#------------------------------------------------------------------------------ #$Date: 2009-05-03 21:56:13 +0300 (Sun, 03 May 2009) $ #$Revision: 691 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217729_Fobs loop_ _publ_author_name 'Ayed, Brahim' 'Haddad, Amor' _publ_section_title ; A new sodium dimangnesium trivanadate, NaMg~2~V~3~O~10~ ; _journal_coeditor_code BR2067 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i21 _journal_volume 64 _journal_year 2008 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 104.325 _cell_angle_beta 100.604 _cell_angle_gamma 101.696 _cell_length_a 6.7369 _cell_length_b 6.7553 _cell_length_c 9.6222 _exptl_crystal_F_000 183.95 _reflns_d_resolution_high 0.7838 _[local]_cod_data_source_file br2067Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bra3 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 143.18 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3161.44 3202.52 66.52 o 2 0 0 13540.21 12594.00 99.43 o 3 0 0 4876.27 5208.14 121.90 o 4 0 0 1509.94 1426.10 47.54 o 5 0 0 17.79 26.78 11.49 o 6 0 0 2733.29 2807.52 216.82 o 7 0 0 983.70 989.05 65.32 o 8 0 0 952.08 1044.22 66.10 o -8 1 0 26.24 -19.87 34.44 o -7 1 0 764.63 801.54 51.25 o -6 1 0 1218.36 1166.57 53.34 o -5 1 0 2181.18 2084.28 94.87 o -4 1 0 9152.34 8602.54 157.78 o -3 1 0 1351.72 1130.03 82.69 o -2 1 0 8990.77 8624.83 523.65 o -1 1 0 670.48 907.76 40.93 o 0 1 0 450.12 524.83 21.18 o 1 1 0 586.84 586.58 61.58 o 2 1 0 1149.12 1106.33 32.64 o 3 1 0 223.94 255.74 14.23 o 4 1 0 4624.94 4372.77 98.44 o 5 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