#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217741.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217741_Fobs loop_ _publ_author_name 'Begum, G. Chanthini' 'Kumar, R. Suresh' 'Suresh, J.' 'Gopinathan, C.' 'Lakshman, P. L. Nilantha' _publ_section_title ; (3R*,4R*,5S*)-4-(4-Methylphenyl)-2,3-diphenyl-7-[(R*)-1-phenylethyl]-1-oxa-2,7-diazaspiro[4.5]decan-10-one oxime ; _journal_coeditor_code CI2561 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o590 _journal_volume 64 _journal_year 2008 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.4482 _cell_length_b 10.5883 _cell_length_c 26.4895 _exptl_crystal_F_000 1104.00 _reflns_d_resolution_high 0.8415 _[local]_cod_data_source_file ci2561Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' noh in P 21 21 21' _shelx_refln_list_code 4 _shelx_F_calc_maximum 183.64 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24040.19 22613.68 102.73 o 4 0 0 90.19 105.95 20.26 o 6 0 0 710.93 660.32 33.23 o 8 0 0 57.71 45.83 49.33 o 10 0 0 85.11 103.02 54.16 o 12 0 0 0.21 87.30 52.83 o 1 1 0 1190.51 1115.75 28.88 o 2 1 0 3907.17 3689.81 51.22 o 3 1 0 925.31 930.93 28.69 o 4 1 0 180.96 179.80 21.30 o 5 1 0 1.74 -9.18 32.95 o 6 1 0 6.77 26.51 32.67 o 7 1 0 70.02 71.30 42.42 o 8 1 0 542.15 474.46 41.00 o 9 1 0 125.98 125.55 39.77 o 10 1 0 54.53 72.62 53.78 o 11 1 0 12.46 58.99 54.63 o 12 1 0 2.43 19.50 58.42 o 0 2 0 1211.27 1157.03 30.49 o 1 2 0 33723.21 32730.21 128.77 o 2 2 0 2870.69 2755.47 57.00 o 3 2 0 432.46 435.35 23.29 o 4 2 0 1784.20 1750.13 46.30 o 5 2 0 35.51 15.72 34.09 o 6 2 0 24.72 21.87 38.35 o 7 2 0 204.79 210.10 32.76 o 8 2 0 351.64 326.94 39.29 o 9 2 0 4.20 -49.14 49.14 o 10 2 0 53.73 68.74 54.63 o 11 2 0 0.28 62.87 56.62 o 12 2 0 44.64 72.53 60.79 o 1 3 0 15.02 36.17 31.91 o 2 3 0 14121.96 14364.59 111.82 o 3 3 0 179.55 180.18 21.49 o 4 3 0 1118.65 1186.57 34.75 o 5 3 0 81.36 71.39 37.02 o 6 3 0 60.16 42.04 38.91 o 7 3 0 40.95 46.96 47.53 o 8 3 0 470.95 492.26 39.39 o 9 3 0 114.92 98.94 51.89 o 10 3 0 183.42 205.75 42.23 o 11 3 0 26.70 50.75 40.52 o 12 3 0 13.24 43.84 56.72 o 0 4 0 4972.93 4971.35 73.47 o 1 4 0 59.14 80.58 21.02 o 2 4 0 209.30 198.55 23.29 o 3 4 0 1605.46 1723.05 45.92 o 4 4 0 108.68 113.15 25.75 o 5 4 0 90.72 42.51 37.97 o 6 4 0 25.31 -45.45 45.45 o 7 4 0 1.44 25.09 45.45 o 8 4 0 6.29 48.48 48.19 o 9 4 0 4.03 -4.92 51.60 o 10 4 0 0.01 34.09 48.19 o 11 4 0 4.45 15.91 56.81 o 1 5 0 0.58 -5.68 35.41 o 2 5 0 2267.03 2447.66 65.90 o 3 5 0 2030.02 2202.33 63.25 o 4 5 0 296.67 286.61 31.34 o 5 5 0 221.51 159.26 31.53 o 6 5 0 0.55 -46.21 46.21 o 7 5 0 0.66 14.68 51.79 o 8 5 0 50.33 -9.47 53.02 o 9 5 0 106.19 115.13 36.64 o 10 5 0 4.47 -56.72 59.84 o 11 5 0 5.82 43.36 56.05 o 0 6 0 1.30 -38.44 38.44 o 1 6 0 215.13 258.77 28.50 o 2 6 0 593.87 561.28 33.61 o 3 6 0 0.01 16.76 38.54 o 4 6 0 120.13 125.36 31.81 o 5 6 0 114.54 132.84 33.33 o 6 6 0 6.19 -32.76 49.52 o 7 6 0 37.16 -8.99 54.44 o 8 6 0 55.26 96.48 48.29 o 9 6 0 14.17 33.52 53.50 o 10 6 0 12.20 50.66 54.63 o 1 7 0 88.08 126.40 30.58 o 2 7 0 4.45 -28.40 43.18 o 3 7 0 12.93 -15.91 45.26 o 4 7 0 41.47 32.48 47.15 o 5 7 0 480.66 468.97 42.32 o 6 7 0 4.91 -13.73 51.22 o 7 7 0 3.60 29.64 46.77 o 8 7 0 37.44 46.77 53.40 o 9 7 0 3.07 -61.07 61.07 o 10 7 0 1.92 -13.54 58.61 o 0 8 0 192.04 172.13 38.82 o 1 8 0 279.74 317.57 38.16 o 2 8 0 117.86 123.28 34.65 o 3 8 0 117.47 99.51 38.06 o 4 8 0 393.63 365.86 43.55 o 5 8 0 70.68 110.40 37.59 o 6 8 0 283.06 253.37 41.47 o 7 8 0 98.93 54.25 54.06 o 8 8 0 64.85 -47.91 60.60 o 9 8 0 2.26 42.13 61.07 o 1 9 0 39.46 32.86 56.90 o 2 9 0 59.38 63.06 56.43 o 3 9 0 89.01 46.77 55.30 o 4 9 0 12.75 58.61 52.45 o 5 9 0 79.56 72.91 53.59 o 6 9 0 2.48 8.43 53.12 o 7 9 0 75.87 187.85 40.71 o 8 9 0 14.05 -55.48 59.46 o 0 10 0 311.19 278.94 42.80 o 1 10 0 33.67 12.50 50.94 o 2 10 0 100.81 89.85 57.95 o 3 10 0 19.57 74.23 38.06 o 4 10 0 9.99 -33.04 53.50 o 5 10 0 16.20 40.81 55.86 o 6 10 0 92.01 68.65 62.87 o 7 10 0 1.21 99.99 58.32 o 1 11 0 31.59 88.24 38.54 o 2 11 0 60.14 17.42 62.11 o 3 11 0 34.72 20.93 60.03 o 4 11 0 0.62 -6.15 59.84 o 5 11 0 0.46 -64.95 64.95 o 6 11 0 17.21 34.56 63.72 o 0 12 0 12.71 -12.78 64.29 o 1 12 0 1.79 19.32 63.91 o 2 12 0 0.02 -58.99 61.64 o 3 12 0 62.23 10.04 65.99 o 1 0 1 6995.86 6671.02 30.66 o 2 0 1 7714.80 7299.72 44.66 o 3 0 1 1562.87 1538.06 71.01 o 4 0 1 984.47 976.79 19.87 o 5 0 1 407.76 431.49 30.96 o 6 0 1 1.63 21.29 25.05 o 7 0 1 7.83 -1.32 29.22 o 8 0 1 199.82 256.31 53.59 o 9 0 1 374.70 417.34 46.35 o 10 0 1 5.23 13.05 37.31 o 11 0 1 18.19 -40.76 40.76 o 12 0 1 7.14 25.00 59.84 o 0 1 1 7259.85 7189.42 127.68 o 1 1 1 6317.83 5902.35 82.42 o 2 1 1 1956.09 1927.61 29.79 o 3 1 1 208.68 180.82 15.40 o 4 1 1 66.96 71.17 14.86 o 5 1 1 700.36 712.81 22.09 o 6 1 1 64.53 81.08 18.14 o 7 1 1 204.50 215.56 27.41 o 8 1 1 15.00 59.75 33.85 o 9 1 1 119.62 138.04 31.62 o 10 1 1 118.04 160.84 28.48 o 11 1 1 14.64 47.14 50.13 o 12 1 1 7.78 -14.31 56.90 o 0 2 1 5196.73 5302.55 53.50 o 1 2 1 12002.78 11568.91 57.04 o 2 2 1 3241.70 3246.84 75.27 o 3 2 1 615.70 613.26 17.51 o 4 2 1 909.12 908.41 43.60 o 5 2 1 2.83 36.01 23.72 o 6 2 1 103.59 92.16 18.98 o 7 2 1 72.15 70.26 25.25 o 8 2 1 13.07 33.11 34.36 o 9 2 1 30.02 48.76 33.06 o 10 2 1 73.48 31.18 37.28 o 11 2 1 3.44 -29.95 40.67 o 12 2 1 10.74 -46.16 46.16 o 0 3 1 2401.63 2443.26 36.66 o 1 3 1 3573.53 3701.11 42.55 o 2 3 1 1012.31 1016.16 22.20 o 3 3 1 747.10 814.14 18.88 o 4 3 1 250.09 272.80 24.24 o 5 3 1 243.43 253.85 25.19 o 6 3 1 223.02 239.04 28.83 o 7 3 1 11.65 25.15 31.42 o 8 3 1 73.93 33.21 42.42 o 9 3 1 20.08 72.30 35.82 o 10 3 1 105.98 129.75 27.78 o 11 3 1 7.56 -12.73 46.21 o 12 3 1 60.58 20.73 60.74 o 0 4 1 3214.45 3130.00 43.38 o 1 4 1 398.94 391.47 17.07 o 2 4 1 334.21 308.58 16.91 o 3 4 1 44.35 54.95 23.33 o 4 4 1 58.53 77.92 20.71 o 5 4 1 297.16 310.40 21.59 o 6 4 1 1.18 3.99 29.59 o 7 4 1 70.53 54.13 30.49 o 8 4 1 45.50 57.27 37.19 o 9 4 1 16.95 33.87 28.88 o 10 4 1 19.13 26.24 62.54 o 11 4 1 16.38 25.55 43.11 o 0 5 1 65.44 65.85 22.77 o 1 5 1 64.66 43.58 25.63 o 2 5 1 1179.61 1155.74 25.43 o 3 5 1 81.54 100.79 26.70 o 4 5 1 448.72 452.81 22.66 o 5 5 1 28.82 8.18 29.79 o 6 5 1 89.91 100.94 26.00 o 7 5 1 32.43 31.06 36.08 o 8 5 1 16.73 53.62 33.81 o 9 5 1 46.30 9.85 40.62 o 10 5 1 64.71 56.77 43.36 o 11 5 1 6.40 41.60 42.48 o 0 6 1 256.76 267.94 36.64 o 1 6 1 247.86 255.51 27.88 o 2 6 1 92.33 132.06 20.05 o 3 6 1 1069.71 1071.12 28.58 o 4 6 1 136.12 114.62 26.16 o 5 6 1 179.96 220.60 34.65 o 6 6 1 80.87 79.18 36.18 o 7 6 1 24.95 -17.71 35.60 o 8 6 1 9.70 23.38 66.04 o 9 6 1 31.23 32.13 44.79 o 10 6 1 34.65 33.62 41.81 o 0 7 1 29.99 3.72 31.53 o 1 7 1 38.56 -16.34 31.70 o 2 7 1 23.01 34.10 43.55 o 3 7 1 138.74 172.49 26.51 o 4 7 1 27.42 18.06 33.82 o 5 7 1 49.60 56.57 36.44 o 6 7 1 143.26 128.79 32.56 o 7 7 1 84.63 85.42 30.77 o 8 7 1 59.47 71.75 31.38 o 9 7 1 1.09 -36.22 40.47 o 10 7 1 1.27 8.77 55.67 o 0 8 1 635.15 609.72 30.09 o 1 8 1 273.63 272.92 27.84 o 2 8 1 124.05 86.84 39.34 o 3 8 1 107.87 121.36 25.94 o 4 8 1 100.60 87.51 32.14 o 5 8 1 220.56 209.30 35.51 o 6 8 1 38.31 84.37 36.75 o 7 8 1 92.92 102.80 42.70 o 8 8 1 8.70 37.78 40.90 o 9 8 1 5.65 25.99 39.43 o 0 9 1 130.88 86.13 32.89 o 1 9 1 414.67 451.58 31.60 o 2 9 1 79.10 98.92 67.08 o 3 9 1 216.67 222.00 35.74 o 4 9 1 101.59 57.17 38.53 o 5 9 1 59.11 74.73 31.30 o 6 9 1 38.04 75.48 40.74 o 7 9 1 96.69 24.42 45.59 o 8 9 1 15.30 -45.36 45.36 o 0 10 1 4.03 -21.24 84.79 o 1 10 1 10.68 77.81 47.67 o 2 10 1 15.88 -33.66 39.81 o 3 10 1 22.81 34.23 38.20 o 4 10 1 43.20 39.67 40.07 o 5 10 1 5.68 30.94 38.55 o 6 10 1 14.60 16.49 34.79 o 7 10 1 95.88 126.22 36.92 o 0 11 1 2.69 4.51 92.13 o 1 11 1 24.11 32.71 40.24 o 2 11 1 55.53 62.71 64.76 o 3 11 1 25.28 33.08 41.34 o 4 11 1 7.80 15.49 33.27 o 5 11 1 13.63 -26.53 93.78 o 6 11 1 52.03 10.38 45.59 o 0 12 1 9.93 -14.10 65.62 o 1 12 1 0.96 -4.84 43.25 o 2 12 1 7.23 10.28 80.29 o 3 12 1 43.20 52.16 50.37 o 1 0 2 1813.18 1692.18 30.49 o 2 0 2 72.70 70.92 18.94 o 3 0 2 50.02 49.52 20.83 o 4 0 2 40.09 43.55 29.64 o 5 0 2 1610.11 1646.83 47.53 o 6 0 2 589.46 600.95 33.61 o 7 0 2 578.75 630.31 37.21 o 8 0 2 94.22 86.54 54.16 o 9 0 2 796.97 879.61 50.18 o 10 0 2 121.80 41.38 55.11 o 11 0 2 14.21 20.07 53.12 o 12 0 2 2.44 -19.41 58.32 o 0 1 2 12.16 14.68 20.55 o 1 1 2 12150.47 11404.41 67.51 o 2 1 2 7746.44 7581.67 69.21 o 3 1 2 4125.58 3992.42 61.64 o 4 1 2 468.38 495.48 24.90 o 5 1 2 257.18 246.65 26.51 o 6 1 2 347.76 364.63 31.34 o 7 1 2 101.33 55.11 30.58 o 8 1 2 60.82 31.06 47.63 o 9 1 2 136.47 145.15 38.91 o 10 1 2 109.48 36.45 55.67 o 11 1 2 25.79 -56.24 58.80 o 12 1 2 9.18 -26.04 58.99 o 0 2 2 4166.49 4348.05 52.74 o 1 2 2 934.24 914.83 28.50 o 2 2 2 2999.06 3046.91 54.63 o 3 2 2 930.94 932.44 26.89 o 4 2 2 239.47 242.01 22.72 o 5 2 2 751.28 824.12 33.71 o 6 2 2 24.21 11.74 37.78 o 7 2 2 12.15 -12.12 42.23 o 8 2 2 64.21 81.71 49.71 o 9 2 2 107.03 89.00 52.64 o 10 2 2 138.05 180.37 37.68 o 11 2 2 13.17 -54.16 57.47 o 12 2 2 31.12 80.95 43.65 o 0 3 2 2446.06 2336.12 50.28 o 1 3 2 1300.31 1254.17 37.68 o 2 3 2 245.48 248.07 23.20 o 3 3 2 233.55 255.83 22.16 o 4 3 2 381.06 414.81 27.74 o 5 3 2 234.32 233.68 27.27 o 6 3 2 233.42 251.67 30.68 o 7 3 2 16.53 27.27 44.22 o 8 3 2 68.44 35.32 49.90 o 9 3 2 70.88 -55.39 55.39 o 10 3 2 78.57 71.11 54.16 o 11 3 2 29.29 -24.71 62.68 o 12 3 2 4.89 16.95 59.08 o 0 4 2 11.57 14.20 30.68 o 1 4 2 2507.26 2494.05 57.19 o 2 4 2 254.62 271.65 22.63 o 3 4 2 221.92 298.73 26.04 o 4 4 2 925.22 908.39 35.41 o 5 4 2 164.19 158.22 27.55 o 6 4 2 159.50 185.48 32.19 o 7 4 2 70.93 19.41 47.53 o 8 4 2 97.04 -2.18 56.34 o 9 4 2 19.91 32.29 50.18 o 10 4 2 52.63 28.50 57.47 o 11 4 2 65.25 -22.44 59.65 o 0 5 2 437.92 454.01 29.26 o 1 5 2 314.60 355.44 26.70 o 2 5 2 236.72 256.78 26.70 o 3 5 2 145.00 140.51 27.08 o 4 5 2 74.98 91.27 26.51 o 5 5 2 29.71 36.36 43.55 o 6 5 2 43.23 55.96 31.72 o 7 5 2 21.00 58.14 48.19 o 8 5 2 22.80 -53.21 53.21 o 9 5 2 43.10 337.64 43.74 o 10 5 2 19.08 -17.99 57.38 o 11 5 2 57.11 103.68 64.10 o 0 6 2 51.67 68.36 37.21 o 1 6 2 502.88 531.65 32.10 o 2 6 2 406.86 400.13 30.30 o 3 6 2 93.14 92.13 28.59 o 4 6 2 183.47 178.48 32.67 o 5 6 2 207.36 137.39 36.64 o 6 6 2 121.53 144.30 36.07 o 7 6 2 16.94 33.99 52.17 o 8 6 2 102.24 163.14 35.79 o 9 6 2 112.67 75.75 60.12 o 10 6 2 2.08 -22.25 58.14 o 0 7 2 248.52 295.22 33.33 o 1 7 2 6.45 44.41 41.76 o 2 7 2 162.54 166.64 33.99 o 3 7 2 172.08 176.87 33.80 o 4 7 2 124.86 17.33 49.90 o 5 7 2 446.69 452.68 42.13 o 6 7 2 109.42 75.65 56.62 o 7 7 2 107.00 143.73 36.93 o 8 7 2 53.08 100.84 39.20 o 9 7 2 2.80 -45.16 55.96 o 10 7 2 0.86 -6.72 62.96 o 0 8 2 519.55 521.61 41.47 o 1 8 2 275.19 280.17 37.02 o 2 8 2 89.11 130.85 35.22 o 3 8 2 351.89 332.72 41.57 o 4 8 2 93.37 80.29 55.30 o 5 8 2 94.83 93.36 54.16 o 6 8 2 27.77 -35.60 52.36 o 7 8 2 17.10 29.92 51.98 o 8 8 2 20.01 15.05 58.32 o 9 8 2 1.75 6.53 58.14 o 0 9 2 362.41 312.36 44.41 o 1 9 2 78.17 118.92 38.91 o 2 9 2 366.55 366.52 42.61 o 3 9 2 68.66 105.29 36.93 o 4 9 2 20.97 2.46 54.82 o 5 9 2 57.89 81.05 51.32 o 6 9 2 25.73 19.79 54.06 o 7 9 2 62.89 76.03 64.10 o 8 9 2 22.99 62.21 61.17 o 0 10 2 117.43 85.03 54.63 o 1 10 2 72.06 -7.57 59.65 o 2 10 2 144.31 234.63 38.63 o 3 10 2 1.81 -45.26 55.01 o 4 10 2 7.81 -22.06 56.05 o 5 10 2 5.39 26.23 51.60 o 6 10 2 129.45 81.43 62.96 o 7 10 2 29.68 33.42 57.76 o 0 11 2 18.47 19.88 53.12 o 1 11 2 46.99 -59.08 59.08 o 2 11 2 10.68 -32.10 57.76 o 3 11 2 23.85 0.00 61.07 o 4 11 2 22.94 0.00 59.27 o 5 11 2 6.25 -59.46 59.46 o 0 12 2 0.53 28.88 61.07 o 1 12 2 9.90 83.79 59.27 o 2 12 2 103.33 226.67 43.93 o 3 12 2 9.69 10.13 65.14 o 1 0 3 3244.28 3168.10 40.43 o 2 0 3 24506.73 23755.18 114.19 o 3 0 3 18.66 -14.58 32.00 o 4 0 3 681.13 651.23 25.94 o 5 0 3 32.21 62.87 23.77 o 6 0 3 400.53 398.90 31.25 o 7 0 3 0.00 13.26 41.47 o 8 0 3 196.69 198.46 37.02 o 9 0 3 18.85 -22.25 53.31 o 10 0 3 8.92 -18.18 37.49 o 11 0 3 40.61 -14.39 56.15 o 12 0 3 0.16 6.53 55.96 o 0 1 3 1428.19 1343.56 31.34 o 1 1 3 768.98 753.30 21.87 o 2 1 3 632.55 643.47 24.05 o 3 1 3 2761.42 2584.10 53.12 o 4 1 3 199.16 183.02 21.59 o 5 1 3 70.33 84.08 23.95 o 6 1 3 720.86 744.12 35.22 o 7 1 3 100.94 156.80 31.34 o 8 1 3 35.38 80.10 34.28 o 9 1 3 310.53 353.74 40.05 o 10 1 3 35.77 13.07 52.83 o 11 1 3 67.19 41.57 57.47 o 12 1 3 43.14 9.85 56.90 o 0 2 3 5972.07 5726.44 60.98 o 1 2 3 4008.42 3868.95 55.39 o 2 2 3 3060.35 2876.76 55.48 o 3 2 3 16.34 33.42 19.98 o 4 2 3 2408.19 2495.76 59.27 o 5 2 3 3211.68 3412.57 73.95 o 6 2 3 35.39 23.77 37.78 o 7 2 3 69.80 75.75 31.34 o 8 2 3 182.47 256.78 37.68 o 9 2 3 90.99 78.02 37.40 o 10 2 3 25.62 55.96 53.69 o 11 2 3 28.49 -3.03 60.03 o 12 2 3 4.13 76.31 59.08 o 0 3 3 2064.24 2048.09 49.80 o 1 3 3 1378.51 1349.33 39.01 o 2 3 3 467.64 435.64 24.33 o 3 3 3 1083.87 1084.12 31.72 o 4 3 3 1578.32 1714.62 48.19 o 5 3 3 318.39 445.39 28.40 o 6 3 3 88.66 73.66 28.59 o 7 3 3 49.09 71.49 45.26 o 8 3 3 323.85 386.69 40.43 o 9 3 3 27.92 52.36 48.67 o 10 3 3 23.52 65.99 55.48 o 11 3 3 8.63 -34.09 55.86 o 12 3 3 11.06 33.99 59.18 o 0 4 3 2198.12 2244.47 55.77 o 1 4 3 592.16 630.87 25.47 o 2 4 3 22.06 -30.96 30.96 o 3 4 3 136.60 112.96 24.90 o 4 4 3 1191.79 1223.88 38.06 o 5 4 3 33.23 62.78 38.44 o 6 4 3 238.29 264.36 33.90 o 7 4 3 231.26 281.11 35.88 o 8 4 3 34.27 62.40 51.41 o 9 4 3 164.18 150.93 38.54 o 10 4 3 208.85 220.52 41.19 o 11 4 3 14.21 35.32 57.76 o 0 5 3 1279.09 1311.46 39.48 o 1 5 3 441.24 473.51 28.59 o 2 5 3 478.68 500.31 29.92 o 3 5 3 232.48 266.72 27.55 o 4 5 3 119.06 1.51 41.38 o 5 5 3 134.09 78.40 46.77 o 6 5 3 8.76 62.11 41.09 o 7 5 3 34.03 10.42 52.45 o 8 5 3 13.96 11.93 50.47 o 9 5 3 1.10 31.72 48.00 o 10 5 3 6.24 81.24 55.86 o 11 5 3 1.73 3.31 62.68 o 0 6 3 3.75 -17.99 35.88 o 1 6 3 966.16 972.97 37.12 o 2 6 3 105.78 67.41 26.89 o 3 6 3 107.91 138.81 28.88 o 4 6 3 117.09 136.72 32.48 o 5 6 3 226.26 261.89 34.75 o 6 6 3 93.66 105.86 54.16 o 7 6 3 51.63 13.63 51.41 o 8 6 3 73.20 -12.78 51.41 o 9 6 3 1.37 -51.60 51.60 o 10 6 3 22.29 -61.83 61.83 o 0 7 3 425.45 451.64 35.60 o 1 7 3 154.39 150.17 32.86 o 2 7 3 417.11 426.26 35.41 o 3 7 3 24.40 -10.79 46.49 o 4 7 3 74.74 63.82 48.19 o 5 7 3 115.58 89.00 38.63 o 6 7 3 6.62 23.10 49.14 o 7 7 3 121.96 79.72 52.93 o 8 7 3 36.25 -22.16 53.78 o 9 7 3 23.73 21.21 50.84 o 10 7 3 3.16 -40.71 64.95 o 0 8 3 372.69 375.89 40.34 o 1 8 3 19.69 36.74 48.10 o 2 8 3 7.96 -23.58 49.61 o 3 8 3 23.82 57.57 53.69 o 4 8 3 150.87 156.04 39.39 o 5 8 3 190.05 139.75 39.39 o 6 8 3 166.85 156.04 40.90 o 7 8 3 21.92 13.63 52.64 o 8 8 3 25.67 -57.38 58.14 o 9 8 3 3.89 42.42 56.05 o 0 9 3 60.40 79.16 55.20 o 1 9 3 332.20 281.30 41.47 o 2 9 3 249.22 198.08 41.09 o 3 9 3 211.10 194.10 41.28 o 4 9 3 62.76 32.10 51.32 o 5 9 3 9.62 21.02 52.08 o 6 9 3 80.47 48.19 56.81 o 7 9 3 9.50 42.70 57.57 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0 25 27.94 74.04 51.89 o 3 0 25 8.19 26.42 51.13 o 4 0 25 0.69 46.77 53.87 o 5 0 25 2.85 40.71 63.91 o 6 0 25 11.72 -64.10 64.10 o 7 0 25 30.95 -9.85 64.01 o 0 1 25 80.11 57.28 60.03 o 1 1 25 120.15 55.48 55.48 o 2 1 25 39.97 79.72 52.36 o 3 1 25 22.82 47.82 55.20 o 4 1 25 41.64 19.41 59.65 o 5 1 25 34.16 14.58 60.69 o 6 1 25 5.85 -24.81 58.80 o 7 1 25 9.29 -26.32 63.34 o 0 2 25 3.94 48.29 50.94 o 1 2 25 38.22 -7.67 56.15 o 2 2 25 56.65 47.15 52.55 o 3 2 25 11.39 48.67 52.55 o 4 2 25 1.81 36.64 55.30 o 5 2 25 6.51 26.80 58.51 o 6 2 25 14.80 -15.91 62.49 o 7 2 25 0.18 20.07 61.26 o 0 3 25 48.28 -2.65 54.82 o 1 3 25 152.27 106.05 59.75 o 2 3 25 4.86 51.32 54.25 o 3 3 25 16.24 83.51 52.83 o 4 3 25 7.13 -23.20 58.42 o 5 3 25 5.20 -27.46 60.03 o 6 3 25 23.58 45.64 60.50 o 0 4 25 8.96 -24.62 56.62 o 1 4 25 88.06 44.22 53.21 o 2 4 25 83.26 112.58 42.42 o 3 4 25 27.25 20.26 55.48 o 4 4 25 16.02 24.05 58.14 o 5 4 25 8.87 -3.12 60.98 o 6 4 25 9.36 3.41 63.06 o 0 5 25 71.54 94.97 57.95 o 1 5 25 18.19 77.17 38.82 o 2 5 25 99.66 86.16 57.19 o 3 5 25 10.12 -33.42 57.28 o 4 5 25 37.34 31.43 58.51 o 5 5 25 13.85 -3.31 63.72 o 0 6 25 12.31 64.48 53.40 o 1 6 25 107.91 52.45 59.93 o 2 6 25 3.85 -44.03 57.47 o 3 6 25 4.72 -57.66 57.66 o 4 6 25 3.50 6.63 62.68 o 0 7 25 40.17 13.07 59.84 o 1 7 25 0.58 -59.75 59.75 o 2 7 25 1.84 -57.38 57.38 o 3 7 25 9.94 -63.06 63.06 o 0 0 26 11.18 85.97 50.84 o 1 0 26 84.39 96.29 39.96 o 2 0 26 125.17 151.87 42.89 o 3 0 26 6.78 83.13 57.19 o 4 0 26 0.50 40.43 58.80 o 5 0 26 23.80 36.45 65.33 o 6 0 26 89.92 109.45 47.06 o 7 0 26 0.40 51.13 68.55 o 0 1 26 59.26 57.66 52.83 o 1 1 26 14.66 -7.95 56.81 o 2 1 26 57.69 24.33 57.57 o 3 1 26 98.22 75.18 59.65 o 4 1 26 38.97 72.53 60.41 o 5 1 26 6.74 -30.58 61.83 o 6 1 26 15.74 -63.72 63.72 o 0 2 26 76.33 100.17 38.25 o 1 2 26 92.60 113.53 40.71 o 2 2 26 12.61 13.73 56.72 o 3 2 26 42.78 -2.84 60.03 o 4 2 26 22.66 32.48 57.76 o 5 2 26 49.96 93.07 61.26 o 6 2 26 17.85 99.42 62.87 o 0 3 26 162.07 143.07 39.96 o 1 3 26 11.10 -55.30 55.30 o 2 3 26 32.83 -61.17 61.17 o 3 3 26 36.64 23.29 57.28 o 4 3 26 41.42 -18.18 59.37 o 5 3 26 13.30 85.97 60.12 o 6 3 26 21.68 47.53 63.44 o 0 4 26 2.78 20.07 51.13 o 1 4 26 75.95 37.68 60.31 o 2 4 26 42.62 55.96 54.06 o 3 4 26 56.77 45.45 57.66 o 4 4 26 10.14 -15.62 55.96 o 5 4 26 5.71 -13.16 55.48 o 0 5 26 20.52 45.07 55.39 o 1 5 26 40.53 51.70 59.93 o 2 5 26 35.44 74.42 56.81 o 3 5 26 4.82 -38.06 59.18 o 4 5 26 21.42 26.23 59.65 o 0 6 26 1.08 12.78 58.99 o 1 6 26 34.55 6.44 61.64 o 2 6 26 8.64 -58.42 58.42 o 3 6 26 4.06 16.76 62.30 o 0 7 26 51.23 -23.86 60.03 o 1 7 26 3.67 66.66 41.76 o 1 0 27 3.04 85.97 54.44 o 2 0 27 1.02 -11.27 60.41 o 3 0 27 92.92 14.49 59.08 o 4 0 27 0.14 -27.17 56.05 o 5 0 27 154.62 149.22 47.72 o 6 0 27 44.82 83.79 67.79 o 0 1 27 0.53 5.49 49.33 o 1 1 27 47.78 41.85 56.62 o 2 1 27 4.58 82.37 54.73 o 3 1 27 18.90 5.87 55.11 o 4 1 27 48.28 97.15 62.40 o 5 1 27 17.32 54.25 62.40 o 6 1 27 11.44 0.00 64.48 o 0 2 27 2.43 25.28 54.82 o 1 2 27 66.72 96.48 40.15 o 2 2 27 23.61 17.33 58.80 o 3 2 27 111.59 17.80 66.66 o 4 2 27 55.99 114.09 59.08 o 5 2 27 12.45 19.41 60.41 o 6 2 27 3.83 72.43 62.30 o 0 3 27 0.86 -43.27 58.14 o 1 3 27 147.00 105.10 43.36 o 2 3 27 8.06 47.53 61.17 o 3 3 27 5.54 -30.49 59.93 o 4 3 27 21.28 -37.97 63.91 o 5 3 27 15.73 -33.14 59.93 o 0 4 27 35.40 32.95 61.35 o 1 4 27 14.61 57.57 54.63 o 2 4 27 13.21 -6.15 59.27 o 3 4 27 20.74 41.09 60.60 o 4 4 27 3.67 -3.31 62.40 o 5 4 27 3.87 -63.91 63.91 o 0 5 27 0.04 -3.12 54.35 o 1 5 27 35.73 -28.59 57.95 o 2 5 27 6.73 46.87 41.00 o 3 5 27 3.01 -62.11 62.11 o 4 5 27 6.12 -62.02 62.02 o 0 6 27 113.66 144.96 43.46 o 1 6 27 4.51 23.48 53.87 o 2 6 27 4.22 23.86 58.51 o 0 0 28 155.56 125.36 43.55 o 1 0 28 43.09 -58.32 60.88 o 2 0 28 156.16 200.07 42.89 o 3 0 28 0.16 -45.64 61.73 o 4 0 28 2.68 34.75 60.88 o 5 0 28 4.81 13.26 65.80 o 0 1 28 74.08 95.63 61.73 o 1 1 28 10.91 -61.73 61.73 o 2 1 28 30.17 80.48 40.15 o 3 1 28 26.36 70.44 59.93 o 4 1 28 28.84 -28.59 62.02 o 5 1 28 22.58 89.85 67.98 o 0 2 28 5.41 70.73 57.28 o 1 2 28 1.04 -17.90 57.47 o 2 2 28 74.70 107.56 43.08 o 3 2 28 23.14 77.73 61.45 o 4 2 28 22.13 32.19 57.28 o 5 2 28 48.03 111.44 64.86 o 0 3 28 8.37 15.15 59.18 o 1 3 28 7.54 -59.93 59.93 o 2 3 28 0.60 34.18 57.38 o 3 3 28 26.21 47.82 59.27 o 4 3 28 19.37 -39.67 64.67 o 0 4 28 10.84 -15.72 53.31 o 1 4 28 10.11 -63.06 63.06 o 2 4 28 21.10 -9.66 62.11 o 3 4 28 52.21 94.02 44.03 o 4 4 28 41.03 112.39 60.41 o 0 5 28 0.16 49.14 61.45 o 1 5 28 1.03 -67.89 67.89 o 2 5 28 1.00 6.72 60.41 o 1 0 29 3.75 24.52 61.92 o 2 0 29 5.38 -24.90 59.84 o 3 0 29 6.90 -67.41 67.41 o 4 0 29 72.21 66.09 66.85 o 0 1 29 0.04 30.39 60.41 o 1 1 29 8.06 -27.65 60.98 o 2 1 29 17.82 -65.33 65.33 o 3 1 29 22.04 51.32 63.63 o 4 1 29 22.32 3.31 64.57 o 0 2 29 26.09 -3.12 58.61 o 1 2 29 24.49 70.25 41.09 o 2 2 29 88.32 41.28 65.14 o 3 2 29 106.04 71.58 63.63 o 4 2 29 0.46 33.71 60.98 o 0 3 29 7.31 17.42 42.51 o 1 3 29 10.07 41.66 62.40 o 2 3 29 41.98 16.29 65.14 o 3 3 29 10.82 30.01 64.57 o 0 4 29 27.87 -13.16 55.86 o 1 4 29 14.86 -16.57 59.75 o 2 4 29 25.79 -67.51 67.51 o 0 0 30 34.63 -31.72 63.34 o 1 0 30 2.73 22.44 59.93 o 2 0 30 35.39 -3.22 69.50 o 3 0 30 10.00 100.17 63.34 o 0 1 30 10.64 9.56 58.23 o 1 1 30 62.82 106.42 61.92 o 2 1 30 20.91 -45.83 61.92 o 3 1 30 16.06 -53.69 64.86 o 0 2 30 12.77 69.59 41.09 o 1 2 30 5.99 -19.60 65.62 o 2 2 30 26.30 69.78 62.78 o 3 2 30 29.91 -23.77 67.60 o 0 3 30 8.02 -29.83 64.20 o 1 3 30 4.61 80.48 58.61 o 2 3 30 3.57 -63.72 63.72 o 1 0 31 6.77 -23.58 65.80 o 2 0 31 6.73 -51.13 66.09 o 0 1 31 72.66 76.88 64.38 o 1 1 31 7.55 -30.39 71.49 o 0 2 31 0.05 13.54 60.31 o