#------------------------------------------------------------------------------ #$Date: 2009-05-05 17:46:52 +0300 (Tue, 05 May 2009) $ #$Revision: 697 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2217786.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2217786_Fobs loop_ _publ_author_name 'Zhang, Peng-Wei' 'Zhang, Tong-Yun' 'Zhang, Li' 'Deng, Yi' _publ_section_title ; 4-Hydroxy-2,2,6,6-tetramethylpiperidinium trichloroacetate ; _journal_coeditor_code HG2380 _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o641 _journal_volume 64 _journal_year 2008 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.193 _cell_angle_gamma 90.000 _cell_length_a 6.3468 _cell_length_b 14.4499 _cell_length_c 8.2175 _exptl_crystal_F_000 336.00 _reflns_d_resolution_high 0.7605 _[local]_cod_data_source_file hg2380Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' R80221E in P2(1)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 67.18 _shelx_F_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -10 0 248.46 243.82 9.67 o 3 -10 0 405.60 421.12 15.31 o 2 -9 0 127.85 129.08 3.75 o 3 -9 0 85.95 88.59 4.10 o 4 -9 0 177.50 178.57 7.49 o 2 -8 0 384.26 403.13 9.51 o 3 -8 0 380.24 372.12 9.58 o 4 -8 0 921.00 892.01 33.19 o 5 -8 0 317.39 326.33 13.60 o 6 -8 0 29.84 28.36 4.95 o 1 -7 0 2101.09 2106.34 35.82 o 2 -7 0 50.87 59.60 2.19 o 3 -7 0 302.55 305.44 7.85 o 4 -7 0 102.12 103.15 7.79 o 5 -7 0 135.30 137.88 8.19 o 6 -7 0 162.27 160.02 10.67 o 7 -7 0 144.30 142.57 9.01 o 1 -6 0 1562.27 1489.22 25.51 o 2 -6 0 1567.65 1505.35 31.95 o 3 -6 0 476.01 490.39 12.18 o 4 -6 0 1686.91 1598.13 58.80 o 5 -6 0 317.12 320.46 13.86 o 6 -6 0 100.32 98.23 6.71 o 7 -6 0 160.40 158.02 9.57 o 1 -5 0 1221.30 1190.36 20.46 o 2 -5 0 39.55 47.99 1.88 o 3 -5 0 486.35 546.08 12.98 o 4 -5 0 479.17 491.98 12.68 o 5 -5 0 1.33 4.10 2.51 o 6 -5 0 656.87 710.09 45.79 o 7 -5 0 88.81 96.51 7.13 o 8 -5 0 1.97 3.23 3.98 o 3 -4 0 605.81 620.97 14.51 o 4 -4 0 95.50 85.78 3.90 o 5 -4 0 578.15 553.50 23.20 o 6 -4 0 300.11 327.13 14.85 o 7 -4 0 158.17 161.15 8.54 o 8 -4 0 50.94 57.24 5.26 o 1 -3 0 1177.21 1006.08 17.32 o 2 -3 0 1947.25 1958.02 33.77 o 3 -3 0 951.63 1002.35 19.11 o 4 -3 0 624.71 619.98 15.28 o 5 -3 0 670.34 682.64 27.59 o 6 -3 0 213.20 217.56 10.58 o 7 -3 0 67.38 82.59 8.70 o 8 -3 0 34.54 28.71 5.15 o 0 -2 0 316.75 332.35 5.93 o 2 -2 0 712.97 657.77 12.48 o 3 -2 0 2265.35 2215.48 47.41 o 4 -2 0 189.31 192.24 6.52 o 5 -2 0 580.07 591.07 22.70 o 6 -2 0 193.74 204.00 10.23 o 7 -2 0 169.04 166.49 11.06 o 8 -2 0 42.73 41.31 4.54 o 1 -1 0 75.05 79.04 1.64 o 2 -1 0 681.04 588.67 12.05 o 3 -1 0 959.77 1041.23 20.04 o 4 -1 0 479.60 493.24 14.26 o 5 -1 0 445.25 450.37 18.23 o 6 -1 0 384.62 364.11 19.48 o 7 -1 0 38.89 32.01 15.32 o 8 -1 0 205.47 202.31 17.14 o 1 0 0 7.70 3.90 0.96 o 2 0 0 2558.03 2199.91 45.88 o 3 0 0 768.51 687.91 15.21 o 4 0 0 475.47 522.08 15.82 o 5 0 0 217.26 226.88 17.77 o 6 0 0 412.00 438.42 23.30 o 7 0 0 498.52 505.56 24.92 o 8 0 0 96.04 99.98 9.79 o 1 1 0 69.30 77.04 1.93 o 2 1 0 664.33 618.11 8.32 o 3 1 0 972.70 970.10 13.33 o 4 1 0 486.60 506.51 13.50 o 5 1 0 416.54 401.19 17.08 o 6 1 0 380.19 359.06 19.42 o 7 1 0 36.47 37.08 18.46 o 8 1 0 205.20 205.72 17.74 o 0 2 0 314.59 333.42 8.77 o 2 2 0 694.06 676.33 23.01 o 3 2 0 2289.44 2260.09 73.05 o 4 2 0 188.02 191.08 4.68 o 5 2 0 592.08 599.16 23.35 o 6 2 0 190.37 204.20 10.77 o 7 2 0 173.31 171.05 10.78 o 8 2 0 37.93 27.09 16.70 o 1 3 0 1152.10 1067.79 12.14 o 2 3 0 1925.78 1972.65 84.12 o 3 3 0 955.80 992.34 17.32 o 4 3 0 639.55 633.80 38.85 o 5 3 0 670.00 658.82 17.53 o 6 3 0 223.08 242.85 12.95 o 7 3 0 69.50 69.68 7.85 o 8 3 0 33.06 32.62 4.79 o 0 4 0 529.05 538.70 10.94 o 1 4 0 2114.34 1932.27 27.80 o 2 4 0 243.26 256.45 6.02 o 3 4 0 591.16 581.12 31.41 o 4 4 0 107.18 103.46 4.83 o 5 4 0 570.49 596.99 16.20 o 6 4 0 303.21 309.38 15.16 o 7 4 0 155.52 179.44 10.58 o 8 4 0 49.74 39.24 4.71 o 1 5 0 1238.18 1189.14 15.87 o 2 5 0 42.10 49.43 1.28 o 3 5 0 502.37 527.31 11.64 o 4 5 0 479.94 481.66 9.18 o 5 5 0 1.18 1.56 1.24 o 6 5 0 653.72 652.21 29.90 o 7 5 0 87.06 86.92 15.61 o 8 5 0 1.99 0.19 2.42 o 0 6 0 1582.59 1547.11 19.39 o 1 6 0 1553.96 1428.14 13.71 o 2 6 0 1575.52 1614.32 24.92 o 3 6 0 485.26 485.13 10.82 o 4 6 0 1680.47 1632.03 30.14 o 5 6 0 313.35 313.00 7.04 o 6 6 0 94.26 96.91 2.81 o 7 6 0 155.62 174.14 9.06 o 1 7 0 2095.40 2009.36 18.53 o 2 7 0 45.78 55.29 2.14 o 3 7 0 305.18 308.98 5.69 o 4 7 0 97.53 100.92 4.07 o 5 7 0 128.19 118.04 3.87 o 6 7 0 160.32 154.23 6.33 o 7 7 0 141.98 153.22 9.13 o 0 8 0 242.57 264.77 10.43 o 1 8 0 1350.32 1315.63 15.11 o 2 8 0 399.25 423.30 7.25 o 3 8 0 387.20 384.99 6.03 o 4 8 0 897.27 871.23 16.26 o 5 8 0 312.09 313.15 7.40 o 6 8 0 30.43 32.29 2.27 o 7 8 0 131.01 137.43 5.99 o 1 9 0 233.72 246.49 3.47 o 2 9 0 127.32 114.14 2.65 o 3 9 0 90.01 92.51 2.88 o 4 9 0 181.11 188.92 5.79 o 5 9 0 219.87 228.14 5.92 o 6 9 0 21.79 22.89 1.97 o 7 9 0 24.62 20.13 8.84 o 0 10 0 228.13 254.20 5.99 o 1 10 0 261.39 273.83 5.79 o 2 10 0 241.32 228.92 5.25 o 3 10 0 412.22 422.05 8.64 o 4 10 0 94.26 96.84 3.86 o 5 10 0 238.34 242.22 8.41 o 6 10 0 139.77 135.95 4.78 o 7 10 0 170.32 172.46 8.50 o 1 11 0 349.08 355.82 6.66 o 2 11 0 490.39 519.11 10.99 o 3 11 0 135.98 144.32 6.77 o 4 11 0 101.57 102.88 3.75 o 5 11 0 314.58 314.29 11.70 o 6 11 0 221.36 219.07 4.99 o 0 12 0 601.46 623.35 17.36 o 1 12 0 878.59 861.53 14.72 o 2 12 0 340.51 344.34 7.60 o 3 12 0 374.29 377.02 8.74 o 4 12 0 211.32 223.48 8.58 o 5 12 0 36.00 39.73 2.60 o 6 12 0 2.86 3.06 1.36 o 1 13 0 59.18 51.55 2.49 o 2 13 0 123.55 117.12 4.16 o 3 13 0 246.64 256.88 9.41 o 4 13 0 165.35 158.06 5.09 o 5 13 0 236.44 234.76 6.75 o 6 13 0 21.77 19.59 2.42 o 0 14 0 521.14 532.00 24.11 o 1 14 0 169.96 181.64 7.55 o 2 14 0 236.92 237.64 8.37 o 3 14 0 12.72 12.44 3.69 o 4 14 0 235.17 237.57 6.04 o 5 14 0 1.65 1.97 1.37 o 1 15 0 23.50 21.37 10.40 o 2 15 0 22.73 23.58 2.23 o 3 15 0 140.88 139.35 4.38 o 4 15 0 398.56 404.89 7.64 o 5 15 0 29.33 28.73 2.71 o 0 16 0 265.48 253.08 16.33 o 1 16 0 114.33 111.11 6.20 o 2 16 0 118.51 109.88 5.47 o 3 16 0 23.71 21.90 2.98 o 4 16 0 37.64 36.96 2.72 o 1 17 0 19.13 20.71 6.98 o 2 17 0 134.90 130.82 7.05 o 3 17 0 64.09 59.84 4.47 o 0 18 0 380.34 402.89 31.93 o 1 18 0 110.26 107.13 8.96 o 2 18 0 53.79 44.94 4.26 o 2 -12 1 660.83 655.02 23.93 o 2 -11 1 356.37 366.57 14.18 o 3 -11 1 369.94 380.26 18.83 o 2 -10 1 178.40 184.25 7.78 o 3 -10 1 483.96 491.54 18.70 o 4 -10 1 257.99 265.24 13.73 o 1 -9 1 503.47 504.66 12.80 o 2 -9 1 142.51 153.13 5.71 o 3 -9 1 816.30 809.01 28.99 o 4 -9 1 210.73 184.88 8.77 o 5 -9 1 158.69 167.41 11.80 o -4 -8 1 96.38 95.21 6.96 o -3 -8 1 60.50 58.77 2.93 o -2 -8 1 942.53 955.45 19.67 o 1 -8 1 1696.55 1673.18 35.98 o 3 -8 1 132.62 139.09 6.34 o 4 -8 1 401.20 411.17 16.05 o 6 -8 1 11.51 9.13 6.16 o -6 -7 1 40.80 37.63 3.46 o -5 -7 1 58.91 59.01 4.36 o -4 -7 1 853.61 893.24 31.78 o -3 -7 1 10.60 10.55 0.98 o -2 -7 1 267.45 252.39 5.69 o 1 -7 1 24.91 26.35 1.73 o 2 -7 1 181.63 182.80 5.31 o 3 -7 1 436.65 433.31 10.91 o 4 -7 1 99.98 104.31 7.99 o 5 -7 1 353.77 390.36 20.23 o 6 -7 1 327.83 355.11 21.69 o 7 -7 1 98.99 87.09 8.31 o -7 -6 1 2.24 0.49 2.80 o -6 -6 1 182.28 166.14 11.82 o -5 -6 1 185.84 171.52 7.78 o -4 -6 1 6.12 8.95 4.53 o -3 -6 1 720.80 722.71 16.63 o -2 -6 1 1118.45 1087.48 22.55 o 1 -6 1 3016.21 2745.58 56.98 o 2 -6 1 2004.08 2054.35 43.52 o 3 -6 1 852.86 825.24 18.79 o 4 -6 1 1082.77 1181.39 43.79 o 5 -6 1 213.01 232.02 12.91 o 6 -6 1 208.76 211.04 13.97 o 7 -6 1 277.48 278.48 15.73 o -8 -5 1 167.02 161.32 10.80 o -7 -5 1 375.95 350.55 17.01 o -6 -5 1 51.71 43.34 3.36 o -5 -5 1 98.69 90.41 4.96 o -4 -5 1 1451.92 1392.73 30.81 o -3 -5 1 871.41 888.43 19.53 o -2 -5 1 132.02 156.61 3.54 o 0 -5 1 436.69 419.24 8.90 o 1 -5 1 337.91 322.87 6.85 o 2 -5 1 274.18 287.59 6.65 o 3 -5 1 954.43 991.54 22.41 o 4 -5 1 39.65 49.15 3.72 o 5 -5 1 10.27 10.63 6.05 o 6 -5 1 240.93 256.19 18.03 o 7 -5 1 40.96 41.05 8.60 o -8 -4 1 114.32 113.09 8.38 o -7 -4 1 35.75 36.60 4.08 o -6 -4 1 380.71 387.58 16.45 o -5 -4 1 56.84 57.04 4.93 o -4 -4 1 892.79 864.13 19.91 o -3 -4 1 15.80 12.33 1.25 o -2 -4 1 130.71 138.01 3.34 o 0 -4 1 1358.87 1281.82 15.70 o 3 -4 1 390.62 437.18 11.12 o 4 -4 1 1005.59 1036.81 24.04 o 5 -4 1 74.59 69.33 4.89 o 6 -4 1 96.16 100.87 6.48 o 7 -4 1 247.52 228.93 11.33 o 8 -4 1 10.38 4.87 6.37 o -8 -3 1 26.95 30.59 4.16 o -7 -3 1 275.65 277.91 14.70 o -6 -3 1 183.77 199.49 9.99 o -5 -3 1 39.83 40.50 4.31 o -4 -3 1 1386.15 1350.54 29.95 o -3 -3 1 355.70 342.79 9.28 o 0 -3 1 880.18 851.30 19.75 o 1 -3 1 420.93 470.50 9.11 o 2 -3 1 1553.98 1450.29 26.01 o 3 -3 1 171.20 176.92 5.81 o 4 -3 1 34.74 31.69 2.79 o 5 -3 1 38.05 46.66 10.46 o 6 -3 1 95.24 98.79 6.55 o 7 -3 1 41.12 36.04 4.37 o 8 -3 1 56.02 53.22 15.89 o -8 -2 1 97.91 86.75 8.77 o -6 -2 1 119.80 122.60 8.02 o -5 -2 1 621.78 632.81 24.10 o -4 -2 1 161.85 175.65 6.29 o -3 -2 1 2682.33 2759.88 57.71 o -2 -2 1 108.99 120.25 3.33 o -1 -2 1 505.40 463.75 8.24 o 1 -2 1 9.50 12.63 1.08 o 2 -2 1 3773.26 3277.58 67.71 o 3 -2 1 517.61 537.30 13.30 o 4 -2 1 414.72 448.64 12.21 o 5 -2 1 124.01 130.71 10.11 o 6 -2 1 170.94 184.51 10.19 o 7 -2 1 96.94 112.77 7.76 o 8 -2 1 276.32 267.44 16.56 o -8 -1 1 48.91 48.18 4.87 o -7 -1 1 273.34 304.99 16.50 o -6 -1 1 7.16 11.67 3.16 o -5 -1 1 503.21 530.35 20.78 o -4 -1 1 160.47 159.73 9.47 o -3 -1 1 618.33 643.12 13.59 o -2 -1 1 532.35 535.15 7.02 o -1 -1 1 418.20 380.37 5.57 o 1 -1 1 3367.25 2564.89 52.62 o 2 -1 1 755.78 788.14 15.11 o 3 -1 1 460.97 489.41 10.99 o 4 -1 1 238.03 213.65 7.24 o 5 -1 1 684.68 650.53 25.00 o 6 -1 1 92.23 96.27 6.55 o 7 -1 1 251.32 249.82 14.06 o 8 -1 1 292.40 265.05 16.55 o -8 0 1 68.36 75.01 7.93 o -7 0 1 180.77 162.91 11.72 o -6 0 1 60.05 73.67 6.53 o -5 0 1 542.22 569.88 23.12 o -4 0 1 626.57 631.03 16.59 o -3 0 1 3027.24 2948.76 61.80 o -2 0 1 704.98 717.43 21.57 o 0 0 1 47.21 53.02 0.62 o 2 0 1 4268.94 3573.88 73.64 o 3 0 1 1555.55 1405.47 27.02 o 4 0 1 115.81 121.16 5.26 o 5 0 1 971.60 1010.60 37.29 o 6 0 1 166.35 165.53 9.12 o 7 0 1 155.74 158.60 10.02 o 8 0 1 20.59 15.08 12.31 o -8 1 1 46.75 47.32 20.96 o -7 1 1 267.36 263.85 14.77 o -6 1 1 7.02 7.07 6.26 o -5 1 1 511.05 486.00 19.45 o -4 1 1 160.80 157.25 6.26 o -3 1 1 625.36 650.58 9.00 o -2 1 1 528.25 511.51 6.88 o -1 1 1 415.30 377.08 9.32 o 2 1 1 787.03 784.22 10.55 o 3 1 1 465.98 487.69 7.66 o 4 1 1 239.18 220.87 7.55 o 5 1 1 698.81 638.59 28.96 o 6 1 1 94.50 106.53 6.90 o 7 1 1 246.85 230.37 13.12 o 8 1 1 295.13 292.06 18.08 o -8 2 1 95.60 98.43 10.16 o -7 2 1 4.52 -0.24 4.00 o -6 2 1 123.16 136.42 9.48 o -5 2 1 623.89 620.71 24.48 o -4 2 1 161.09 164.34 4.20 o -3 2 1 2678.11 2577.85 38.13 o -2 2 1 108.09 117.05 1.84 o -1 2 1 496.27 456.55 5.30 o 1 2 1 8.45 10.95 0.68 o 2 2 1 3819.51 3496.97 51.07 o 3 2 1 504.01 513.75 9.06 o 4 2 1 410.62 453.93 8.62 o 5 2 1 115.77 115.04 9.49 o 6 2 1 165.59 170.59 9.72 o 7 2 1 97.00 105.88 7.76 o 8 2 1 273.66 282.91 18.11 o -8 3 1 27.02 19.58 12.61 o -7 3 1 276.38 280.17 15.59 o -6 3 1 186.20 187.25 10.47 o -5 3 1 33.10 31.80 2.26 o -4 3 1 1356.69 1320.94 20.68 o -3 3 1 353.12 340.48 5.19 o -2 3 1 3916.34 4059.86 193.21 o -1 3 1 2627.49 2461.90 38.01 o 0 3 1 844.87 856.24 15.74 o 1 3 1 430.07 452.64 5.10 o 2 3 1 1522.68 1483.87 19.02 o 3 3 1 162.35 170.06 4.53 o 4 3 1 36.28 33.18 4.03 o 5 3 1 42.71 48.63 3.37 o 6 3 1 93.84 91.87 6.53 o 7 3 1 39.59 34.89 16.26 o 8 3 1 57.24 62.95 6.60 o -8 4 1 115.64 116.23 9.50 o -7 4 1 36.06 37.60 18.33 o -6 4 1 382.29 432.28 19.66 o -5 4 1 63.23 65.80 3.13 o -4 4 1 883.97 885.85 15.36 o -3 4 1 17.08 12.60 1.02 o -2 4 1 137.14 133.19 2.05 o -1 4 1 407.52 469.54 14.69 o 0 4 1 1363.33 1274.13 14.10 o 1 4 1 3214.26 3088.86 51.15 o 2 4 1 421.26 460.63 12.55 o 3 4 1 387.33 445.24 20.51 o 4 4 1 1013.47 990.29 22.83 o 5 4 1 71.85 68.68 3.37 o 6 4 1 96.16 94.27 6.56 o 7 4 1 245.00 223.27 14.87 o 8 4 1 10.41 8.16 6.31 o -8 5 1 170.60 168.24 9.32 o -7 5 1 380.87 370.74 12.81 o -6 5 1 52.49 46.88 6.23 o -5 5 1 101.64 105.80 3.59 o -4 5 1 1468.36 1416.88 22.46 o -3 5 1 866.98 903.86 18.72 o -2 5 1 135.43 162.35 3.20 o -1 5 1 3766.33 3510.72 64.72 o 0 5 1 440.44 428.20 4.39 o 1 5 1 343.21 320.03 4.03 o 2 5 1 272.46 286.80 8.80 o 3 5 1 947.05 983.74 34.02 o 4 5 1 37.15 41.30 2.73 o 5 5 1 10.05 6.29 2.93 o 6 5 1 237.90 232.72 12.25 o 7 5 1 40.83 42.83 5.57 o -7 6 1 2.23 2.40 2.19 o -6 6 1 185.41 176.00 9.31 o -5 6 1 189.53 185.39 4.42 o -4 6 1 5.81 7.52 1.12 o -3 6 1 724.54 758.18 24.20 o -2 6 1 1065.57 1044.07 11.77 o -1 6 1 1226.00 1229.53 16.40 o 0 6 1 771.23 737.32 8.51 o 1 6 1 3042.71 2828.19 59.62 o 2 6 1 1988.89 1935.85 28.74 o 3 6 1 837.06 811.35 20.80 o 4 6 1 1073.82 1031.81 22.44 o 5 6 1 217.47 229.10 7.41 o 6 6 1 202.58 194.84 9.19 o 7 6 1 276.10 300.26 12.46 o -7 7 1 0.98 1.46 2.59 o -6 7 1 39.36 41.98 4.55 o -5 7 1 52.69 53.37 2.17 o -4 7 1 850.68 872.03 16.32 o -3 7 1 13.35 14.67 2.55 o -2 7 1 273.46 269.16 6.16 o -1 7 1 73.09 78.03 1.65 o 0 7 1 484.24 508.92 9.62 o 1 7 1 26.60 28.28 2.21 o 2 7 1 175.60 173.30 3.71 o 3 7 1 430.95 438.19 10.19 o 4 7 1 95.40 93.42 4.06 o 5 7 1 364.30 378.24 10.75 o 6 7 1 336.08 355.16 11.05 o 7 7 1 100.11 98.40 6.02 o -7 8 1 357.81 370.47 13.30 o -6 8 1 160.00 168.32 7.87 o -5 8 1 274.94 292.25 7.95 o -4 8 1 103.87 103.19 4.10 o -3 8 1 59.51 58.39 2.31 o -2 8 1 973.82 960.34 10.54 o -1 8 1 284.87 293.55 3.58 o 0 8 1 704.58 744.98 9.13 o 1 8 1 1673.81 1668.17 20.93 o 2 8 1 95.66 87.00 2.01 o 3 8 1 122.78 127.66 3.42 o 4 8 1 412.02 407.20 8.41 o 5 8 1 3.42 2.74 1.05 o 6 8 1 11.32 12.33 2.01 o 7 8 1 234.33 237.88 15.51 o -7 9 1 13.48 9.13 4.45 o -6 9 1 96.63 98.06 6.54 o -5 9 1 339.25 329.09 7.41 o -4 9 1 148.69 145.48 4.32 o -3 9 1 855.14 840.96 17.56 o -2 9 1 870.83 847.24 14.53 o -1 9 1 128.06 136.25 2.33 o 0 9 1 437.99 445.36 5.70 o 1 9 1 500.38 481.90 10.61 o 2 9 1 142.24 154.82 3.29 o 3 9 1 815.47 812.71 15.44 o 4 9 1 210.06 203.33 4.75 o 5 9 1 156.43 163.83 6.15 o 6 9 1 69.38 62.22 2.92 o 7 9 1 136.45 140.76 7.54 o -7 10 1 102.82 102.59 6.24 o -6 10 1 25.01 29.36 4.53 o -5 10 1 183.53 175.28 6.23 o -4 10 1 349.76 369.76 10.03 o -3 10 1 48.26 50.09 2.46 o -2 10 1 481.02 509.56 11.42 o -1 10 1 114.90 117.18 2.77 o 0 10 1 193.23 185.41 3.01 o 1 10 1 185.20 189.86 3.02 o 2 10 1 190.60 202.86 8.05 o 3 10 1 473.78 465.02 9.69 o 4 10 1 253.18 247.93 7.11 o 5 10 1 218.29 221.15 7.73 o 6 10 1 96.88 94.05 3.40 o -6 11 1 179.91 171.24 7.04 o -5 11 1 362.79 357.72 9.51 o -4 11 1 3.30 2.29 1.10 o -3 11 1 346.21 373.83 7.96 o -2 11 1 512.03 515.99 10.41 o -1 11 1 39.36 44.35 1.49 o 0 11 1 832.80 822.07 15.90 o 1 11 1 26.51 27.41 1.34 o 2 11 1 365.18 366.72 8.03 o 3 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