 193.33 185.35 1.87 o 1 -5 2 2.53 2.65 0.11 o 2 -5 2 90.83 87.86 1.36 o 3 -5 2 0.02 -0.07 0.20 o 4 -5 2 47.41 46.94 1.52 o 5 -5 2 21.17 20.92 1.09 o -7 -4 2 4.04 4.97 0.59 o -6 -4 2 34.89 31.90 0.68 o -5 -4 2 87.25 88.52 1.05 o -4 -4 2 2.87 2.72 0.11 o -3 -4 2 121.83 125.40 1.31 o -2 -4 2 27.20 21.12 0.26 o -1 -4 2 164.22 156.30 1.48 o 0 -4 2 488.54 478.18 4.33 o 1 -4 2 109.08 116.51 1.22 o 2 -4 2 122.43 120.24 1.14 o 3 -4 2 86.47 89.82 1.28 o 4 -4 2 62.49 60.67 1.87 o 5 -4 2 129.03 126.33 2.64 o 6 -4 2 1.28 1.90 0.42 o -7 -3 2 0.64 1.07 0.37 o -6 -3 2 10.24 8.76 0.32 o -5 -3 2 133.31 140.14 1.45 o -4 -3 2 4.22 3.52 0.11 o -3 -3 2 393.53 414.90 3.99 o -2 -3 2 58.06 85.77 0.90 o -1 -3 2 1217.26 1229.96 10.47 o 0 -3 2 47.46 67.84 0.79 o 1 -3 2 3.93 9.03 0.15 o 2 -3 2 425.70 447.16 4.11 o 3 -3 2 0.79 0.63 0.11 o 4 -3 2 70.42 68.96 0.91 o 5 -3 2 46.87 47.95 1.14 o 6 -3 2 70.14 65.15 2.29 o -7 -2 2 10.46 11.84 0.77 o -6 -2 2 31.53 29.37 0.65 o -5 -2 2 122.48 130.39 1.63 o -4 -2 2 44.97 52.00 0.50 o -3 -2 2 35.42 40.82 0.46 o -2 -2 2 226.27 218.84 1.79 o -1 -2 2 316.53 344.39 3.08 o 0 -2 2 1511.52 1465.39 13.17 o 1 -2 2 72.52 65.08 0.97 o 2 -2 2 4.15 4.57 0.10 o 3 -2 2 4.06 4.53 0.10 o 4 -2 2 2.71 2.25 0.11 o 5 -2 2 48.99 51.98 0.93 o 6 -2 2 59.41 59.09 2.92 o 7 -2 2 0.59 0.10 0.31 o -7 -1 2 0.43 0.80 0.32 o -6 -1 2 1.18 0.70 0.18 o -5 -1 2 61.84 61.73 0.82 o -4 -1 2 122.96 137.03 1.75 o -3 -1 2 8.74 8.76 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